CN106220142A - Artificial jade based on granite mine tailing and preparation method thereof - Google Patents

Artificial jade based on granite mine tailing and preparation method thereof Download PDF

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Publication number
CN106220142A
CN106220142A CN201610552769.3A CN201610552769A CN106220142A CN 106220142 A CN106220142 A CN 106220142A CN 201610552769 A CN201610552769 A CN 201610552769A CN 106220142 A CN106220142 A CN 106220142A
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Prior art keywords
mine tailing
artificial jade
granite mine
granite
preparation
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CN201610552769.3A
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Inventor
黄聿新
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Shenzhen Super Technology Development Co Ltd
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Shenzhen Super Technology Development Co Ltd
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Priority to CN201610552769.3A priority Critical patent/CN106220142A/en
Publication of CN106220142A publication Critical patent/CN106220142A/en
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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C04B33/132—Waste materials; Refuse; Residues
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3232—Titanium oxides or titanates, e.g. rutile or anatase
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3244—Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74—Physical characteristics
    • C04B2235/77—Density
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00—Technologies relating to the processing of minerals
    • Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Environmental & Geological Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Cosmetics (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The invention discloses a kind of artificial jade based on granite mine tailing and preparation method thereof, artificial jade calculates by weight percentage, including following component: granite mine tailing 10 85%, clay 5 20%, aluminium oxide or aluminium hydroxide 5 20%, zirconium oxide 5 15%, Pulvis Talci 2 10%, sodium carbonate 5 15%, titanium dioxide 1 5%, Borax 5 15%, inorganic color 0 10%, each constituent content percent sum is 100%.By weighing each raw material, broken, mixing during preparation.Pressing mold, sinter, cool down, polish, the step such as polishing prepares artificial jade.The artificial jade of the present invention not only environmental protection, and preparation technology is simple, and the artificial jade obtained has high intensity, high tenacity, color is various and the feature of high refractive index, and without Organic substance, be unlikely to deform, the most inflammable, aging resistance hole corrosivity is strong, has great application prospect.

Description

Artificial jade based on granite mine tailing and preparation method thereof
Technical field
The present invention relates to the synthetic field of jade, be specifically related to a kind of artificial jade based on granite mine tailing and Preparation method.
Background technology
Beautiful exquisite quality is tough and tensile, and color and luster is gentle soft, the most very popular, but, natural output Beautiful resource-constrained, and expensive, it is impossible to meet the needs that people are growing, thus people use synthetic technology system Make jade material.Artificial jade's product in the market is most with Organic substance and aluminium hydroxide for raw material manufacture, and it is in outward appearance And far away from natural jade in performance, and the most aging, yielding, the most fire-resistant.
Summary of the invention
For overcoming above-mentioned technical problem, it is an object of the invention to provide a kind of have high intensity, high tenacity based on Artificial jade of granite mine tailing and preparation method thereof.
The technical scheme used is:
A kind of artificial jade based on granite mine tailing, calculates, by weight percentage including following component:
Granite mine tailing 10-85%, clay 5-20%, aluminium oxide or aluminium hydroxide 5-20%, zirconium oxide 5-15%, Talcum Powder 2-10%, sodium carbonate 5-15%, titanium dioxide 1-5%, Borax 5-15%, inorganic color 0-10%, each constituent content percentage Number sum is 100%.
Preferably, calculate by weight percentage, including following component:
Granite mine tailing 40-60%, clay 5-20%, aluminium oxide or aluminium hydroxide 5-20%, zirconium oxide 5-15%, Talcum Powder 2-10%, sodium carbonate 5-15%, titanium dioxide 1-5%, Borax 5-15%, inorganic color 0-10%.
Preferably, calculate by weight percentage, including following component:
Granite mine tailing 45-55%, clay 5-10%, aluminium oxide or aluminium hydroxide 5-10%, zirconium oxide 5-10%, Talcum Powder 2-8%, sodium carbonate 5-10%, titanium dioxide 1-5%, Borax 5-10%, inorganic color 0-10%.
Described inorganic color such as ferrum oxide, zinc yellow or white carbon black etc., select to add according to actual needs.
The preparation method of the artificial jade based on granite mine tailing of the present invention, comprises the steps:
(1) press the formula of artificial jade based on granite mine tailing in such scheme, weigh various raw material；
(2) sieve broken for various raw materials；
(3) various raw materials are put into mix homogeneously in stirring container；
(4) material being stirred is passed through molding press pressing mold molding, obtain base substrate；
(5) base substrate is at room temperature put into sintering furnace, be warming up to 900-1500 DEG C with stove, be incubated 1-3h；
(6) product cools to room temperature with the furnace, takes out from stove, through polishing, polishing, finally gives artificial jade.
Preferably, in step (5), it is incubated 2h.
The beneficial effects of the present invention is:
The present invention utilize granite mine tailing for primary raw material, not only environmental protection, and preparation technology is simple, the people obtained Make jade and there is high intensity, high tenacity, color is various and the feature of high refractive index, and without Organic substance, be unlikely to deform, The most inflammable, aging resistance hole corrosivity is strong, has great application prospect.
The bulk density of the artificial jade of the present invention is 300-1500Kg/m3, comprcssive strength >=5MPa, rupture strength >= 3MPa。
Detailed description of the invention
Below by specific embodiment, the present invention is described in detail, but the purposes of these exemplary embodiments and Purpose is only used for enumerating the present invention, and not the real protection scope to the present invention constitutes any type of any restriction, more non-general Protection scope of the present invention is confined to this.
It addition, unless stated otherwise, below percentage ratio used by component be all weight percentage.
Embodiment 1
A kind of artificial jade based on granite mine tailing, including following component:
Granite mine tailing 40%, clay 10%, aluminium oxide or aluminium hydroxide 10%, zirconium oxide 10%, Pulvis Talci 6%, carbon Acid sodium 10%, titanium dioxide 4%, Borax 10%.
Preparation method is as follows:
(1) press the formula of artificial jade based on granite mine tailing in such scheme, weigh various raw material；
(2) sieve broken for various raw materials；
(3) various raw materials are put into mix homogeneously in stirring container；
(4) material being stirred is passed through molding press pressing mold molding, obtain base substrate；
(5) base substrate is at room temperature put into sintering furnace, be warming up to 900-1500 DEG C with stove, be incubated 2h；
(6) product cools to room temperature with the furnace, takes out from stove, through polishing, polishing, finally gives artificial jade.
Embodiment 2
A kind of artificial jade based on granite mine tailing, including following component:
Granite mine tailing 45%, clay 10%, aluminium oxide or aluminium hydroxide 5%, zirconium oxide 10%, Pulvis Talci 5%, carbonic acid Sodium 10%, titanium dioxide 5%, Borax 5%, inorganic color 5%.
Preparation method is with reference to embodiment 1.
Embodiment 3
A kind of artificial jade based on granite mine tailing, including following component:
Granite mine tailing 50%, clay 10%, aluminium oxide or aluminium hydroxide 5%, zirconium oxide 5%, Pulvis Talci 7%, carbonic acid Sodium 5%, titanium dioxide 3%, Borax 10%, inorganic color 5%.
Preparation method is with reference to embodiment 1.
Embodiment 4
A kind of artificial jade based on granite mine tailing, including following component:
Granite mine tailing 60%, clay 5%, aluminium oxide or aluminium hydroxide 5%, zirconium oxide 5%, Pulvis Talci 8%, sodium carbonate 5%, titanium dioxide 2%, Borax 5%, inorganic color 5%.
Preparation method is with reference to embodiment 1.
The artificial jade that embodiment 1-embodiment 4 prepares being tested, test result sees table 1 below.
Table 1
Should be appreciated that the purposes of these embodiments is merely to illustrate the present invention and is not intended to limit the protection model of the present invention Enclose.Additionally, it will also be appreciated that after the technology contents having read the present invention, the present invention can be made respectively by those skilled in the art Planting change, amendment and/or modification, all these equivalent form of value falls within the guarantor that the application appended claims is limited equally Within the scope of protecting.

Claims (5)

1. an artificial jade based on granite mine tailing, it is characterised in that calculate by weight percentage, including following component:
Granite mine tailing 10-85%, clay 5-20%, aluminium oxide or aluminium hydroxide 5-20%, zirconium oxide 5-15%, Pulvis Talci 2- 10%, sodium carbonate 5-15%, titanium dioxide 1-5%, Borax 5-15%, inorganic color 0-10%, each constituent content percent it With for 100%.
Artificial jade based on granite mine tailing the most according to claim 1, it is characterised in that calculate by weight percentage, Including following component:
Granite mine tailing 40-60%, clay 5-20%, aluminium oxide or aluminium hydroxide 5-20%, zirconium oxide 5-15%, Pulvis Talci 2- 10%, sodium carbonate 5-15%, titanium dioxide 1-5%, Borax 5-15%, inorganic color 0-10%.
Artificial jade based on granite mine tailing the most according to claim 1, it is characterised in that calculate by weight percentage, Including following component:
Granite mine tailing 45-55%, clay 5-10%, aluminium oxide or aluminium hydroxide 5-10%, zirconium oxide 5-10%, Pulvis Talci 2- 8%, sodium carbonate 5-10%, titanium dioxide 1-5%, Borax 5-10%, inorganic color 0-10%.
4. the preparation method of an artificial jade based on granite mine tailing, it is characterised in that comprise the steps:
(1) by the formula of the arbitrary described artificial jade based on granite mine tailing of claim 1-3, various raw material is weighed；
(2) sieve broken for various raw materials；
(3) various raw materials are put into mix homogeneously in stirring container；
(4) material being stirred is passed through molding press pressing mold molding, obtain base substrate；
(5) base substrate is at room temperature put into sintering furnace, be warming up to 900-1500 DEG C with stove, be incubated 1-3h；
(6) product cools to room temperature with the furnace, takes out from stove, through polishing, polishing, finally gives artificial jade.
The preparation method of artificial jade based on granite mine tailing the most according to claim 4, it is characterised in that
In step (5), it is incubated 2h.
CN201610552769.3A 2016-07-13 2016-07-13 Artificial jade based on granite mine tailing and preparation method thereof Pending CN106220142A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107572826A (en) * 2017-10-31 2018-01-12 广西旭腾实业集团有限公司 A kind of microcrystalline jade ornament materials based on graphene and preparation method thereof
CN107602080A (en) * 2017-10-31 2018-01-19 广西旭腾实业集团有限公司 Based on graphene and stone material mine tailing foamed light high temperature resistant wallboard and preparation method thereof
CN107698238A (en) * 2017-10-31 2018-02-16 广西旭腾实业集团有限公司 Based on graphene and nonmetallic tailings foamed light decorative integrated plate and preparation method
CN107759211A (en) * 2017-10-31 2018-03-06 广西旭腾实业集团有限公司 Based on graphene foamed light fire resistant heat preserving decorative panel and preparation method thereof
CN109320171A (en) * 2018-12-07 2019-02-12 袁建辉 A kind of high rigidity artificial stone material and preparation method

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CN103319090A (en) * 2013-06-04 2013-09-25 广西华锡集团股份有限公司 Technology method of preparing deep-color microcrystal glass from lead-zinc tailing
CN103553554A (en) * 2013-10-25 2014-02-05 由伟 Artificial jade with high refractive index and manufacturing method thereof

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107572826A (en) * 2017-10-31 2018-01-12 广西旭腾实业集团有限公司 A kind of microcrystalline jade ornament materials based on graphene and preparation method thereof
CN107602080A (en) * 2017-10-31 2018-01-19 广西旭腾实业集团有限公司 Based on graphene and stone material mine tailing foamed light high temperature resistant wallboard and preparation method thereof
CN107698238A (en) * 2017-10-31 2018-02-16 广西旭腾实业集团有限公司 Based on graphene and nonmetallic tailings foamed light decorative integrated plate and preparation method
CN107759211A (en) * 2017-10-31 2018-03-06 广西旭腾实业集团有限公司 Based on graphene foamed light fire resistant heat preserving decorative panel and preparation method thereof
CN107698238B (en) * 2017-10-31 2018-11-09 广西旭腾实业集团有限公司 Based on graphene and nonmetallic tailings foamed light decorative integrated plate and preparation method
CN109320171A (en) * 2018-12-07 2019-02-12 袁建辉 A kind of high rigidity artificial stone material and preparation method

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