CN109554006A - A kind of preparation method with A grades of fire-proof function interior wall inorganic environment-friendly coating - Google Patents

A kind of preparation method with A grades of fire-proof function interior wall inorganic environment-friendly coating Download PDF

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Publication number
CN109554006A
CN109554006A CN201811360064.7A CN201811360064A CN109554006A CN 109554006 A CN109554006 A CN 109554006A CN 201811360064 A CN201811360064 A CN 201811360064A CN 109554006 A CN109554006 A CN 109554006A
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CN
China
Prior art keywords
fire
grades
interior wall
solution
coating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811360064.7A
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Chinese (zh)
Inventor
段霞勇
杨玉娟
白小燕
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sichuan Winbond And Coatings Co Ltd
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Sichuan Winbond And Coatings Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sichuan Winbond And Coatings Co Ltd filed Critical Sichuan Winbond And Coatings Co Ltd
Priority to CN201811360064.7A priority Critical patent/CN109554006A/en
Publication of CN109554006A publication Critical patent/CN109554006A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • C09D1/02Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates
    • C09D1/04Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates with organic additives
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18Fireproof paints including high temperature resistant paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Cosmetics (AREA)
  • Paints Or Removers (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention discloses a kind of preparation methods with A grades of fire-proof function interior wall inorganic environment-friendly coating.For the present invention mainly with inorganic silicic acid lithium, silica solution is main film forming matter, titanium dioxide, talcum powder, the heat proof materials such as kaolin are as pigments and fillers, and magnesium hydroxide is as fire retardant, with dispersing agent, defoaming agent, wetting agent, thickener etc. collectively constitute, the coating category ordor removing environment-friendly type coating, Diamond Search content, it is water-fast, mildew resistant moistureproof performance is good, have the inorganic interior wall functional coating of A grades of fire-protection ratings.

Description

A kind of preparation method with A grades of fire-proof function interior wall inorganic environment-friendly coating
Technical field
The present invention relates to interior wall fireproofing inorganic environmental protection coating material preparation methods.
Background technique
With the development of social economy and being constantly progressive for scientific level, people increasingly focus on indoor environmental quality, are good for Kang Huanbao, the inorganic coating of fire safety are just gradually approved and are used by market and client.
Interior decoration traditional at present uses emulsion paint substantially, and environmental protection and performance can satisfy daily required.But it is some to want Higher client's household or such as market, hotel public place are asked, may require that in addition to product quality and environmental protection, it is also contemplated that one Critically important fire safety factor.Selection has the environmental protection coating material of fire-proof function
Product of the present invention is used using inorganic material as main film forming matter, is provided by using inorganic silicic acid lithium solution preferable resistance to It cleans, outside water resistance, it is often more important that excellent fire protecting performance is provided, while selecting the pigments and fillers with certain fire resistance, Using modified magnesium hydroxide as fire retardant, and reduce the smog generated in burning.And it is inorganic to add a small amount of elastic emulsion improvement The risk of the firmly possible cracking phenomena of coating paint film.Addition stabilizer mainly improves the stability of modified magnesium hydroxide and system.Body It is the addition of organic solvent-free, the almost nil interior wall inorganic coating of VOC content.
Summary of the invention
1, the present invention selects the environment protection elastic lotion of low film formation temperature, can not have to addition coalescing agent.
2, after elastic emulsion is added, addition potassium methyl silicate is adjusted the system after lotion is added and is in alkaline shape State, prevention lotion are reacted with subsequent alkaline silicate potassium solution and silica solution, it is ensured that the stability under storing does not occur obvious Rear thickening behavior.
3, before adding silica solution and lithium metasilicate solution, it is necessary to stirring first be added to stabilizer and add after five minutes.
4, silicon sol solution is added in the present invention, can preferably improves the storage stability of finished product paint.
5, the thickener that adds selects the alkali soluble of hydrophobically modified to rise thickener in the present invention.
Specific embodiment:
More detailed elaboration is carried out to the present invention below, in order to be understood by industry field technical staff, thus to the present invention Protection scope be bound.
Embodiment one,
It is as follows for the preparation ratio of each section in the present invention:
Deionized water 27%
Dispersing agent 0.4%
Wetting agent 0.3%
Hydroxyethylmethylcellulose .0.3%
Defoaming agent 0.4%
Titanium dioxide 15%
Kaolin 12%
Talcum powder 8%
Modified magnesium hydroxide 3%
Ordor removing lotion 3%
Stabilizer 0.2%
Methane-siliconic acid potassium solution 0.1%
Silica solution 5%
Lithium metasilicate solution 25%
Defoaming agent 0.4%
Thickener 0.2%
Production explanation: 1, deionized water, dispersing agent, wetting agent low speed 300-500 are weighed and turns stirring 3 minutes in advance, adds hydroxyl second Defoaming agent is added in ylmethyl cellulose, stirring after five minutes.2, turn that titanium dioxide, kaolin, talcum is added in middling speed 800-1000 Powder and modified magnesium hydroxide, high speed dispersion 30-40 minutes.3, lotion is added, is in alkali with methane-siliconic acid potassium solution regulation system Character state.4, lithium metasilicate solution, defoaming agent, thickener are added.5, the thickener added is slowly added to after need to being diluted with water.
Embodiment two,
It is as follows for the preparation ratio of each section in the present invention:
Deionized water 17%
Dispersing agent 0.8%
Wetting agent 0.1%
Hydroxyethylmethylcellulose 0.1%
Defoaming agent 0.15%
Titanium dioxide 20%
Kaolin 5%
Talcum powder 4%
Modified magnesium hydroxide 8%
Ordor removing lotion 8%
Stabilizer 0.8%
Methane-siliconic acid potassium solution 0.4%
Silica solution 15%
Lithium metasilicate solution 20%
Defoaming agent 0.1%
Thickener 1%
Production explanation: 1, deionized water, dispersing agent, wetting agent low speed 300-500 are weighed and turns stirring 3 minutes in advance, adds hydroxyl second Defoaming agent is added in ylmethyl cellulose, stirring after five minutes.2, turn that titanium dioxide, kaolin, talcum is added in middling speed 800-1000 Powder and modified magnesium hydroxide, high speed dispersion 30-40 minutes.3, lotion is added, is in alkali with methane-siliconic acid potassium solution regulation system Character state.4, lithium metasilicate solution, defoaming agent, thickener are added.5, the thickener added is slowly added to after need to being diluted with water.
Embodiment three,
It is as follows for the preparation ratio of each section in the present invention:
Deionized water 18%
Dispersing agent 0.6%
Wetting agent 0.2%
Hydroxyethylmethylcellulose 0.3%
Defoaming agent 0.3%
Titanium dioxide 22%
Kaolin 6%
Talcum powder 5%
Modified magnesium hydroxide 4%
Ordor removing lotion 5%
Stabilizer 0.4%
Methane-siliconic acid potassium solution 0.3%
Silica solution 7%
Lithium metasilicate solution 30%
Defoaming agent 0.2%
Thickener 0.7%
Production explanation: 1, deionized water, dispersing agent, wetting agent low speed 300-500 are weighed and turns stirring 3 minutes in advance, adds hydroxyl second Defoaming agent is added in ylmethyl cellulose, stirring after five minutes.2, turn that titanium dioxide, kaolin, talcum is added in middling speed 800-1000 Powder and modified magnesium hydroxide, high speed dispersion 30-40 minutes.3, lotion is added, is in alkali with methane-siliconic acid potassium solution regulation system Character state.4, lithium metasilicate solution, defoaming agent, thickener are added.5, the thickener added is slowly added to after need to being diluted with water.
The present invention is not limited to the above embodiments, can be implemented described in the content of present invention and has the good result.

Claims (5)

1. a kind of preparation method with A grades of fire-proof function interior wall inorganic environment-friendly coating
Deionized water 17-27%
Dispersing agent 0.4-0.8%
Wetting agent 0.1-0.3%
Hydroxyethylmethylcellulose 0.1-0.3%
Defoaming agent 0.15-0.4%
Titanium dioxide 15-22%
Kaolin 5-12%
Talcum powder 4-8%
Modified magnesium hydroxide 3-8%
Elastic emulsion 3-8%
Stabilizer 0.2-0.8%
Methane-siliconic acid potassium solution 0.1-0.4%
Silica solution 5-15%
Lithium metasilicate solution 20-30%
Defoaming agent 0.1-0.4%
Thickener 0.2-1%.
2. being free of APEO according to the method described in claim 1, the wetting agent has to comply with environmental requirement.
3. according to the method described in claim 1, the silica sol modulus is greater than 2.5;Lithium metasilicate solution production modulus is greater than 3.0。
4. according to the method described in claim 1, must assure that slurry is in alkaline state after addition methane-siliconic acid potassium solution.
5. according to the method described in claim 1, modified magnesium hydroxide need to be with partial size less than 40 microns.
CN201811360064.7A 2018-11-15 2018-11-15 A kind of preparation method with A grades of fire-proof function interior wall inorganic environment-friendly coating Pending CN109554006A (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201811360064.7A CN109554006A (en) 2018-11-15 2018-11-15 A kind of preparation method with A grades of fire-proof function interior wall inorganic environment-friendly coating

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110776765A (en) * 2019-10-26 2020-02-11 沪宝新材料科技(上海)股份有限公司 Inorganic primer for interior walls and preparation method thereof
CN113278313A (en) * 2021-04-29 2021-08-20 亚士创能科技(乌鲁木齐)有限公司 Single-component water-based inorganic coating and preparation method and application thereof
CN114410138A (en) * 2021-12-01 2022-04-29 广州昊特建材有限公司 Inorganic waterproof flame-retardant coating and preparation method thereof
CN115260810A (en) * 2022-07-28 2022-11-01 广州集泰化工股份有限公司 Environment-friendly flame-retardant anti-pollution coating and preparation method and application thereof
CN115717003A (en) * 2022-11-30 2023-02-28 江苏集萃道路工程技术与装备研究所有限公司 Environment-friendly inorganic water-resistant anti-cracking fireproof interior wall coating and preparation method thereof

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JP2014148444A (en) * 2013-02-01 2014-08-21 Kansai Thermal Insulating Industry Co Ltd Refractory coating material containing aluminum hydroxide as main component and its manufacturing method
CN107216693A (en) * 2017-05-19 2017-09-29 海洋化工研究院有限公司 Inorganic expansive fireproof coating and preparation method
CN107267006A (en) * 2016-04-08 2017-10-20 南京唯才新能源科技有限公司 A kind of aeroge water-borne heat-insulating fireproof coating and preparation method thereof
CN107619626A (en) * 2017-08-21 2018-01-23 合肥科天水性科技有限责任公司 A kind of aqueous high-temperature-resistant high humidity inorganic coating and preparation method thereof
CN107779090A (en) * 2017-10-18 2018-03-09 厦门固克涂料集团有限公司 Coating of the compound organic fluorinated silicone of inorganic silicic acid lithium potassium solution and preparation method thereof

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CN107267006A (en) * 2016-04-08 2017-10-20 南京唯才新能源科技有限公司 A kind of aeroge water-borne heat-insulating fireproof coating and preparation method thereof
CN107216693A (en) * 2017-05-19 2017-09-29 海洋化工研究院有限公司 Inorganic expansive fireproof coating and preparation method
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CN107779090A (en) * 2017-10-18 2018-03-09 厦门固克涂料集团有限公司 Coating of the compound organic fluorinated silicone of inorganic silicic acid lithium potassium solution and preparation method thereof

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110776765A (en) * 2019-10-26 2020-02-11 沪宝新材料科技(上海)股份有限公司 Inorganic primer for interior walls and preparation method thereof
CN113278313A (en) * 2021-04-29 2021-08-20 亚士创能科技(乌鲁木齐)有限公司 Single-component water-based inorganic coating and preparation method and application thereof
CN113278313B (en) * 2021-04-29 2022-05-24 亚士创能科技(乌鲁木齐)有限公司 Single-component water-based inorganic coating and preparation method and application thereof
CN114410138A (en) * 2021-12-01 2022-04-29 广州昊特建材有限公司 Inorganic waterproof flame-retardant coating and preparation method thereof
CN114410138B (en) * 2021-12-01 2023-02-28 广州昊特建材有限公司 Inorganic waterproof flame-retardant coating and preparation method thereof
CN115260810A (en) * 2022-07-28 2022-11-01 广州集泰化工股份有限公司 Environment-friendly flame-retardant anti-pollution coating and preparation method and application thereof
CN115717003A (en) * 2022-11-30 2023-02-28 江苏集萃道路工程技术与装备研究所有限公司 Environment-friendly inorganic water-resistant anti-cracking fireproof interior wall coating and preparation method thereof
CN115717003B (en) * 2022-11-30 2023-11-14 江苏集萃道路工程技术与装备研究所有限公司 Environment-friendly inorganic water-resistant, crack-resistant and fireproof interior wall coating and preparation method thereof

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Application publication date: 20190402

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