CN109537316A - A kind of coloring agent, preparation method and the application on fabric printing - Google Patents
A kind of coloring agent, preparation method and the application on fabric printing Download PDFInfo
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- CN109537316A CN109537316A CN201811451633.9A CN201811451633A CN109537316A CN 109537316 A CN109537316 A CN 109537316A CN 201811451633 A CN201811451633 A CN 201811451633A CN 109537316 A CN109537316 A CN 109537316A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/667—Organo-phosphorus compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/002—Locally enhancing dye affinity of a textile material by chemical means
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/10—After-treatment with compounds containing metal
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Coloring (AREA)
Abstract
The invention discloses a kind of coloring agent, preparation method and the applications on fabric printing.The coloring agent is composed of the following raw materials in parts by weight: 60-80 parts of garden balsam, 30-50 parts of pimiento, 10-15 parts of 10-20 parts of 20-40 parts of pomelo peel, sesame oil, sticking agent, the nano-TiO for removing epidermis28-10 parts、3-5 parts and surfactant 3-5 parts of initiator.The coloring agent of invention is using natural prodcuts as raw material, green non-pollution, garden balsam and pimiento are used in mixed way, garden balsam is mixed with the slurries that pimiento boils, sticking agent is added, coloring agent printed fabrics are made in surfactant and initiator, so that fabric color is more bright-coloured, color is more bright.
Description
Technical field
The present invention relates to field of printing and dyeing, more particularly, to a kind of coloring agent, preparation method and answering on fabric printing
With.
Background technique
Textile material is handled with dye bath, makes dyestuff and fiber occur chemically or physically to be chemically combined, or generate on fiber
The technical process of insoluble coloring matter.Dyestuff should have on fiber it is certain it is water-fastness, shine, the performances such as friction, this performance
The almost the same dyestuff of dyefastness can be selected to inhomogeneous fiber in referred to as dyefastness.Chemical property phase exclusive or is done mutually
The dyestuff disturbed, can successively divide bath different fibers are dyed, dyeability it is almost the same can co-bathing dyeing.Terylene/fiber
The blended or intertexture of cellulose fiber can first use disperse dyeing of polyester, then contaminate cellulose fibre with reduction or reactive dye.Nitrile
Synthetic fibre/wool-blend fabric can successively divide bath to dye with the dye of positive ion and acid dyes.Polyamide fibre/wool-blend fabric can be selected
To wool and the lesser acid dyes of polyamide fibre dyeing ability difference or the acid mordant dye that contains with contaminating in bath, conventional dyes dyeing is uneven
It is even, and chroma-luminance is low.
Meanwhile with a large amount of introducing and application of chemical synthesis reagent, dyeing bring water body, atmosphere pollution are
Through increasingly serious.
Garden balsam contains a kind of dye molecule of reddish orange, referred to as lawsone, and this ingredient and protein have well
Affinity, the dyestuff for being often used as skin, hair, nail, leather, silk and wool use.It can also be as cloth and skin
The dyestuff and preservative of leather；Garden balsam also has antimycotic effect.And it is environmentally friendly.
Summary of the invention
In view of this, having avoided synthesis in view of the deficiencies of the prior art, it is an object of the present invention to provide a kind of coloring agent
Coloring agent bring environmental problem has reached ideal dyeing effect simultaneously.
In order to achieve the above objectives, the invention adopts the following technical scheme:
A kind of coloring agent is composed of the following raw materials in parts by weight: 60-80 parts of garden balsam, removes epidermis at 30-50 parts of pimiento
20-40 parts of pomelo peel, 10-20 parts of sesame oil, 10-15 parts of sticking agent, nano-TiO28-10 parts, 3-5 parts of initiator and surface-active
3-5 parts of agent.
Further, it is 30-50wt% dried albumen amidin that the sticking agent, which is mass fraction,.
Further, the initiator is alum.
Further, the surfactant is lecithin.
Preparation method includes the following steps:
S1: the pomelo peel of epidermis will be gone to squeeze juice, taking juice is spare；By pimiento coring, deseeding, 70-100 DEG C of hot water
It soaks 3-5 minutes thin；Capsicum meat is cut into the segment of 2-3cm long；
S2: the pimiento segment for adopting fresh garden balsam and S1, which adds, decocts 3-10 with the boiling of the weight such as capsicum and garden balsam boiling
Minute, sesame oil is added, sticking agent and surfactant continue to decoct 50-60 minutes, obtain slurries；
S3: it is dried to powder: slurries obtained by S2 being mixed with juice obtained by S1, nano-TiO is added2, after uniform stirring, freeze-drying
It is ground into uniform powdery, both obtains coloring agent.
Its purposes on fabrics printing and dyeing is printed fabrics, is included the following steps:
Step 1: pre-treatment, by immersion treatment 10-15 minutes in textile acid supplemented solution, pH=4-5；Taking-up is dried；
Step 2: dyeing: coloring agent being dissolved in ethanol water, the coloring agent ethyl alcohol that mass fraction is 5-10% is made
Aqueous solution；Fabric obtained by step 1 is placed in the solution, 60-70 DEG C is exerted a gradual, corrupting influence on 7-12 hours, dry；The ethanol water
In, ethyl alcohol and water volume ratio 1:4-5.
Step 3: salt is washed: by step 2 treated fabric soaking and water washing 1-3 in the NaCl aqueous solution of 1-2mol/L
It is secondary, each 20-30min；
Step 4: washing: adding water to clean 2-3 times in fabric obtained by step 3, until eluate is substantially colorless；
Step 5: dry: printing and dyeing are completed in the fabric drying processing after step 4 is washed.
The beneficial effects of the present invention are:
1. coloring agent of the invention, using natural prodcuts as raw material, garden balsam and pimiento are used in mixed way by green non-pollution,
As garden balsam mass percent increases, the uniformity of color is more easy to control in dyeing process, is painted faster, with pimiento
The increase of mass percent, colouring speed is slower and slower, and the bright and beautiful degree of color is higher and higher.Garden balsam and pimiento are boiled
Slurries mixing, sticking agent is added, coloring agent printed fabrics are made in surfactant and initiator, so that fabric color is more fresh
Gorgeous, color is more bright.
2. pomelo peel is added in coloring agent, on the one hand the juice of extraction can be improved the brightness of color, on the other hand have
Improve the advantage of coloring agent smell.By nano-TiO2It is added in coloring agent, it is main in nano-titanium dioxide and garden balsam first
Ingredient lawsone forms hexa-atomic chelate by chelation, and the hydrogen bond of lawsone acts on each other with nano-titanium dioxide,
The stability for enhancing coloring agent has research surface in the case where intermolecular distance is close enough, and lawsone can be by from group
Entering inside the porous structure of nano-titanium dioxide equipped with sequence further enhances the stability and cloth of coloring agent
Acid and alkali-resistance, high/low temperature and oil resistance.
3. dyeing preparation method of the invention is simple, environmental protection, dyeing is simple and easy to do, convenient for promoting.
Specific embodiment
Embodiment 1
A kind of coloring agent is composed of the following raw materials in parts by weight: 60 parts of garden balsam, 30 parts of pimiento, the pomelo peel for removing epidermis
20 parts, 10 parts of sesame oil, 10 parts of sticking agent, nano-TiO28 parts, 3 parts of initiator and 3 parts of surfactant；The sticking agent is matter
Amount score is 30wt% dried albumen amidin；The initiator is alum；The surfactant is lecithin.
Preparation method includes the following steps:
S1: the pomelo peel of epidermis will be gone to squeeze juice, taking juice is spare；Pimiento coring, deseeding, 70 DEG C of hot water leachings are thin
3 minutes；Capsicum meat is cut into the segment of 2cm long；
S2: the pimiento segment for adopting fresh garden balsam and S1, which adds, decocts 3 points with the boiling of the weight such as capsicum and garden balsam boiling
Clock is added sesame oil, sticking agent initiator and surfactant and continues to decoct 50 minutes, obtains slurries；
S3: it is dried to powder: slurries obtained by S2 being mixed with juice obtained by S1, nano-TiO is added2, after uniform stirring, freeze-drying
It is ground into uniform powdery, both obtains complex staining agent.
Its purposes on fabrics printing and dyeing is printed fabrics, is included the following steps:
Step 1: pre-treatment, by immersion treatment 10 minutes, pH=4 in textile acid supplemented solution；Taking-up is dried；
Step 2: dyeing: coloring agent being dissolved in ethanol water, the coloring agent ethyl alcohol that mass fraction is 5wt% is made
Aqueous solution；Fabric obtained by step 1 is placed in the solution, 60 DEG C are exerted a gradual, corrupting influence on 7 hours, dry；In the ethanol water, second
Pure and mild water volume ratio 1:4.
Step 3: salt is washed: by step 2 treated fabric soaking and water washing 1 time in the NaCl aqueous solution of 1mol/L, often
Secondary 20min；
Step 4: washing: adding water to clean 2 times in fabric obtained by step 3, until eluate is substantially colorless；
Step 5: dry: printing and dyeing are completed in the fabric drying processing after step 4 is washed.
Embodiment 2
A kind of coloring agent is composed of the following raw materials in parts by weight: 80 parts of garden balsam, 50 parts of pimiento, the pomelo peel for removing epidermis
40 parts, 20 parts of sesame oil, 15 parts of sticking agent, nano-TiO210 parts, 5 parts of initiator and 5 parts of surfactant；The sticking agent is matter
Amount score is 50wt% dried albumen amidin；The initiator is alum；The surfactant is lecithin.
Preparation method includes the following steps:
S1: the pomelo peel of epidermis will be gone to squeeze juice, taking juice is spare；By pimiento coring, deseeding, 100 DEG C of hot water leachings
It is 5 minutes thin；Capsicum meat is cut into the segment of 3cm long；
S2: the pimiento segment for adopting fresh garden balsam and S1, which adds, decocts 10 points with the boiling of the weight such as capsicum and garden balsam boiling
Clock is added sesame oil, sticking agent initiator and surfactant and continues to decoct 60 minutes, obtains slurries；
S3: it is dried to powder: slurries obtained by S2 being mixed with juice obtained by S1, nano-TiO is added2, after uniform stirring, freeze-drying
It is ground into uniform powdery, both obtains complex staining agent.
Its purposes on fabrics printing and dyeing is printed fabrics, is included the following steps:
Step 1: pre-treatment, by immersion treatment 15 minutes, pH=5 in textile acid supplemented solution；Taking-up is dried；
Step 2: dyeing: coloring agent being dissolved in ethanol water, the coloring agent ethanol water that mass fraction is 10% is made
Solution；Fabric obtained by step 1 is placed in the solution, 70 DEG C are exerted a gradual, corrupting influence on 12 hours, dry；In the ethanol water, ethyl alcohol
With water volume ratio 1:5.
Step 3: salt is washed: by step 2 treated fabric soaking and water washing 3 times in the NaCl aqueous solution of 2mol/L, often
Secondary 30min；
Step 4: washing: adding water to clean 3 times in fabric obtained by step 3, until eluate is substantially colorless；
Step 5: dry: printing and dyeing are completed in the fabric drying processing after step 4 is washed.
Embodiment 3
A kind of coloring agent is composed of the following raw materials in parts by weight: 60-80 parts of garden balsam, removes epidermis at 30-50 parts of pimiento
30 parts of pomelo peel, 15 parts of sesame oil, 12 parts of sticking agent, nano-TiO29 parts, 4 parts of initiator and 4 parts of surfactant；The fixation
Agent is that mass fraction is 40% dried albumen amidin；The initiator is alum；The surfactant is lecithin.
Preparation method includes the following steps:
S1: the pomelo peel of epidermis will be gone to squeeze juice, taking juice is spare；Pimiento coring, deseeding, 85 DEG C of hot water leachings are thin
4 minutes；Capsicum meat is cut into the segment of 2.5cm long；
S2: the pimiento segment for adopting fresh garden balsam and S1, which adds, decocts 6 points with the boiling of the weight such as capsicum and garden balsam boiling
Clock is added sesame oil, sticking agent, initiator and surfactant and continues to decoct 55 minutes, obtains slurries；
S3: it is dried to powder: slurries obtained by S2 being mixed with juice obtained by S1, nano-TiO is added2, after uniform stirring, freeze-drying
It is ground into uniform powdery, both obtains complex staining agent.
Its purposes on fabrics printing and dyeing is printed fabrics, is included the following steps:
Step 1: pre-treatment, by immersion treatment 10-15 minutes in textile acid supplemented solution, pH=4.5；Taking-up is dried；
Step 2: dyeing: coloring agent being dissolved in ethanol water, the coloring agent ethanol water that mass fraction is 8% is made
Solution；Fabric obtained by step 1 is placed in the solution, 65 DEG C are exerted a gradual, corrupting influence on 10 hours, dry；In the ethanol water, ethyl alcohol
With water volume ratio 1:4.5.
Step 3: salt is washed: by step 2 treated fabric soaking and water washing 2 times in the NaCl aqueous solution of 1.5mol/L,
Each 25min；
Step 4: washing: adding water to clean 2 times in fabric obtained by step 3, until eluate is substantially colorless；
Step 5: dry: printing and dyeing are completed in the fabric drying processing after step 4 is washed.
Embodiment 4
A kind of coloring agent is composed of the following raw materials in parts by weight: 70 parts of garden balsam, 35 parts of pimiento, the pomelo peel for removing epidermis
25 parts, 14 parts of sesame oil, 11 parts of sticking agent, nano-TiO28 parts, 3 parts of initiator and 5 parts of surfactant；The sticking agent is matter
Amount score is 35wt% dried albumen amidin；The initiator is alum；The surfactant is lecithin.
Preparation method is shown in embodiment 3.
Its purposes on fabrics printing and dyeing is printed fabrics, and specific steps are shown in embodiment 3.
Embodiment 5
A kind of coloring agent is composed of the following raw materials in parts by weight: 75 parts of garden balsam, 45 parts of pimiento, the pomelo peel for removing epidermis
35 parts, 18 parts of sesame oil, 14 parts of sticking agent, nano-TiO29 parts, 5 parts of initiator and 5 parts of surfactant；The sticking agent is matter
Amount score is 45wt% dried albumen amidin；The initiator is alum；The surfactant is lecithin.
Preparation method is shown in embodiment 3.
Its purposes on fabrics printing and dyeing is printed fabrics, and specific steps are shown in embodiment 3.
Comparative example 1
Comparative example 1 is substantially the same manner as Example 3, the difference is that, remove nano-TiO2。
Comparative example 2
Comparative example 2 is substantially the same manner as Example 3, the difference is that, with etc. the garden balsams of weight replace pimiento.
Comparative example 3
Comparative example 3 is substantially the same manner as Example 3, the difference is that, with etc. the pimientos of weight replace garden balsam.
The Apparent Depth and fastness of 1 fabric of table
| Sample | K/S | Dry grinding fastness | Wet fastness of rubbing |
| Embodiment 1 | 10.62 | 4-5 | 4-5 |
| Embodiment 2 | 10.63 | 4-5 | 4-5 |
| Embodiment 3 | 10.86 | 4-5 | 4-5 |
| Embodiment 4 | 10.70 | 4-5 | 4-5 |
| Embodiment 5 | 10.72 | 4-5 | 4-5 |
| Comparative example 1 | 10.80 | 3-4 | 3-4 |
| Comparative example 2 | 11.22 | 4 | 4 |
| Comparative example 3 | 10.10 | 4 | 4 |
As shown in Table 1, coloring agent provided by the invention has excellent dry, wet fastness of rubbing, apparent deep at 4 grades or more
Degree is uniform, between 10.60-10.86；Apparent Depth is deeper compared with Example 3 for comparative example 1, illustrates to remove nano-TiO2
Afterwards, nano-TiO2With the intermolecular event resolves of garden balsam, while it also disappears to the bridging effect of Anthraquinones molecule；It is dry,
Wet fastness of rubbing reduces, and illustrates nano-TiO2Have the function of enhancing its dry, wet fastness of rubbing.Dry, the wet fastness of rubbing of comparative example 2,3
It reduces, it is more secured to illustrate that garden balsam cooperates with dyeing to dye than one-component with pimiento.
Finally, it is stated that the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, this field is common
Other modifications or equivalent replacement that technical staff makes technical solution of the present invention, without departing from technical solution of the present invention
Spirit and scope, be intended to be within the scope of the claims of the invention.
Claims (7)
1. a kind of coloring agent, which is characterized in that be composed of the following raw materials in parts by weight: 60-80 parts of garden balsam, pimiento 30-50
Part, 10-15 parts of 10-20 parts of 20-40 parts of pomelo peel, sesame oil, sticking agent, the nano-TiO for removing epidermis28-10 parts、3-5 parts of initiator
With 3-5 parts of surfactant.
2. coloring agent according to claim 1, which is characterized in that the sticking agent is that mass fraction is the dry egg of 30-50wt%
White powder aqueous solution.
3. coloring agent according to claim 1, which is characterized in that the initiator is alum.
4. coloring agent according to claim 1, which is characterized in that the surfactant is lecithin.
5. a kind of preparation method of any one of -4 coloring agents according to claim 1, which comprises the steps of:
S1: the pomelo peel of epidermis will be gone to squeeze juice, taking juice is spare；Pimiento coring, deseeding, 70-100 DEG C of hot water leaching is thin
3-5 minutes；Capsicum meat is cut into the segment of 2-3cm long；
S2: the pimiento segment for adopting fresh garden balsam and S1, which adds, decocts 3-10 points with the boiling of the weight such as capsicum and nail petal boiling
Sesame oil is added in clock, and sticking agent and surfactant continue to decoct 50-60 minutes, obtains slurries；
S3: it is dried to powder: slurries obtained by S2 being mixed with juice obtained by S1, nano-TiO is added2, after uniform stirring, freeze-drying is crushed
At uniform powdery, coloring agent is both obtained.
6. the method for any one of the application claim 1-4 coloring agent printed fabrics, which comprises the steps of:
Step 1: pre-treatment, by immersion treatment 10-15 minutes in textile acid supplemented solution, pH=4-5；Taking-up is dried；
Step 2: dyeing: coloring agent being dissolved in ethanol water, it is water-soluble that the coloring agent ethyl alcohol that mass fraction is 5-10% is made
Liquid；Fabric obtained by step 1 is placed in the solution, 60-70 DEG C is exerted a gradual, corrupting influence on 7-12 hours, dry；In the ethanol water,
Ethyl alcohol and water volume ratio 1:4-5；
Step 3: salt is washed: by step 2 treated fabric soaking and water washing 1-3 times in the NaCl aqueous solution of 1-2mol/L, often
Secondary 20-30min；
Step 4: washing: adding water to clean 2-3 times in fabric obtained by step 3, until eluate is substantially colorless；
Step 5: dry: printing and dyeing are completed in the fabric drying processing after step 4 is washed.
7. according to the method described in claim 6, it is characterized in that, the coloring agent side of preparation according to claim 5
Method is prepared.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113026399A (en) * | 2020-12-30 | 2021-06-25 | 盐城工学院 | Dyeing method of nylon fiber |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113026399A (en) * | 2020-12-30 | 2021-06-25 | 盐城工学院 | Dyeing method of nylon fiber |
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