CN109516767A - A kind of ceramics modelled after an antique and preparation method thereof - Google Patents

A kind of ceramics modelled after an antique and preparation method thereof Download PDF

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Publication number
CN109516767A
CN109516767A CN201910013497.3A CN201910013497A CN109516767A CN 109516767 A CN109516767 A CN 109516767A CN 201910013497 A CN201910013497 A CN 201910013497A CN 109516767 A CN109516767 A CN 109516767A
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China
Prior art keywords
antique
preparation
modelled
parts
ceramics
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CN201910013497.3A
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Chinese (zh)
Inventor
张全争
李英姿
刘婉
徐康
李旭
徐创业
张雪强
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Hefei University
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Hefei University
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Priority to CN201910013497.3A priority Critical patent/CN109516767A/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/13Compounding ingredients
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00Clay-wares
    • C04B33/02Preparing or treating the raw materials individually or as batches
    • C04B33/04Clay; Kaolin
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201Alkali metal oxides or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567Treatment time
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/66Specific sintering techniques, e.g. centrifugal sintering
    • C04B2235/661Multi-step sintering

Abstract

A kind of ceramics modelled after an antique and preparation method thereof, belong to field of ceramic preparation technology.Main ceramic composition modelled after an antique is made of 40~50 parts of kaolin, 50~60 parts and 3~5 parts of sodium carbonate of Jining of Shandong Province Nanyang lake area hard paste.Ceramic system, first through ball mill ball milling mixing, forms in injection model for raw material after being sieved, being aging, and the moulded pottery not yet put in a kiln to bake for drying demoulding is fired by high temperature.Ceramic product color modelled after an antique is soft, and surface shows slightly gloss, and frosted texture is strong, and antique effect is good.The raw materials used type of preparation method is few, and preparation method is simple, can directly be burnt into without glazing, and firing temperature is low, does not need special atmosphere.

Description

A kind of ceramics modelled after an antique and preparation method thereof
Technical field
The invention belongs to field of ceramic preparation technology, it is specifically related to a kind of ceramics modelled after an antique and preparation method thereof.
Background technique
Ceramics are the great inventions of Ancient Times in China, and nowadays with the development of epoch and manufacturing technology, ceramics are not only With practical value, it is often more important that there is art culture value, it represents the improvement of people's aesthetic conceptions and living standard.With The improvement of people's living standards, enjoyment aesthetically is increasingly pursued to ceramics, the gentle and kind simple and unsophisticated art pottery is plain because of its Quality be loved by consumers, be commonly used for putting the art work or flower arrangement vessel etc., this is opened extensively to the development of ceramics modelled after an antique Wealthy market.However, existing ceramics modelled after an antique generally use surface glazing, the method for high-temperature calcination manufactures, raw materials used complexity, Technique is cumbersome, high production cost.
Summary of the invention
It is an object of the invention to the problems above-mentioned for the prior art, provide a kind of ceramics modelled after an antique, do not need at glazing Reason, does not need special atmosphere, can directly be burnt into ceramics modelled after an antique.
To solve technical problem of the invention, used technical solution are as follows: a kind of ceramics modelled after an antique, main component is by such as The raw material of lower parts by weight forms: 40~50 parts of kaolin, 50~60 parts of Jining of Shandong Province Nanyang lake area hard paste and sodium carbonate 3 ~5 parts.
The preparation method of above-mentioned ceramics modelled after an antique, steps are as follows:
1) kaolin, Jining of Shandong Province Nanyang lake area hard paste and sodium carbonate, are weighed by weight, add water in ball mill Upper ball milling mixing;
2), the mud for obtaining ball milling is sieved, is aging;
3) it is formed in the mud injection gypsum mold after, will be aging, waits and demould to obtain moulded pottery not yet put in a kiln to bake after drying;
4) moulded pottery not yet put in a kiln to bake after natural drying is fired in high temperature furnace, ceramics modelled after an antique can be obtained.
As the preferred technical solution of the present invention, in ceramic preparation modelled after an antique, with weight ratio material in step 1): ball: water For=0.8~1.2:1.0~1.4:0.4~0.8 ratio in mixing on ball mill, the ball milling mixing time is 20~40min.Step 2) mud for obtaining ball milling in crosses 80 meshes, and the aging time is 12~36h.Burning process in step 4) are as follows: first 250~ 0.5~1.5h is calcined at 350 DEG C, and 1.5~2.5h is then calcined at 700~900 DEG C, is finally calcined at 1050~1100 DEG C 0.5~1.5h, cooled to room temperature.
The beneficial effect of the present invention compared with the existing technology is:
The present invention provides a kind of ceramics modelled after an antique, and raw materials used type is few, and preparation method is simple, can directly burn without glazing At, and firing temperature is low, does not need special atmosphere, product colour is soft, and surface shows slightly gloss, and frosted texture is strong, effect modelled after an antique Fruit is good.
Detailed description of the invention
The present invention is made with attached drawing with reference to embodiments and being discussed further.
Fig. 1 is the ceramic product photo modelled after an antique of embodiment preparation.
Specific embodiment
Embodiment 1
A kind of preparation method of ceramics modelled after an antique, steps are as follows:
1) 50 parts of kaolin, 50 parts of Jining of Shandong Province Nanyang lake area hard pastes and 4 parts of sodium carbonate are weighed, with weight ratio Material: ball: water=0.8:1.2:0.8 ratio adds water in ball milling mixing 20min on ball mill.
2), the mud for obtaining ball milling crosses 80 meshes, then aging 12h.
3) it is formed in the mud injection gypsum mold after, will be aging, waits and demould to obtain moulded pottery not yet put in a kiln to bake after drying.
4) moulded pottery not yet put in a kiln to bake after natural drying is fired in high temperature furnace, ceramics modelled after an antique can be obtained.Burning process are as follows: first exist 1h is calcined at 350 DEG C, 2.5h is then calcined at 700 DEG C, and 1h, cooled to room temperature are finally calcined at 1100 DEG C.
As seen in Figure 1, the surface of firing sample shows slightly gloss, and frosted texture is strong, and antique effect is good.
Embodiment 2
A kind of preparation method of ceramics modelled after an antique, steps are as follows:
1) 40 parts of kaolin, 60 parts of Jining of Shandong Province Nanyang lake area hard pastes and 5 parts of sodium carbonate are weighed, with weight ratio Material: ball: water=1.1:1.0:0.6 ratio adds water in ball milling mixing 40min on ball mill.
2), the mud for obtaining ball milling crosses 80 meshes, then aging 36h.
3) it is formed in the mud injection gypsum mold after, will be aging, waits and demould to obtain moulded pottery not yet put in a kiln to bake after drying.
4) moulded pottery not yet put in a kiln to bake after natural drying is fired in high temperature furnace, ceramics modelled after an antique can be obtained.Burning process are as follows: first exist 1.5h is calcined at 250 DEG C, 1h is then calcined at 800 DEG C, finally calcines 1.5h at 1050 DEG C, cooled to room temperature, i.e., Ceramics modelled after an antique as shown in Figure 1 can be obtained.
Embodiment 3
A kind of preparation method of ceramics modelled after an antique, steps are as follows:
1) 46 parts of kaolin, 54 parts of Jining of Shandong Province Nanyang lake area hard pastes and 3 parts of sodium carbonate are weighed, with weight ratio Material: ball: water=1.2:1.4:0.4 ratio adds water in ball milling mixing 35min on ball mill.
2), the mud for obtaining ball milling crosses 80 meshes, then aging 25h.
3) it is formed in the mud injection gypsum mold after, will be aging, waits and demould to obtain moulded pottery not yet put in a kiln to bake after drying.
4) moulded pottery not yet put in a kiln to bake after natural drying is fired in high temperature furnace, ceramics modelled after an antique can be obtained.Burning process are as follows: first exist 0.5h is calcined at 300 DEG C, 1.5h is then calcined at 900 DEG C, finally calcines 0.5h at 1080 DEG C, cooled to room temperature, Ceramics modelled after an antique as shown in Figure 1 can be obtained.
The above content is just an example and description of the concept of the present invention, affiliated those skilled in the art It makes various modifications or additions to the described embodiments or is substituted in a similar manner, without departing from invention Design or beyond the scope defined by this claim, be within the scope of protection of the invention.

Claims (6)

1. a kind of ceramics modelled after an antique, which is characterized in that its main component is composed of the following raw materials in parts by weight: kaolin 40~50 Part, 50~60 parts and 3~5 parts of sodium carbonate of Jining of Shandong Province Nanyang lake area hard paste.
2. a kind of method for preparing ceramics modelled after an antique as described in claim 1, which is characterized in that steps are as follows:
1) kaolin, Jining of Shandong Province Nanyang lake area hard paste and sodium carbonate, are weighed by weight, add water in ball on ball mill Mill mixing;
2), the mud for obtaining ball milling is sieved, is aging;
3) it is formed in the mud injection gypsum mold after, will be aging, waits and demould to obtain moulded pottery not yet put in a kiln to bake after drying;
4) moulded pottery not yet put in a kiln to bake after natural drying is fired in high temperature furnace, ceramics modelled after an antique can be obtained.
3. preparation method as claimed in claim 2, which is characterized in that with weight ratio material in step 1): ball: water=0.8~ The ratio of 1.2:1.0~1.4:0.4~0.8 on ball mill in mixing.
4. preparation method as claimed in claim 2 or claim 3, which is characterized in that the ball milling mixing time is 20~40min.
5. preparation method as claimed in claim 2, which is characterized in that the mud for obtaining ball milling in step 2) crosses 80 meshes, The aging time is 12~36h.
6. preparation method as claimed in claim 2, which is characterized in that burning process in step 4) are as follows: first at 250~350 DEG C 0.5~1.5h of lower calcining, then at 700~900 DEG C calcine 1.5~2.5h, finally at 1050~1100 DEG C calcining 0.5~ 1.5h, cooled to room temperature.
CN201910013497.3A 2019-01-07 2019-01-07 A kind of ceramics modelled after an antique and preparation method thereof Pending CN109516767A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111187056A (en) * 2020-01-14 2020-05-22 广西职业技术学院 Preparation method of antique ceramic artware

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005162592A (en) * 2003-12-03 2005-06-23 Tonari Emura Method for forming low-temperature fired clay
CN103601464A (en) * 2013-11-16 2014-02-26 王爽 Anti-corrosion ceramic tile
CN106219981A (en) * 2016-08-05 2016-12-14 福建省德化县杰艺陶瓷有限公司 High white ceramic glaze thoroughly and the method making high ceramic whiteware thoroughly with it

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2005162592A (en) * 2003-12-03 2005-06-23 Tonari Emura Method for forming low-temperature fired clay
CN103601464A (en) * 2013-11-16 2014-02-26 王爽 Anti-corrosion ceramic tile
CN106219981A (en) * 2016-08-05 2016-12-14 福建省德化县杰艺陶瓷有限公司 High white ceramic glaze thoroughly and the method making high ceramic whiteware thoroughly with it

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
叶国珍: "南宋官窑瓷玉质感形成要素研究", 《中国陶瓷工业》 *
陈熙媛: "瓷器中国源的分析", 《2017年湖北省科学技术史学会年会》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111187056A (en) * 2020-01-14 2020-05-22 广西职业技术学院 Preparation method of antique ceramic artware

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Application publication date: 20190326