CN109470543A - The hot method for embedding of metallographic sample - Google Patents

The hot method for embedding of metallographic sample Download PDF

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Publication number
CN109470543A
CN109470543A CN201811588227.7A CN201811588227A CN109470543A CN 109470543 A CN109470543 A CN 109470543A CN 201811588227 A CN201811588227 A CN 201811588227A CN 109470543 A CN109470543 A CN 109470543A
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China
Prior art keywords
sample
increment
embedding
metallographic
tested
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CN201811588227.7A
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Chinese (zh)
Inventor
王永泽
杨燕
李英叶
赵松林
李学健
张建旗
陈志军
刘莹
吴萌萌
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Yingli Energy China Co Ltd
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Yingli Energy China Co Ltd
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Priority to CN201811588227.7A priority Critical patent/CN109470543A/en
Publication of CN109470543A publication Critical patent/CN109470543A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The present invention provides a kind of hot method for embedding of metallographic sample, are related to metallographic sample embedding technique field, comprising the following steps: prepare increment, cut sample to be tested, sample increment is made, then pass through metallographic specimen cloth and heat, metallographic specimen is finally made.The hot method for embedding of metallographic sample provided by the invention, it is pasted on increment by using by the sample to be tested of preparation, it recycles and carries out the production method of the embedding metallographic sample of hot insert in the two sides up and down of increment setting inlay, fine material such as welding can be rapidly completed, the materials such as backboard and cell piece inlay sample preparation, improve preparation efficiency, it ensure that vertical efficiency of the sample to be tested in metallographic specimen, avoid the problem of causing the exterior appearance and integrity breaks of test sample after metallographic specimen grinding and polishing, it ensure that the accuracy of test speed and testing result, this is easy to operate, preparation demand suitable for a large amount of samples to be tested, detection speed and detection effect can be effectively ensured.

Description

The hot method for embedding of metallographic sample
Technical field
The invention belongs to metallographic sample embedding technique fields, are to be related to a kind of embedding side of metallographic sample hot insert more specifically Method.
Background technique
The photovoltaic materials such as photovoltaic welding belt, backboard, cell piece are the main materials of photovoltaic module, and the quality of quality will be direct Photovoltaic module performance and safety are influenced, the power of photovoltaic module is influenced very big.During welding is welding photovoltaic component Important raw material, the quality of welding quality will directly influence the collection efficiency of photovoltaic module electric current, to the power of photovoltaic module It influences very big.The reflective solder strip of especially current large-scale popularization, welding surface reflection angle directly influence the effect of photovoltaic module Rate is promoted.Backboard is located at the back side of solar panel, to cell piece rise protection and supporting role, have reliable insulating properties, Water preventing ability, resistance to ag(e)ing.Aging important role of the structural stability of backboard to component service life and resistance to environment.Electricity Its structure of main material and technique that pond piece generates electricity as photovoltaic module have photovoltaic module performance and industry development decisive Effect.
The mode that the existing quality to welding, backboard, cell piece is tested is by being made into sample to be tested Afterwards, then to sample to be tested progressive it can detect.But since existing sample making course generallys use the cold mode inlayed, need manually Different proportion liquid is mixed, ratio is not easy to grasp in sample making course, so being easy to cause the sample of different batches The time of solidification and quality difference, cause the difference in sample making course, so there is a problem of that manufacture difficulty is big, while sample preparation The smell of middle generation also has certain harm to tester, is unfavorable for guaranteeing employee's health.
Summary of the invention
The purpose of the present invention is to provide a kind of hot method for embedding of metallographic sample, to solve cold edge existing in the prior art Panel carries out the technical issues of sample preparation difficulty is big, smell is unfavorable for operator's health.
To achieve the above object, the technical solution adopted by the present invention is that: a kind of hot method for embedding of metallographic sample is provided, including Following steps:
It prepares increment: according to the specification of embedding die, making increment, the height of increment in embedding die using inlay Bottom surface for the 1/3-3/4 of embedding die height, embedding die is vertical with side wall;
It cuts sample to be tested: according to the height of increment, cutting height sample to be tested 3-5mm shorter than increment height;
Sample increment is made: standing increment to cooling, sample to be tested is bonded in the peripheral surface of increment with viscose glue, is obtained Sample increment, increment are arranged along the direction of the bottom surface perpendicular to sample to be tested;
Metallographic specimen cloth: after the bottom of the sample preparation chamber of pointing machine spreads one layer of smooth inlay, sample increment is put Enter, spreads inlay to surfacing in the periphery of sample increment and top;
Metallographic specimen is made: opening pointing machine, inlay and sample increment heat is set into metallographic specimen.
As further optimization, sample to be tested is equipped with several in the periphery of increment, and several samples to be tested are in son It uniformly arranges the periphery of sample.
As further optimization, the outer peripheral surface of increment and the top surface of increment are vertical.
As further optimization, viscose glue is double faced adhesive tape or glue.
As further optimization, the height of sample to be tested is lower than the top surface 2-3mm of increment in sample increment.
As further optimization, the lower end of sample to be tested is higher than the bottom surface 2-3mm of increment in sample increment.
As further optimization, increment is cylinder component, and sample to be tested is strip component, and the main shaft of strip component is flat Row is in increment main shaft.
As further optimization, increment is cuboid component, and sample to be tested is tabular component, the plate face of tabular component with The bonding of increment outer wall.
As further optimization, pointing machine is controllable temperature pointing machine.
As further optimization, the interior chamber size of embedding die is less than the interior chamber size of sample preparation chamber.
The beneficial effect of the hot method for embedding of metallographic sample provided by the invention is: metallographic sample hot insert provided by the invention Embedding method pastes on increment by using by the sample to be tested of preparation, recycles and inlay is arranged in the two sides up and down of increment The production method for carrying out the embedding metallographic sample of hot insert, can be rapidly completed the fine material such as materials such as welding, backboard and cell piece Inlay sample preparation, improve preparation efficiency, ensure that vertical efficiency of the sample to be tested in metallographic specimen, avoid metallographic specimen The problem of exterior appearance and integrity breaks of test sample are caused after grinding and polishing, ensure that the standard of test speed and testing result True property, this is easy to operate, and suitable for the preparation demand of a large amount of samples to be tested, detection speed and detection effect can be effectively ensured.
Detailed description of the invention
It to describe the technical solutions in the embodiments of the present invention more clearly, below will be to embodiment or description of the prior art Needed in attached drawing be briefly described, it should be apparent that, the accompanying drawings in the following description is only of the invention some Embodiment for those of ordinary skill in the art without any creative labor, can also be according to these Attached drawing obtains other attached drawings.
Fig. 1 is the overlooking structure diagram for the metallographic sample that the embodiment of the present invention one provides;
Fig. 2 is the schematic view of the front view of Fig. 1;
Fig. 3 is the overlooking structure diagram of metallographic sample provided by Embodiment 2 of the present invention;
Fig. 4 is the schematic view of the front view of Fig. 3;
Wherein, each appended drawing reference in figure:
100- increment;200- sample to be tested.
Specific embodiment
In order to which technical problems, technical solutions and advantages to be solved are more clearly understood, tie below Accompanying drawings and embodiments are closed, the present invention will be described in further detail.It should be appreciated that specific embodiment described herein is only To explain the present invention, it is not intended to limit the present invention.
It should be noted that the orientation or positional relationship of the instructions such as term " on ", "lower", "top", "bottom", "inner", "outside" To be based on the orientation or positional relationship shown in the drawings, be merely for convenience of description of the present invention and simplification of the description, rather than indicate or It implies that signified device or element must have a particular orientation, be constructed and operated in a specific orientation, therefore should not be understood as Limitation of the present invention.
Also referring to Fig. 1 to Fig. 4, now the hot method for embedding of metallographic sample provided by the invention is illustrated.Metallographic phase sample The hot method for embedding of product, comprising the following steps:
It prepares increment 100: according to the specification of embedding die, making increment 100, increment in embedding die using inlay 100 height is the 1/3-3/4 of embedding die height.Because the side wall of the embedding die used with bottom surface be it is vertical, The outer peripheral surface for the increment 100 produced is also vertical with the top surface of increment 100;
It cuts sample to be tested 200: according to the height of increment 100, cutting the to be measured of height 3-5mm highly shorter than increment 100 Sample 200;
Sample increment is made: standing increment 100 to cooling, sample to be tested 200 is bonded in son with double faced adhesive tape or glue The peripheral surface of sample 100 obtains sample increment, and increment 100 is arranged along the direction of the bottom surface perpendicular to the sample to be tested 200,; Sample to be tested 200 is equipped with several in the periphery of increment 100, and several samples to be tested 200 are uniformly arranged in the periphery of increment 100 Cloth.The height of sample to be tested 200 is lower than the top surface 2-3mm of increment 100 in sample increment.Sample to be tested 200 is if it is strip structure Part then can choose the increment 100 using cylindrical shape or rectangular-shape, if sample to be tested 200 is tabular component, most The increment 100 of rectangular-shape is used well." several " are meant that two or more, unless otherwise clearly specific limit It is fixed.
Metallographic specimen cloth: one layer of smooth inlay is spread in the bottom of the sample preparation chamber of the pointing machine with temperature controlling function Afterwards, sample increment is put into, finally spreads the surfacing of inlay to inlay in the periphery of sample increment and top;Sample preparation chamber Interior chamber size be greater than embedding die interior chamber size.The ingredient of the inlay of the inlay and production increment that are added in sample preparation chamber It is identical.
Metallographic specimen is made: opening pointing machine, inlay and sample increment heat is set into metallographic specimen.
The hot method for embedding of metallographic sample provided by the invention, compared with prior art, metallographic sample heat provided by the invention Method for embedding pastes on increment by using by the sample to be tested of preparation, and the setting in the two sides up and down of increment is recycled to inlay Material carries out the production method of the embedding metallographic sample of hot insert, and the fine material such as materials such as welding, backboard and cell piece can be rapidly completed Material inlays sample preparation, improves preparation efficiency, ensure that vertical efficiency of the sample to be tested in metallographic specimen, avoids metallographic examination The problem of exterior appearance and integrity breaks of test sample are caused after sample grinding and polishing ensure that test speed and testing result Accuracy, this is easy to operate, and suitable for the preparation demand of a large amount of samples to be tested, detection speed and detection effect can be effectively ensured, The health of operator will not be impacted simultaneously, there is good practicability.
Embodiment one:
Also referring to Fig. 1 to Fig. 2, the following are strip samples to be tested to carry out the embedding step of hot insert:
According to the strip structure and length dimension of strip sample to be tested, cylindrical embedding die is selected, using inlaying Material makes increment 100 in embedding die, and the height of increment 100 is the 1/2 of embedding die height, guarantees increment 100 obtained The top surface of circumferential surface and increment 100 be mutually perpendicular to;
According to the height of increment 100, cut the height sample to be tested 200 4mm shorter than 100 height of increment, select six to Cut six samples to be tested 200 are bonded in increment 100 with double faced adhesive tape or glue after increment 100 is cooling by sample Peripheral surface, six samples to be tested 200 uniformly arrange on the periphery of increment 100, and the main shaft of sample to be tested and increment Main shaft is parallel, obtains sample increment, and the height of sample to be tested 200 is lower than the top surface 2mm of increment 100 in sample increment;
Using the pointing machine with temperature controlling function, interior chamber size is greater than to the bottom of the sample preparation chamber of the interior chamber size of embedding die After portion is put into inlay, sample increment is put into, is finally putting into inlay, opens pointing machine, by inlay and sample increment heat It is set into metallographic specimen.
Embodiment two:
Also referring to Fig. 3 to Fig. 4, the following are plate samples to be tested to carry out the embedding step of hot insert:
According to the plate structure of strip sample to be tested and the length and width dimensions of shape, the embedding die of rectangular-shape is selected, Increment 100 is made in embedding die using inlay, the height of increment 100 is the 1/2 of embedding die height, made from guarantee The circumferential surface of increment 100 and the top surface of increment 100 are mutually perpendicular to;
According to the height of increment 100, cut the height sample to be tested 200 4mm shorter than 100 height of increment, select four to Cut four samples to be tested 200 are bonded in increment 100 with double faced adhesive tape or glue after increment 100 is cooling by sample Periphery four surfaces, and the surrounding outer wall of the plate face of sample to be tested and increment fits closely, and obtains sample increment, sample The height of sample to be tested 200 is lower than the top surface 2mm of increment 100 in sample;
Using the pointing machine with temperature controlling function, interior chamber size is greater than to the bottom of the sample preparation chamber of the interior chamber size of embedding die After portion is put into inlay, sample increment is put into, is finally putting into inlay, opens pointing machine, by inlay and sample increment heat It is set into metallographic specimen.
The mode of original cold inlay production metallographic sample, usually the cold inlay of tester's hand, which makes sample, has Once disadvantage: 1, different proportion liquid being mixed manually, and ratio, which is not easy to grasp, in sample making course leads to different batches Sample solidification time and quality it is different.2, manual sample preparation waste time, the temperature that distributes have to tester it is uncertain Harm.
Metallographic sample inlay refer to specimen size it is too small or it is in irregular shape cause grinding and polishing difficult, just need to inlay Embedding or clamping can make sample rubbing down convenient in this way, improve the accuracy of working efficiency and experiment.In general, needing to inlay Embedding sample has following several: tiny machine components, such as complex-shaped and superfine small sample or fine small electronics member device Part, the sample that workpiece surface decarburization layer tissue and depth need to be protected to measure.Cell piece, welding and backboard in the present embodiment is equal Belong to small part, just needs to carry out metallographic sample before testing its performance to inlay operation.
The embedding sample not deformed in the case where little suitable for low temperature and pressure of hot insert.Plastics are generally mostly used at present As inlaid material.Inlaid material has thermosetting property plastics, such as bakelite powder;There are also thermoplastics, such as polyvinyl chloride;In addition also Condensability plastics, such as epoxy resin reinforcing agent.Bakelite powder is opaque, has various colors, and harder, sample is not easy down The corrosion resistance at angle, anti-strong acid and strong base is poor.Polyvinyl chloride is translucent or transparent, the corrosion resistance of antiacid alkali It is good but softer.
The hot method for embedding of metallographic sample provided by the invention, pastes on increment by using by the sample to be tested of preparation, It recycles and carries out the production method of the embedding metallographic sample of hot insert in the two sides up and down of increment setting inlay, can be rapidly completed thin The small material such as materials such as welding, backboard and cell piece inlay sample preparation, improve preparation efficiency, ensure that sample to be tested in metallographic Vertical efficiency in sample causes the exterior appearance of test sample and asking for integrity breaks after avoiding metallographic specimen grinding and polishing Topic, ensure that the accuracy of test speed and testing result, this is easy to operate, suitable for the preparation demand of a large amount of samples to be tested, Detection speed and detection effect can be effectively ensured, while the health of operator will not be impacted, there is good reality The property used.
The above is merely preferred embodiments of the present invention, be not intended to limit the invention, it is all in spirit of the invention and Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within principle.

Claims (10)

1. the hot method for embedding of metallographic sample, it is characterised in that: the following steps are included:
It prepares increment (100): according to the specification of embedding die, making increment (100) in the embedding die using inlay, The height of the increment (100) is the 1/3-3/4 of the embedding die height, and the bottom surface of the embedding die is vertical with side wall;
It cuts sample to be tested (200): according to the height of the increment (100), it is shorter than the height of the increment (100) to cut height The sample to be tested (200) of 3-5mm;
Sample increment is made: standing the increment (100) to cooling, is bonded in the sample to be tested (200) with viscose glue described The peripheral surface of increment (100) obtains the sample increment, and the increment (100) is along perpendicular to the sample to be tested (200) The direction of bottom surface is arranged;
Metallographic specimen cloth: after the bottom of the sample preparation chamber of pointing machine is put into one layer of smooth inlay, by the sample increment It is put into, spreads inlay to surfacing in the periphery of the sample increment and top;
Metallographic specimen is made: opening the pointing machine, the inlay and the sample increment heat is set into metallographic specimen.
2. the hot method for embedding of metallographic sample as described in claim 1, it is characterised in that: the sample to be tested (200) is described The periphery of increment (100) is equipped with several, and several samples to be tested (200) are uniformly arranged in the periphery of the increment (100).
3. the hot method for embedding of metallographic sample as described in claim 1, it is characterised in that: the outer peripheral surface of the increment (100) with The top surface of the increment (100) is vertical.
4. the hot method for embedding of metallographic sample as described in claim 1, it is characterised in that: the viscose glue is double faced adhesive tape or glue Water.
5. the hot method for embedding of metallographic sample as described in claim 1, it is characterised in that: sample to be tested in the sample increment (200) height is lower than the top surface 2-3mm of the increment (100).
6. the hot method for embedding of metallographic sample as described in claim 1, it is characterised in that: sample to be tested in the sample increment (200) lower end is higher than the bottom surface 2-3mm of the increment (100).
7. the hot method for embedding of metallographic sample as described in claim 1, it is characterised in that: the increment (100) is cylindrical body structure Part, the sample to be tested (200) are strip component, and the main shaft of the strip component is parallel to the increment (100) main shaft.
8. the hot method for embedding of metallographic sample as described in claim 1, it is characterised in that: the increment (100) is cuboid structure Part, the sample to be tested (200) are tabular component, and the plate face of the tabular component and the increment (100) outer wall bond.
9. the hot method for embedding of metallographic sample as described in claim 1, it is characterised in that: the pointing machine is inlayed for controllable temperature Machine.
10. the hot method for embedding of metallographic sample as described in claim 1, it is characterised in that: the interior chamber size of the embedding die Less than the interior chamber size of the sample preparation chamber.
CN201811588227.7A 2018-12-25 2018-12-25 The hot method for embedding of metallographic sample Pending CN109470543A (en)

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Cited By (4)

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Publication number Priority date Publication date Assignee Title
CN111257092A (en) * 2020-04-10 2020-06-09 昆明理工大学 Fixing method for polished metal and mineral sheet samples
CN111487113A (en) * 2020-04-08 2020-08-04 西安泰力松新材料股份有限公司 Metallographic sample preparation embedding tool and embedding method
CN112683182A (en) * 2020-12-30 2021-04-20 国高材高分子材料产业创新中心有限公司 Method for testing thickness of metal wire coating
CN112781966A (en) * 2020-12-10 2021-05-11 崇义章源钨业股份有限公司 Method for estimating consumption of hard alloy insert

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111487113A (en) * 2020-04-08 2020-08-04 西安泰力松新材料股份有限公司 Metallographic sample preparation embedding tool and embedding method
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CN111257092A (en) * 2020-04-10 2020-06-09 昆明理工大学 Fixing method for polished metal and mineral sheet samples
CN112781966A (en) * 2020-12-10 2021-05-11 崇义章源钨业股份有限公司 Method for estimating consumption of hard alloy insert
CN112781966B (en) * 2020-12-10 2023-05-16 崇义章源钨业股份有限公司 Method for estimating amount of cemented carbide inserts
CN112683182A (en) * 2020-12-30 2021-04-20 国高材高分子材料产业创新中心有限公司 Method for testing thickness of metal wire coating

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Application publication date: 20190315