CN109464344A - A kind of plant flowers water spot-eliminating composition and preparation method thereof and skin care application - Google Patents
A kind of plant flowers water spot-eliminating composition and preparation method thereof and skin care application Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
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Abstract
The present invention relates to skin care fields, more particularly to a kind of plant flowers water spot-eliminating composition and preparation method thereof and skin care application.It will contain in the present invention and be applied in facial treatment essence by the plant flowers water spot-eliminating composition of primary raw material of peach blossom water, in conjunction with trehalose, print plus fruit seed oil, the effect of beauty and skin care of camellia seed oil and peony seed oil, a kind of leading nti-freckle is prepared according to the dispensing method of monarch in Chinese medicine, brilliant white and reparation skin, also it can achieve the facial treatment essence liquid for nourishing moisturizing, and apply it among facial mask.
Description
Technical field
The present invention relates to skin care fields, more particularly to a kind of plant flowers water spot-eliminating composition and preparation method thereof
With skin care application.
Background technique
China's facial mask market scale is big, and demand of the consumer to facial mask effect still focuses primarily upon replenishing water and preserving moisture instantly,
Future customer will increasingly segment the demand of cosmetics and polynary, and in addition to traditional moisturizing whitening, consumer expects to have more
For the facial mask of sexual function, its specific skin, such as careful pore, after-sun recovery, whitening skin lightening are solved the problems, such as.
Peach blossom is the traditional gardens flowers and trees in China, and tree state is graceful, and limb is luxuriant and well-spaced, and flower is plump, beautiful in colour, is early spring
One of important sight flower tree species.The fruit of peach is famous fruit;Peach-pit can extract oil;Its branch, leaf, fruit, root can be used as medicine;Mahogany
It is fine and closely woven hard, it is used for engraving.
Contain the nutriments such as Kaempferol, coumarin, trifolin and vitamin A, B, C in peach blossom, these substances can expand
Blood vessel, promotion of blood circulation are opened, skin of moistening improves blood circulation, promotes skin-nourishing and oxygen supply, makes the rouge for promoting human senility
Brown quality accelerates excretion, prevents melanin from depositing in skin, so as to effectively prevent chloasma, freckle, blackspot.And peach blossom
In also be rich in vegetable protein and the amino acid in free state, be easy to be absorbed by the skin, to prevention and treatment dry skin, coarse and wrinkle
Deng effectively, the disease resistance of skin can also be enhanced, it is of great advantage to skin.
Nowadays people greatly increase the time in life and work in face of computer and mobile phone, and will cause dry skin has
Microgroove, the colour of skin turn yellow, long spottiness, and black eye is serious etc., and there are a large amount of electrostatic charges, Yi Jiju dust, behaviour in computer screen surface
The exposed place such as the face of author, becomes easily infected by these pollutants, on the face it is possible that macula, can cause cutaneous pigmentation.
Existing freckle-removing mask effect is unobvious, though and contain in facial mask nti-freckle ingredient use have freckle effect, skin can be made
At certain damage, new skin problem is formed.
Summary of the invention
Aiming at the shortcomings in the prior art, providing a kind of plant flowers water spot-eliminating composition will not using natural component nti-freckle
It injures skin and causes new skin problem, and have effects that moisturizing whitening to skin while nti-freckle.
Another object of the present invention is to provide a kind of applications of plant flowers water spot-eliminating composition.
A further purpose of the present invention is to provide a kind of tender type facial mask of skin lightening of spot-eliminating composition of water containing plant flowers.
A further object of the present invention is to provide a kind of preparation method and application of the tender type facial mask essence of skin lightening.
In order to solve the above technical problems, the technical solution adopted by the present invention is that:
A kind of plant flowers water spot-eliminating composition, by peach blossom water, Jasmine flower water, bigarabe flower extract, print plus fruit seed oil, oil
Tea-seed oil, peony seed oil composition.
Further, the plant flowers water spot-eliminating composition, is grouped as by each group of following parts by weight: peach blossom water 62.33
~79.85 parts, Jasmine 8~12 parts of water of flower, 8~12 parts of bigarabe flower extract, print adds 0.1~0.15 part of fruit seed oil, tea seed
0.1~0.15 part, 0.1~0.15 part of peony seed oil of oil.
Preferably, 71.39~74.48 parts of peach blossom water, Jasmine 9~12 parts of water of flower, 8~11 parts of bigarabe flower extract, print
Add 0.1~0.12 part of fruit seed oil, 0.1~0.12 part of camellia seed oil, 0.1~0.12 part of peony seed oil.
A kind of application of the plant flowers water spot-eliminating composition in facial mask.
Further, the facial mask includes mask substrate and the tender type facial mask essence of skin lightening;The mask substrate is eucalyptus
Suede facial mask cloth, the tender type facial mask essence of skin lightening contain the plant flowers water spot-eliminating composition.
Mask substrate uses eucalyptus suede facial mask cloth in the present invention, and eucalyptus suede facial mask cloth is relatively thick but not generates when in use negative
Load, the small carrier fluid amount in eucalyptus suede mask substrate aperture is high, and drain rate is high when use, eucalyptus suede facial mask cloth using natural fiber eucalyptus fibers with
Lyocell fibers carry out mixing manufacture, safety and environmental protection.The eucalyptus suede facial mask cloth that the present invention uses is purchased from Xi Fu Science and Technology Ltd..
A kind of application of the plant flowers water spot-eliminating composition in facial mask, the tender type facial mask essence of skin lightening is by A
It is mutually made with B phase raw material, the plant flowers water spot-eliminating composition is contained in the B phase.
Further, the A phase is grouped as by each group of following parts by weight: 0.6~1 part of trehalose, butanediol 1~1.5
Part, methyl gluceth -200.5~0.9 part, 0.1~0.3 part of dipotassium glycyrrhizinate, 0.1~0.3 part of Sodium Hyaluronate, glycerol
0.6~0.9 part, 0.1~0.3 part of allantoin, 0.05~0.1 part of laruyl alcohol phosphate potassium, 0.3~0.5 part of Scleroglucan, propylene
Sour (ester) class/0.1~0.3 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and 0.2~0.3 part of parahydroxyacet-ophenone;
The B phase is grouped as by each group of following parts by weight: 62.33~79.85 parts of peach blossom water, Jasmine flower water 8~12
Part, 8~12 parts of bigarabe flower extract, print plus 0.1~0.15 part of fruit seed oil, 0.1~0.15 part of camellia seed oil, peony seed oil 0.1
~0.15 part, 0.05~0.15 part of arginine, 0.2~0.5 part of decoyl hydroximic acid, 0.03~0.05 part of glycerol caprylate and 1,2-
0.2~0.5 part of pentanediol.
Preferably, in the A phase: 1.2~1.4 parts of butanediol, methyl gluceth -200.7~0.9 part, glycyrrhizic acid
0.2~0.3 part of dipotassium, 0.2~0.3 part of Sodium Hyaluronate, 0.7~1 part of trehalose, 0.7~0.9 part of glycerol, allantoin 0.2~
0.3 part, 0.08~0.1 part of laruyl alcohol phosphate potassium, 0.4~0.5 part of Scleroglucan, acrylic acid (ester) class/C10-30 alkanol third
0.1~0.2 part of olefin(e) acid ester cross-linked polymer, 0.1~0.2 part of parahydroxyacet-ophenone;
62.33~79.85 parts of peach blossom water in the B phase, Jasmine 8~12 parts of water of flower, 8~12 parts of bigarabe flower extract,
Print plus 0.1~0.15 part of fruit seed oil, 0.1~0.15 part of camellia seed oil, 0.1~0.15 part of peony seed oil, decoyl hydroximic acid 0.03
~0.04 part, 0.04~0.05 part of glycerol caprylate, 1,2- 0.3~0.5 part of pentanediol, 0.08~0.12 part of arginine.
A kind of application of the plant flowers water spot-eliminating composition in facial mask, specific preparation step are as follows:
S1. A phase raw material is added in water phase pot, stirring heating is stirred, kept the temperature spare;
S2. it by the A phase raw material homogeneous in step S1, vacuumizes, constant temperature is for a period of time;
When being S3. cooled to certain temperature, B phase raw material is added, stirs;
S4. it discharges after cooling down, stands a period of time;
S5. examine qualification to obtain the final product.
Further, which is characterized in that warming temperature is 80~87 DEG C in the step S1, and holding temperature is 80 DEG C;
In step S2, homogenizing time is 2~5 minutes;Thermostat temperature is 82 DEG C, and constant temperature time is 15 minutes;
The temperature that cools down in step S3 is 45 DEG C;
The temperature that cools down in step S4 is 38 DEG C, and time of repose is 30 minutes.
Using the combination principle of monarch in Chinese medicine in the present invention, wherein peach blossom water primarily serves desalination color as monarch drug in a prescription
Spot accelerates the discharge of lipofuscin element and melanin in skin, achievees the effect that nti-freckle.Ministerial drug is bigarabe extract, camellia seed oil
And peony seed oil, three kinds of ministerial drugs all have and lighten the stain, and improve the effect of the colour of skin, but effectiveness is imitated not as good as the nti-freckle of monarch drug in a prescription peach blossom water
Fruit, as a kind of auxiliary nti-freckle ingredient, the effect of certain reparation moisturizing can also be played.Adjutant is Jasmine Hua Shui and Yin Jia
Fruit seed oil, Jasmine flower water can play the role of cleaning skin, reduce skin surface grease, facilitate monarch drug in a prescription and ministerial drug to skin
The infiltration of skin, makes skin fully absorb nutriment, improves the utilization rate of effective component, and print plus fruit seed oil can repair stemness skin
Skin forms one layer of water-retaining film in skin surface, plays the role of moisturizing.
Trehalose is added in the present invention, is formed one layer of special film in skin surface, skin can be helped to resist extraneous
Poor environment has very strong moistening effect.
Compared with prior art, beneficial effect is:
1. peach blossom used in the present invention flower water can moisturize the skin, improve the vigor of cell, reach have rosy cheeks, skin
It moistens bright and clean, flexible cosmetic result, blood vessel can also be expanded, improve blood circulation, promote skin-nourishing and oxygen supply,
So that the lipofuscin element for promoting human senility is accelerated excretion, prevent melanin chronic deposition in skin, so that effectively prevention is yellow
Foxiness, freckle, blackspot;The Jasmine flower effective pore refining of water energy used, can help to clean with the fat secretion of balance skin
Skin drives away greasy and goes acne;The bigarabe flower extract used can highlight with whitening, Kohakuhi, to improve the colour of skin not uniform dark
It is heavy, reduction fat secretion can also be reduced.
It, can be special in one layer of cell surface formation 2. trehalose used in the present invention has very excellent moisture-keeping function
Protective film, the mucus being precipitated from film can not only moisturize the skin cell, can also radiate external heat, prevent
Keratinization occurs for skin, can also avoid skin sunburn and melanin deposition.
3. VA, VE, niacin, carrotene, unsaturated fatty acid content are abundant in peony seed oil used in the present invention,
The fine and smooth sense and elasticity of skin, while energy delaying senility, wrinkle resistant, the calm pigment of removing can be enhanced;Used in the present invention
Content of polyunsaturated fatty acid is up to 90% in print plus fruit seed oil, is easy to be absorbed by the skin, can repair dry skin, can be with
Ventilative water-retaining film is formed in skin surface, weakens the moisture loss of deep skin, moistens skin holding smooth flexible;It uses
Camellia seed oil in ingredient be easy to be absorbed by the skin, can uvioresistant, prevent sunburn and reduce wrinkle, to chloasma, sunburn
It is very effective, the skin smooth of people can also be made, moistened.
4. the flower water of Jasmine used in the present invention can clean the skin, then promote skin by peach blossom flower water and peony seed oil
The quick discharge of the pigementation and skin excreta of skin, bigarabe flower extract have the function of desalination to skin speckle, may be used also
To improve skin complexion, then further moisturizing carried out to skin by camellia seed oil, print plus fruit seed oil, trehalose etc., it is moist
The effects of, it allows the skin to access and adequately repairs and maintain.And the present invention is matched by the administrated method of monarch in Chinese medicine
Other compositions are closed, the effectiveness of each component is fully played, being capable of mutually coordinated cooperation conditioning skin.
Specific embodiment
To facilitate the understanding of the present invention, present invention work more comprehensively, is meticulously described below in conjunction with embodiment, but this hair
Bright protection scope is not limited to embodiment in detail below.
Unless otherwise defined, all technical terms used hereinafter and the normally understood meaning of those skilled in the art
It is identical.Technical term used herein is intended merely to the purpose of description specific embodiment, it is no intended to limit of the invention
Protection scope.
Unless otherwise specified, various raw material, reagent, the instrument and equipment etc. used in the present invention can pass through city
Field is commercially available or can be prepared by existing method.
Material composition of the present invention removes specified otherwise, is that regular market purchase obtains, and for convenience of description, provides part original
Expect that optional acquiring way is as follows:
Peach blossom is spent water (be purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd): peach blossom spend in contain Kaempferol, coumarin, three
Leaf beans glucoside and the nutriments such as vitamin A, B, C.These substances can expand blood vessel, promotion of blood circulation, and skin of moistening improves blood and follows
Ring promotes skin-nourishing and oxygen supply, promotes the lipofuscin element of human senility to accelerate excretion, prevents melanin chronic in skin
Deposition is also rich in vegetable protein so as to enable skin profit white light pool while effectively preventing chloasma, freckle, blackspot, prevention
Amino acid with being in free state, is easy to be absorbed by the skin, and effectively to prevention and treatment dry skin, coarse and wrinkle etc., can also enhance
The disease resistance of skin, so that skin disease, seborrhea, suppurative dermatitis, scurvy etc. are prevented and treated, it is of great advantage to skin.
A kind of autonomic function skin care raw material in the miscellaneous present invention as core.
Jasmine spends water (being purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd): containing benzyl alcohol or its rouge in Jasmine
Class, jasmone, linalool, benzoic acid linalool ester etc..Jasmine spends the effective pore refining of water energy, can be with balance skin
Fat secretion, help clean skin, drive away greasy and go acne.Cleaning is played as secondary raw material cooperation peach blossom water in the present invention
Skin, the effect of pore refining.
Bigarabe flower extract (is purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd): containing lemon in bigarabe flower extract
Alkene, capraldehyde, aldehyde C-9, dodecanoic acid, bergamio, neryl acetate, acetic acid dragon ox ester, hesperidine and neohesperidin etc.,
The sense of discomfort of small pox and acne can be cleaned, pore, bright color are restrained.It is risen in the present invention as secondary raw material cooperation peach blossom water
To the clean effect of skin care.
Print plus fruit seed oil (being purchased from bright Ji Ya): unsaturated fatty acid content reaches 90% or more in print plus fruit seed oil, wherein
Linolenic acid content is 48%, linoleic acid content 35%, oleic acid content 9%.Alpha-linolenic acid is up in print plus fruit seed oil
42.4%-51.4%, is flax acid type vegetable oil few in number, alpha-linolenic acid be human body must fatty acid, there is important life
Object function.Print plus fruit seed oil can form one layer of natural protective film in skin surface, prevent the loss of moisture and nutritional ingredient.
Camellia seed oil (is purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd): camellia seed oil is full of nutrition, and fatty acids are (no
Saturated fatty acid 93%, wherein oleic acid 82%, linoleic acid 11%), camellianin, tea polyphenols, saponin, tannin, and rich in anti-oxidant
Agent and squalene with anti-inflammatory effect, squalene and Flavonoid substances, play the role of anticancer splendid.Camellia oil is also rich in
The microelements such as vitamin E and calcium, iron, zinc, and type amino acid contained in tea oil is most in all edible oil.This hair
Bright middle as a kind of secondary raw material have the function of moisturizing, moist.
Peony seed oil (is purchased from bright Ji Ya): alpha-linolenic acid rich in peony seed oil.Peony seed oil, which has, to be promoted carefully
Born of the same parents' regeneration, the effect of anti-aging.Reach a kind of elimination skin pigment as a kind of secondary raw material cooperation peach blossom water in the present invention
Precipitating reduces wrinkle, makes that skin exquisiteness is bright and clean, flexible effect.
Trehalose (purchased from remittance thinkling sound) (CAS 99-20-7): trehalose is by two glucose molecules with 1,1- glycosidic bond structure
At nonreducing sugar, have 3 kinds of isomers i.e. trehalose (α, α), isotrehalose (β, β) and neotrehalose (α, β), and to a variety of
Bioactive substance has non-specific protective effect.Trehalose has excellent holding cell viability and large biological molecule activity
Characteristic, trehalose can form one layer of special protective film in cell surface, and the mucus being precipitated from film not only moisten skin
Skin cell also has the function of radiateing external heat.Trehalose is cooked in the present invention as a kind of secondary raw material, at it
His ingredient protects skin not by the damage of external environment to layer protecting film is capable of forming after skin nursing in skin surface, right
Skin provides further protection.
Embodiment 1
A kind of preparation method of the tender type facial mask essence of skin lightening, each group distribution ratio is as shown in embodiment 1~6.
A phase raw material are as follows: 0.9 part of trehalose, 1.4 parts of butanediol, -200.8 parts of methyl gluceth, dipotassium glycyrrhizinate
0.3 part, 0.3 part of Sodium Hyaluronate, 0.8 part of glycerol, 0.3 part of allantoin, 0.1 part of laruyl alcohol phosphate potassium, Scleroglucan 0.5
Part, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.1 and 0.2 part of parahydroxyacet-ophenone.
B phase raw material are as follows: 73.42 parts of peach blossom water, 10 parts of water of Jasmine flower, 10 parts of bigarabe flower extract, print plus fruit seed oil 0.1
Part, 0.1 part of camellia seed oil, 0.1 part of peony seed oil, 0.1 part of arginine, 0.03 part of decoyl hydroximic acid, 0.05 part of glycerol caprylate
With 0.4 part of 1,2- pentanediol.
Specific preparation step are as follows:
S1. A phase raw material is added in water phase pot, stirring is warming up to 85 DEG C, stirs, keeps the temperature at 80 DEG C standby
With;
S2. it by A phase raw material homogeneous 3 minutes in step S1, vacuumizes, constant temperature 15 minutes at 82 DEG C;
When being S3. cooled to 45 DEG C, B phase raw material is added, stirs;
S4. 38 DEG C of dischargings are cooled to, stand 30 minutes;
S5. examine qualification to obtain the final product.
Facial mask is prepared into using eucalyptus suede facial mask cloth and prepared facial mask essence.
Embodiment 2
A kind of preparation method of the tender type facial mask essence of skin lightening, each group distribution ratio is as shown in embodiment 1~6.
A phase raw material are as follows: 1 part of trehalose, 1 part of butanediol, -200.9 parts of methyl gluceth, 0.3 part of dipotassium glycyrrhizinate,
0.3 part of Sodium Hyaluronate, 0.9 part of glycerol, 0.3 part of allantoin, 0.1 part of laruyl alcohol phosphate potassium, 0.5 part of Scleroglucan, propylene
Sour (ester) class/0.3 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and 0.3 part of parahydroxyacet-ophenone.
B phase raw material are as follows: 62.33 parts of peach blossom water, 12 parts of water of Jasmine flower, 12 parts of bigarabe flower extract, print plus fruit seed oil
0.15 part, 0.15 part of camellia seed oil, 0.15 part of peony seed oil, 0.15 part of arginine, 0.04 part of decoyl hydroximic acid, glycerol caprylate
0.05 part and 0.5 part of 1,2- pentanediol.
Specific preparation step are as follows:
S1. A phase raw material is added in water phase pot, stirring is warming up to 80 DEG C, stirs, keeps the temperature at 80 DEG C standby
With;
S2. it by A phase raw material homogeneous 3 minutes in step S1, vacuumizes, constant temperature 15 minutes at 82 DEG C;
When being S3. cooled to 45 DEG C, B phase raw material is added, stirs;
S4. 38 DEG C of dischargings are cooled to, stand 30 minutes;
S5. examine qualification to obtain the final product.
Facial mask is prepared into using eucalyptus suede facial mask cloth and prepared facial mask essence.
Embodiment 3
A kind of preparation method of the tender type facial mask essence of skin lightening, each group distribution ratio is as shown in embodiment 1~6.
A phase raw material are as follows: 0.6 part of trehalose, 1 part of butanediol, -200.5 parts of methyl gluceth, dipotassium glycyrrhizinate 0.1
Part, 0.1 part of Sodium Hyaluronate, 0.6 part of glycerol, 0.1 part of allantoin, 0.05 part of laruyl alcohol phosphate potassium, 0.3 part of Scleroglucan,
Acrylic acid (ester) class/0.1 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and 0.1 part of parahydroxyacet-ophenone.
B phase raw material are as follows: 79.85 parts of peach blossom water, 8 parts of water of Jasmine flower, 8 parts of bigarabe flower extract, print plus fruit seed oil 0.1
Part, 0.1 part of camellia seed oil, 0.1 part of peony seed oil, 0.05 part of arginine, 0.02 part of decoyl hydroximic acid, 0.03 part of glycerol caprylate
With 0.2 part of 1,2- pentanediol.
Specific preparation step are as follows:
S1. A phase raw material is added in water phase pot, stirring is warming up to 85 DEG C, stirs, keeps the temperature at 80 DEG C standby
With;
S2. it by A phase raw material homogeneous 5 minutes in step S1, vacuumizes, constant temperature 15 minutes at 82 DEG C;
When being S3. cooled to 45 DEG C, B phase raw material is added, stirs;
S4. 38 DEG C of dischargings are cooled to, stand 30 minutes;
S5. examine qualification to obtain the final product.
Facial mask is prepared into using eucalyptus suede facial mask cloth and prepared facial mask essence.
Embodiment 4
A kind of preparation method of the tender type facial mask essence of skin lightening, each group distribution ratio is as shown in embodiment 1~6.
A phase raw material are as follows: 0.7 part of trehalose, 1.2 parts of butanediol, -200.6 parts of methyl gluceth, dipotassium glycyrrhizinate
0.2 part, 0.2 part of Sodium Hyaluronate, 0.7 part of glycerol, 0.2 part of allantoin, 0.06 part of laruyl alcohol phosphate potassium, Scleroglucan 0.4
Part, acrylic acid (ester) class/0.2 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and 0.2 part of parahydroxyacet-ophenone.
B phase raw material are as follows: 74.48 parts of peach blossom water, 9 parts of water of Jasmine flower, 11 parts of bigarabe flower extract, print plus fruit seed oil 0.12
Part, 0.13 part of camellia seed oil, 0.12 part of peony seed oil, 0.12 part of arginine, 0.03 part of decoyl hydroximic acid, glycerol caprylate 0.04
Part and 0.3 part of 1,2- pentanediol.
Specific preparation step are as follows:
S1. A phase raw material is added in water phase pot, stirring is warming up to 87 DEG C, stirs, keeps the temperature at 80 DEG C standby
With;
S2. it by A phase raw material homogeneous 2 minutes in step S1, vacuumizes, constant temperature 15 minutes at 82 DEG C;
When being S3. cooled to 45 DEG C, B phase raw material is added, stirs;
S4. 38 DEG C of dischargings are cooled to, stand 30 minutes;
S5. examine qualification to obtain the final product.
Facial mask is prepared into using eucalyptus suede facial mask cloth and prepared facial mask essence.
Embodiment 5
A kind of preparation method of the tender type facial mask essence of skin lightening, each group distribution ratio is as shown in embodiment 1~6.
A phase raw material are as follows: 0.8 part of trehalose, 1.3 parts of butanediol, -200.7 parts of methyl gluceth, dipotassium glycyrrhizinate
0.1 part, 0.1 part of Sodium Hyaluronate, 0.8 part of glycerol, 0.2 part of allantoin, 0.08 part of laruyl alcohol phosphate potassium, Scleroglucan 0.3
Part, acrylic acid (ester) class/0.1 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and 0.3 part of parahydroxyacet-ophenone.
B phase raw material are as follows: 72.3 parts of peach blossom water, 10 parts of water of Jasmine flower, 12 parts of bigarabe flower extract, print plus fruit seed oil 0.13
Part, 0.12 part of camellia seed oil, 0.14 part of peony seed oil, 0.14 part of arginine, 0.04 part of decoyl hydroximic acid, glycerol caprylate 0.05
Part and 0.3 part of 1,2- pentanediol.
Specific preparation step are as follows:
S1. A phase raw material is added in water phase pot, stirring is warming up to 80 DEG C, stirs, keeps the temperature at 80 DEG C standby
With;
S2. it by A phase raw material homogeneous 5 minutes in step S1, vacuumizes, constant temperature 15 minutes at 82 DEG C;
When being S3. cooled to 45 DEG C, B phase raw material is added, stirs;
S4. 38 DEG C of dischargings are cooled to, stand 30 minutes;
S5. examine qualification to obtain the final product.
Facial mask is prepared into using eucalyptus suede facial mask cloth and prepared facial mask essence.
Embodiment 6
A kind of preparation method of the tender type facial mask essence of skin lightening, each group distribution ratio is as shown in embodiment 1~6.
A phase raw material are as follows: 0.9 part of trehalose, 1.1 parts of butanediol, -200.5 parts of methyl gluceth, dipotassium glycyrrhizinate
0.3 part, 0.3 part of Sodium Hyaluronate, 0.6 part of glycerol, 0.1 part of allantoin, 0.07 part of laruyl alcohol phosphate potassium, Scleroglucan 0.5
Part, acrylic acid (ester) class/0.2 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and 0.1 part of parahydroxyacet-ophenone.
B phase raw material are as follows: 71.39 parts of peach blossom water, 12 parts of water of Jasmine flower, 11 parts of bigarabe flower extract, print plus fruit seed oil
0.14 part, 0.14 part of camellia seed oil, 0.13 part of peony seed oil, 0.08 part of arginine, 0.02 part of decoyl hydroximic acid, glycerol caprylate
0.03 part and 0.4 part of 1,2- pentanediol.
Specific preparation step are as follows:
S1. A phase raw material is added in water phase pot, stirring is warming up to 80 DEG C, stirs, keeps the temperature at 80 DEG C standby
With;
S2. after mixing evenly, homogeneous 2 minutes, vacuumize, constant temperature 15 minutes at 82 DEG C;
When being S3. cooled to 45 DEG C, B phase raw material is added, stirs;
S4. 38 DEG C of dischargings are cooled to, stand 30 minutes;
S5. examine qualification to obtain the final product.
Facial mask is prepared into using eucalyptus suede facial mask cloth and prepared facial mask essence.
Comparative example 1~4
This comparative example 1~4 provides the tender type facial mask essence of skin lightening of different component number, referring to the preparation in embodiment 1
Method, the specific following table 1 of each group number:
Comparative example 5
Preparation method in this comparative example reference embodiment 1, the difference is that, whipping temp is 75 DEG C in step S1;
Homogenizing time is 7 minutes in step S2.
Comparative example 6
Preparation method in this comparative example reference embodiment 1, the difference is that, whipping temp is 90 DEG C in step S1;
Homogenizing time is 1 minute in step S2.
Comparative example 7
Preparation method in this comparative example reference embodiment 1, the difference is that, do not cool down in step S3 and is directly added into B
The stirring of phase raw material.
Comparative example 8
Preparation method in this comparative example reference embodiment 1, the difference is that, it is not added with peach blossom water.
Comparative example 9
Preparation method in this comparative example reference embodiment 1, the difference is that, it is not added with peony seed oil, camellia seed oil
With print plus fruit seed oil.
Comparative example 10
Preparation method in this comparative example reference embodiment 1, the difference is that, it is not added with trehalose.
Comparative example 11
Preparation method in this comparative example reference embodiment 1, the difference is that, it is not added with Jasmine flower water and bigarabe flower
Extract.
Security risks substance assesses table (table 2)
Hygienic chemistry index
Chemical hygiene detection is carried out to the facial mask of preparation, examination criteria such as the following table 3:
Table 3
Chemical hygiene detection is carried out to the facial mask of Examples 1 to 6 preparation, testing result is as shown in table 4 below:
Table 4
Sensory judgments
Appearance: translucent liquid.
Smell: there is peach blossom fragrance, meet regulation odor type.
Other: nothing.
[physical and chemical index] executes standard detection by product
Cold-resistant (- 20 DEG C of 7 days test returns are without exception to room temperature): its appearance and test are preceding without obvious poor after recovery room temperature
It is different.
Heat-resisting (45 DEG C of 7 days test returns are without exception to room temperature): restore its appearance and the preceding no significant difference of test after room temperature.
Photostability (test in ultraviolet light 24 hours is without exception): without exception.
PH value (straight to survey): 6.25 " cosmetics safety technical specifications " (version in 2015) " health chemical testing method " pH value
Measurement.
Viscosity (2#, 6rpm): 1920mpa.s.
Examination criteria: QB/T 2872.
Other: nothing.
Crowd's test
The facial mask prepared in Examples 1 to 6 is subjected to crowd's test respectively, 20 people of number is divided to two groups, and every group of 10 people survey
Period 30d is tried, finds no the abnormal responses such as allergy in test.According to table test result it is found that skin in tester
The person that has spot obviously can be observed spot color and shoal, and the not spotted obvious glossiness of tester's skin rises, dry skin
Degree has clear improvement.Standards of grading are as shown in table 5, and test result is shown in Table 6.
Table 5
Scoring | Description |
80~100 | Effect is obvious/without allergic phenomena |
60~80 | Effect is general/without allergic phenomena |
40~60 | Having a degree of improves/has a little allergic phenomena |
< 40 points | No effect/allergy serious |
Table 6
Skin Irritation Test
The facial mask essence prepared in Examples 1 to 6 is done into multiple intact skin irritant test
Above-mentioned facial mask essence is observed to the irritation and allergic reaction of skin, provides reference to evaluate its safety.
(1) skin irritation test is carried out using rabbit, divides intact skin group and damage skin group, for 24 hours by rabbit before test
Back backbone diamond wool shaves off, and wipes 1d with pure water and rabbit skin and mucosa respectively, three times a day, after continuous 7d, observes skin
Whether there is or not the stimulate the reactions such as erythema, oedema.
(2) skin allergy experiment is carried out using cavy, wipes 1d with facial mask essence and guinea pig skin mucous membrane weekly, one day
3 times, continuous 5 weeks, whether there is or not the allergic reactions such as erythema, oedema for observation skin.
Experimental result:
The intact skin and damaged skin of rabbit, remove after being intended for single use or be used for multiple times for 24 hours, respectively at 1,24,48,
72h observation, is showed no erythema and oedema, and stimulate the reaction mean scores are < 0.5, nonirritant.
In guinea pig skin allergic experiment, does not occur the cutaneous anaphylaxises such as the obvious erythema of skin, oedema and other are systemic
Allergic reaction.
Therefore, facial mask essence of the invention will not cause irritative response to rabbit intact skin and damage skin, right
Guinea pig skin has good cutaneous safety without allergic reaction.
TYR enzyme inhibits test
The facial mask essence prepared in embodiment 1 is done into TYR enzyme and inhibits test.Table 7 designs for test system.
In system, by test solution, final concentration (mg/mL) gradient including positive control arbutin is 0.03125,0.0625,
0.125,0.25,0.5.
When experiment, sequentially added into test tube buffer, various concentration by test solution (including positive control), enzyme solution,
Water-bath 10min in 30 DEG C.Then substrate L- tyrosine is added, immediately begins to timing.475nm is up and down when measurement reaction 20min
Light absorption value.Using corresponding negative control as reference when measurement, calculate by test solution (including positive control) to TYR enzyme
Inhibiting rate, and according to concentration-enzyme inhibition rate estimation half-inhibitory concentration approximation.
Testing result such as the following table 8:
By testing result it is found that within the scope of experimental concentration, with the raising of concentration, become at rising to the inhibiting rate of enzyme,
And positive controls are consistently higher than by inhibiting rate of the test solution to TYR enzyme, therefore the facial mask essence in the present invention is with excellent
Whitening effect, have apparent inhibiting effect to melanin production.
Obviously, the above embodiment of the present invention be only to clearly illustrate example of the present invention, and not be pair
The restriction of embodiments of the present invention.For those of ordinary skill in the art, may be used also on the basis of the above description
To make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.It is all this
Made any modifications, equivalent replacements, and improvements etc., should be included in the claims in the present invention within the spirit and principle of invention
Protection scope within.
Claims (10)
1. a kind of plant flowers water spot-eliminating composition, which is characterized in that added by peach blossom water, Jasmine flower water, bigarabe flower extract, print
Fruit seed oil, camellia seed oil, peony seed oil composition.
2. plant flowers water spot-eliminating composition according to claim 1, which is characterized in that be grouped by each group of following parts by weight
At: 62.33 ~ 79.85 parts of peach blossom water, Jasmine 8 ~ 12 parts of water of flower, 8 ~ 12 parts of bigarabe flower extract, print adds fruit seed oil 0.1 ~ 0.15
Part, 0.1 ~ 0.15 part of camellia seed oil, 0.1 ~ 0.15 part of peony seed oil.
3. plant flowers water spot-eliminating composition according to claim 1 or claim 2, which is characterized in that by each component of following parts by weight
Composition: 71.39 ~ 74.48 parts of peach blossom water, Jasmine flower 9 ~ 12 parts of water, 8 ~ 11 parts of bigarabe flower extract, print plus fruit seed oil 0.1 ~
0.12 part, 0.1 ~ 0.12 part of camellia seed oil, 0.1 ~ 0.12 part of peony seed oil.
4. a kind of application of any one of claim 1 ~ 3 plant flowers water spot-eliminating composition in facial mask.
5. application according to claim 4, which is characterized in that the facial mask includes mask substrate and the tender type facial mask of skin lightening
Essence;The mask substrate is eucalyptus suede facial mask cloth, and the tender type facial mask essence of skin lightening contains claim 1 ~ 3 plant
Object spends water spot-eliminating composition.
6. application according to claim 4, which is characterized in that the tender type facial mask essence of skin lightening is former with B phase by A phase
Material is made, and the claim 1 ~ 3 plant flowers water spot-eliminating composition is contained in the B phase.
7. application according to claim 6, which is characterized in that the A phase is grouped as by each group of following parts by weight: seaweed
It is 0.6 ~ 1 part of sugar, 1 ~ 1.5 part of butanediol, 0.5 ~ 0.9 part of methyl gluceth -20,0.1 ~ 0.3 part of dipotassium glycyrrhizinate, transparent
0.1 ~ 0.3 part of matter acid sodium, 0.6 ~ 0.9 part of glycerol, 0.1 ~ 0.3 part of allantoin, 0.05 ~ 0.1 part of laruyl alcohol phosphate potassium, pyrenomycetes
0.3 ~ 0.5 part of glue, acrylic acid (ester) class/0.1 ~ 0.3 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and parahydroxyacet-ophenone
0.2 ~ 0.3 part;
The B phase is grouped as by each group of following parts by weight: 62.33 ~ 79.85 parts of peach blossom water, Jasmine 8 ~ 12 parts of water of flower, and bigarabe
8 ~ 12 parts of flower extract, print plus 0.1 ~ 0.15 part of fruit seed oil, 0.1 ~ 0.15 part of camellia seed oil, 0.1 ~ 0.15 part of peony seed oil, essence
0.05 ~ 0.15 part of propylhomoserin, 0.2 ~ 0.5 part of decoyl hydroximic acid, 0.03 ~ 0.05 part of glycerol caprylate and 1,2- pentanediol 0.2 ~ 0.5
Part.
8. application according to claim 7, which is characterized in that be grouped as by each group of following parts by weight:
In the A phase: 1.2 ~ 1.4 parts of butanediol, 0.7 ~ 0.9 part of methyl gluceth -20, dipotassium glycyrrhizinate 0.2 ~ 0.3
Part, 0.2 ~ 0.3 part of Sodium Hyaluronate, 0.7 ~ 1 part of trehalose, 0.7 ~ 0.9 part of glycerol, 0.2 ~ 0.3 part of allantoin, laruyl alcohol phosphoric acid
0.08 ~ 0.1 part of ester potassium, 0.4 ~ 0.5 part of Scleroglucan, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer
0.1 ~ 0.2 part, 0.1 ~ 0.2 part of parahydroxyacet-ophenone;
In the B phase: 62.33 ~ 79.85 parts of peach blossom water, Jasmine 8 ~ 12 parts of water of flower, 8 ~ 12 parts of bigarabe flower extract, Yin Jiaguo
It is 0.1 ~ 0.15 part of seed oil, 0.1 ~ 0.15 part of camellia seed oil, 0.1 ~ 0.15 part of peony seed oil, 0.03 ~ 0.04 part of decoyl hydroximic acid, sweet
0.04 ~ 0.05 part of oily caprylate, 1,2- 0.3 ~ 0.5 part of pentanediol, 0.08 ~ 0.12 part of arginine.
9. application described in a kind of claim 5 ~ 8, which is characterized in that the specific system of the tender type facial mask essence of skin lightening
Standby step are as follows:
S1. A phase raw material is added in water phase pot, stirring heating is stirred, kept the temperature spare;
S2. it by the A phase raw material homogeneous in step S1, vacuumizes, constant temperature is for a period of time;
When being S3. cooled to certain temperature, B phase raw material is added, stirs;
S4. it discharges after cooling down, stands a period of time;
S5. examine qualification to obtain the final product.
10. application according to claim 9, which is characterized in that warming temperature is 80 ~ 87 DEG C in the step S1, heat preservation
Temperature is 80 DEG C;
In step S2, homogenizing time is 2 ~ 5 minutes;Thermostat temperature is 82 DEG C, and constant temperature time is 15 minutes;
The temperature that cools down in step S3 is 45 DEG C;
The temperature that cools down in step S4 is 38 DEG C, and time of repose is 30 minutes.
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