CN109418422B - Bean milk rich in folic acid and production method thereof - Google Patents

Bean milk rich in folic acid and production method thereof Download PDF

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Publication number
CN109418422B
CN109418422B CN201710798445.2A CN201710798445A CN109418422B CN 109418422 B CN109418422 B CN 109418422B CN 201710798445 A CN201710798445 A CN 201710798445A CN 109418422 B CN109418422 B CN 109418422B
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folic acid
soybean
rich
soybean milk
germination
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CN109418422A (en
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杨润强
任文芳
王沛
顾振新
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Nanjing Agricultural University
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Nanjing Agricultural University
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23CDAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C11/00Milk substitutes, e.g. coffee whitener compositions
    • A23C11/02Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins
    • A23C11/10Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins containing or not lactose but no other milk components as source of fats, carbohydrates or proteins
    • A23C11/103Milk substitutes, e.g. coffee whitener compositions containing at least one non-milk component as source of fats or proteins containing or not lactose but no other milk components as source of fats, carbohydrates or proteins containing only proteins from pulses, oilseeds or nuts, e.g. nut milk
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/90Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Beans For Foods Or Fodder (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention relates to a bean milk rich in folic acid and a production method thereof, belonging to the technical field of food processing, and being characterized in that soybean seeds germinate by being sprayed by a citric acid buffer solution with specific pH and cultured for a certain time, wherein folic acid is enriched; the folic acid-rich germinated soybean is taken as a raw material, is pulped, is added with sodium ascorbate, white granulated sugar, xanthan gum, sodium carboxymethylcellulose, sucrose ester and monoglyceride, and is subjected to secondary homogenization, degassing, sterilization and sterile filling to prepare the folic acid-rich germinated soybean milk. The soybean milk prepared by the invention has rich nutrition and fine taste, and the rich folic acid has the functions of preventing cancer, preventing cardiovascular diseases, promoting cell metabolism and the like, thereby being an ideal health-care beverage. The folic acid content in the product reaches 10-50 mug/100 mL.

Description

Bean milk rich in folic acid and production method thereof
One, the technical field
The invention relates to a bean milk rich in folic acid and a production method thereof, belonging to the technical field of food processing.
Second, background art
Folic acid refers to tetrahydrofolic acid and derivatives thereof, and is a water-soluble B vitamin. Folic acid is present in all organisms as a cofactor for the one-carbon transfer reaction in one-carbon metabolism. Important one-carbon metabolism is nucleotide biosynthesis, amino acid metabolism (e.g., serine to glycine, histidine breakdown), and the methylation cycle (e.g., the conversion of homocysteine to methionine by demethylation), which provides a number of methyl and methylation reactions. Therefore, the influence of folate and its metabolism on cellular metabolism is of crucial importance. Inadequate folic acid intake has been shown to induce megaloblastic anemia; especially, the lack of folic acid in pregnant women can cause the development defect of fetal neural tubes. Meanwhile, low levels of folic acid intake are closely related to the occurrence of senile dementia, cardiovascular diseases and various cancers.
The soybean is rich in nutrition, high in protein content and relatively complete in amino acid composition; the fat is high in quality and contains a large amount of unsaturated fatty acid; the soybean oligosaccharide has low calorie, and the dietary fiber can reduce the serum cholesterol level; is rich in various physiologically active components such as isoflavone, gamma-aminobutyric acid, etc. After the soybean seeds germinate, life metabolic activity begins, a series of physiological and biochemical changes occur in vivo, and a large amount of endogenous enzymes are activated, so that substances with physiological activity to a human body are enriched. The lipid substance is decomposed into glycerol and fatty acid under the action of enzyme, and finally, the saccharide which can be absorbed by human body is generated; the protein is also hydrolyzed into micromolecular peptide and amino acid, which is convenient for human body to absorb; the contents of folic acid, gamma-aminobutyric acid, isoflavone and other physiologically active components are correspondingly increased. Buds and related foods thereof are unique in the food industry due to the special medical care function and are very popular with people.
The method adopts citric acid buffer solution with specific pH to spray the germinated soybean seeds, activates endogenous enzyme, enriches folic acid and strengthens the health care function of the soybean milk beverage. After the compound is compounded with sodium ascorbate, the content of vitamin C in the product is improved, and folic acid is protected to a certain extent and prevented from being degraded, so that the bean milk rich in folic acid is a functional beverage rich in vitamins.
Third, the invention
The technical problem is as follows:
the invention aims to provide the bean milk rich in folic acid and the production method thereof, which uses the citric acid buffer solution with specific pH value to spray the germinated soybean seeds, enriches the folic acid, improves the nutritional quality of the raw materials, and the product is rich in beneficial components such as folic acid, vitamin C, gamma-aminobutyric acid and the like.
The technical scheme is as follows:
the technology of the invention is as follows: spraying the soybean seeds with a citric acid buffer solution at a certain temperature for germination, and enriching folic acid; the preparation method comprises the following steps of pulping the raw materials, adding sodium ascorbate, white granulated sugar, xanthan gum, sodium carboxymethylcellulose, sucrose ester and monoglyceride, and performing secondary homogenization, degassing, sterilization and sterile filling to obtain the product, wherein the preparation method specifically comprises the following steps:
(1) spray germination
A. Selecting raw materials: selecting soybean seeds with bright color, high germination rate and complete surface as raw materials;
B. surface disinfection: introducing ozone into the soaking solution to sterilize soybean seeds for 10min, and cleaning with water to neutrality;
C. fully soaking: soaking in distilled water of 25-40 deg.C for 4-8 hr to make it fully absorb water;
D. spraying and germinating: placing the soaked soybean seeds in a germination machine, and spraying citric acid buffer solution with pH of 5-8 at 20-35 deg.C in dark for germination for 2-6 d;
(2) Preparing cooked pulp: cleaning germinated soybean, thermally activating with 90 deg.C hot steam for 4-8min, peeling, adding purified water at a ratio of material to liquid of 1: 5-1: 8, grinding with colloid mill, feeding soybean milk into a pulp storage tank via pipeline, decocting at 80 deg.C for 2-5min, and filtering with 80 mesh filter cloth to obtain cooked pulp;
(3) mixing and blending: after cooling the cooked paste, adding 1-2% of sodium ascorbate, 1-3% of white granulated sugar, 0.1-0.3% of xanthan gum, 0.08-0.13% of sodium carboxymethylcellulose, 0.07-0.09% of sucrose ester and 0.07-0.09% of monoglyceride according to the material-to-liquid ratio (w/v);
(4) homogenizing and degassing: homogenizing the blended slurry under 25-30MPa, performing secondary homogenization under 30-40MPa, and degassing at 65-75 deg.C under 0.06-0.08 MPa;
(5) and (3) sterilization and filling: instantly sterilizing soybean milk at 135 deg.C for 5-10s by known method, cooling to room temperature with plate heat exchanger, and aseptically packaging.
Has the advantages that:
compared with the prior art, the invention has the following advantages:
(1) the soybean seeds are sprayed by a citric acid buffer solution to germinate and enrich folic acid, so that the nutritive value and the health-care function of the soybean milk are improved;
(2) the folic acid content of the product prepared by the invention is 10-50 mug/100 mL, and the product is particularly suitable for pregnant women.
Fourth, detailed description of the invention
Example 1
Selecting soybean seeds with bright color, high germination rate and complete surface, introducing ozone into the soaking solution to sterilize the soybean seeds for 10min, soaking in distilled water at 30 ℃ for 6h, placing the soybean seeds in a germination machine, and spraying citric acid buffer solution with pH of 6 to sprout in dark for 2 d; cleaning germinated soybean, thermally activating with 90 deg.C hot steam for 4-8min, peeling, adding purified water at a ratio of 1: 6, grinding with colloid mill, feeding soybean milk into a pulp storage tank via pipeline, decocting at 80 deg.C for 2-5min, and filtering with 80 mesh filter cloth to obtain cooked pulp; after the cooked paste is cooled, 1 percent of sodium ascorbate, 3 percent of white granulated sugar, 0.2 percent of xanthan gum, 0.10 percent of sodium carboxymethyl cellulose, 0.07 percent of sucrose ester and 0.09 percent of monoglyceride are added according to the material-to-liquid ratio; performing secondary homogenization on the blended slurry under 25MPa and 40MPa respectively, and then degassing at 75 ℃ under the vacuum degree of 0.06 MPa; sterilizing soybean milk at 135 deg.C for 5-10s, cooling to room temperature with plate heat exchanger, and aseptically packaging. The folic acid content in the product is 30 mug/100 mL.
Example 2
The soybean seed selection, disinfection, soaking and spray germination method is the same as that of the example 1, the spray solution uses a citric acid buffer solution with the pH value of 7, and the germination is carried out for 4 days in a dark place; cleaning germinated soybean, thermally activating with 90 deg.C hot steam for 4-8min, peeling, adding purified water at a ratio of 1: 7, grinding with colloid mill, feeding soybean milk into a pulp storage tank via pipeline, decocting at 80 deg.C for 2-5min, and filtering with 80 mesh filter cloth to obtain cooked pulp; after the cooked paste is cooled, adding 2 percent of sodium ascorbate, 2 percent of white granulated sugar, 0.1 percent of xanthan gum, 0.2 percent of sodium carboxymethylcellulose, 0.09 percent of sucrose ester and 0.07 percent of monoglyceride according to the material-liquid ratio; performing secondary homogenization on the mixed and blended slurry under the pressure of 30MPa and 35MPa respectively, and then degassing at the temperature of 75 ℃ under the vacuum degree of 0.07 MPa; sterilizing, cooling, and aseptically packaging the same as example 1. The folic acid content of the product is 50 mug/100 mL.
Example 3
The soybean seed selection, disinfection, soaking and spray germination method is the same as that of the example 1, the spray solution uses a citric acid buffer solution with the pH value of 8, and the germination is carried out for 4 days in a dark place; cleaning germinated soybean, thermally activating with 90 deg.C hot steam for 4-8min, peeling, adding purified water at a ratio of 1: 8, grinding with colloid mill, feeding soybean milk into a pulp storage tank via pipeline, decocting at 80 deg.C for 2-5min, and filtering with 80 mesh filter cloth to obtain cooked pulp; after the cooked paste is cooled, 1.5 percent of sodium ascorbate, 3 percent of white granulated sugar, 0.15 percent of xanthan gum, 0.15 percent of sodium carboxymethyl cellulose, 0.08 percent of sucrose ester and 0.08 percent of monoglyceride are added according to the material-to-liquid ratio; performing secondary homogenization on the mixed and blended slurry under the pressure of 30MPa and 35MPa respectively, and then degassing at the temperature of 75 ℃ under the vacuum degree of 0.07 MPa; sterilizing, cooling, and aseptically packaging the same as example 1. The folic acid content in the product is 40 mug/100 mL.
The embodiments of the present invention have been described in detail above, but this is only an example for easy understanding and should not be construed as limiting the scope of the present invention. Also, various equivalent changes or substitutions are possible for those skilled in the art according to the technical solution of the present invention and the description of the preferred embodiment thereof, but all such changes or substitutions shall fall within the protection scope of the claims of the present invention.

Claims (2)

1. A production method of soybean milk rich in folic acid is characterized in that soybean seeds are sprayed and germinated by citric acid buffer solution to obtain soybean sprouts rich in folic acid, sodium ascorbate, white granulated sugar, xanthan gum, sodium carboxymethylcellulose, sucrose ester and monoglyceride are added after pulping, and the soybean milk is prepared by secondary homogenization, degassing, sterilization and sterile filling, and specifically comprises the following steps:
(1) spray germination
A. Selecting raw materials: selecting soybean seeds with bright color, high germination rate and complete surface as raw materials;
B. surface disinfection: introducing ozone into the soaking solution to sterilize soybean seeds for 10min, and cleaning with water to neutrality;
C. fully soaking: soaking in distilled water of 25-40 deg.C for 4-8 hr to make it fully absorb water;
D. spraying and germinating: placing the soaked soybean seeds in a germination machine, and spraying citric acid buffer solution with pH of 5-8 at 20-35 deg.C in dark for germination for 2-6 d;
(2) preparing cooked slurry: cleaning germinated soybean, thermally activating with 90 deg.C hot steam for 4-8min, peeling, adding purified water at a ratio of material to liquid of 1: 5-1: 8, grinding with colloid mill, feeding soybean milk into a pulp storage tank via pipeline, decocting at 80 deg.C for 2-5min, and filtering with 80 mesh filter cloth to obtain cooked pulp;
(3) Mixing and blending: after the cooked paste is cooled, adding 1-2% of sodium ascorbate, 1-3% of white granulated sugar, 0.1-0.3% of xanthan gum, 0.08-0.13% of sodium carboxymethylcellulose, 0.07-0.09% of sucrose ester and 0.07-0.09% of monoglyceride according to the material-to-liquid ratio (w/v);
(4) homogenizing and degassing: homogenizing the blended slurry under 25-30MPa, performing secondary homogenization under 30-40MPa, and degassing at 65-75 deg.C under 0.06-0.08 MPa;
(5) and (3) sterilization and filling: instantly sterilizing soybean milk at 135 deg.C for 5-10s by known method, cooling to room temperature with plate heat exchanger, and aseptically packaging.
2. The method for producing folic acid-rich soybean milk according to claim 1, wherein the folic acid content of the product is 10 to 50 μ g/100 mL.
CN201710798445.2A 2017-09-05 2017-09-05 Bean milk rich in folic acid and production method thereof Active CN109418422B (en)

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CN111700201A (en) * 2020-06-18 2020-09-25 南京农业大学 Production process of highland barley solid beverage rich in flavone
CN111700120A (en) * 2020-06-18 2020-09-25 南京农业大学 Fruit and vegetable germ soybean milk rich in phenols and production method thereof
EP4163000B1 (en) * 2021-02-19 2024-04-10 Anhui Jinhe Industrial Co., Ltd. Production apparatus and production method for sucrose-6-ester
CN115997894A (en) * 2022-12-06 2023-04-25 苏州金记食品有限公司 Germinated soybean rich in folic acid, preparation method and protein milk prepared by using germinated soybean

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CN1218631A (en) * 1997-11-27 1999-06-09 张振东 Method for producing bean milk of black soy bean
CN104286188B (en) * 2014-09-22 2017-03-29 晋城市伊健食品有限公司 A kind of soybean milk and preparation method thereof
CN106070659B (en) * 2016-06-29 2019-07-09 南京农业大学 A kind of soya-bean milk and its production technology rich in inositol -3- phosphoric acid
CN106417621A (en) * 2016-09-21 2017-02-22 徐州工程学院 Sour soybean milk and preparation technology thereof

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Inventor after: Yang Runqiang

Inventor after: Ren Wenfang

Inventor after: Wang Pei

Inventor after: Gu Zhenxin

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Inventor before: Ren Wenfang

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