CN109402727A - A kind of bio-photon crystal and preparation method thereof - Google Patents
A kind of bio-photon crystal and preparation method thereof Download PDFInfo
- Publication number
- CN109402727A CN109402727A CN201811433915.6A CN201811433915A CN109402727A CN 109402727 A CN109402727 A CN 109402727A CN 201811433915 A CN201811433915 A CN 201811433915A CN 109402727 A CN109402727 A CN 109402727A
- Authority
- CN
- China
- Prior art keywords
- bio
- raw material
- crystal
- photon
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/16—Oxides
- C30B29/22—Complex oxides
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
The invention discloses a kind of bio-photon crystal and preparation method thereof, first by the ingredient in proportion of the oxide raw material containing metal ions such as nickel magnesium calcium iron neodymium aluminium, calcination, drying are carried out to many oxide mixed raw material and weighed, by this raw material, it is pressed into fixed shape, raw material roasting is then synthesized into a kind of polycrystalline compounds crystal raw material；Then, roasting raw material is put into single crystal growing furnace with this method is lifted by pulling growth photonic crystal after material melts, will be used after the crystal boule grown up to cutting, obtains corresponding to more bio-photon frequency photonic crystals.Crystal of the present invention can not need any electric power load at normal temperature can generate the crystal photon radiation frequency to match with human-body biological photon radiation frequency.
Description
Technical field
The invention belongs to Material Fields, and in particular to a kind of crystal manufacture.
Background technique
Modern Pathological Physiology proposes: the generation of all diseases (including human senility) all with gene (i.e.DNA) damage have
It closes.Since bio-photon byDNA It generates, turnes back, bio-photon participates in againDNA Synthesis.Accordingly, bio-light is utilized
Son radiation is to repairDNA Damage, i.e. repair cell damage, until repair tissue, organ damage are possibly realized.One as a result,
Novel medicine——Bio-photon medicine (or bio-photon medical science of recovery therapy) is come into being！Countries in the world scientist is grinding
Study carefully, develop and find a kind of biophoton emission frequency spectrum that can be generated with human body match, directly itself can generate biology
The material of photon radiation, then, for human body diseases prevention and treatment and rehabilitation.
Summary of the invention
The invention discloses a kind of biophoton emission crystal, scientific matching prescription, can wide spectrum eradiation go out and human body
Itself transmitted spectrum matches.It can reach and occur with human-body biological photon frequency spectrum“It is relevant”, that is, generate“It tangles”, can be used for disease
In rehabilitation.
The present invention is first by the ingredient in proportion of the oxide raw material containing metal ions such as nickel magnesium calcium iron neodymium aluminium, to a variety of oxygen
Compound mixed raw material carries out calcination, drying and weighs, and by this raw material, is pressed into fixed shape, then roasts raw material and synthesizes
A kind of polycrystalline compounds crystal raw material；Then, roasting raw material is put into single crystal growing furnace to use and lifts this method for material melts
Pulling growth photonic crystal afterwards will use after the crystal boule grown up to cutting, obtain corresponding to more bio-photon frequency photons crystalline substances
Body.
A kind of preparation method of bio-photon crystal, the specific steps are as follows:
(1) metal oxide powder raw material of the purity more than or equal to 99.9995% are mixed and is added in alumina powder, every kind
The additive amount of metal oxide powder is the 0.1 ~ 1% of alumina powder quality；It is then pressed into bulk, at 700 ~ 1000 DEG C
Burn 9 ~ 15h under environment, suppressed again after cooling, after 6 ~ 10h is burnt in 1000 ~ 1300 DEG C, take out cooling stand-by；
(2) raw material are made in step (1) and are put into the lifting speed for using crystal pull furnace in Iridium Crucible according to 0.5-1.5mm/h
Degree, the revolving speed shape of 6-20r/min lift to form monocrystal；Cutting uses shape after taking-up.
Metal oxide of the present invention is nickel, magnesium, calcium, iron and neodymium oxides.
Preferably, the additive amount of every kind of metal oxide powder is the 0.2% of alumina powder quality in the present invention.
Preferably, in step (1) of the present invention, it is pressed into bulk, 12h is burnt in the environment of 900 DEG C, is pressed again after cooling
System, after burn 8h in 1200 DEG C, take out cooling stand-by.
Preferably, lumpy sizes are diameter 60cm thickness 2cm in step (1) of the present invention.
The invention also discloses the bio-photon crystal being prepared using the above method.
Beneficial effects of the present invention:
The present invention prepares photonic crystal by Multimetal oxide, and preferred nickel, magnesium, calcium, iron, neodymium and aluminum metal, optimization
The combination matching of each metal oxide makes its play optimal synergistic effect, it is burnt according to the compacting of best product performance
It is re-compacted burn after, the bio-photon crystal of the more bio-photon frequencies of the correspondence is obtained after lifting is handled.It is reacting
In the process, the non-uniform volatilization and absorption water for avoiding component participate in chemical reaction.Crystal of the present invention can not need at normal temperature
Any electric power load can generate the crystal photon radiation frequency to match with human-body biological photon radiation frequency.
Specific embodiment
Embodiment 1
A kind of preparation method of bio-photon crystal, the specific steps are as follows:
(1) nickel, magnesium, calcium, iron and the neodymium metal oxide powder raw material that purity is both greater than equal to 99.9995% mix addition
In alumina powder, the additive amount of every kind of metal oxide powder is the 0.2% of alumina powder quality；Bulk is then pressed into,
Burn 12h in the environment of 900 DEG C, suppressed again after cooling, after 8h is burnt in 1200 DEG C, take out cooling stand-by；
(2) step (1) obtained raw material are put into Iridium Crucible the pull rate with crystal pull furnace according to 1.0mm/h,
The revolving speed shape of 15r/min lifts to form monocrystal；Cutting uses shape after taking-up.
Embodiment 2
A kind of preparation method of bio-photon crystal, the specific steps are as follows:
(1) nickel by purity more than or equal to 99.9995%, magnesium, calcium, iron and neodymium metal oxide powder raw material, which mix, is added oxygen
Change in aluminium powder, the additive amount of every kind of metal oxide powder is the 0.1% of alumina powder quality；It is then pressed into bulk,
Burn 15h in the environment of 700 DEG C, suppressed again after cooling, after 10h is burnt in 1000 DEG C, take out cooling stand-by；
(2) raw material are made in step (1) to be put into Iridium Crucible with pull rate of the crystal pull furnace according to 0.5mm/h, 6r/
The revolving speed shape of min lifts to form monocrystal；Cutting uses shape after taking-up.
Embodiment 3
A kind of preparation method of bio-photon crystal, the specific steps are as follows:
(1) nickel by purity more than or equal to 99.9995%, magnesium, calcium, iron and neodymium metal oxide powder raw material, which mix, is added oxygen
Change in aluminium powder, the additive amount of every kind of metal oxide powder is the 1.0% of alumina powder quality；It is then pressed into bulk,
Burn 9h in the environment of 1000 DEG C, suppressed again after cooling, after 6h is burnt in 1300 DEG C, take out cooling stand-by；
(2) step (1) obtained raw material are put into Iridium Crucible the pull rate with crystal pull furnace according to 1.5mm/h,
The revolving speed shape of 20r/min lifts to form monocrystal；Cutting uses shape after taking-up.
Claims (6)
1. a kind of preparation method of bio-photon crystal, which is characterized in that specific step is as follows:
(1) metal oxide powder raw material of the purity more than or equal to 99.9995% are mixed and is added in alumina powder, every kind
The additive amount of metal oxide powder is the 0.1 ~ 1% of alumina powder quality；It is then pressed into bulk, at 700 ~ 1000 DEG C
Burn 9 ~ 15h under environment, suppressed again after cooling, after 6 ~ 10h is burnt in 1000 ~ 1300 DEG C, take out cooling stand-by；
(2) raw material are made in step (1) and are put into the lifting speed for using crystal pull furnace in Iridium Crucible according to 0.5-1.5mm/h
Degree, the revolving speed shape of 6-20r/min lift to form monocrystal；Cutting uses shape after taking-up.
2. the preparation method of bio-photon crystal according to claim 1, which is characterized in that the metal oxide is
Nickel, magnesium, calcium, iron and neodymium oxides.
3. the preparation method of bio-photon crystal according to claim 1, which is characterized in that every kind of metal oxide powder
Additive amount be alumina powder quality 0.2%.
4. the preparation method of bio-photon crystal according to claim 1, which is characterized in that briquet in step (1)
After shape, burn 12h in the environment of 900 DEG C, suppressed again after cooling, after 8h is burnt in 1200 DEG C, take out cooling stand-by.
5. the preparation method of bio-photon crystal according to claim 1, which is characterized in that lumpy sizes in step (1)
For diameter 60cm thickness 2cm.
6. a kind of bio-photon crystal being prepared using any one of claim 1-5 the method.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811433915.6A CN109402727A (en) | 2018-11-28 | 2018-11-28 | A kind of bio-photon crystal and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811433915.6A CN109402727A (en) | 2018-11-28 | 2018-11-28 | A kind of bio-photon crystal and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109402727A true CN109402727A (en) | 2019-03-01 |
Family
ID=65455989
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811433915.6A Pending CN109402727A (en) | 2018-11-28 | 2018-11-28 | A kind of bio-photon crystal and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109402727A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001002497A (en) * | 1999-06-18 | 2001-01-09 | Nikon Corp | Optical substrate, optical device, optical system and photolithography devices using the same, and inspection of optical substrate |
| CN102485975A (en) * | 2010-12-02 | 2012-06-06 | 元亮科技有限公司 | Growth method of terbium gallium garnet crystal |
| CN104775155A (en) * | 2015-05-05 | 2015-07-15 | 山东天岳先进材料科技有限公司 | Growing method for colored alumina gem mono-crystal |
| CN106544734A (en) * | 2016-11-08 | 2017-03-29 | 黑龙江科技大学 | Double-doped potassium sodium strontium barium niobate monocrystal of Preset grating and preparation method thereof |
| CN108505117A (en) * | 2018-04-18 | 2018-09-07 | 苏州四海常晶光电材料有限公司 | Sodium calcium ytterbium ion is co-doped with YAG fast flashing crystal and preparation method thereof |
-
2018
- 2018-11-28 CN CN201811433915.6A patent/CN109402727A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001002497A (en) * | 1999-06-18 | 2001-01-09 | Nikon Corp | Optical substrate, optical device, optical system and photolithography devices using the same, and inspection of optical substrate |
| CN102485975A (en) * | 2010-12-02 | 2012-06-06 | 元亮科技有限公司 | Growth method of terbium gallium garnet crystal |
| CN104775155A (en) * | 2015-05-05 | 2015-07-15 | 山东天岳先进材料科技有限公司 | Growing method for colored alumina gem mono-crystal |
| CN106544734A (en) * | 2016-11-08 | 2017-03-29 | 黑龙江科技大学 | Double-doped potassium sodium strontium barium niobate monocrystal of Preset grating and preparation method thereof |
| CN108505117A (en) * | 2018-04-18 | 2018-09-07 | 苏州四海常晶光电材料有限公司 | Sodium calcium ytterbium ion is co-doped with YAG fast flashing crystal and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110205674B (en) | Method for preparing two-dimensional black phosphorus crystal by taking white phosphorus as raw material | |
| CN106757354A (en) | The growth of low-cost rare earth scintillation crystal | |
| CN111020697A (en) | Sn-doped tin4P3Method for efficiently preparing two-dimensional black phosphorus crystal for catalyst | |
| CN109305661A (en) | A method of preparing rhombic system black phosphorus monocrystalline | |
| CN109402727A (en) | A kind of bio-photon crystal and preparation method thereof | |
| CN108298573B (en) | Preparation method of anhydrous yttrium chloride | |
| JP2010520326A (en) | Method for producing ultraviolet-emitting magnesium pentaborate phosphor | |
| CN109502590A (en) | A method of improving sic powder yield | |
| Jouini et al. | Crystal structure and optical study of praseodymium polyphosphate Pr (PO3) 3 | |
| CN106835270A (en) | The growth of low-cost rare earth scintillation crystal | |
| JPS5935009A (en) | Preparation of silicon nitride | |
| Wang et al. | Density functional theory calculations of structural, electronic and optical properties of LaPO4: Eu | |
| CN101704673A (en) | Method for synthesizing and preparing nano-crystalline titanium carbide ceramic micro-powder at room temperature | |
| CN1034020A (en) | Preparation and the application of the plant of biological value have been improved | |
| Wang et al. | Synthesis process dependent photoluminescent properties of Zn2SiO4: Mn2+ upon VUV region | |
| CN1229473C (en) | Far infraved ray radiator and making method thereof | |
| CN102060544B (en) | Quick crystallization method for realizing amorphous silicon nitride powder by taking silica powder as additive | |
| CN109678147A (en) | A kind of production method of high purity graphite | |
| CN107501009A (en) | A kind of fertilizer specially for peanut prepared using peanut straw and preparation method thereof | |
| CN109225201A (en) | A kind of preparation method and application of micro-nano tungsten oxide | |
| Lim | Synthesis of microcrystalline LiNaCaLa (MoO 4) 3: Yb 3+/Ho 3+ upconversion phosphors and effect of Li+ on their spectroscopic properties | |
| CN101780959B (en) | Preparation method of Bi4Si3O12 nanocrystals | |
| CN107746190A (en) | Calcium oxide, calcium hydroxide preparation method, the calciner for preparing calcium oxide | |
| CN102963923B (en) | Large-scale production method for preparing gallium nitrate by using gallium | |
| Pazik et al. | Up-conversion emission and in vitro cytotoxicity characterization of blue emitting, biocompatible SrTiO 3 nanoparticles activated with Tm 3+ and Yb 3+ ions |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |