CN109381344B - Preparation method of synergistic beauty mask for improving blood circulation - Google Patents
Preparation method of synergistic beauty mask for improving blood circulation Download PDFInfo
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- CN109381344B CN109381344B CN201811303718.2A CN201811303718A CN109381344B CN 109381344 B CN109381344 B CN 109381344B CN 201811303718 A CN201811303718 A CN 201811303718A CN 109381344 B CN109381344 B CN 109381344B
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the field of beauty masks, and aims to provide a preparation method of a synergistic beauty mask for improving blood circulation. The method comprises the following steps: performing ball milling and heating reaction on lanthanum hydroxide and sodium borohydride, washing, separating and drying to obtain nano single-crystal lanthanum boride, and preparing to obtain silicon dioxide coated nano single-crystal lanthanum boride; the silicon dioxide coated nano monocrystal lanthanum boride and a gelatin solution are subjected to ultrasonic dispersion and mixing to form a suspension, and then the suspension is sprayed on one side of a non-woven fabric and is dried; and spraying the gelatin solution on the other side of the non-woven fabric, and drying to obtain the synergistic beauty mask. The invention enhances the mass transfer of the nutrient components, thereby greatly reducing the use amount of the nutrient components and further reducing the risk of skin allergy. By utilizing the light heating effect, the facial skin cooling caused by the veneering film is avoided, and particularly in winter, the facial paralysis risk can be effectively reduced. The facial mask can be preserved in dry state for a long time, and is suitable for commercialization.
Description
Technical Field
The invention relates to the field of beauty masks, in particular to a preparation method of a synergistic beauty mask for improving blood circulation.
Background
The facial mask is a category of skin care products, and is prepared by loading beauty maintaining components on a carrier such as kaolin and the like, and coating the carrier on a film material such as non-woven fabric, silk mask, tencel mask, biological fiber mask, non-woven fabric and the like. The facial mask is widely used, and the most important purpose is to make up for insufficient cleaning work of makeup removal and face washing, and realize other maintenance functions such as moisturizing, whitening, anti-aging, grease balancing and the like by matching with other essence components on the basis.
The beauty principle of the facial mask is that the facial mask temporarily isolates outside air and pollution within a short time by covering the facial mask, the skin temperature is increased, pores of the skin are expanded, sweat gland secretion and metabolism are promoted, the oxygen content of the skin is increased, products of epidermal cell metabolism and accumulated grease substances are favorably removed from the skin, moisture and nutrient components in the facial mask permeate into the cuticle of the epidermis, the skin becomes soft, and the skin is naturally bright and elastic.
Traditional masks can be classified into 7 types according to functions: cleaning facial mask, moisturizing facial mask, soothing facial mask, firming facial mask, regenerating facial mask, whitening facial mask, and moisturizing facial mask. The cleaning facial mask is the most common facial mask and can remove dirt and redundant grease in pores and remove aged cutin to make skin fresh and clean. The moisture mask contains a humectant, locks water in the mask, softens cuticles, helps skin to absorb nutrition, and is suitable for various skins. The soothing mask can quickly soothe skin, eliminate fatigue feeling, recover the luster and elasticity of the skin and is suitable for sensitive skin. The firming facial mask can shrink pores and lighten wrinkles, and is particularly suitable for people who do not have time to go to a beauty shop for nursing. The regeneration facial mask contains plant essence, softens epidermal tissues, promotes skin metabolism, and is suitable for dry or water-deficient skin. The whitening mask can thoroughly eliminate dead skin cells, has dual effects of cleaning and whitening, and ensures that the skin is tender and smooth, white and transparent. The whitening and moisturizing mask can suck out dirt and simultaneously astringe pores, thoroughly remove dead skin cells and simultaneously replenish moisture, so that the skin is soft, moist, glossy and elastic.
The mask generally needs 10-30 minutes, but the temperature of the mask and the facial skin is reduced due to the evaporation of the moisture of the mask, so that the speed of the mask for transmitting nutrient components to the skin is reduced, and the capillary vessels are shrunk due to the reduction of the temperature of the skin, so that pores are blocked, and the cosmetic effect is finally reduced. The mask from vendors usually overcomes this drawback by increasing the content of active ingredients in the mask or by using drugs that dilate blood vessels, but this also increases the risk of skin allergy. Moreover, the facial mask can also cause the microcirculation of the body surface to be interfered by the reduction of the skin temperature, and the blood vessels of local trophic nerves can be spasmodized, so that the nerve tissues are subjected to ischemia, edema and compression, and facial paralysis is easily caused. Therefore, a mask that can prevent the temperature of the face pack from dropping is very important for enhancing the beauty effect and eliminating the side effects.
Disclosure of Invention
The invention aims to solve the technical problem of overcoming the defects in the prior art and provides a preparation method of a synergistic beauty mask for improving blood circulation.
In order to solve the technical problem, the solution of the invention is as follows:
the preparation method of the synergistic beauty mask for improving blood circulation comprises the following steps:
(1) preparation of nano single crystal lanthanum boride
Dissolving sodium borohydride in Tetrahydrofuran (THF) in a ball milling tank to form a saturated solution;
weighing lanthanum hydroxide powder and sodium borohydride powder according to the molar ratio of lanthanum to boron of 1: 6, and adding the lanthanum hydroxide powder and the sodium borohydride powder into the ball milling tank; ball-milling for 2 hours to form paste, transferring the paste into a reactor, heating at 120 ℃ for 30 minutes to evaporate a solvent THF, and obtaining a mechanical mixture of lanthanum hydroxide and sodium borohydride; continuously heating to 500 ℃, preserving the heat for 2 hours, and releasing hydrogen generated by the reaction;
La(OH)3+6NaBH4→LaB6+3Na2O+13.5H2
cooling the solid product to room temperature, washing with water, centrifugally separating, and vacuum drying at 80 deg.c to obtain nanometer monocrystal lanthanum boride; (sodium oxide reacts with water to form sodium hydroxide when washed with water, and the sodium hydroxide is dissolved in water);
(2) preparation of silicon dioxide coated nano monocrystal lanthanum boride
Adding 1-5 ml of ammonia water into 90 ml of ethanol, and stirring for 30min to form a uniform solution; then 0.1-0.5 g of tetraethoxysilane is dripped, and ultrasonic dispersion is carried out for 40 minutes to form solution A;
adding 10 ml of ammonia water into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of nano single-crystal lanthanum boride to form a suspension;
dropwise adding the solution A into the suspension for silica coating, and stirring for 12h to complete coating; centrifugally separating to obtain silicon dioxide coated nano monocrystal lanthanum boride;
(3) preparing a beauty mask
Dissolving 10-30 g of gelatin in 100mL of deionized water to obtain a gelatin solution;
taking part of gelatin solution, adding 2-10 g of silicon dioxide coated nano monocrystal lanthanum boride into the gelatin solution, and performing ultrasonic dispersion and mixing to form suspension; spraying the suspension on one side of the non-woven fabric, and drying;
and spraying the rest gelatin solution on the other side of the non-woven fabric, and drying to obtain the synergistic beauty mask.
In the invention, in the step (1), the rotation speed of the ball mill is controlled to be 400 rpm; the heating rate during heating was 2 ℃/min.
In the invention, in the step (3), the gelatin is food-grade gelatin; when the suspension is used for spraying, the using amount of the suspension is controlled so that the spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is 1-15 mg/cm2。
In the present invention, the mass concentration of the ammonia water is 30 wt%.
The invention also provides a using method of the synergistic beauty mask prepared by the previous method, which is characterized in that before use, the mask is soaked in purified water at room temperature for no more than 5 min; after being taken out, the side which is not added with the silicon dioxide coated nano single crystal lanthanum boride and is only sprayed with gelatin is pasted on the face and is irradiated by an infrared lamp or exposed to sunlight, and the pasting time is not more than 30 minutes.
The invention also provides another using method of the synergistic beauty mask prepared by the previous method, before use, the mask is soaked in the natural plant extracting solution for no more than 5min at room temperature; after being taken out, the side which is not added with the silicon dioxide coated nano monocrystal lanthanum boride and is only sprayed with gelatin is pasted on the face and is irradiated by infrared rays or exposed to sunlight, and the pasting time is not more than 30 minutes; the natural plant extracting solution is prepared by the following method: pulverizing vegetables or Chinese medicinal materials with dermatogic disease treating effect, extracting, and filtering to obtain natural plant extractive solution.
As an alternative technical scheme, the gelatin preparation method can also be used for dissolving 10-30 g of gelatin in 100mL of deionized water to obtain a gelatin solution; dissolving the natural plant extract in a gelatin solution to obtain a nutrient solution, and replacing the gelatin solution for spraying in the step (3) with the nutrient solution; in the nutrient solution, the mass ratio of the natural plant extract, the gelatin and the deionized water is 0.1-5: 10-30: 100, respectively; the natural plant extract is prepared by the following method: pulverizing vegetables or Chinese medicinal materials with dermatogic disease treating effect, extracting, and filtering to obtain plant stock solution; drying the plant stock solution, and obtaining the powdered natural plant extract.
The application method of the synergistic beauty mask prepared in the alternative technical scheme comprises the following steps: before use, the mask is soaked in purified water at the temperature of 25-80 ℃, and the soaking time is not more than 5 min; after being taken out, the side which is not added with the silicon dioxide coated nano monocrystal lanthanum boride and is only sprayed with the nutrient solution is pasted on the face and is irradiated by infrared rays or exposed to sunlight, and the pasting time is not more than 30 minutes.
Description of the inventive principles:
lanthanum boride is a purple crystal, has a melting point of 2715 ℃ and is decomposed above the melting point. Insoluble in water and acid at normal temperature. Lanthanum trioxide and borax are typically dissolved in a suitable molten salt and lanthanum hexaboride is deposited on a graphite or steel cathode by electrolysis at elevated temperatures using a graphite anode. The alloy has the characteristics of high melting point and high thermionic emission performance, and can replace high-melting-point metals and alloys in the aspects of nuclear fusion reactors, thermionic power generation and the like. Lanthanum boride has a wide range of applications, and has been successfully applied to more than twenty military and high-tech fields such as radar aerospace, electronic industry, instrument and instrument, medical equipment, household appliance metallurgy, environmental protection and the like. The lanthanum hexaboride product mainly comprises amorphous, polycrystalline and monocrystal lanthanum hexaboride. In particular, lanthanum hexaboride single crystal has good characteristic of converting near infrared radiation absorption into heat, and is an ideal modifying material for avoiding the temperature reduction of the coated surface through light irradiation.
According to the invention, the photo-thermal nano material silicon dioxide is added into the facial mask to coat the nano monocrystal lanthanum boride, so that the temperature of the facial mask can be increased by utilizing light irradiation in the using process, and the speed of the facial mask for transferring nutrient components to the skin is enhanced. Avoid capillary constriction and pore occlusion, and improve skin care effect. The irradiation light used is infrared light (or sunlight).
Compared with the prior art, the invention has the beneficial effects that:
1. the invention enhances the mass transfer of the nutrient components, thereby greatly reducing the use amount of the nutrient components and further reducing the risk of skin allergy.
2. By utilizing the photoinduced heat effect, the facial skin cooling caused by the veneering film is avoided, and the facial paralysis risk can be effectively reduced particularly in winter.
3. The facial mask can be preserved in dry state for a long time, and is suitable for commercialization.
Drawings
FIG. 1 shows the morphology of the silicon dioxide coated nano-monocrystal lanthanum boride obtained in example II.
Detailed Description
The present invention will be described in further detail with reference to specific embodiments below:
the first embodiment is as follows: synthesis of lanthanum boride
Dissolving sodium borohydride in sufficient Tetrahydrofuran (THF) in a ball milling tank to form a saturated solution, and then mixing the saturated solution according to the molar ratio of the lanthanum to the boron elements of 1: weighing lanthanum hydroxide (0.19g) and sodium borohydride (0.227g) powder, adding the lanthanum hydroxide and the sodium borohydride powder into a ball milling tank, ball milling for 2 hours at the rotating speed of 400rpm, placing the mixture into a reactor, heating the mixture at 120 ℃ for 30 minutes to evaporate THF (tetrahydrofuran) solvent to obtain a mechanical mixture of lanthanum hydroxide and sodium borohydride, heating the mixture to 500 ℃ at the heating rate of 2 ℃/min, preserving the heat for 2 hours, releasing hydrogen, cooling the mixture to room temperature, washing the mixture with water, reacting the sodium oxide and the water to generate sodium hydroxide during washing with the water, dissolving the sodium hydroxide in the water, performing centrifugal separation, and performing vacuum drying at 80 ℃ to obtain the nano monocrystal lanthanum boride.
Example two: synthesis of thin-wall silicon dioxide coated nano monocrystal lanthanum boride
Sequentially adding 1 ml of ammonia water (the mass concentration is 30 wt%) into 90 ml of ethanol, continuously stirring for 30min to form a uniform solution, then dropwise adding 0.1 g of tetraethoxysilane, and performing ultrasonic dispersion for 40 min to form a solution A; adding 10 ml of ammonia water (with the mass concentration of 30 wt%) into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of the single-crystal lanthanum boride obtained in the first embodiment to form a suspension; dropwise adding the solution A into the suspension for silica coating; stirring for 12h, finishing coating, and performing centrifugal separation to obtain the thin-wall silicon dioxide coated nano monocrystal lanthanum boride.
Example three: synthesis of thickened silicon dioxide coated nano monocrystal lanthanum boride
Sequentially adding 2.5 ml of ammonia water (the mass concentration is 30 wt%) into 90 ml of ethanol, continuously stirring for 30min to form a uniform solution, dropwise adding 0.25 g of tetraethoxysilane, and performing ultrasonic dispersion for 40 min to form a solution A; adding 10 ml of ammonia water (with the mass concentration of 30 wt%) into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of the single-crystal lanthanum boride obtained in the first embodiment to form a suspension; dropwise adding the solution A into the suspension for silica coating; stirring for 12h, finishing coating, and performing centrifugal separation to obtain the thickened silicon dioxide coated nano monocrystal lanthanum boride.
Example four: synthesis of thick-wall silicon dioxide coated nano monocrystal lanthanum boride
Sequentially adding 5 ml of ammonia water (the mass concentration is 30 wt%) into 90 ml of ethanol, continuously stirring for 30min to form a uniform solution, dropwise adding 0.5 g of tetraethoxysilane, and performing ultrasonic dispersion for 40 min to form a solution A; adding 10 ml of ammonia water (with the mass concentration of 30 wt%) into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of the single-crystal lanthanum boride obtained in the first embodiment to form a suspension; dropwise adding the solution A into the suspension for silica coating; stirring for 12h, finishing coating, and performing centrifugal separation to obtain the thick-wall silicon dioxide coated nano monocrystal lanthanum boride.
Example five: preparation of synergistic beauty mask
Sequentially adding 2 ml of ammonia water (the mass concentration is 30 wt%) into 90 ml of ethanol, continuously stirring for 30min to form a uniform solution, dropwise adding 0.3 g of tetraethoxysilane, and performing ultrasonic dispersion for 40 min to form a solution A; adding 10 ml (with the mass concentration of 30 wt%) into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of the single-crystal lanthanum boride obtained in the first embodiment to form a suspension; dropwise adding the solution A into the suspension for silica coating; stirring for 12h, finishing coating, and performing centrifugal separation to obtain the silicon dioxide coated nano monocrystal lanthanum boride.
Dissolving 10g of edible gelatin from vendor in 100mL of deionized water to obtain gelatin solution; taking part of gelatin solution, adding 2g of silicon dioxide coated nano monocrystal lanthanum boride, performing ultrasonic dispersion and mixing to form suspension, and spraying the suspension on one side of a non-woven fabric for drying; spraying the rest gelatin solution on the other side of the non-woven fabric; the spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is controlled to be 1mg/cm2The gelatin spraying amount on both sides is 5mg/cm2And drying to obtain the synergistic beauty mask.
Before the facial mask is used, soaking in purified water at room temperature for 5min, taking out, and sticking one side of the non-woven fabric coated with gelatin on the face. After 30 minutes of irradiation by a 15W infrared lamp, the mask is taken down, and the beauty is finished after the face is washed by clear water, so that the skin is fully moisturized.
Example six: quick synergistic beauty mask
Sequentially adding 3 ml of ammonia water (the mass concentration is 30 wt%) into 90 ml of ethanol, continuously stirring for 30min to form a uniform solution, dropwise adding 0.4 g of tetraethoxysilane, and performing ultrasonic dispersion for 40 min to form a solution A; adding 10 ml of ammonia water (with the mass concentration of 30 wt%) into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of the single-crystal lanthanum boride obtained in the first embodiment to form a suspension; dropwise adding the solution A into the suspension for silica coating; stirring for 12h, finishing coating, and performing centrifugal separation to obtain the silicon dioxide coated nano monocrystal lanthanum boride.
Dissolving 20g of edible gelatin of vendor in 100mL of deionized water to obtain a gelatin solution; taking part of gelatin solution, adding 5g of silicon dioxide coated nano monocrystal lanthanum boride, performing ultrasonic dispersion and mixing to form suspension, and spraying the suspension on one side of a non-woven fabric for drying; spraying the rest gelatin solution on the other side of the non-woven fabric; the spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is controlled to be 8mg/cm2The spraying amount of gelatin on both sides is 32mg/cm2And drying to obtain the synergistic beauty mask.
Before the facial mask is used, soaking in purified water at room temperature for 5min, taking out, and sticking one side of the non-woven fabric coated with gelatin on the face. Because the facial mask contains more silicon dioxide coated nano monocrystal lanthanum boride, after the nano monocrystal lanthanum boride is irradiated by a 15W infrared lamp for 20 minutes, the facial mask is taken down, and the beauty is finished after the face is washed by clear water, so that the skin is quickly moisturized.
Example seven: ultrafast synergistic beauty mask
Sequentially adding 3 ml of ammonia water (the mass concentration is 30 wt%) into 90 ml of ethanol, continuously stirring for 30min to form a uniform solution, dropwise adding 0.4 g of tetraethoxysilane, and performing ultrasonic dispersion for 40 min to form a solution A; adding 10 ml of ammonia water (with the mass concentration of 30 wt%) into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of the single-crystal lanthanum boride obtained in the first embodiment to form a suspension; dropwise adding the solution A into the suspension for silica coating; stirring for 12h, finishing coating, and performing centrifugal separation to obtain the silicon dioxide coated nano monocrystal lanthanum boride.
Dissolving 20g of edible gelatin of vendor in 100mL of deionized water to obtain a gelatin solution; taking part of gelatin solution, adding 5g of silicon dioxide coated nano monocrystal lanthanum boride, performing ultrasonic dispersion and mixing to form suspension, and spraying the suspension on one side of a non-woven fabric for drying; spraying the rest gelatin solution on the other side of the non-woven fabric; the spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is controlled to be 15mg/cm2The spraying amount of gelatin on both sides is 60mg/cm2And drying to obtain the quick synergistic beauty mask.
Before the facial mask is used, soaking in purified water at room temperature for 5min, taking out, and sticking one side of the non-woven fabric coated with gelatin on the face. Because the mask contains more silicon dioxide coated nano monocrystal lanthanum boride, the mask can be taken down after being irradiated by a 15W infrared lamp for 5 minutes, and the beauty treatment is finished after the face is washed by clear water, so that the skin can be replenished with water very quickly.
Example eight: preparation of functional synergistic beauty mask
Sequentially adding 2 ml of ammonia water (the mass concentration is 30 wt%) into 90 ml of ethanol, continuously stirring for 30min to form a uniform solution, dropwise adding 0.3 g of tetraethoxysilane, and performing ultrasonic dispersion for 40 min to form a solution A; adding 10 ml (with the mass concentration of 30 wt%) into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of the single-crystal lanthanum boride obtained in the first embodiment to form a suspension; dropwise adding the solution A into the suspension for silica coating; stirring for 12h, finishing coating, and performing centrifugal separation to obtain the silicon dioxide coated nano monocrystal lanthanum boride.
Dissolving 10g of edible gelatin from vendor in 100mL of deionized water to obtain gelatin solution; taking part of gelatin solution, adding 2g of silicon dioxide coated nano monocrystal lanthanum boride, performing ultrasonic dispersion and mixing to form suspension, and spraying the suspension on one side of a non-woven fabric for drying; spraying the rest gelatin solution on the other side of the non-woven fabric; the spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is controlled to be 1mg/cm2The gelatin spraying amount on both sides is 5mg/cm2And drying to obtain the synergistic beauty mask.
100g of celery is taken, mashed and then extracted by adding 50mL of purified water, and the celery extract is obtained by filtering. Before the facial mask is used, soaking in herba Apii Graveolentis extractive solution at room temperature for 5min, taking out, and sticking one side of the non-woven fabric coated with gelatin onto face. After 30 minutes of irradiation by a 15W infrared lamp, the mask is taken down, and the beauty is finished after the face is washed by clear water, so that the effect of skin tightening is achieved.
Example nine: daily use method of functional synergistic type beauty mask
Sequentially adding 3 ml of ammonia water (the mass concentration is 30 wt%) into 90 ml of ethanol, continuously stirring for 30min to form a uniform solution, dropwise adding 0.4 g of tetraethoxysilane, and performing ultrasonic dispersion for 40 min to form a solution A; adding 10 ml of ammonia water (with the mass concentration of 30 wt%) into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of the single-crystal lanthanum boride obtained in the first embodiment to form a suspension; dropwise adding the solution A into the suspension for silica coating; stirring for 12h, finishing coating, and performing centrifugal separation to obtain the silicon dioxide coated nano monocrystal lanthanum boride.
Dissolving 20g of edible gelatin of vendor in 100mL of deionized water to obtain a gelatin solution; taking part of gelatin solution, adding 5g of silicon dioxide coated nano monocrystal lanthanum boride, performing ultrasonic dispersion and mixing to form suspension, and spraying the suspension on one side of a non-woven fabric for drying; spraying the rest gelatin solution on the other side of the non-woven fabric; the spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is controlled to be 8mg/cm2The spraying amount of gelatin on both sides is 32mg/cm2And drying to obtain the synergistic beauty mask.
100g of celery is taken, mashed and then extracted by adding 50mL of purified water, and the celery extract is obtained by filtering. Before the facial mask is used, soaking in herba Apii Graveolentis extractive solution at room temperature for 5min, taking out, and sticking one side of the non-woven fabric coated with gelatin onto face. Because the facial mask contains more silicon dioxide coated nano monocrystal lanthanum boride, the facial mask is taken down after being dried in the sun for 20 minutes, and the beauty is finished after the face is washed by clear water, so that the effect of skin tightening is achieved.
Example ten: simple preparation of beauty mask
Sequentially adding 5 ml of ammonia water (the mass concentration is 30 wt%) into 90 ml of ethanol, continuously stirring for 30min to form a uniform solution, dropwise adding 0.5 g of tetraethoxysilane, and performing ultrasonic dispersion for 40 min to form a solution A; adding 10 ml of ammonia water (with the mass concentration of 30 wt%) into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of the single-crystal lanthanum boride obtained in the first embodiment to form a suspension; dropwise adding the solution A into the suspension for silica coating; stirring for 12h, finishing coating, and performing centrifugal separation to obtain the silicon dioxide coated nano monocrystal lanthanum boride.
Dissolving 30g of edible gelatin from vendors in 100mL of deionized water to obtain a gelatin solution, adding 10g of silicon dioxide coated nano monocrystal lanthanum boride, performing ultrasonic dispersion and mixing to form a suspension, and spraying the suspension on one side of a non-woven fabric for drying; the spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is 5mg/cm2The spraying amount of the gelatin is 15mg/cm2。
Smashing 100g of mint, adding 50mL of purified water for extraction, filtering to obtain a mint extracting solution, drying to obtain an extract, dissolving the extract in 100mL of 10 wt% gelatin solution to obtain a nutrient solution, wherein the mass ratio of the extract, gelatin and deionized water in the nutrient solution is 0.1: 10: 100, respectively; spraying onto the opposite side of the non-woven fabric coated with silicon dioxide coated with nanometer single crystal lanthanum boride in an amount of 15mg/cm2Wherein the extract content is 0.15mg/cm2Gelatin content of 14.85mg/cm2The simple beauty mask is obtained by drying and has the effect of killing mites.
Example eleven: simple beauty mask using method
The simple beauty mask obtained in the tenth example is soaked in purified water at 25 ℃ for 5min, and one side of the non-woven fabric sprayed with the nutrient solution is attached to the face. After being dried in the sun for 10 minutes, the facial mask is taken off, and the face is washed by clear water to finish the beauty treatment.
Example twelve: application method of onion beauty mask
Dissolving 30g of edible gelatin from vendors in 100mL of deionized water to obtain a gelatin solution, adding 10g of the silicon dioxide coated nano single-crystal lanthanum boride obtained in the second embodiment, performing ultrasonic dispersion and mixing to form a suspension, spraying the suspension on one side of a non-woven fabric, and drying. The spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is 5mg/cm2The spraying amount of the gelatin is 15mg/cm2。
Smashing 100g of onion, adding 50mL of purified water for extraction, filtering to obtain an onion extracting solution, drying to obtain an extract, dissolving the extract in 100mL of 20 wt% gelatin solution to obtain a nutrient solution, wherein the mass ratio of the extract, gelatin and deionized water in the nutrient solution is 2.5: 20: 100, respectively; spraying onto the opposite side of the non-woven fabric coated with silicon dioxide coated with nanometer single crystal lanthanum boride in an amount of 15mg/cm2Wherein the extract content is 1.67mg/cm2Gelatin of 13.33mg/cm2And drying to obtain the simple beauty mask.
Soaking in 50 deg.C purified water for 5min, and applying the non-woven fabric side only sprayed with nutrient solution to face. After being dried in the sun for 20 minutes, the facial mask is taken off, and the face is washed by clear water to finish the beauty treatment, thereby achieving the effect of promoting blood circulation of the facial skin.
Example thirteen: application method of ginger beauty mask
Dissolving 30g of edible gelatin from vendors in 100mL of deionized water to obtain a gelatin solution, adding 10g of the silicon dioxide coated nano single-crystal lanthanum boride obtained in the second embodiment, performing ultrasonic dispersion and mixing to form a suspension, spraying the suspension on one side of a non-woven fabric, and drying. The spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is 5mg/cm2The spraying amount of the gelatin is 15mg/cm2。
20g of ginger is mashed and then 50mL of purified water is addedExtracting, filtering to obtain onion extract, drying to obtain extract, dissolving in 100mL of 30 wt% gelatin solution to obtain nutrient solution, wherein the mass ratio of the extract, gelatin and deionized water in the nutrient solution is 5: 30: 100, respectively; spraying on the other side of the non-woven fabric coated with silicon dioxide coated with nano monocrystal lanthanum boride, wherein the spraying amount is 15mg/cm2Wherein the extract content is 2.14mg/cm2Gelatin of 12.86mg/cm2And drying to obtain the simple beauty mask.
Soaking in 80 deg.C purified water for 5min, and applying the non-woven fabric side only sprayed with nutrient solution to face. After being dried in the sun for 30 minutes, the facial mask is taken off, and the face is washed by clear water to finish the beauty treatment, thereby achieving the effect of eliminating acne.
Finally, it should be noted that the above-mentioned list is only a specific embodiment of the present invention. It is obvious that the present invention is not limited to the above embodiments, but many variations are possible. All modifications which can be derived or suggested by a person skilled in the art from the disclosure of the present invention are to be considered within the scope of the invention.
Claims (5)
1. A preparation method of a synergistic beauty mask for improving blood circulation is characterized by comprising the following steps:
(1) preparation of nano single crystal lanthanum boride
Dissolving sodium borohydride in tetrahydrofuran in a ball milling tank to form a saturated solution;
weighing lanthanum hydroxide powder and sodium borohydride powder according to the molar ratio of lanthanum to boron of 1: 6, and adding the lanthanum hydroxide powder and the sodium borohydride powder into the ball milling tank; ball-milling for 2 hours to form paste, transferring the paste into a reactor, heating at 120 ℃ for 30 minutes to evaporate a solvent THF, and obtaining a mechanical mixture of lanthanum hydroxide and sodium borohydride; continuously heating to 500 ℃, preserving the heat for 2 hours, and releasing hydrogen generated by the reaction; cooling the solid product to room temperature, washing with water, centrifugally separating, and vacuum drying at 80 deg.c to obtain nanometer monocrystal lanthanum boride; controlling the rotating speed of the ball mill to be 400 rpm; the heating rate during heating is 2 ℃/min;
(2) preparation of silicon dioxide coated nano monocrystal lanthanum boride
Adding 1-5 ml of ammonia water into 90 ml of ethanol, and stirring for 30min to form a uniform solution; then 0.1-0.5 g of tetraethoxysilane is dripped, and ultrasonic dispersion is carried out for 40 minutes to form solution A;
adding 10 ml of ammonia water into 20 ml of ethanol, and then adding 10 ml of deionized water and 2g of nano single-crystal lanthanum boride to form a suspension;
dropwise adding the solution A into the suspension for silica coating, and stirring for 12h to complete coating; centrifugally separating to obtain silicon dioxide coated nano monocrystal lanthanum boride;
the mass concentration of the ammonia water is 30 wt%;
(3) preparing a beauty mask
Dissolving 10-30 g of gelatin in 100mL of deionized water to obtain a gelatin solution; the gelatin is food-grade gelatin;
taking part of gelatin solution, adding 2-10 g of silicon dioxide coated nano monocrystal lanthanum boride into the gelatin solution, and performing ultrasonic dispersion and mixing to form suspension; spraying the suspension on one side of the non-woven fabric, and drying; when the suspension is used for spraying, the using amount of the suspension is controlled so that the spraying amount of the silicon dioxide coated nano monocrystal lanthanum boride is 1-15 mg/cm2；
And spraying the rest gelatin solution on the other side of the non-woven fabric, and drying to obtain the synergistic beauty mask.
2. The method for using the synergistic beauty mask prepared in the method of claim 1 for non-therapeutic purposes, wherein the mask is immersed in purified water at room temperature for not more than 5min before use; after being taken out, the side which is not added with the silicon dioxide coated nano single crystal lanthanum boride and is only sprayed with gelatin is pasted on the face and is irradiated by an infrared lamp or exposed to sunlight, and the pasting time is not more than 30 minutes.
3. The method for using the synergistic beauty mask prepared by the method of claim 1 for non-therapeutic purposes, wherein before use, the mask is soaked in the natural plant extract at room temperature for not more than 5 min; after being taken out, the side which is not added with the silicon dioxide coated nano monocrystal lanthanum boride and is only sprayed with gelatin is pasted on the face and is irradiated by infrared rays or exposed to sunlight, and the pasting time is not more than 30 minutes;
the natural plant extracting solution is prepared by the following method: pulverizing vegetables, extracting, and filtering to obtain natural plant extractive solution.
4. The method according to claim 1, wherein 10-30 g of gelatin is dissolved in 100mL of deionized water to obtain a gelatin solution; dissolving the natural plant extract in a gelatin solution to obtain a nutrient solution, and replacing the gelatin solution for spraying in the step (3) with the nutrient solution; in the nutrient solution, the mass ratio of the natural plant extract, the gelatin and the deionized water is 0.1-5: 10-30: 100, respectively;
the natural plant extract is prepared by the following method: crushing vegetables, extracting and filtering to obtain a plant stock solution; drying the plant stock solution to obtain powdered natural plant extract.
5. The method for using the synergistic beauty mask prepared by the method of claim 4 for a non-treatment purpose is characterized in that before use, the mask is soaked in purified water at the temperature of 25-80 ℃ for no more than 5 min; after being taken out, the side which is not added with the silicon dioxide coated nano monocrystal lanthanum boride and is only sprayed with the nutrient solution is pasted on the face and is irradiated by infrared rays or exposed to sunlight, and the pasting time is not more than 30 minutes.
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