CN109381344A - A kind of preparation method improving sanguimotor Synergistic type beauty mask - Google Patents
A kind of preparation method improving sanguimotor Synergistic type beauty mask Download PDFInfo
- Publication number
- CN109381344A CN109381344A CN201811303718.2A CN201811303718A CN109381344A CN 109381344 A CN109381344 A CN 109381344A CN 201811303718 A CN201811303718 A CN 201811303718A CN 109381344 A CN109381344 A CN 109381344A
- Authority
- CN
- China
- Prior art keywords
- gelatin
- solution
- lanthanum boride
- added
- mask
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to beauty mask fields, it is desirable to provide a kind of preparation method for improving sanguimotor Synergistic type beauty mask.It include: that lanthanum hydroxide and through ball milling and after heating reaction of sodium borohydride through washing, separation and drying, are obtained into nano crystal lanthanum boride, then silicon dioxide coated nano monocrystalline lanthanum boride is prepared；After silicon dioxide coated nano monocrystalline lanthanum boride and gelatin solution ultrasonic disperse are mixed to form suspension, it is sprayed at non-woven fabrics side, is dried；Gelatin solution is sprayed at the other side of non-woven fabrics, is dried, obtains Synergistic type beauty mask.Since invention enhances the mass transfers of nutritional ingredient, thus the usage amount of nutritional ingredient is greatly reduced, to also reduce the risk of skin allergy.By heating effect using light, the cooling of skin of face caused by veneer film is avoided, especially winter, can effectively reduce facial paralysis risk.Facial mask can be saved with drying regime, long shelf-life, be conducive to commercialization.
Description
Technical field
The present invention relates to beauty mask field, in particular to a kind of preparation for improving sanguimotor Synergistic type beauty mask
Method.
Background technique
Facial mask is a classification in skin care item, and cosmetology ingredient is supported on the carriers such as kaolin, nothing is coated in
It is made on the membrane materials such as woven fabric, silk mask, tencel facial mask, Biofibre facial mask, nonwoven fabric face.Facial mask using very extensive,
Its most basic and most important purpose is to make up makeup removing and the still insufficient cleaning that washes one's face, cooperate on this basis other
Essential ingredient realizes other maintenance functions, such as replenishing water and preserving moisture, whitening and anti-aging, Sage Extract etc..
The beauty principle of facial mask is to be temporarily isolating extraneous air and pollution using the of short duration time for being covered on face, mention
High skin temperature allows the pore of skin to expand, and promotes sweat gland secretion and metabolism, increase the oxygen content of skin, be conducive to
Skin excludes the product of epidermal cell metabolism and the oil substances of accumulation, and the moisture and nutritional ingredient in facial mask penetrate into table
The cuticula of skin, skin become soft, and skin is naturally bright flexible.
Traditional facial mask can be divided into 7 classes by function: cleaning pack, moisture saver mask, facial mask of releiving, extra firming facial mask, regenerating mask,
Whitening mask, MASQUE APAISANT HYDRATANT.This is one of the most common type facial mask to cleaning pack, can remove dirt in pore and extra
Grease, and aging cutin is removed, keep skin salubrious, clean.Moisture saver mask contains moisturizer, by moisture content lock in film, cutin-softening
Layer, and percutaneous absorption nutrition is helped, it is suitble to all kinds of skin.Facial mask of releiving is releived rapidly skin, is banished the feeling of languor, is restored skin
Gloss and elasticity are suitable for sensibility skin.Extra firming facial mask pore refining, aufhellung wrinkle go beauty especially suitable for no time
Hold institute and is the personage nursed.Regenerating mask includes plant essence, softens epidermal tissue, promotes skin metabolism, is suitable for dry
Property or water deficient skin.Whitening mask thoroughly removes dead skin cells, has both cleaning, whitening double effects, so that skin is reappeared children tender
It is smooth, it is pale transparent.Whitening and moisturizing facial mask is sucked out dirt and restrains pore simultaneously, while thoroughly removing dead skin cells, supplements water
Point, enable skin soft and moist full of gloss, high resilience.
Face mask film generally requires 10~30 minutes, but due to the evaporation of facial mask moisture, leads to facial mask and face temperature
Decline, this does not only result in facial mask slowing to skin transmitting nutritional ingredient, and also due to skin temperature decline causes hair
Thin vessel retraction, chosure of pores eventually lead to the reduction of cosmetic result.City's dealer's facial mask usually contains by increasing effective component in facial mask
Amount overcomes this defect using the drug of expansion blood vessel, but which increases the risks of skin allergy.Moreover, surface application
Film also results in the interference that body surface microcirculation is declined by skin temperature, and the blood vessel of local trophic nerve will occur spasm, lead
It causes nerve fiber ischemic, oedema, suffer oppression, easily cause facial paralysis.Therefore, a kind of facial mask being avoided that surface application cooling is for enhancing beauty
Hold effect and elimination side effect is particularly important.
Summary of the invention
The technical problem to be solved by the present invention is to overcome deficiency in the prior art, it is sanguimotor to provide a kind of improvement
The preparation method of Synergistic type beauty mask.
In order to solve the above technical problems, solution of the invention is:
A kind of preparation method improving sanguimotor Synergistic type beauty mask is provided, comprising the following steps:
(1) nano crystal lanthanum boride is prepared
Sodium borohydride is dissolved in tetrahydrofuran (THF) in ball grinder and forms saturated solution；
It is 1: 6 powder for weighing lanthanum hydroxide and sodium borohydride by the molar ratio of lanthanum and boron, aforementioned ball grinder is added together
In；Ball milling formed paste after 2 hours, was transferred in reactor, heats 30 minutes at 120 DEG C and evaporates solvent THF, obtains hydrogen
The mechanical impurity of lanthana and sodium borohydride；Continue after being heated to 500 DEG C, after heat preservation 2 hours, the hydrogen of release reaction generation
Gas；
La(OH)3+6NaBH4→LaB6+3Na2O+13.5H2
After solid product is cooled to room temperature, through being dried in vacuo at washing, centrifuge separation and 80 DEG C, nano crystal boronation is obtained
Lanthanum；(sodium oxide molybdena is reacted with water when washing generates sodium hydroxide, and sodium hydroxide is dissolved in water)；
(2) silicon dioxide coated nano monocrystalline lanthanum boride is prepared
1~5 milliliter of ammonium hydroxide is added in 90 milliliters of ethyl alcohol, stirring 30min forms homogeneous solution；0.1~0.5 gram is added dropwise again
Ethyl orthosilicate, ultrasonic wave disperse 40 minutes, formed solution A；
10 milliliters of ammonium hydroxide are added in 20 milliliters of ethyl alcohol, the nano crystal boronation of 10 ml deionized waters and 2 grams is added
Lanthanum forms suspension；
Solution A is added dropwise in suspension and carries out coated with silica, completes cladding after stirring 12h；Centrifuge separation,
Obtain silicon dioxide coated nano monocrystalline lanthanum boride；
(3) beauty mask is prepared
10~30g gelatin is dissolved in 100mL deionized water, gelatin solution is obtained；
Part of gelatin solution is taken, 2~10g silicon dioxide coated nano monocrystalline lanthanum boride is added thereto, ultrasonic disperse is mixed
Conjunction forms suspension；The suspension is sprayed at non-woven fabrics side, is dried；
Remaining gelatin solution is sprayed to the other side of non-woven fabrics, is dried, Synergistic type beauty mask is obtained.
In the present invention, in step (1), control rotational speed of ball-mill is 400rpm；Heating rate when heating is 2 DEG C/min.
In the present invention, in step (3), the gelatin is food-grade gelatin；When carrying out spraying operation with suspension, control
Its dosage makes 1~15mg/cm of silicon dioxide coated nano monocrystalline lanthanum boride quantity for spray2。
In the present invention, the mass concentration of the ammonium hydroxide is 30wt%.
The present invention also provides the application methods of the Synergistic type beauty mask prepared in the method for front, which is characterized in that
It is being no more than 5min before use, facial mask is soaked in pure water at room temperature；After taking-up, silicon dioxide coated nano will be not added with
The side that monocrystalline lanthanum boride only coats gelatin is pasted on face and with infra-red light irradiation or is exposed under sunlight, when sticking
Between be no more than 30 minutes.
The present invention also provides another application methods of the Synergistic type beauty mask prepared in the method for front, are using
Before, facial mask is soaked in natural botanical extraction liquid is no more than 5min at room temperature；After taking-up, coated with silica will be not added with and received
The side that meter Dan Jing lanthanum boride only coats gelatin is pasted on face and with infrared radiation or is exposed under sunlight, when sticking
Between be no more than 30 minutes；The natural botanical extraction liquid is prepared by following methods: by vegetables or having treating skin disease
The Chinese herbal medicine of effect crushes, and is extracted, is filtered, obtains natural botanical extraction liquid.
As a kind of replacement technology scheme, 10~30g gelatin can also be dissolved in 100mL deionized water by the present invention, be obtained
To gelatin solution；Natural plant extracts are dissolved in gelatin solution and obtain nutrient solution, to be used in the nutrient solution alternative steps (3)
The gelatin solution of spraying；In nutrient solution, the mass ratio relationships of natural plant extracts, gelatin and deionized water is 0.1~
5:10~30:100；The natural plant extracts are prepared by following methods: by vegetables or having treating skin disease effect
The Chinese herbal medicine of fruit crushes, and is extracted, original plant juice is obtained by filtration；Original plant juice is through drying, powdered natural plant extracts.
The application method of the Synergistic type beauty mask prepared in aforementioned replacement technology scheme is: before use, by facial mask
It is immersed in 25~80 DEG C of pure water, soaking time is no more than 5min；After taking-up, silicon dioxide coated nano list will be not added with
The side that brilliant lanthanum boride only coats nutrient solution is pasted on face and with infrared radiation or is exposed under sunlight, application time
No more than 30 minutes.
Inventive principle description:
Lanthanum boride is a kind of reddish violet crystal, and fusing point is high, is 2715 DEG C, is higher than fusing point lanthanum boride and decomposes.Under room temperature not
It is dissolved in water and acid.Usually lanthanum sesquioxide and borax are dissolved in a kind of suitable fused salt, and utilize graphite sun at high temperature
Pole electrolysis, lanthanum hexaboride is deposited on the cathode of graphite or steel.Due to the spy high with fusing point, thermionic emission performance is high
Point, fusion reactor, in terms of alternative refractory metal and alloy.The purposes of lanthanum boride is very wide
It is general, it has been successfully applied to radar aerospace, electronics industry, instrument, medical instrument, family's electrometallurgy, environmental protection etc. more than 20
A military and high-tech area.Lanthanum hexaboride product mainly includes amorphous, polycrystal, monocrystal lanthanum hexaboride.Especially six
There is boronation langasite single crystal the absorption of good near-infrared radiation to be transformed into thermal property, be that a kind of preferably irradiated by light is kept away
Exempt from the decorative material of surface application cooling.
The present invention heats nano material silicon dioxide coated nano monocrystalline lanthanum boride by adding light in facial mask, is using
Facial mask temperature can be improved using light irradiation in the process, strengthen speed of the facial mask to skin transmitting nutritional ingredient.Avoid capillary
Vessel retraction and chosure of pores increase cosmetic result.The irradiation light used is infrared ray (or sunlight).
Compared with prior art, the beneficial effects of the present invention are:
1, since invention enhances the mass transfers of nutritional ingredient, thus the usage amount of nutritional ingredient is greatly reduced, thus
Also reduce the risk of skin allergy.
2, effect is heated using light, avoids the cooling of skin of face caused by veneer film, especially winter, can effectively reduce
Facial paralysis risk.
3, facial mask can be saved with drying regime, long shelf-life, be conducive to commercialization.
Detailed description of the invention
Fig. 1 is silicon dioxide coated nano monocrystalline lanthanum boride pattern obtained in embodiment two.
Specific embodiment
Present invention is further described in detail With reference to embodiment:
Embodiment one: the synthesis of lanthanum boride
Sodium borohydride is dissolved in enough tetrahydrofurans (THF) in ball grinder and forms saturated solution, then presses lanthanum and boron
Elemental mole ratios be 1:6 (La:B=1:6) weigh lanthanum hydroxide (0.19g) and sodium borohydride (0.227g) powder addition ball milling
Tank, ball milling formed paste after 2 hours under 400rpm revolving speed, was placed in reactor, heats 30 minutes at 120 DEG C and evaporates solvent
THF obtains the mechanical impurity of lanthanum hydroxide and sodium borohydride, and 2 DEG C/min of heating rate keeps the temperature 2 hours after being heated to 500 DEG C,
Hydrogen is discharged, is washed after being cooled to room temperature, sodium oxide molybdena is reacted with water when washing generates sodium hydroxide, and sodium hydroxide is dissolved in water,
It is centrifugated, vacuum drying obtains nano crystal lanthanum boride at 80 DEG C.
Embodiment two: the synthesis of thin-walled silicon dioxide coated nano monocrystalline lanthanum boride
Sequentially added in 90 milliliters of ethyl alcohol 1 milliliter of ammonium hydroxide (mass concentration 30wt%) continue stir 30min formed
Even solution, then 0.1 gram of ethyl orthosilicate is added dropwise, ultrasonic wave disperses 40 minutes, forms solution A；By 10 milliliters of ammonium hydroxide, (quality is dense
Degree is 30wt%) it adds in 20 milliliters of ethyl alcohol, add monocrystalline boronation obtained in 10 ml deionized waters and 2 grams of embodiments one
Lanthanum forms suspension；Solution A is added dropwise in suspension, coated with silica is carried out；12h is stirred, is covered to complete, from
The isolated thin-walled silicon dioxide coated nano monocrystalline lanthanum boride of the heart.
Embodiment three: the synthesis of silicon dioxide coated nano monocrystalline lanthanum boride is thickened
Sequentially added in 90 milliliters of ethyl alcohol 2.5 milliliters of ammonium hydroxide (mass concentration 30wt%) continue stir 30min formed
Homogeneous solution, then 0.25 gram of ethyl orthosilicate is added dropwise, ultrasonic wave disperses 40 minutes, forms solution A；By 10 milliliters of ammonium hydroxide (matter
Amount concentration is 30wt%) it adds in 20 milliliters of ethyl alcohol, add monocrystalline obtained in 10 ml deionized waters and 2 grams of embodiments one
Lanthanum boride forms suspension；Solution A is added dropwise in suspension, coated with silica is carried out；12h is stirred, has been coated
At being centrifugally separating to obtain and thicken silicon dioxide coated nano monocrystalline lanthanum boride.
Example IV: the synthesis of heavy wall silicon dioxide coated nano monocrystalline lanthanum boride
Sequentially added in 90 milliliters of ethyl alcohol 5 milliliters of ammonium hydroxide (mass concentration 30wt%) continue stir 30min formed
Even solution, then 0.5 gram of ethyl orthosilicate is added dropwise, ultrasonic wave disperses 40 minutes, forms solution A；By 10 milliliters of ammonium hydroxide, (quality is dense
Degree is 30wt%) it adds in 20 milliliters of ethyl alcohol, add monocrystalline boronation obtained in 10 ml deionized waters and 2 grams of embodiments one
Lanthanum forms suspension；Solution A is added dropwise in suspension, coated with silica is carried out；12h is stirred, is covered to complete, from
The isolated heavy wall silicon dioxide coated nano monocrystalline lanthanum boride of the heart.
Embodiment five: Synergistic type beauty mask preparation
Sequentially added in 90 milliliters of ethyl alcohol 2 milliliters of ammonium hydroxide (mass concentration 30wt%) continue stir 30min formed
Even solution, then 0.3 gram of ethyl orthosilicate is added dropwise, ultrasonic wave disperses 40 minutes, forms solution A；By 10 grams of milliliter (mass concentrations
It is added in 20 milliliters of ethyl alcohol for 30wt%), adds monocrystalline boronation obtained in 10 ml deionized waters and 2 grams of embodiments one
Lanthanum forms suspension；Solution A is added dropwise in suspension, coated with silica is carried out；12h is stirred, is covered to complete, from
The isolated silicon dioxide coated nano monocrystalline lanthanum boride of the heart.
The city 10g dealer's edible gelatin is dissolved in 100mL deionized water and obtains gelatin solution；Part of gelatin solution is taken, is added
2g silicon dioxide coated nano monocrystalline lanthanum boride, ultrasonic disperse are mixed to form suspension, are sprayed at non-woven fabrics side and are dried；
Remaining gelatin solution is sprayed to the other side of non-woven fabrics；Controlling silicon dioxide coated nano monocrystalline lanthanum boride quantity for spray is
1mg/cm2, the gelatin quantity for spray of two sides is 5mg/cm2, by being dried to obtain Synergistic type beauty mask.
Facial mask will only coat the non-woven fabrics side of gelatin before use, impregnate 5min in pure water at room temperature after taking-up
It is affixed on face.Under 15W infra-red light irradiation after 30 minutes, facial mask is removed, clear water completes beauty after washing one's face, fills skin
Divide moisturizing.
Embodiment six: quick Synergistic type beauty mask
Sequentially added in 90 milliliters of ethyl alcohol 3 milliliters of ammonium hydroxide (mass concentration 30wt%) continue stir 30min formed
Even solution, then 0.4 gram of ethyl orthosilicate is added dropwise, ultrasonic wave disperses 40 minutes, forms solution A；By 10 milliliters of ammonium hydroxide, (quality is dense
Degree is 30wt%) it adds in 20 milliliters of ethyl alcohol, add monocrystalline boronation obtained in 10 ml deionized waters and 2 grams of embodiments one
Lanthanum forms suspension；Solution A is added dropwise in suspension, coated with silica is carried out；12h is stirred, is covered to complete, from
The isolated silicon dioxide coated nano monocrystalline lanthanum boride of the heart.
The city 20g dealer's edible gelatin is dissolved in 100mL deionized water and obtains gelatin solution；Part of gelatin solution is taken, is added
5g silicon dioxide coated nano monocrystalline lanthanum boride, ultrasonic disperse are mixed to form suspension, are sprayed at non-woven fabrics side and are dried；
Remaining gelatin solution is sprayed to the other side of non-woven fabrics；Controlling silicon dioxide coated nano monocrystalline lanthanum boride quantity for spray is
8mg/cm2, the gelatin quantity for spray of two sides is 32mg/cm2, by being dried to obtain Synergistic type beauty mask.
Facial mask will only coat the non-woven fabrics side of gelatin before use, impregnate 5min in pure water at room temperature after taking-up
It is affixed on face.Since facial mask is containing more silicon dioxide coated nano monocrystalline lanthanum boride, at 15W infra-red light irradiation 20 minutes
Afterwards, facial mask is removed, clear water completes beauty after washing one's face, and skin is made to obtain quick moisturizing.
Embodiment seven: ultrafast Synergistic type beauty mask
Sequentially added in 90 milliliters of ethyl alcohol 3 milliliters of ammonium hydroxide (mass concentration 30wt%) continue stir 30min formed
Even solution, then 0.4 gram of ethyl orthosilicate is added dropwise, ultrasonic wave disperses 40 minutes, forms solution A；By 10 milliliters of ammonium hydroxide, (quality is dense
Degree is 30wt%) it adds in 20 milliliters of ethyl alcohol, add monocrystalline boronation obtained in 10 ml deionized waters and 2 grams of embodiments one
Lanthanum forms suspension；Solution A is added dropwise in suspension, coated with silica is carried out；12h is stirred, is covered to complete, from
The isolated silicon dioxide coated nano monocrystalline lanthanum boride of the heart.
The city 20g dealer's edible gelatin is dissolved in 100mL deionized water and obtains gelatin solution；Part of gelatin solution is taken, is added
5g silicon dioxide coated nano monocrystalline lanthanum boride, ultrasonic disperse are mixed to form suspension, are sprayed at non-woven fabrics side and are dried；
Remaining gelatin solution is sprayed to the other side of non-woven fabrics；Controlling silicon dioxide coated nano monocrystalline lanthanum boride quantity for spray is
15mg/cm2, the gelatin quantity for spray of two sides is 60mg/cm2, by being dried to obtain quick Synergistic type beauty mask.
Facial mask will only coat the non-woven fabrics side of gelatin before use, impregnate 5min in pure water at room temperature after taking-up
It is affixed on face.Since facial mask is containing more silicon dioxide coated nano monocrystalline lanthanum boride, 15W infra-red light irradiation after five minutes,
Facial mask can be removed, clear water completes beauty after washing one's face, and skin is made to obtain ultrafast moisturizing.
Embodiment eight: function Synergistic type beauty mask preparation
Sequentially added in 90 milliliters of ethyl alcohol 2 milliliters of ammonium hydroxide (mass concentration 30wt%) continue stir 30min formed
Even solution, then 0.3 gram of ethyl orthosilicate is added dropwise, ultrasonic wave disperses 40 minutes, forms solution A；By 10 grams of milliliter (mass concentrations
It is added in 20 milliliters of ethyl alcohol for 30wt%), adds monocrystalline boronation obtained in 10 ml deionized waters and 2 grams of embodiments one
Lanthanum forms suspension；Solution A is added dropwise in suspension, coated with silica is carried out；12h is stirred, is covered to complete, from
The isolated silicon dioxide coated nano monocrystalline lanthanum boride of the heart.
The city 10g dealer's edible gelatin is dissolved in 100mL deionized water and obtains gelatin solution；Part of gelatin solution is taken, is added
2g silicon dioxide coated nano monocrystalline lanthanum boride, ultrasonic disperse are mixed to form suspension, are sprayed at non-woven fabrics side and are dried；
Remaining gelatin solution is sprayed to the other side of non-woven fabrics；Controlling silicon dioxide coated nano monocrystalline lanthanum boride quantity for spray is
1mg/cm2, the gelatin quantity for spray of two sides is 5mg/cm2, by being dried to obtain Synergistic type beauty mask.
100g celery is taken, after mashing plus 50mL pure water extracts, and celery extracting solution is obtained by filtration.Facial mask is before use, room temperature
Under 5min is impregnated in celery extracting solution, the non-woven fabrics side for only coating gelatin is affixed on face after taking-up.In 15W infrared ray
After lower 30 minutes of light irradiation, facial mask is removed, clear water completes beauty after washing one's face, achievees the effect that skin-tightening.
Embodiment nine: the routine use method of function Synergistic type beauty mask
Sequentially added in 90 milliliters of ethyl alcohol 3 milliliters of ammonium hydroxide (mass concentration 30wt%) continue stir 30min formed
Even solution, then 0.4 gram of ethyl orthosilicate is added dropwise, ultrasonic wave disperses 40 minutes, forms solution A；By 10 milliliters of ammonium hydroxide, (quality is dense
Degree is 30wt%) it adds in 20 milliliters of ethyl alcohol, add monocrystalline boronation obtained in 10 ml deionized waters and 2 grams of embodiments one
Lanthanum forms suspension；Solution A is added dropwise in suspension, coated with silica is carried out；12h is stirred, is covered to complete, from
The isolated silicon dioxide coated nano monocrystalline lanthanum boride of the heart.
The city 20g dealer's edible gelatin is dissolved in 100mL deionized water and obtains gelatin solution；Part of gelatin solution is taken, is added
5g silicon dioxide coated nano monocrystalline lanthanum boride, ultrasonic disperse are mixed to form suspension, are sprayed at non-woven fabrics side and are dried；
Remaining gelatin solution is sprayed to the other side of non-woven fabrics；Controlling silicon dioxide coated nano monocrystalline lanthanum boride quantity for spray is
8mg/cm2, the gelatin quantity for spray of two sides is 32mg/cm2, by being dried to obtain Synergistic type beauty mask.
100g celery is taken, after mashing plus 50mL pure water extracts, and celery extracting solution is obtained by filtration.Facial mask is before use, room temperature
Under 5min is impregnated in celery extracting solution, the non-woven fabrics side for only coating gelatin is affixed on face after taking-up.Since facial mask contains
More silicon dioxide coated nano monocrystalline lanthanum boride, shines after twenty minutes in the sunlight, removes facial mask, and clear water completes beauty after washing one's face
Hold, achievees the effect that skin-tightening.
Embodiment ten: easy beauty mask preparation
Sequentially added in 90 milliliters of ethyl alcohol 5 milliliters of ammonium hydroxide (mass concentration 30wt%) continue stir 30min formed
Even solution, then 0.5 gram of ethyl orthosilicate is added dropwise, ultrasonic wave disperses 40 minutes, forms solution A；By 10 milliliters of ammonium hydroxide, (quality is dense
Degree is 30wt%) it adds in 20 milliliters of ethyl alcohol, add monocrystalline boronation obtained in 10 ml deionized waters and 2 grams of embodiments one
Lanthanum forms suspension；Solution A is added dropwise in suspension, coated with silica is carried out；12h is stirred, is covered to complete, from
The isolated silicon dioxide coated nano monocrystalline lanthanum boride of the heart.
The city 30g dealer's edible gelatin is dissolved in 100mL deionized water and obtains gelatin solution, adds 10g silica packet
Nano crystal lanthanum boride is covered, ultrasonic disperse is mixed to form suspension, is sprayed at non-woven fabrics side and is dried；Coated with silica
Nano crystal lanthanum boride quantity for spray is 5mg/cm2, gelatin quantity for spray is 15mg/cm2。
After 100g peppermint grass is mashed plus 50mL pure water extracts, and is dried to obtain extract after peppermint extracting solution is obtained by filtration,
The gelatin solution 100mL for being dissolved in 10wt% obtains nutrient solution, in nutrient solution, the mass ratio of extract, gelatin and deionized water
Relationship is 0.1:10:100；It is sprayed at the opposite other side for having sprayed the non-woven fabrics of silicon dioxide coated nano monocrystalline lanthanum boride,
Quantity for spray is 15mg/cm2, wherein extract is 0.15mg/cm2, gelatin 14.85mg/cm2, by being dried to obtain easy beauty
Facial mask has the effect of killing acarid.
Embodiment 11: the application method of easy beauty mask
By simplicity beauty mask obtained in embodiment ten, 5min is impregnated in 25 DEG C of pure water, will only coat nutrient solution
Non-woven fabrics side be affixed on face.It shines in the sunlight after ten minutes, removes facial mask, clear water completes beauty after washing one's face.
Embodiment 12: the application method of onion beauty mask
The city 30g dealer's edible gelatin is dissolved in 100mL deionized water and obtains gelatin solution, adds in embodiment two and obtains
Silicon dioxide coated nano monocrystalline lanthanum boride 10g, ultrasonic disperse is mixed to form suspension, is sprayed at non-woven fabrics side and done
It is dry.Silicon dioxide coated nano monocrystalline lanthanum boride quantity for spray is 5mg/cm2, gelatin quantity for spray is 15mg/cm2。
After 100g onion is mashed plus 50mL pure water extracts, and is dried to obtain extract after onions extracting liquid is obtained by filtration, molten
Nutrient solution is obtained in the gelatin solution 100mL of 20wt%, and in nutrient solution, the mass ratio of extract, gelatin and deionized water is closed
System is 2.5:20:100；It is sprayed at the opposite other side for having sprayed the non-woven fabrics of silicon dioxide coated nano monocrystalline lanthanum boride, is sprayed
Painting amount is 15mg/cm2, wherein extract is 1.67mg/cm2, gelatin 13.33mg/cm2, by being dried to obtain easy beauty face
Film.
5min is impregnated in 50 DEG C of pure water, the non-woven fabrics side for only coating nutrient solution is affixed on face.It shines in the sunlight
After twenty minutes, facial mask is removed, clear water completes beauty after washing one's face, and can reach the effect of skin of face promoting blood circulation.
Embodiment 13: the application method of ginger beauty mask
The city 30g dealer's edible gelatin is dissolved in 100mL deionized water and obtains gelatin solution, adds in embodiment two and obtains
Silicon dioxide coated nano monocrystalline lanthanum boride 10g, ultrasonic disperse is mixed to form suspension, is sprayed at non-woven fabrics side and done
It is dry.Silicon dioxide coated nano monocrystalline lanthanum boride quantity for spray is 5mg/cm2, gelatin quantity for spray is 15mg/cm2。
After 20g ginger is mashed plus 50mL pure water extracts, and is dried to obtain extract after onions extracting liquid is obtained by filtration, is dissolved in
The gelatin solution 100mL of 30wt% obtains nutrient solution, in nutrient solution, the mass ratio relationship of extract, gelatin and deionized water
For 5:30:100；It is sprayed at the other side for having sprayed the non-woven fabrics of silicon dioxide coated nano monocrystalline lanthanum boride, quantity for spray is
15mg/cm2, wherein extract is 2.14mg/cm2, gelatin 12.86mg/cm2, by being dried to obtain easy beauty mask.
5min is impregnated in 80 DEG C of pure water, the non-woven fabrics side for only coating nutrient solution is affixed on face.It shines in the sunlight
After 30 minutes, facial mask is removed, clear water completes beauty after washing one's face, and can reach the effect for eliminating acne.
Finally it should be noted that the above enumerated are only specific embodiments of the present invention.It is clear that the invention is not restricted to
Above embodiments can also have many variations.Those skilled in the art can directly lead from present disclosure
Out or all deformations for associating, it is considered as protection scope of the present invention.
Claims (8)
1. a kind of preparation method for improving sanguimotor Synergistic type beauty mask, which comprises the following steps:
(1) nano crystal lanthanum boride is prepared
Sodium borohydride is dissolved in tetrahydrofuran in ball grinder and forms saturated solution；
It is 1: 6 powder for weighing lanthanum hydroxide and sodium borohydride by the molar ratio of lanthanum and boron, is added in aforementioned ball grinder together；Ball
Mill formed paste after 2 hours, is transferred in reactor, heats 30 minutes at 120 DEG C and evaporate solvent THF, obtain hydroxide
The mechanical impurity of lanthanum and sodium borohydride；Continue after being heated to 500 DEG C, after heat preservation 2 hours, the hydrogen of release reaction generation；Gu
After body product is cooled to room temperature, through being dried in vacuo at washing, centrifuge separation and 80 DEG C, nano crystal lanthanum boride is obtained；
(2) silicon dioxide coated nano monocrystalline lanthanum boride is prepared
1~5 milliliter of ammonium hydroxide is added in 90 milliliters of ethyl alcohol, stirring 30min forms homogeneous solution；0.1~0.5 gram is added dropwise again just
Silester, ultrasonic wave disperse 40 minutes, form solution A；
10 milliliters of ammonium hydroxide are added in 20 milliliters of ethyl alcohol, the nano crystal lanthanum boride of 10 ml deionized waters and 2 grams, shape are added
At suspension；
Solution A is added dropwise in suspension and carries out coated with silica, completes cladding after stirring 12h；Centrifuge separation, obtains
Silicon dioxide coated nano monocrystalline lanthanum boride；
(3) beauty mask is prepared
10~30g gelatin is dissolved in 100mL deionized water, gelatin solution is obtained；
Part of gelatin solution is taken, 2~10g silicon dioxide coated nano monocrystalline lanthanum boride is added thereto, ultrasonic disperse mixes shape
At suspension；The suspension is sprayed at non-woven fabrics side, is dried；
Remaining gelatin solution is sprayed to the other side of non-woven fabrics, is dried, Synergistic type beauty mask is obtained.
2. the method according to claim 1, wherein control rotational speed of ball-mill is 400rpm in step (1)；Add
Heating rate when hot is 2 DEG C/min.
3. the method according to claim 1, wherein the gelatin is food-grade gelatin in step (3)；With
When suspension carries out spraying operation, controlling its dosage makes 1~15mg/ of silicon dioxide coated nano monocrystalline lanthanum boride quantity for spray
cm2。
4. the method according to claim 1, wherein the mass concentration of the ammonium hydroxide is 30wt%.
5. the application method of the Synergistic type beauty mask prepared in any one method of Claims 1-4, feature exist
In before use, facial mask is soaked in pure water no more than 5min at room temperature；After taking-up, coated with silica will be not added with
The side that nano crystal lanthanum boride only coats gelatin is pasted on face and with infra-red light irradiation or is exposed under sunlight, pastes
The time is applied no more than 30 minutes.
6. the application method of the Synergistic type beauty mask prepared in any one method of Claims 1-4, feature exist
In before use, facial mask is soaked in natural botanical extraction liquid no more than 5min at room temperature；After taking-up, dioxy will be not added with
The side that SiClx cladding nano crystal lanthanum boride only coats gelatin is pasted on face and with infrared radiation or is exposed to the sun
Under light, application time is no more than 30 minutes；
The natural botanical extraction liquid is prepared by following methods: by vegetables or Chinese herbal medicine with treating skin disease effect
It crushes, is extracted, filtered, obtain natural botanical extraction liquid.
7. being obtained the method according to claim 1, wherein 10~30g gelatin is dissolved in 100mL deionized water
To gelatin solution；Natural plant extracts are dissolved in gelatin solution and obtain nutrient solution, to be used in the nutrient solution alternative steps (3)
The gelatin solution of spraying；In nutrient solution, the mass ratio relationships of natural plant extracts, gelatin and deionized water is 0.1~
5:10~30:100；
The natural plant extracts are prepared by following methods: by vegetables or Chinese herbal medicine with treating skin disease effect
It crushes, is extracted, original plant juice is obtained by filtration；Original plant juice is through drying, powdered natural plant extracts.
8. the application method of the Synergistic type beauty mask prepared in claim 7 the method, which is characterized in that use
Before, facial mask is immersed in 25~80 DEG C of pure water, soaking time is no more than 5min；After taking-up, silica will be not added with
The side that cladding nano crystal lanthanum boride only coats nutrient solution is pasted on face and with infrared radiation or is exposed to sunlight
Under, application time is no more than 30 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811303718.2A CN109381344B (en) | 2018-11-02 | 2018-11-02 | Preparation method of synergistic beauty mask for improving blood circulation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811303718.2A CN109381344B (en) | 2018-11-02 | 2018-11-02 | Preparation method of synergistic beauty mask for improving blood circulation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109381344A true CN109381344A (en) | 2019-02-26 |
| CN109381344B CN109381344B (en) | 2021-09-10 |
Family
ID=65428381
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811303718.2A Active CN109381344B (en) | 2018-11-02 | 2018-11-02 | Preparation method of synergistic beauty mask for improving blood circulation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109381344B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2792498Y (en) * | 2005-06-01 | 2006-07-05 | 上海弘康科技发展有限公司 | Face mould with tourmaline |
| TW201442740A (en) * | 2013-05-08 | 2014-11-16 | Univ Nat Cheng Kung | Nanoparticle having properties of photoluminescence and near-infrared radiation sensitivity and preparation method thereof |
| CN105197952A (en) * | 2015-09-06 | 2015-12-30 | 浙江大学 | Preparation of nano single crystal lanthanum hexaboride and application of nano single crystal lanthanum hexaboride in electron microscope filament preparation |
| CN106880504A (en) * | 2017-02-08 | 2017-06-23 | 潍坊荣尊堂生物科技有限公司 | The manufacture method of dry type facial mask |
| CN108601711A (en) * | 2016-01-20 | 2018-09-28 | 太阳化学公司 | Optical diffuser particle |
-
2018
- 2018-11-02 CN CN201811303718.2A patent/CN109381344B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2792498Y (en) * | 2005-06-01 | 2006-07-05 | 上海弘康科技发展有限公司 | Face mould with tourmaline |
| TW201442740A (en) * | 2013-05-08 | 2014-11-16 | Univ Nat Cheng Kung | Nanoparticle having properties of photoluminescence and near-infrared radiation sensitivity and preparation method thereof |
| CN105197952A (en) * | 2015-09-06 | 2015-12-30 | 浙江大学 | Preparation of nano single crystal lanthanum hexaboride and application of nano single crystal lanthanum hexaboride in electron microscope filament preparation |
| CN108601711A (en) * | 2016-01-20 | 2018-09-28 | 太阳化学公司 | Optical diffuser particle |
| CN106880504A (en) * | 2017-02-08 | 2017-06-23 | 潍坊荣尊堂生物科技有限公司 | The manufacture method of dry type facial mask |
Non-Patent Citations (1)
| Title |
|---|
| 王雨: "纳米LaB6的制备及近红外光吸收性能研究", 《中国优秀博硕士学位论文全文数据库(硕士)工程科技Ⅰ辑》 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109381344B (en) | 2021-09-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102702833B (en) | Anion powder | |
| CN106038411B (en) | Multi-form melanin precursor substance hair dye and its application method | |
| CN102697351B (en) | Anion healthy boccaro teapot | |
| CN110142416A (en) | A kind of method that dried orange peel extracting solution prepares nano-Ag particles | |
| CN107184823A (en) | A kind of extracting method of dendrobium candidum leaf and its extract and application | |
| CN110341251B (en) | Graphene mask cloth and preparation method thereof | |
| CN102697682A (en) | Preparation method of bean dreg whitening powdery mask and mask cream | |
| CN101700215B (en) | Abyssal fishskin collagen peptide peel off pack and preparation method thereof | |
| CN105919906A (en) | Beauty and health care composition | |
| CN109908030A (en) | A kind of manufacture craft of anhydrous facial mask | |
| CN109381344A (en) | A kind of preparation method improving sanguimotor Synergistic type beauty mask | |
| CN109846810A (en) | A kind of beauty mask and preparation method thereof | |
| CN107440917A (en) | A kind of application process of electrolytic reduction water in cosmetics | |
| CN107970293A (en) | A kind of Chinese medicine composition for improving skin sub-health state and preparation method thereof, skin care item | |
| CN111939108A (en) | Kumquat essential oil hydrolat mask and preparation method thereof | |
| CN109498479A (en) | A kind of graphene facial mask | |
| CN107157902B (en) | Skin-refreshing and nourishing facial mask and preparation method thereof | |
| CN102206289A (en) | Extraction process for polysaccharide from Bassia rapa L. | |
| CN105832638A (en) | Whitening pearl facial mask moist essence with deep moisturizing function and preparation method thereof | |
| CN105342917A (en) | Whitening cream based on natural extracts, and preparation method thereof | |
| CN111759774A (en) | Whitening anti-wrinkle essence | |
| CN109620761A (en) | A kind of stem body facial mask | |
| CN109700698A (en) | A kind of whitening spot-removing essence facial mask | |
| CN109700669A (en) | A kind of collagen protein face and preparation method thereof | |
| CN109646331A (en) | A kind of facial mask and its application method of preservative free |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |