CN109370779A - A kind of production method of olive floral type olive oil - Google Patents
A kind of production method of olive floral type olive oil Download PDFInfo
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- CN109370779A CN109370779A CN201811442737.3A CN201811442737A CN109370779A CN 109370779 A CN109370779 A CN 109370779A CN 201811442737 A CN201811442737 A CN 201811442737A CN 109370779 A CN109370779 A CN 109370779A
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- Prior art keywords
- olive
- flower
- oil
- extraction
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Fats And Perfumes (AREA)
Abstract
A kind of production method of olive floral type olive oil provided by the invention, the preparation including the extraction of olive flower essential oil, the squeezing of olive oil and olive floral type olive oil.A kind of production method of olive floral type olive oil provided by the invention, the olive flower extraction olive flower essential oil extractd when flower thinning being made full use of to handle, realizes waste utilization, olive flower essential oil is added in traditional olive oil, keep olive oil fragrance more mellow, there are preferable market prospects.
Description
Technical field
The present invention relates to vegetable oil manufacture fields, and in particular to a kind of production method of olive floral type olive oil.
Background technique
Olive oil is considered as the grease that human nutrition is most suitable in the grease found so far.High-grade olive that can be edible
Olive oil is the natural fruit oil juice extracted with just ripe or mature olive fresh fruit by the cold squeezing process of physics.
Olive spends fragrance, and color is white, is hermaphrodite flower, spend in a variety of nutritions for being wanted containing needed by human body, such as bitter glycosides, Huang
Ketone, polyphenol, squalene, amino acid, a variety of sugared parts, protein, oleic acid, linoleic acid etc..It is the high-quality olive of acquisition in Chinese garden planting
Tree fruit need to do flower thinning processing to olive tree, that is, extract extra flower.And the flower extractd often directly is discarded under tree.
There is no olive flower ingredient in olive oil product on the market, olive fragrance is light.
Summary of the invention
For the defects in the prior art, the production method of a kind of olive floral type olive oil provided by the invention solves
The problem of olive oil fragrance on the market is light, and the flower that when Chinese olive tree flower thinning extracts is not utilized.
To achieve the goals above, the present invention realizes by following technical solution:
A kind of production method of olive floral type olive oil, making step are as follows:
S1, the extraction of olive flower essential oil
A. the picking of olive flower: spending the time in full bloom in olive, when the intensive place of flower carries out flower thinning processing, will pluck
The olive flower removed collects；
B. the pre-treatment of olive flower: the olive flower of collection is cleaned after 2~4 times with mountain spring water and pulverizes to obtain olive flower juice
Liquid；
C. extraction and separation: making solvent with methyl ether, extracts to the olive flower juice through pre-treatment, carries out after extraction
It is separated by solid-liquid separation；
D. distillation condensation: the liquid phase that extraction and separation obtain is filtered or is settled, fine impurities therein is removed, subtracts
Pressure distillation is separated into gas phase and concentrate；
E. negative pressure separates: the control of gained concentrate being removed solvent under 30~50 DEG C of subnormal ambient, obtains olive flower
Essential oil, olive flower lipid, olive spend the mixed liquor of aqueous solution；
F. static separation: it is olive flower essential oil that the separating obtained mixed liquor of negative pressure, which is settled, is static, is separated to get upper layer,
Lower layer is olive flower aqueous solution and lipid；
G. stored under refrigeration: collecting upper layer olive flower essential oil and stored under refrigeration is stand-by；
S2, it is ripe or mature at the beginning of Chinese olive tree fruit when, picking olive fresh fruit through the cold squeezing process of physics obtains olive after cleaning
Olive oil；
S3, it will be stirred evenly in the olive flower essential oil instillation resulting olive oil of step S2 of stored under refrigeration in step S1, it is quiet
Olive floral type olive oil is obtained after only.
Optionally, in the step a of the S1 further include: screened to gained olive flower is collected, by hypogenetic flower
Piece and other sundries reject.
Optionally, in the step c of the S1 further include: repeated to the solid phase after extraction and separation by above-mentioned extraction and separation technology
Extraction and separation 3~5 times, gained liquid-phase collection is got up.
Optionally, the overall process of the olive flower essential oil extraction is completed under completely enclosed process environments.
Optionally, 2~6 drop olive flower essential oils are instilled in the step S3, in 1L olive oil.
Beneficial effects of the present invention: a kind of production method of olive floral type olive oil provided by the invention, including olive
Flower essential oil extraction, the squeezing of olive oil and olive floral type olive oil preparation.A kind of olive floral type olive provided by the invention
The production method of olive oil, the olive flower extraction olive flower essential oil extractd when flower thinning being made full use of to handle, realizes waste utilization,
Olive flower essential oil is added in traditional olive oil, keeps olive oil fragrance more mellow, there are preferable market prospects.
Specific embodiment
The embodiment of technical solution of the present invention will be described in detail below.Following embodiment is only used for clearer
Ground illustrates technical solution of the present invention, therefore is only used as example, and not intended to limit the protection scope of the present invention.
It should be noted that unless otherwise indicated, technical term or scientific term used in this application should be this hair
The ordinary meaning that bright one of ordinary skill in the art are understood.
A kind of production method of olive floral type olive oil provided in this embodiment, making step are as follows:
S1, the extraction of olive flower essential oil
A. the picking of olive flower: spending the time in full bloom in olive, when the intensive place of flower carries out flower thinning processing, will pluck
The olive flower removed collects；
B. the pre-treatment of olive flower: the olive flower of collection is cleaned after 2~4 times with mountain spring water and pulverizes to obtain olive flower juice
Liquid is cleaned multiple times, the impurity such as removal petal surface dust；
C. extraction and separation: making solvent with methyl ether, extracts to the olive flower juice through pre-treatment, carries out after extraction
It is separated by solid-liquid separation.Specifically, olive spends the proportion of juice and methyl ether for 1:1.5~3, and 40~50 DEG C of extraction temperature, pressure 0.2~
1.0MPa, extraction time are 30~40min.Solid phase extracted is degreasing (water) peony petal (silk), liquid phase extracted
That is the mixed liquor of olive flower essential oil, olive flower lipid, olive flower aqueous solution and solvent.
D. distillation condensation: the liquid phase that extraction and separation obtain is filtered or is settled, fine impurities therein is removed, subtracts
Pressure distillation is separated into gas phase and concentrate, and gas phase is solvent, is recycled after vapor condensation is liquefied, concentrate, that is, olive anthosin
Oil, olive flower lipid, olive spend the mixed liquor of aqueous solution and a small amount of solvent；
E. negative pressure separates: the control of gained concentrate being removed solvent under 30~50 DEG C of subnormal ambient, obtains olive flower
Essential oil, olive flower lipid, olive spend the mixed liquor of aqueous solution；
F. static separation: it is olive flower essential oil that the separating obtained mixed liquor of negative pressure, which is settled, is static, is separated to get upper layer,
Lower layer is olive flower aqueous solution and lipid；
G. stored under refrigeration: collecting upper layer olive flower essential oil and stored under refrigeration is stand-by；
The overall process of above-mentioned olive flower essential oil extraction is completed under completely enclosed process environments.Flower thinning is handled
When the useless olive flower of the script extractd collect and extract olive flower essential oil, realize waste utilization.
S2, it is ripe or mature at the beginning of Chinese olive tree fruit when, picking olive fresh fruit through the cold squeezing process of physics obtains olive after cleaning
Olive oil；
S3, it will be stirred evenly in the olive flower essential oil instillation resulting olive oil of step S2 of stored under refrigeration in step S1, it is quiet
Olive floral type olive oil is only obtained after 3~5 days.
As further improvement to above-mentioned technical proposal, in the step a of the S1 further include: spent to gained olive is collected
It is screened, hypogenetic flower and other sundries is rejected.Hypogenetic flower and other sundries such as leaf etc. influence
The olive anthosin oil quality of extraction.
As further improvement to above-mentioned technical proposal, in the step c of the S1 further include: to consolidating after extraction and separation
It is mutually repeated extraction and separation 3~5 times by above-mentioned extraction and separation technology, gained liquid-phase collection is got up.Multiple extraction and separation, as far as possible
More extracts the mixed liquor containing olive flower essential oil.
As further improvement to above-mentioned technical proposal, in the step S2, the method for picking fruit is first to use wooden peg
Nail is set, then a little salt is put into bark, finally the mulch on tree lower berth, places the material that the reductions such as foam collide on mulch,
It voluntarily drops onto foam after fruit maturation, collects fruit.
As further improvement to above-mentioned technical proposal, 2~6 drop olives are instilled in the step S3, in 1L olive oil
Flower essential oil can make olive oil fragrance more mellow.
Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the present invention., rather than its limitations；To the greatest extent
Pipe present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that: its according to
So be possible to modify the technical solutions described in the foregoing embodiments, or to some or all of the technical features into
Row equivalent replacement；And these are modified or replaceed, various embodiments of the present invention technology that it does not separate the essence of the corresponding technical solution
The range of scheme should all cover within the scope of the claims and the description of the invention.
Claims (5)
1. a kind of production method of olive floral type olive oil, which is characterized in that making step is as follows:
S1, the extraction of olive flower essential oil
A. the picking of olive flower: spending the time in full bloom in olive, when the intensive place of flower carries out flower thinning processing, by excision
Olive flower collects；
B. the pre-treatment of olive flower: the olive flower of collection is cleaned after 2~4 times with mountain spring water and pulverizes to obtain olive flower juice；
C. extraction and separation: making solvent with methyl ether, extracts to the olive flower juice through pre-treatment, solid-liquid is carried out after extraction
Separation；
D. distillation condensation: being filtered or settle to the liquid phase that extraction and separation obtain, and removes fine impurities therein, and decompression is steamed
It evaporates and is separated into gas phase and concentrate；
E. negative pressure separates: the control of gained concentrate under 30~50 DEG C of subnormal ambient is removed into solvent, obtain olive flower essential oil,
Olive spends the mixed liquor of lipid, olive flower aqueous solution；
F. static separation: it is olive flower essential oil, lower layer that the separating obtained mixed liquor of negative pressure, which is settled, is static, is separated to get upper layer
For olive flower aqueous solution and lipid；
G. stored under refrigeration: collecting upper layer olive flower essential oil and stored under refrigeration is stand-by；
S2, it is ripe or mature at the beginning of Chinese olive tree fruit when, picking olive fresh fruit through the cold squeezing process of physics obtains olive oil after cleaning；
S3, it will be stirred evenly in the olive flower essential oil instillation resulting olive oil of step S2 of stored under refrigeration in step S1, after static
Obtain olive floral type olive oil.
2. a kind of production method of olive floral type olive oil according to claim 1, which is characterized in that the step of the S1
In rapid a further include: screened to gained olive flower is collected, hypogenetic flower and other sundries are rejected.
3. a kind of production method of olive floral type olive oil according to claim 1, which is characterized in that the step of the S1
In rapid c further include: repeated extraction and separation 3~5 times to the solid phase after extraction and separation by above-mentioned extraction and separation technology, by gained liquid phase
It collects.
4. a kind of production method of olive floral type olive oil according to claim 1, it is characterised in that: the olive flower
The overall process of essential oil extraction is completed under completely enclosed process environments.
5. a kind of production method of olive floral type olive oil according to claim 1, it is characterised in that: the step
2~6 drop olive flower essential oils are instilled in S3, in 1L olive oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811442737.3A CN109370779A (en) | 2018-11-29 | 2018-11-29 | A kind of production method of olive floral type olive oil |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811442737.3A CN109370779A (en) | 2018-11-29 | 2018-11-29 | A kind of production method of olive floral type olive oil |
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| Publication Number | Publication Date |
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| CN109370779A true CN109370779A (en) | 2019-02-22 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201811442737.3A Pending CN109370779A (en) | 2018-11-29 | 2018-11-29 | A kind of production method of olive floral type olive oil |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104087424A (en) * | 2014-08-04 | 2014-10-08 | 安阳市晶华油脂工程有限公司 | Method for one-step extraction and separation of essential oil, water solution and lipid of fresh peony flowers |
| CN104171023A (en) * | 2014-07-14 | 2014-12-03 | 和县绿源油脂有限公司 | Olive blending oil for maintaining beauty and keeping young |
| CN106561914A (en) * | 2016-11-01 | 2017-04-19 | 陇南市祥宇油橄榄开发有限责任公司 | Manufacturing method of olive flowering tea and bud tea |
-
2018
- 2018-11-29 CN CN201811442737.3A patent/CN109370779A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104171023A (en) * | 2014-07-14 | 2014-12-03 | 和县绿源油脂有限公司 | Olive blending oil for maintaining beauty and keeping young |
| CN104087424A (en) * | 2014-08-04 | 2014-10-08 | 安阳市晶华油脂工程有限公司 | Method for one-step extraction and separation of essential oil, water solution and lipid of fresh peony flowers |
| CN106561914A (en) * | 2016-11-01 | 2017-04-19 | 陇南市祥宇油橄榄开发有限责任公司 | Manufacturing method of olive flowering tea and bud tea |
Non-Patent Citations (1)
| Title |
|---|
| YOU DREAMHOME公众号: "微信，自然力量之橄榄相关产品， You DreamHome公众号，2016年6月3日", 《微信，YOU DREAMHOME公众号》 * |
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