CN109369268A - The production method of amino acid Water soluble fertilizer - Google Patents
The production method of amino acid Water soluble fertilizer Download PDFInfo
- Publication number
- CN109369268A CN109369268A CN201811413563.8A CN201811413563A CN109369268A CN 109369268 A CN109369268 A CN 109369268A CN 201811413563 A CN201811413563 A CN 201811413563A CN 109369268 A CN109369268 A CN 109369268A
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- Prior art keywords
- amino acid
- parts
- soluble fertilizer
- acid water
- production method
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
- C05G5/23—Solutions
Abstract
The present invention provides the production methods of amino acid Water soluble fertilizer, its technical characteristic is squid leftover bits and pieces, fish head fish-bone, shell leftover bits and pieces, useless milk after proteases for decomposing, it is sufficiently mixed with composite aminophenol powder, blackstrap, potassium sulfate, magnesium sulfate, is made through microbial fermentation, filtering.The present invention produces amino acid water-soluble fertilizer using aquatic product leftovers, and waste material is utilized, reduces production cost；It undergoes microbial fermentation, containing there are many amino acid, microelement, organic matter etc., nutriment enriches, is balanced, can significantly promote plant growth；Soil activation can be increased, improve soil texture, so that crop is resisted the enhancing of disease ability, reduce the application of pesticide, achieve the purpose that upgrading is increased production.
Description
Technical field
The invention patent belongs to technical field of fertilizer production, and in particular to a kind of to utilize disposal from fishery product processing for raw material
Amino acid Water soluble fertilizer production method.
Background technique
In recent years, China's Aquatic Product Process Industry flourishes, and generates a large amount of leftover bits and pieces every year, yield accounts for about aquatic products
Process 60% or more of total amount.These leftover protein matter contents are high, have good amino acid composition, are good amino acid
Source, but effective rate of utilization is very low at present, if can not only cause damages, will also result in environment without being effectively treated
A large amount of wastes of nutritional resource.It makes full use of these leftover bits and pieces that the added value of fish processing can be improved, there is good economy
And social benefit.
Amino acid is the organic compound that one group of molecular weight differs in size, and is the basic unit of synthetic proteins matter, amino acid
It is nutriment necessary to plant growth, is the basic material for constructing cell, repair tissue.Due to the spy of amino acid itself
Point can be used as the promotor and catalyst of synzyme in plant, play an important role to plant metabolism, it can increase
Add chlorophyll content of plant, improve the activity of enzyme, promote the infiltration of carbon dioxide, keep photosynthesis more vigorous, makees to improving
Article matter increases the content important role of vitamin C and sugar.The metabolin that microorganism generates during the growth process, Ke Yixiu
Multiple and improvement Land Environment, promotes root growth, reduces soil-borne disease, plays important work to the usage amount for reducing chemical pesticide
With.As people are food-safe, the continuous enhancing of ecological protection consciousness, the research of new type functional fertilizer is increasingly by people
Attention.
Current market sales of water-soluble fertilizer containing amino acid executes Ministry of Agriculture NY1429-2010 standard, micro member mostly
Cellulose content is greater than 20g/L or moderate-element content is greater than 30g/L, and only containing microelement in one or two, plant growth
Other nutriments also need in addition to supplement, be not only difficult to reach mutual balance between each element, but also increase fertilising cost.
The amino acid water-soluble fertilizer containing microorganism is even more fewer and fewer at present, and existing product effect is single, is not able to satisfy agricultural production
Demand.Therefore, the amino acid water-soluble fertilizer containing microorganism for producing a kind of high fertilizer efficiency is of great significance.
Summary of the invention
Amino acid is prepared using aquatic product leftovers it is an object of the invention to overcome the deficiencies of the prior art and provide a kind of
The production method of Water soluble fertilizer, water-soluble fertilizer obtained contain the various nutrient elements such as 16 kinds of amino acid, calcium, magnesium, potassium and organic matter,
Multiple beneficial microorganism, nutrition is balanced, can significantly promote plant growth, improves the ability that crop resists disease.
To achieve the goals above, the technical solution adopted by the present invention includes the following steps:
By weight, it is put in after 20-30 parts of squid leftover bits and pieces, 20-25 parts of fish head fish-bone, 8-10 parts of shell leftover bits and pieces being crushed anti-
It answers in kettle, give up milk 20-35 parts .5-1 parts of proteinase-10 is added, is digested 15 days under the conditions of 20-50 DEG C of temperature, obtain containing amino
Acid solution；
Above-mentioned containing in amino acid solution, microbial inoculum 1.5-3.0 parts, 5-8 parts of composite aminophenol powder, blackstrap 0-3 is added
Part, 0-2.5 parts of potassium sulfate, 2.5-3 parts of magnesium sulfate, are thoroughly mixed in reaction kettle, under the conditions of 15-50 DEG C of temperature, hair
Obtain fermentation liquid within ferment 15 days；
Above-mentioned fermentation liquid is subjected to three-stage filtration, filtering fineness is respectively set to 80 mesh, 120 mesh, 200 mesh, granule foreign is removed,
Metering is packed to get amino acid water-soluble fertilizer is arrived.
Preferably, the protease is papain, neutral proteinase, alkali protease, one in flavor protease
Kind or several mixtures.
The microbial inoculum be saccharomycete, lactic acid bacteria and the mixed liquor of actinomyces, total viable bacteria content >=108/mL, than
Example is 1:1:1.
The composite aminophenol powder be glutamic acid, histidine, aspartic acid, proline, valine, alanine, leucine,
Lysine, arginine, serine, tryptophan, methionine, phenylalanine, tyrosine, glycine and threonine at least two it is mixed
Close object.
Free aminoacid content >=100g/L of the amino acid water-soluble fertilizer, pH value 7.5-8.5.
Beneficial effects of the present invention:
The present invention produces amino acid water-soluble fertilizer using aquatic product leftovers, is decomposed into protein macromolecule by zymolysis technique more
The small-molecule substances such as peptide, amino acid are utilized aquatic products waste plant protein resource, reduce production cost；By complex microorganism
Combined ferment effect, further decompose and be difficult to the macromolecular degraded, generate more free amino acids.Ammonia produced by the present invention
Base acid water-soluble fertilizer, containing there are many amino acid, microelement, organic matter etc., nutriment enriches, is balanced, is easy to absorb, can show
It writes and promotes plant growth；Soil activation can be increased simultaneously, improve soil texture, so that crop is resisted the enhancing of disease ability, reduce agriculture
The application of medicine achievees the purpose that upgrading is increased production.
Specific embodiment
Technical solution of the present invention is described further below with reference to embodiment:
Embodiment one:
The production method of amino acid Water soluble fertilizer, includes the following steps:
By weight, it is put after 35 parts of useless milk, 20 parts of squid leftover bits and pieces, 20 parts of fish head fish-bone, 10 parts of shell leftover bits and pieces being crushed
In reaction kettle, 0.3 part of neutral proteinase, 0.2 part of papain is added, digests 15 days, obtains under the conditions of temperature 50 C
Containing amino acid solution；
Above-mentioned containing in amino acid solution, 1.5 parts of microbial inoculum, 5 parts of composite aminophenol powder, 3 parts of blackstrap, potassium sulfate is added
2.5 parts, 2.5 parts of magnesium sulfate, are thoroughly mixed in reaction kettle, under the conditions of temperature 45 C, obtain fermentation liquid within fermentation 15 days；
Above-mentioned mixed liquor is subjected to three-stage filtration, filtering fineness is respectively set to 80 mesh, 120 mesh, 200 mesh, granule foreign is removed,
Metering, packaging, obtain amino acid water-soluble fertilizer.
Embodiment two:
The production method of amino acid Water soluble fertilizer, includes the following steps:
By weight, it is put in after 22 parts of useless milk, 30 parts of squid leftover bits and pieces, 25 parts of fish head fish-bone, 8 parts of shell leftover bits and pieces being crushed
In reaction kettle, 0.4 part of neutral proteinase, 0.4 part of alkali protease is added, digests 15 days, is contained under the conditions of temperature 45 C
Amino acid solution；
Above-mentioned containing in amino acid solution, 2.5 parts of microbial inoculum, 6 parts of composite aminophenol powder, 2 parts of blackstrap, potassium sulfate is added
1 part, 2.7 parts of magnesium sulfate, are thoroughly mixed in reaction kettle, under the conditions of 30 DEG C of temperature, obtain fermentation liquid within fermentation 15 days；
Above-mentioned mixed liquor is subjected to three-stage filtration, filtering fineness is respectively set to 80 mesh, 120 mesh, 200 mesh, granule foreign is removed,
Metering, packaging, obtain amino acid water-soluble fertilizer.
Embodiment three:
The production method of amino acid Water soluble fertilizer, includes the following steps:
By weight, it is put after 33 parts of useless milk, 20 parts of squid leftover bits and pieces, 21 parts of fish head fish-bone, 10 parts of shell leftover bits and pieces being crushed
In reaction kettle, 0.5 part of neutral proteinase, 0.5 part of flavor protease is added, digests 15 days, obtains under the conditions of 35 DEG C of temperature
Containing amino acid solution；
Above-mentioned containing in amino acid solution, 3 parts of microbial inoculum, 5 parts of composite aminophenol powder, 3 parts of blackstrap, potassium sulfate is added
1.2 parts, 2.8 parts of magnesium sulfate, are thoroughly mixed in reaction kettle, under the conditions of 30 DEG C of temperature, obtain fermentation liquid within fermentation 15 days；
Above-mentioned mixed liquor is subjected to three-stage filtration, filtering fineness is respectively set to 80 mesh, 120 mesh, 200 mesh, granule foreign is removed,
Metering, packaging, obtain amino acid water-soluble fertilizer.
Example IV:
The production method of amino acid Water soluble fertilizer, includes the following steps:
By weight, it is put in after 31 parts of useless milk, 25 parts of squid leftover bits and pieces, 20 parts of fish head fish-bone, 9 parts of shell leftover bits and pieces being crushed
In reaction kettle, it is added 1 part of neutral proteinase, is digested 15 days under the conditions of 30 DEG C of temperature, obtained containing amino acid solution；
Above-mentioned containing in amino acid solution, 3 parts of microbial inoculum, 8 parts of composite aminophenol powder, 3 parts of magnesium sulfate is added, in reaction kettle
In be thoroughly mixed, under the conditions of 25 DEG C of temperature, fermentation 15 days fermentation liquid；
Above-mentioned mixed liquor is subjected to three-stage filtration, filtering fineness is respectively set to 80 mesh, 120 mesh, 200 mesh, granule foreign is removed,
Metering, packaging, obtain amino acid water-soluble fertilizer.
The amino acid water-soluble fertilizer as made from embodiment one to four meets NY1429-2010 " water-soluble fertilizer containing amino acid "
Standard requirements, wherein the amino acid water-soluble fertilizer the key technical indexes is as follows: free aminoacid content >=100g/L, in
Secondary element content >=30g/L, water insoluble matter content≤50g/L, mercury (based on the element)≤5mg/kg, arsenic (based on the element)≤
10mg/kg, cadmium (based on the element)≤10mg/kg, lead (based on the element)≤50mg/kg, chromium (based on the element)≤50mg/kg, pH
Value is 7.5-8.5.
Test example: influence of the water-soluble fertilizer product of the present invention to tomato growth and yield
It experimental field selects: selecting representational plot in the five estrade town village Gu Jingzi of Shenyang City, Liaoning Province Faku County, topography is flat
Smooth, fertility is uniform, tests have no occluder around plot；Test totally 0.9 mu of plot.
Test period: in May, 2018 to September
Test variety: legend
Test method: three processing groups of setting handle I: commercially available amino acid water-soluble fertilizer；Handle II: amino acid of the present invention is water-soluble
Fertilizer；Handle III: equivalent clear water.1000 times of the water-soluble fertilizer dilution that I will be handled, handle II, interval spray once for 10 days, even
Continuous to spray 4 times, processing III sprays the clear water of equivalent；Each processing group repeats three times, random alignment, and test result is averaged.
Test results and analysis:
1. influence of the different disposal to tomato biological character
Influence of the different disposal to tomato biological character the results are shown in Table 1.
Influence of 1 different disposal of table to tomato biological character
| Processing | Plant height (cm) | Leaf color | Single fruit weight (g) | Single plant fruit number (a) | Sugar content |
| Handle I | 135.2 | It is dark green | 162.3 | 20.4 | 5.26 |
| Handle II | 140.7 | It is dark green | 171.4 | 22.5 | 5.72 |
| Handle III | 128.1 | Green | 150.3 | 15.6 | 4.83 |
Influence result from 1 different disposal of table to tomato biological character is it is found that application amino acid water-soluble fertilizer and application equivalent are clear
Water is compared, and is significantly improved to tomato plant height, leaf color, single fruit weight, single plant fruit number, the sugar content of fruit, and of the invention
Amino acid water-soluble fertilizer obtained, compared with commercially available conventional amino acid water-soluble fertilizer, better effect.After applying product of the present invention,
The dark green plump, fruit type of tomato leaf just, fruit color it is consistent, in good taste.
2. influence of the different disposal to tomato yield
Influence of the different disposal to tomato yield the results are shown in Table 2.
Influence of 2 different disposal of table to tomato yield
Test result shows to apply amino acid water-soluble fertilizer compared with applying equivalent clear water, can dramatically increase tomato yield, this hair
Tomato mu volume increase 2872.5kg of the bright obtained product than applying equivalent clear water, rate of growth 64%, than commercially available amino acid water-soluble fertilizer
Product is high by 23%, has better effect of increasing production.
Claims (5)
1. the production method of amino acid Water soluble fertilizer, it is characterised in that include the following steps:
A. by weight, it is put in after 20-30 parts of squid leftover bits and pieces, 20-25 parts of fish head fish-bone, 8-10 parts of shell leftover bits and pieces being crushed
In reaction kettle, give up milk 20-35 parts .5-1 parts of proteinase-10 is added, is digested 15 days under the conditions of 20-50 DEG C of temperature, obtains containing ammonia
Base acid solution；
B. microbial inoculum 1.5-3.0 parts, 5-8 parts of composite aminophenol powder, blackstrap 0- is added containing in amino acid solution above-mentioned
3 parts, 0-2.5 parts of potassium sulfate, 2.5-3 parts of magnesium sulfate, are thoroughly mixed in reaction kettle, under the conditions of 15-50 DEG C of temperature, hair
Obtain fermentation liquid within ferment 15 days；
C. above-mentioned fermentation liquid is subjected to three-stage filtration, filtering fineness is respectively set to 80 mesh, 120 mesh, 200 mesh, except degranulation is miscellaneous
Matter, metering are packed to get amino acid water-soluble fertilizer is arrived.
2. the production method of amino acid Water soluble fertilizer according to claim 1, it is characterised in that: the protease is pawpaw egg
The mixture of one or more of white enzyme, neutral proteinase, alkali protease, flavor protease.
3. the production method of amino acid Water soluble fertilizer according to claim 1, it is characterised in that: the microbial inoculum is ferment
The mixed liquor of female bacterium, lactic acid bacteria and actinomyces, total viable bacteria content >=108A/mL, ratio 1:1:1.
4. the production method of amino acid Water soluble fertilizer according to claim 1, it is characterised in that: the composite aminophenol powder is
Glutamic acid, histidine, aspartic acid, proline, valine, alanine, leucine, lysine, arginine, serine, color ammonia
Acid, methionine, phenylalanine, tyrosine, glycine and threonine at least two mixture.
5. the production method of amino acid Water soluble fertilizer according to claim 1, it is characterised in that: the amino acid water-soluble fertilizer
Free aminoacid content >=100g/L, pH value 6.5-7.5.
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110218106A (en) * | 2019-06-27 | 2019-09-10 | 京博农化科技有限公司 | A kind of organic amino acid liquid punching fertilising |
| CN110683882A (en) * | 2019-11-13 | 2020-01-14 | 湛江市绿海生物工程有限公司 | Process method for preparing amino acid water-soluble fertilizer from feather meal |
| CN111362748A (en) * | 2020-04-02 | 2020-07-03 | 宁夏顺宝现代农业股份有限公司 | Preparation method and application of amino acid fermentation liquor |
| CN111533607A (en) * | 2020-05-27 | 2020-08-14 | 广西宇花灵科技发展有限公司 | Foliar fertilizer for promoting flower and fruit retention of tomatoes and preparation method thereof |
| CN112142519A (en) * | 2020-09-27 | 2020-12-29 | 浙华欣农(嘉兴)生物科技有限公司 | Utilize equipment of abandonment eggshell protein preparation amino acid calcium magnesium liquid fertilizer |
| WO2021135911A1 (en) * | 2019-12-31 | 2021-07-08 | 广西神冠胶原生物集团有限公司 | Method for enzymatically producing high-activity biological organic fertilizer |
| CN113831201A (en) * | 2021-08-03 | 2021-12-24 | 浙大宁波理工学院 | Method for producing organic matter-containing foliar fertilizer by using fish meal squeezed liquid |
| CN113956112A (en) * | 2021-12-04 | 2022-01-21 | 北海宝农农业科技有限公司 | Method for producing full water-soluble microbial fertilizer by using aquatic product processing leftovers |
| CN114195596A (en) * | 2021-12-16 | 2022-03-18 | 山西欣普旺农业科技有限公司 | Aroma-enhancing organic water-soluble fertilizer for sunshine grapes and preparation method thereof |
| CN114349560A (en) * | 2021-12-29 | 2022-04-15 | 韩德新 | Sea snake tail hydrolysate, water-soluble fertilizer and preparation method thereof |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110218106A (en) * | 2019-06-27 | 2019-09-10 | 京博农化科技有限公司 | A kind of organic amino acid liquid punching fertilising |
| CN110683882A (en) * | 2019-11-13 | 2020-01-14 | 湛江市绿海生物工程有限公司 | Process method for preparing amino acid water-soluble fertilizer from feather meal |
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| CN111533607A (en) * | 2020-05-27 | 2020-08-14 | 广西宇花灵科技发展有限公司 | Foliar fertilizer for promoting flower and fruit retention of tomatoes and preparation method thereof |
| CN112142519A (en) * | 2020-09-27 | 2020-12-29 | 浙华欣农(嘉兴)生物科技有限公司 | Utilize equipment of abandonment eggshell protein preparation amino acid calcium magnesium liquid fertilizer |
| CN113831201A (en) * | 2021-08-03 | 2021-12-24 | 浙大宁波理工学院 | Method for producing organic matter-containing foliar fertilizer by using fish meal squeezed liquid |
| CN113956112A (en) * | 2021-12-04 | 2022-01-21 | 北海宝农农业科技有限公司 | Method for producing full water-soluble microbial fertilizer by using aquatic product processing leftovers |
| CN114195596A (en) * | 2021-12-16 | 2022-03-18 | 山西欣普旺农业科技有限公司 | Aroma-enhancing organic water-soluble fertilizer for sunshine grapes and preparation method thereof |
| CN114349560A (en) * | 2021-12-29 | 2022-04-15 | 韩德新 | Sea snake tail hydrolysate, water-soluble fertilizer and preparation method thereof |
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Application publication date: 20190222 |