CN109355044A - A kind of textile cloth glue and preparation method thereof - Google Patents
A kind of textile cloth glue and preparation method thereof Download PDFInfo
- Publication number
- CN109355044A CN109355044A CN201811131003.3A CN201811131003A CN109355044A CN 109355044 A CN109355044 A CN 109355044A CN 201811131003 A CN201811131003 A CN 201811131003A CN 109355044 A CN109355044 A CN 109355044A
- Authority
- CN
- China
- Prior art keywords
- weight
- parts
- textile cloth
- solvent
- cloth glue
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000003292 glue Substances 0.000 title claims abstract description 33
- 239000004744 fabric Substances 0.000 title claims abstract description 31
- 239000004753 textile Substances 0.000 title claims abstract description 29
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000002904 solvent Substances 0.000 claims abstract description 29
- 229920005989 resin Polymers 0.000 claims abstract description 22
- 239000011347 resin Substances 0.000 claims abstract description 22
- -1 aldehyde ketone Chemical class 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 13
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 claims abstract description 8
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 claims abstract description 8
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical group OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 63
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 42
- 235000019441 ethanol Nutrition 0.000 claims description 21
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims description 19
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 6
- 239000003610 charcoal Substances 0.000 claims description 2
- 150000004702 methyl esters Chemical class 0.000 claims description 2
- 235000021419 vinegar Nutrition 0.000 claims description 2
- 239000000052 vinegar Substances 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims 1
- 238000004026 adhesive bonding Methods 0.000 claims 1
- 229920002451 polyvinyl alcohol Polymers 0.000 claims 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract description 6
- 239000006229 carbon black Substances 0.000 abstract description 6
- 239000007788 liquid Substances 0.000 abstract description 3
- 230000003796 beauty Effects 0.000 abstract description 2
- 238000004851 dishwashing Methods 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 230000002087 whitening effect Effects 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 239000004698 Polyethylene Substances 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- 206010023126 Jaundice Diseases 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J161/00—Adhesives based on condensation polymers of aldehydes or ketones; Adhesives based on derivatives of such polymers
- C09J161/02—Condensation polymers of aldehydes or ketones only
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J129/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Adhesives based on hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Adhesives based on derivatives of such polymers
- C09J129/14—Homopolymers or copolymers of acetals or ketals obtained by polymerisation of unsaturated acetals or ketals or by after-treatment of polymers of unsaturated alcohols
Abstract
The invention discloses a kind of textile cloth glue and preparation method thereof, be made of the raw material for including following parts by weight: polyvinyl butyral resin 15~30%, meteorological white carbon black 0.5~2%, citrate 1~3%, aldehyde ketone resin 20~30%, solvent 45~58%, the present invention have the advantages that bonding is strong, durable, burn into glue softness is not hardened, non-whitening, environmental protection, dry rapid, water-fastness, resistance to dish washing liquid, glue is colorless and transparent, the beauty that do not influence then object, will not damage cloth.
Description
Technical field
The present invention relates to repairing glue fields, more specifically, being a kind of textile cloth glue and preparation method thereof.
Background technique
Currently, in textile cloth glue using essential, but the textile cloth after using glue is because of contact
After cleaning liquid, it may appear that bonding force decline, abutting edge are hardened, the drawbacks such as colloid jaundice, to influence the integrated beauty of textile cloth
It sees.
Summary of the invention
In order to make up the above deficiency, the present invention provides a kind of textile cloth glue and preparation method thereof.
The scheme of the invention is:
A kind of textile cloth glue is made of the raw material for including following parts by weight:
The solvent is the composition that methanol, ethyl alcohol and methyl acetate mix as a preferred technical solution,.
The solvent is made from the following raw materials in parts by weight as a preferred technical solution:
Methanol 15~25%；
Ethyl alcohol 5~15%；
Methyl acetate 16~24%.
The solvent is made from the following raw materials in parts by weight as a preferred technical solution:
Methanol 20%；
Ethyl alcohol 10%；
Methyl acetate 22%.
As a preferred technical solution, by including that the raw material of following parts by weight is made:
The present invention also provides a kind of methods for preparing the textile cloth glue, comprising steps of
1) solvent of 45~58% parts by weight is put into reaction kettle, although putting into the polyethylene of 15~30% parts by weight afterwards
Polyvinyl butyral resin is stirred 2~4 hours with blender, is completely dissolved；
2) aldehyde ketone resin, the meteorology of 0.5~2% parts by weight of 20~30% parts by weight are then put into the reaction kettle
The citrate of white carbon black and 1~3% parts by weight；Stirring 1~2 hour, after the aldehyde ketone resin therein is completely dissolved, stirring
It is miscible to be filtered, textile cloth glue is made.
The solvent is the composition that methanol, ethyl alcohol and methyl acetate mix as a preferred technical solution,.
The preparation method of the solvent as a preferred technical solution: take 5~15% parts by weight methanol, 15~25%
The ethyl alcohol of parts by weight is added in mixer with the methyl acetate of 16~24% parts by weight and is mixed.
By adopting the above-described technical solution, a kind of textile cloth glue, 1) solvent of 45~58% parts by weight is put into reaction
In kettle, although putting into the polyvinyl butyral resin of 15~30% parts by weight afterwards, stirred 2~4 hours with blender, it is completely molten
Solution；2) aldehyde ketone resin of 20~30% parts by weight, the meteorological hard charcoal of 0.5~2% parts by weight are then put into the reaction kettle
The black citrate with 1~3% parts by weight；Stirring 1~2 hour after the aldehyde ketone resin therein is completely dissolved, is stirred miscible
It is filtered, textile cloth glue is made.
Invention advantage: the present invention have bond it is strong, durable, not burn into glue softness do not harden, non-whitening.Environmental protection, drying
Rapidly, that water-fastness, resistance to dish washing liquid, glue are colorless and transparent, not influence then object is beautiful, will not damage the characteristics of cloth, and
Product is environmentally friendly, and the link effect and bonding effect between molecule are strong, and Efficient Adhesive Promotion is good, and plasticising and softening performance are strong, make the present invention
It is provided with soft or hard balance, improves the adhesive strength and wilfulness of glue, there is high waterproof effect and increases adhesive strength effect.
Specific embodiment
In order to make up the above deficiency, the present invention provides a kind of textile cloth glue and preparation method thereof, to solve above-mentioned background
The problems in technology.
A kind of textile cloth glue is made of the raw material for including following parts by weight:
The solvent is the composition that methanol, ethyl alcohol and methyl acetate mix.
The solvent is made from the following raw materials in parts by weight:
Methanol 5~15%；
Ethyl alcohol 15~25%；
Methyl acetate 16~24%.
The solvent is made from the following raw materials in parts by weight:
Methanol 10%；
Ethyl alcohol 20%；
Methyl acetate 22%.
It is made of the raw material for including following parts by weight:
The present invention also provides a kind of methods for preparing the textile cloth glue, comprising steps of
1) solvent of 45~58% parts by weight is put into reaction kettle, although putting into the polyethylene of 15~30% parts by weight afterwards
Polyvinyl butyral resin is stirred 2~4 hours with blender, is completely dissolved；
2) aldehyde ketone resin, the meteorology of 0.5~2% parts by weight of 20~30% parts by weight are then put into the reaction kettle
The citrate of white carbon black and 1~3% parts by weight；Stirring 1~2 hour, after the aldehyde ketone resin therein is completely dissolved, stirring
It is miscible to be filtered, textile cloth glue is made.
The solvent is the composition that methanol, ethyl alcohol and methyl acetate mix.
The preparation method of the solvent: take the methanol of 5~15% parts by weight, the ethyl alcohol of 15~25% parts by weight and 16~
The methyl acetate of 24% parts by weight is added in mixer and is mixed.
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment one:
1) solvent of 45% parts by weight is put into reaction kettle, although the polyvinyl butyral of 15% parts by weight of investment afterwards
Resin is stirred 2 hours with blender, is completely dissolved；
2) aldehyde ketone resin of 20% parts by weight, the meteorological white carbon black of 0.5% parts by weight are then put into the reaction kettle
With the citrate of 1% parts by weight；Stirring 1 hour after the aldehyde ketone resin therein is completely dissolved, stirs miscible carried out
Textile cloth glue is made in filter.
The solvent is the composition that methanol, ethyl alcohol and methyl acetate mix.
The preparation method of the solvent: the vinegar of the methanol of 5% parts by weight, the ethyl alcohol of 15% parts by weight and 16% parts by weight is taken
Sour methyl esters is added in mixer and is mixed.
Embodiment two:
1) solvent of 58% parts by weight is put into reaction kettle, although the polyvinyl butyral of 30% parts by weight of investment afterwards
Resin is stirred 4 hours with blender, is completely dissolved；
2) then put into the reaction kettle aldehyde ketone resins of 30% parts by weight, 2% parts by weight meteorological white carbon black and
The citrate of 3% parts by weight；Stirring 2 hours, after the aldehyde ketone resin therein is completely dissolved, stirring is miscible to be filtered,
Textile cloth glue is made.
The solvent is the composition that methanol, ethyl alcohol and methyl acetate mix.
The preparation method of the solvent: the methanol of 15% parts by weight, the ethyl alcohol of 25% parts by weight and 24% parts by weight are taken
Methyl acetate is added in mixer and is mixed.
Embodiment three:
1) solvent of 52% parts by weight is put into reaction kettle, although the polyvinyl butyral of 20% parts by weight of investment afterwards
Resin is stirred 3 hours with blender, is completely dissolved；
2) then put into the reaction kettle aldehyde ketone resins of 25% parts by weight, 1% parts by weight meteorological white carbon black and
The citrate of 2% parts by weight；Stirring 2 hours, after the aldehyde ketone resin therein is completely dissolved, stirring is miscible to be filtered,
Textile cloth glue is made.
The solvent is the composition that methanol, ethyl alcohol and methyl acetate mix.
The preparation method of the solvent: the methanol of 10% parts by weight, the ethyl alcohol of 20% parts by weight and 22% parts by weight are taken
Methyl acetate is added in mixer and is mixed.
The above shows and describes the basic principle, main features and advantages of the invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent circle.
Claims (8)
1. a kind of textile cloth glue, which is characterized in that be made of the raw material for including following parts by weight:
2. a kind of textile cloth glue as described in claim 1, it is characterised in that: the solvent is methanol, ethyl alcohol and methyl acetate
The composition mixed.
3. a kind of textile cloth glue as claimed in claim 2, which is characterized in that the solvent by following parts by weight raw material system
At:
Methanol 5~15%；
Ethyl alcohol 15~25%；
Methyl acetate 16~24%.
4. a kind of textile cloth glue as claimed in claim 3, which is characterized in that the solvent by following parts by weight raw material system
At:
Methanol 10%；
Ethyl alcohol 20%；
Methyl acetate 22%.
5. a kind of textile cloth glue as described in claim 1, which is characterized in that be made of the raw material for including following parts by weight:
6. a kind of textile cloth gluing method prepared as described in Claims 1 to 5, characterized in that it comprises the following steps:
1) solvent of 45~58% parts by weight is put into reaction kettle, although putting into the polyvinyl alcohol contracting of 15~30% parts by weight afterwards
Butyral resin is stirred 2~4 hours with blender, is completely dissolved；
2) aldehyde ketone resin of 20~30% parts by weight, the meteorological hard charcoal of 0.5~2% parts by weight are then put into the reaction kettle
The black citrate with 1~3% parts by weight；Stirring 1~2 hour after the aldehyde ketone resin therein is completely dissolved, is stirred miscible
It is filtered, textile cloth glue is made.
7. the method for preparation textile cloth glue as claimed in claim 6, it is characterised in that: the solvent is methanol, ethyl alcohol and vinegar
The composition that sour methyl esters mixes.
8. the method for preparation textile cloth glue as claimed in claims 6 or 7, which is characterized in that the preparation method of the solvent: take
Mixer is added in the methyl acetate of the methanol of 5~15% parts by weight, the ethyl alcohol of 15~25% parts by weight and 16~24% parts by weight
It is mixed in ware.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811131003.3A CN109355044A (en) | 2018-09-27 | 2018-09-27 | A kind of textile cloth glue and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811131003.3A CN109355044A (en) | 2018-09-27 | 2018-09-27 | A kind of textile cloth glue and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109355044A true CN109355044A (en) | 2019-02-19 |
Family
ID=65347883
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811131003.3A Pending CN109355044A (en) | 2018-09-27 | 2018-09-27 | A kind of textile cloth glue and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109355044A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI923022A0 (en) * | 1991-07-03 | 1992-06-29 | Basf Ag | REQUIRED PREPARATIONS, SOM INNEHAOLLER SYNTHETIC HARTS OCH SOM AER TVAERBINDBART VID RUMS- TEMPERATUR, OCH ANVAENDNING AV DETTA SOM LAMINERINGSLIM. |
| CN101838509A (en) * | 2010-05-20 | 2010-09-22 | 李能虎 | Formula of badminton adhesive |
| CN102449092A (en) * | 2009-06-09 | 2012-05-09 | 日本合成化学工业株式会社 | Pressure-sensitive adhesive composition, pressure-sensitive adhesive, pressure-sensitive adhesive for optical member, and optical member with pressure-sensitive adhesive layer obtained using same |
| CN106147644A (en) * | 2016-08-04 | 2016-11-23 | 中国西电集团公司 | A kind of high inorganic filler content laminate surface adhesive plaster and manufacture method thereof |
-
2018
- 2018-09-27 CN CN201811131003.3A patent/CN109355044A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI923022A0 (en) * | 1991-07-03 | 1992-06-29 | Basf Ag | REQUIRED PREPARATIONS, SOM INNEHAOLLER SYNTHETIC HARTS OCH SOM AER TVAERBINDBART VID RUMS- TEMPERATUR, OCH ANVAENDNING AV DETTA SOM LAMINERINGSLIM. |
| CN102449092A (en) * | 2009-06-09 | 2012-05-09 | 日本合成化学工业株式会社 | Pressure-sensitive adhesive composition, pressure-sensitive adhesive, pressure-sensitive adhesive for optical member, and optical member with pressure-sensitive adhesive layer obtained using same |
| CN101838509A (en) * | 2010-05-20 | 2010-09-22 | 李能虎 | Formula of badminton adhesive |
| CN106147644A (en) * | 2016-08-04 | 2016-11-23 | 中国西电集团公司 | A kind of high inorganic filler content laminate surface adhesive plaster and manufacture method thereof |
Non-Patent Citations (3)
| Title |
|---|
| 吉林化学工业公司设计院: "《聚乙烯醇生产工艺》", 31 August 1975, 轻工业出版社, pages: 281 * |
| 姚日生等: "《药用高分子材料，第2版》", 30 April 2008, 北京：化学工业出版社, pages: 194 * |
| 李广宇等: "《胶黏剂原材料手册》", 31 August 2004, pages: 534 * |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190219 |