CN1093107A - Natural spice-xinjiang saussurea involucrata essence and preparation method thereof - Google Patents
Natural spice-xinjiang saussurea involucrata essence and preparation method thereof Download PDFInfo
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- CN1093107A CN1093107A CN 93104205 CN93104205A CN1093107A CN 1093107 A CN1093107 A CN 1093107A CN 93104205 CN93104205 CN 93104205 CN 93104205 A CN93104205 A CN 93104205A CN 1093107 A CN1093107 A CN 1093107A
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- essence
- medicinal extract
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- spices
- snow lotus
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- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The present invention relates to a kind of natural spice-xinjiang saussurea involucrata essence and preparation method thereof, it mainly is earlier to adopt certain preparation method to make Snow Lotus Herb spices bright Snow Lotus Herb, and then spices and the required fluffy medicinal extract of lattice, first-class 15 kinds of components of Dihydrojasmone acid are mixed in proportion is adjustable the have aroma component of uniqueness and the essence of odour characteristics.Makeup, hair shampoo article, perfume that utilize this essence perfuming etc. are very popular.
Description
The invention belongs to daily cosmetics
Herba Saussureae Involueratae has another name called the snow lotus, is that the composite family hieracioides belongs to per nnial herb, mainly grows in slope, Xinjiang Tianshan north and south and Kun Lun Mountain.Because growing environment is special, take to be difficult for, so seem rare famous and precious, to record according to the Chinese Medicine document and carry and among the people continuing to use, the root of Snow Lotus Herb and herb all can be used as medicine.The medicinal material that Snow Lotus Herb is still not famous and precious, it also has unique fragrance ingredient, and odour characteristics, utilizes the makeup, hair shampoo article, perfume etc. of this essence perfuming very popular.
The objective of the invention is to, Saussurea involucrata is adopted certain Titian technology, extract the Snow Lotus Herb spice oil,, mix the Snow Lotus Herb flavor essence through the fragrance analysis.
Task of the present invention is with the Snow Lotus Herb spice oil that extracts animal to be carried out oral toxicity test and externally used coating test, and toxicity is lower as a result for it, nonirritant.
Natural perfume of the present invention-Herba Saussureae Involueratae extrait and preparation method thereof, it respectively consists of:
Component weight %
The fluffy medicinal extract 2-5 of lattice
Methyl dihydrojasmonate 8-12
Ling Lanquan 8-12
Lily of the valley base 8-12
Synthetic moss 1-3
Neryl C10H17-Nb
43-5
Lemon oil 5-8
Jasmine concrete 1-3
Tonka bean camphor 4-6
Phantol 8-12
Diethyl phthalate 5-8
The blue or green plain 2-6 of plum
Dun Bai is as medicinal extract 1-3
Musk xylene 4-6
Longifolene 8-11
Snow Lotus Herb concrete 3-5
This Snow Lotus Herb essence preparation method gets bright Snow Lotus Herb fraction sherwood oil lixiviate three times for (a), and decompression desolventizes concentrated; Again with enriched material with anhydrous alcohol solution, cooling, suction filtration, take off cured, filtration, concentrating under reduced pressure promptly gets spices; (b) again with spices dative lotus medicinal extract, methyl dihydrojasmonate, Ling Lanquan, lily of the valley base, synthetic moss, flores aurantii benzene Nb
4, lemon oil, jasmine concrete, tonka bean camphor, phantol, O-phthalic diethyl ester, Mei Qingsu, a uncle when medicinal extract, musk xylene, come into leaves rare, mix saussurea involucrata essence by proportioning.
Natural perfume of the present invention-Herba Saussureae Involueratae essence and preparation method thereof, the spice oil of its gained is carried out the oral toxicity experiment to 20 white mouse with various dose to be shown, its toxicity is lower, and oral medium lethal dose (L050) is about 4-4.5 milliliter/kilogram small white mouse.According to tame lagophthalmos conjunctiva coating experiment is shown, the Snow Lotus Herb spice oil is to the mucous membrane nonirritant, adopt gas chromatography/mass spectrometry, infrared spectra, computer coupling technique that Snow Lotus Herb spices is carried out the fragrance ingredient analysis simultaneously, its major ingredient is sesquiterpene and oxygenatedchemicals thereof, also contain a certain amount of ester fat alcohol, aldehyde etc. and have delicate fragrance, medicine perfume (or spice), the chrysanthemum sample fragrance of a flower, slightly sweet cream perfume (or spice), lasting power is preferably arranged.
Embodiment 1:
(a) 60 ℃ of-90 ℃ of fraction sherwood oil lixiviates of sampling Snow Lotus Herb are three times, and decompression desolventizes concentrated, and enriched material promptly gets spices with 3-5 times of anhydrous alcohol solution (50 ℃) at 1-5 ℃ of cooling, suction filtration, dewaxing, filtration, concentrating under reduced pressure.
(b) various required components are mixed in proportion mix saussurea involucrata essence
Component weight %
Lattice lotus medicinal extract 2
Methyl dihydrojasmonate 12
Ling Lanquan 8
Lily of the valley base 8
Synthetic moss 1
Neryl C10H17-Nb
45
Lemon oil 5
Jasmine concrete 3
Tonka bean camphor 4
Phantol 12
Diethyl phthalate 5
Plum blue or green plain 6
Dun Bai is when medicinal extract 1
Musk xylene 6
Longifolene 8
Snow Lotus Herb concrete 5
Embodiment 2:
(a) 60 ℃ of-90 ℃ of fraction sherwood oil lixiviates of sampling Snow Lotus Herb are three times, and decompression desolventizes concentrated, and enriched material promptly gets spices with 3-5 times of anhydrous alcohol solution (50 ℃) at 1-5 ℃ of cooling, suction filtration, dewaxing, filtration, concentrating under reduced pressure.
(b) various required components are mixed in proportion mix saussurea involucrata essence
Component weight %
Lattice lotus medicinal extract 5
Methyl dihydrojasmonate 8
Ling Lanquan 12
Lily of the valley base 4
Synthetic moss 3
Neryl C10H17-Nb
43
Lemon oil 8
Jasmine concrete 1
Coumarin 6
Phantol 8
Diethyl phthalate 8
Plum blue or green plain 2
Dun Bai is when medicinal extract 3
Musk xylene 4
Longifolene 11
Snow Lotus Herb concrete 3.
Claims (2)
1, a kind of natural perfume-Herba Saussureae Involueratae extrait and preparation method thereof is characterized in that, this spices respectively consists of:
Component weight %
The fluffy medicinal extract 2-5 of lattice
Methyl dihydrojasmonate 8-12
Ling Lanquan 8-12
Lily of the valley base 8-12
Synthetic moss 1-3
Neryl C10H17-Nb
43-5
Lemon oil 5-8
Jasmine concrete 1-3
Tonka bean camphor 4-6
Phantol 8-12
Diethyl phthalate 5-8
The blue or green plain 2-6 of plum
Dun Bai is as medicinal extract 1-3
Musk xylene 4-6
Longifolene 8-11
Snow Lotus Herb concrete 3-5
2, a kind of natural perfume-Herba Saussureae Involueratae extrait and preparation method thereof is characterized in that:
(a) get bright Snow Lotus Herb fraction sherwood oil lixiviate three times, decompression desolventizes concentrated; Again with the enriched material anhydrous alcohol solution, cooling, suction filtration, take off cured, filtration, concentrating under reduced pressure promptly gets spices.
(b) again with spices dative lotus medicinal extract, methyl dihydrojasmonate, Ling Lanquan, lily of the valley base, synthetic moss, flores aurantii benzene Nb
4, lemon oil, jasmine concrete, tonka bean camphor, phantol, O-phthalic diethyl ester, Mei Qingsu, a uncle when medicinal extract, musk xylene, come into leaves rare, mix saussurea involucrata essence by proportioning.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93104205 CN1093107A (en) | 1993-04-02 | 1993-04-02 | Natural spice-xinjiang saussurea involucrata essence and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 93104205 CN1093107A (en) | 1993-04-02 | 1993-04-02 | Natural spice-xinjiang saussurea involucrata essence and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1093107A true CN1093107A (en) | 1994-10-05 |
Family
ID=4985069
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 93104205 Pending CN1093107A (en) | 1993-04-02 | 1993-04-02 | Natural spice-xinjiang saussurea involucrata essence and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1093107A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101961300A (en) * | 2010-09-29 | 2011-02-02 | 重庆市超临界精细化工生产力促进中心有限公司 | Perfume composition containing pepper aroma essential oil and preparation method thereof |
| CN103966023A (en) * | 2014-05-22 | 2014-08-06 | 广西平果华莲科技研究所 | Method for extracting essence from lotus stamens |
-
1993
- 1993-04-02 CN CN 93104205 patent/CN1093107A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101961300A (en) * | 2010-09-29 | 2011-02-02 | 重庆市超临界精细化工生产力促进中心有限公司 | Perfume composition containing pepper aroma essential oil and preparation method thereof |
| CN101961300B (en) * | 2010-09-29 | 2011-12-28 | 重庆市超临界精细化工生产力促进中心有限公司 | Perfume composition containing pepper aroma essential oil and preparation method thereof |
| CN103966023A (en) * | 2014-05-22 | 2014-08-06 | 广西平果华莲科技研究所 | Method for extracting essence from lotus stamens |
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| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
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| C12 | Rejection of a patent application after its publication | ||
| RJ01 | Rejection of invention patent application after publication |