CN109294744A - A method of extracting yulan magnolia hydrosol - Google Patents
A method of extracting yulan magnolia hydrosol Download PDFInfo
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- CN109294744A CN109294744A CN201811314839.7A CN201811314839A CN109294744A CN 109294744 A CN109294744 A CN 109294744A CN 201811314839 A CN201811314839 A CN 201811314839A CN 109294744 A CN109294744 A CN 109294744A
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- Prior art keywords
- hydrosol
- yulan magnolia
- extracting
- steam
- yulan
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The present invention relates to a kind of technical fields for extracting hydrosol, more particularly to a kind of method for extracting yulan magnolia hydrosol, it is characterized by: this method are as follows: pick fresh yulan magnolia, net material, dry the moisture of yulan flower surface, it is uniformly spread again in the air-conditioned room that temperature is 20 DEG C~24 DEG C, and in air-conditioned room internal spraying alcohol blend, humidity reaches 90% or more in room, 1~2 hour is stood, then, taking-up is placed in and is distilled using steam, distillation gained hydrosol steam is condensed, and condensation acquired solution is yulan magnolia hydrosol.The present invention effectively improves the amount for extracting yulan magnolia hydrosol, and yulan magnolia hydrosol can be made to maximize the features such as keeping yulan magnolia characteristic.
Description
Technical field
The present invention relates to a kind of technical field for extracting hydrosol, in particular to a kind of method for extracting yulan magnolia hydrosol.
Background technique
Hydrosol, also known as crystal oil (Hydrolate), refer to that essential oil during distillation extraction, is separated when refining essential oil
The distillation stoste that one kind 100% out is saturated, is a kind of byproduct of essential oil, composition is naturally pure, and fragrance is light pleasant.
How to extract to obtain hydrosol in the prior art, and discloses some technical solutions.
Related Chinese patent literature is retrieved, as follows:
1, a kind of centella hydrosol of Chinese patent<application number>201710037023.3<denomination of invention>and preparation method thereof and use
Way<summary>discloses a kind of centella hydrosol and its preparation method and application.It picks fresh centella to clean, clean, cutting is set
In distiller, hot deionized water being added and impregnates, heat temperature raising distills later, connects circulating cooling liquid, condenser distillate is collected,
Stop distillation when the distillate volume of collection is to feed intake 0. 8-1.2 times of yulan magnolia quality, distillate is micro- through 0.22 micron
Hole membrane filtration degerming, obtains centella hydrosol.
2, a kind of bitter water rose hydrosol extracting method of Chinese patent<application number>201711099869.6<denomination of invention><
Make a summary > disclose bitter water rose hydrosol extracting method, including successively carry out equipment wash phase, Rosa Damascana extract the stage and
Rose extracts the stage, and the Rosa Damascana extraction stage persistently carries out at the first time, when Rosa Damascana extracts the stage, opens
Oil water separator closes oil water separator to rose reservoir valve, by rhodamine toner to outlet valve between fuliu column
Oil is led in Rosa Damascana holding vessel；The rose extracts the stage: closing oil water separator to water outlet between fuliu column
Valve opens oil water separator to rose reservoir valve, Rosa Damascana is led in rose holding vessel；Pass through tune
Section cooling water inflow or steam inlet valve make the temperature of condenser condensed water water outlet be maintained at the first temperature, steam inlet
Mouth pressure control is in the first atmospheric pressure；Persistently distill steam off air intake valve after the second time.
3, a kind of spray of Chinese patent<application number>201510777693.X<denomination of invention>hydrosol containing wormwood and its
Preparation method<summary>belongs to cosmetic technical field, and in particular to a kind of spray of the hydrosol containing wormwood and preparation method thereof.
The spray of wormwood hydrosol is mainly by wormwood hydrosol, rose, camomile extract, trehalose, allantoin, glycyrrhizic acid two
Potassium, hyaluronic acid, glycerol, preservative and water composition.
4, a kind of jasmine essential oil and head of extracting of Chinese patent<application number>201510868175.9<denomination of invention>is fragrant
Method<summary>disclose it is a kind of extraction jasmine essential oil and head perfume method, this method including distillation, condensation, water-oil separating,
Absorption, a rectifying concentration, alcohol analysis, secondary rectifying concentration and etc..
From the document retrieved we it can be appreciated that also there is the method to plant extract hydrosol in the prior art, still,
Required equipment, preparation process used is complex, takes time and effort；So how to carry out technological improvement to the prior art.
Summary of the invention
The purpose of the present invention is in view of the drawbacks of the prior art, and provide a kind of method for extracting yulan magnolia hydrosol.
To achieve the purpose of the present invention, the technical solution taken are as follows:
A method of extracting yulan magnolia hydrosol, this method are as follows: pick fresh yulan magnolia, net material dries yulan flower surface
Moisture, then uniformly spread and be in 20 DEG C~24 DEG C of air-conditioned room in temperature, and in air-conditioned room internal spraying alcohol blend, room
Humidity reaches 90% or more, stands 1~2 hour, then, takes out and is distilled using steam, and distillation gained hydrosol steam carries out
Condensation, condensation acquired solution is yulan magnolia hydrosol.
Preferably, stop when the weight of the yulan magnolia hydrosol and the yulan magnolia weight of drying moisture are 1.2~1.6:1
Distillation.
Preferably, the alcohol blend are as follows: 10% alcohol, 5% ethyl acetate and surplus are pure water；Preparation method
Are as follows: ethyl acetate is dissolved in alcohol, is uniformly mixed, then be watered to get alcohol blend.
Preferably, to realize that equipment used by this method includes steam boiler, raw material cabin and cooling tank, the steam copper
Furnace is connected to by steam pipe with raw material cabin, and the raw material cabin is connected to by hydrosol steam pipe with cooling tank, and the cooling tank passes through
Hydrosol pipe is connected to collecting means.
Preferably, the hydrosol steam pipe is equipped with cooling piece, and the cooling piece is equipped with water inlet pipe and outlet pipe.
Preferably, the outlet pipe is connect with the condenser pipe in drainer.
Preferably, the collecting means are equipped with liquidometer.
Preferably, the raw material cabin is equipped with pressure gauge.
Yulan magnolia: Classification system:Magnolia denudata Desr. , alias Flos micheliae Albae, prestige spring, yulan magnolia etc.；Wood
Orchid family subgenus Yulania, deciduous tree.Grey color is to lilac red, and large-scale, fragrance, corolla cup-shaped is spent and first opened, long after leaf,
Florescence 10 days or so；Dissolving phlegm, beneficial lung is gentle, candied outstanding good.Yulan magnolia contains volatile oil, wherein predominantly citral, caryophyllus oil
Acid etc. has certain medicine also containing ingredients such as magnoflorine, alkaloid, Magnolin, capric acid, rutin, oleic acid, vitamin As
With value.Yulan magnolia nature and flavor are pungent, warm, have effects that expelling wind and clearing away cold is sensible, promoting the dispersing function of the lung leads to nose.Can be used for having a headache, blood stasis type dysmenorrhea,
The diseases such as nasal obstruction, acute and chronic nasal sinusitis, allergic rhinitis.Modern pharmacology research shows that yulan magnolia has suppression to common skin fungi
Production is used.
Ethyl acetate is also known as ethyl acetate, and hypotoxicity is pleasantly sweet, and irritant smell, volatile when concentration is higher, is one
The widely used fine chemical product of kind.Widely used with excellent dissolubility, quick-drying, being that one kind is important organises
Work raw material and industrial solvent.
Compared with prior art, the present invention being with substantive distinguishing features outstanding and significant progress: the present invention is used
Extracting method its operating procedure it is simple, be easy to facilitate operation, and required equipment is small, area occupied is small；Before distillation, will first it steam
Evaporate raw material to be placed in air-conditioned room and mix up temperature, then spray alcohol blend, state fog-like, guarantee in room moisture reach 90% with
On, raw material surface sorbing liquor essence mixed liquor, by alcohol and ethyl acetate catalytic action, so that raw material discharges solable matter,
Convenient for subsequent distillation, entire extraction process is with steam for extraction medium, then without other additives；Distilling gained hydrosol amount is
1.2~1.6 times of raw material weight, and hydrosol its purity level height obtained, can maximize the characteristic for retaining distillating material, from
And the pharmacological property that raw material is presented can be maximized；It can be that manufacturing enterprise brings biggish economic benefit.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram for the used equipment of method for extracting yulan magnolia hydrosol of the present invention；
Each component corresponds to the title of serial number: steam boiler -1, steam pipe -2, pressure gauge -3, raw material cabin -4, hydrosol steam in figure
Pipe -5, water inlet pipe -6, cooling piece -7, outlet pipe -8, cooling tank -9, drainpipe -10, collecting means -11, liquidometer -12, hydrosol
Pipe -13.
Specific embodiment
It is the embodiment of the present invention below, for invention is further described in detail:
Embodiment 1:
A method of extracting yulan magnolia hydrosol, this method are as follows: pick fresh yulan magnolia, net material dries yulan flower surface
Moisture, then uniformly spread and be in 20 DEG C~24 DEG C of air-conditioned room in temperature, and in air-conditioned room internal spraying alcohol blend, room
Humidity reaches 90% or more, stands 1~2 hour, then, takes out, and when taking-up, raw material is contacted with air, and raw material surface is promoted to adhere to
Alcohol and ethyl acetate volatilization, and distilled using steam, distillation gained hydrosol steam is condensed, and condensation gained is molten
Liquid is yulan magnolia hydrosol.
The weight of the yulan magnolia hydrosol and the yulan magnolia weight of drying moisture stop distilling when being 1.2:1.
The alcohol blend are as follows: 10% alcohol, 5% ethyl acetate and surplus are pure water；The preparation method comprises the following steps: by acetic acid
Ethyl ester is dissolved in alcohol, is uniformly mixed, then be watered to get alcohol blend.
As shown in Figure 1, to realize that equipment used by this method includes steam boiler 1, raw material cabin 4 and cooling tank 9, it is described
Steam boiler 1 is connected to by steam pipe 2 with raw material cabin 4, and the raw material cabin 4 is connected to by hydrosol steam pipe 5 with cooling tank 9, institute
Cooling tank 9 is stated to be connected to by hydrosol pipe 13 with collecting means 11.
The hydrosol steam pipe 5 is equipped with cooling piece 7, and the cooling piece 7 is equipped with water inlet pipe 6 and outlet pipe 8, water inlet pipe 6
Interior conveying condensed water, condensed water is delivered in cooling piece 7, is realized and is carried out just to the hydrosol in hydrosol steam pipe being in steam condition
Secondary condensation can be effectively reduced the impact velocity of steam hydrosol through condensation, enter when through first condensed steam hydrosol
After drainer 9, realizes rapid condensation effect, greatly shorten the time of condensation.
The outlet pipe 8 is connect with the condenser pipe in drainer 9, realizes condensed water secondary use.
The collecting means 11 are equipped with liquidometer 12；Liquidometer 12 can facilitate hydrosol obtained by the distillation in observation collecting means 11 molten
The amount of liquid, by the amount of hydrosol in liquidometer 12 accurately measurement collecting means 11, when the weight of hydrosol and the yulan magnolia of drying moisture
Stop distillation when weight is 1.2:1, this can guarantee the quality of distillation gained hydrosol.
The raw material cabin 4 is equipped with pressure gauge 3, can facilitate the pressure of steam in observation raw material cabin 4.
Embodiment 2:
A method of extracting yulan magnolia hydrosol, this method are as follows: pick fresh yulan magnolia, net material dries yulan flower surface
Moisture, then uniformly spread and be in 20 DEG C~24 DEG C of air-conditioned room in temperature, and in air-conditioned room internal spraying alcohol blend, room
Humidity reaches 90% or more, stands 1~2 hour, then, takes out, and when taking-up, raw material is contacted with air, and raw material surface is promoted to adhere to
Alcohol and ethyl acetate volatilization, and distilled using steam, distillation gained hydrosol steam is condensed, and condensation gained is molten
Liquid is yulan magnolia hydrosol.
The weight of the yulan magnolia hydrosol and the yulan magnolia weight of drying moisture stop distilling when being 1.4:1.
The alcohol blend are as follows: 10% alcohol, 5% ethyl acetate and surplus are pure water；The preparation method comprises the following steps: by acetic acid
Ethyl ester is dissolved in alcohol, is uniformly mixed, then be watered to get alcohol blend.
As shown in Figure 1, to realize that equipment used by this method includes steam boiler 1, raw material cabin 4 and cooling tank 9, it is described
Steam boiler 1 is connected to by steam pipe 2 with raw material cabin 4, and the raw material cabin 4 is connected to by hydrosol steam pipe 5 with cooling tank 9, institute
Cooling tank 9 is stated to be connected to by hydrosol pipe 13 with collecting means 11.
The hydrosol steam pipe 5 is equipped with cooling piece 7, and the cooling piece 7 is equipped with water inlet pipe 6 and outlet pipe 8, water inlet pipe 6
Interior conveying condensed water, condensed water is delivered in cooling piece 7, is realized and is carried out just to the hydrosol in hydrosol steam pipe being in steam condition
Secondary condensation can be effectively reduced the impact velocity of steam hydrosol through condensation, enter when through first condensed steam hydrosol
After drainer 9, realizes rapid condensation effect, greatly shorten the time of condensation.
The outlet pipe 8 is connect with the condenser pipe in drainer 9, realizes condensed water secondary use.
The collecting means 11 are equipped with liquidometer 12；Liquidometer 12 can facilitate hydrosol obtained by the distillation in observation collecting means 11 molten
The amount of liquid, by the amount of hydrosol in liquidometer 12 accurately measurement collecting means 11, when the weight of hydrosol and the yulan magnolia of drying moisture
Stop distillation when weight is 1.4:1, this can guarantee the quality of distillation gained hydrosol.
The raw material cabin 4 is equipped with pressure gauge 3, can facilitate the pressure of steam in observation raw material cabin 4.
Embodiment 3:
A method of extracting yulan magnolia hydrosol, this method are as follows: pick fresh yulan magnolia, net material dries yulan flower surface
Moisture, then uniformly spread and be in 20 DEG C~24 DEG C of air-conditioned room in temperature, and in air-conditioned room internal spraying alcohol blend, room
Humidity reaches 90% or more, stands 1~2 hour, then, takes out, and when taking-up, raw material is contacted with air, and raw material surface is promoted to adhere to
Alcohol and ethyl acetate volatilization, and distilled using steam, distillation gained hydrosol steam is condensed, and condensation gained is molten
Liquid is yulan magnolia hydrosol.
The weight of the yulan magnolia hydrosol and the yulan magnolia weight of drying moisture stop distilling when being 1.5:1.
The alcohol blend are as follows: 10% alcohol, 5% ethyl acetate and surplus are pure water；The preparation method comprises the following steps: by acetic acid
Ethyl ester is dissolved in alcohol, is uniformly mixed, then be watered to get alcohol blend.
As shown in Figure 1, to realize that equipment used by this method includes steam boiler 1, raw material cabin 4 and cooling tank 9, it is described
Steam boiler 1 is connected to by steam pipe 2 with raw material cabin 4, and the raw material cabin 4 is connected to by hydrosol steam pipe 5 with cooling tank 9, institute
Cooling tank 9 is stated to be connected to by hydrosol pipe 13 with collecting means 11.
The hydrosol steam pipe 5 is equipped with cooling piece 7, and the cooling piece 7 is equipped with water inlet pipe 6 and outlet pipe 8, water inlet pipe 6
Interior conveying condensed water, condensed water is delivered in cooling piece 7, is realized and is carried out just to the hydrosol in hydrosol steam pipe being in steam condition
Secondary condensation can be effectively reduced the impact velocity of steam hydrosol through condensation, enter when through first condensed steam hydrosol
After drainer 9, realizes rapid condensation effect, greatly shorten the time of condensation.
The outlet pipe 8 is connect with the condenser pipe in drainer 9, realizes condensed water secondary use.
The collecting means 11 are equipped with liquidometer 12；Liquidometer 12 can facilitate hydrosol obtained by the distillation in observation collecting means 11 molten
The amount of liquid, by the amount of hydrosol in liquidometer 12 accurately measurement collecting means 11, when the weight of hydrosol and the yulan magnolia of drying moisture
Stop distillation when weight is 1.5:1, this can guarantee the quality of distillation gained hydrosol.
The raw material cabin 4 is equipped with pressure gauge 3, can facilitate the pressure of steam in observation raw material cabin 4.
Embodiment 4:
A method of extracting yulan magnolia hydrosol, this method are as follows: pick fresh yulan magnolia, net material dries yulan flower surface
Moisture, then uniformly spread and be in 20 DEG C~24 DEG C of air-conditioned room in temperature, and in air-conditioned room internal spraying alcohol blend, room
Humidity reaches 90% or more, stands 1~2 hour, then, takes out, and when taking-up, raw material is contacted with air, and raw material surface is promoted to adhere to
Alcohol and ethyl acetate volatilization, and distilled using steam, distillation gained hydrosol steam is condensed, and condensation gained is molten
Liquid is yulan magnolia hydrosol.
The weight of the yulan magnolia hydrosol and the yulan magnolia weight of drying moisture stop distilling when being 1.6:1.
The alcohol blend are as follows: 10% alcohol, 5% ethyl acetate and surplus are pure water；The preparation method comprises the following steps: by acetic acid
Ethyl ester is dissolved in alcohol, is uniformly mixed, then be watered to get alcohol blend.
As shown in Figure 1, to realize that equipment used by this method includes steam boiler 1, raw material cabin 4 and cooling tank 9, it is described
Steam boiler 1 is connected to by steam pipe 2 with raw material cabin 4, and the raw material cabin 4 is connected to by hydrosol steam pipe 5 with cooling tank 9, institute
Cooling tank 9 is stated to be connected to by hydrosol pipe 13 with collecting means 11.
The hydrosol steam pipe 5 is equipped with cooling piece 7, and the cooling piece 7 is equipped with water inlet pipe 6 and outlet pipe 8, water inlet pipe 6
Interior conveying condensed water, condensed water is delivered in cooling piece 7, is realized and is carried out just to the hydrosol in hydrosol steam pipe being in steam condition
Secondary condensation can be effectively reduced the impact velocity of steam hydrosol through condensation, enter when through first condensed steam hydrosol
After drainer 9, realizes rapid condensation effect, greatly shorten the time of condensation.
The outlet pipe 8 is connect with the condenser pipe in drainer 9, realizes condensed water secondary use.
The collecting means 11 are equipped with liquidometer 12；Liquidometer 12 can facilitate hydrosol obtained by the distillation in observation collecting means 11 molten
The amount of liquid, by the amount of hydrosol in liquidometer 12 accurately measurement collecting means 11, when the weight of hydrosol and the yulan magnolia of drying moisture
Stop distillation when weight is 1.6:1, this can guarantee the quality of distillation gained hydrosol.
The raw material cabin 4 is equipped with pressure gauge 3, can facilitate the pressure of steam in observation raw material cabin 4.
It is that virtue treats the resulting condensation aqueous solution of plant distillation by above-mentioned acquired yulan magnolia hydrosol, primary efficacy is to mend
Water plays the role of similar and effect with plants essential oil itself, and uses more convenient, can there is various treatments to skin
Effect and maintenance；Oil-control anti-aging, activation aged cells, moisturizing promote blood circulation, balance oil；Oral efficacy: improvement nasal obstruction,
The symptoms such as acute and chronic nasal sinusitis, allergic rhinitis, cough, pneumonia.
The above are wherein specific implementations of the invention, and the description thereof is more specific and detailed, but can not therefore manage
Solution is limitation of the scope of the invention.It should be pointed out that for those of ordinary skill in the art, not departing from this hair
Under the premise of bright design, various modifications and improvements can be made, these obvious alternative forms belong to of the invention
Protection scope.
Claims (8)
1. a kind of method for extracting yulan magnolia hydrosol, it is characterised in that: this method are as follows: pick fresh yulan magnolia, net material, drying
The moisture of yulan flower surface, then uniformly spread and be in 20 DEG C~24 DEG C of air-conditioned room in temperature, and in air-conditioned room internal spraying alcohol
Mixed liquor, humidity reaches 90% or more in room, stands 1~2 hour, then, takes out and is simultaneously distilled using steam, distills institute
It obtains hydrosol steam to be condensed, condensation acquired solution is yulan magnolia hydrosol.
2. the method according to claim 1 for extracting yulan magnolia hydrosol, it is characterised in that: the weight of the yulan magnolia hydrosol
Yulan magnolia weight with drying moisture stops distilling when being 1.2~1.6:1.
3. the method according to claim 1 for extracting yulan magnolia hydrosol, which is characterized in that the alcohol blend are as follows: 10%
Alcohol, 5% ethyl acetate and surplus be pure water；The preparation method comprises the following steps: ethyl acetate is dissolved in alcohol, it is uniformly mixed, then convert
Water is to get alcohol blend.
4. the method according to claim 1 for extracting yulan magnolia hydrosol, which is characterized in that realize used by this method
Equipment includes steam boiler (1), raw material cabin (4) and cooling tank (9), and the steam boiler (1) passes through steam pipe (2) and raw material cabin
(4) it is connected to, the raw material cabin (4) is connected to by hydrosol steam pipe (5) with cooling tank (9), and the cooling tank (9) passes through hydrosol pipe
(13) it is connected to collecting means (11).
5. the method according to claim 4 for extracting yulan magnolia hydrosol, it is characterised in that: on the hydrosol steam pipe (5)
Equipped with cooling piece (7), the cooling piece (7) is equipped with water inlet pipe (6) and outlet pipe (8).
6. the method according to claim 5 for extracting yulan magnolia hydrosol, it is characterised in that: the outlet pipe (8) and condensation
Condenser pipe connection in tank (9).
7. the method according to claim 4 for extracting yulan magnolia hydrosol, it is characterised in that: the collecting means (11) are equipped with liquid
Position meter (12).
8. the method according to claim 4 for extracting yulan magnolia hydrosol, it is characterised in that: the raw material cabin (4) is equipped with pressure
Power table (3).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811314839.7A CN109294744A (en) | 2018-11-06 | 2018-11-06 | A method of extracting yulan magnolia hydrosol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811314839.7A CN109294744A (en) | 2018-11-06 | 2018-11-06 | A method of extracting yulan magnolia hydrosol |
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| Publication Number | Publication Date |
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| CN109294744A true CN109294744A (en) | 2019-02-01 |
Family
ID=65145449
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811314839.7A Withdrawn CN109294744A (en) | 2018-11-06 | 2018-11-06 | A method of extracting yulan magnolia hydrosol |
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| Country | Link |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109576062A (en) * | 2019-02-12 | 2019-04-05 | 无锡薇泰药物技术有限公司 | A kind of Chinese yew hydrosol extraction process |
| CN113462477A (en) * | 2020-03-31 | 2021-10-01 | 广东省禾基生物科技有限公司 | Extraction method and application of magnolia cell water and magnolia essential oil |
-
2018
- 2018-11-06 CN CN201811314839.7A patent/CN109294744A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109576062A (en) * | 2019-02-12 | 2019-04-05 | 无锡薇泰药物技术有限公司 | A kind of Chinese yew hydrosol extraction process |
| CN113462477A (en) * | 2020-03-31 | 2021-10-01 | 广东省禾基生物科技有限公司 | Extraction method and application of magnolia cell water and magnolia essential oil |
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Application publication date: 20190201 |