CN109289070A - A kind of volatile-type liquid air freshener of suspension goldleaf particle and preparation method thereof - Google Patents
A kind of volatile-type liquid air freshener of suspension goldleaf particle and preparation method thereof Download PDFInfo
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- CN109289070A CN109289070A CN201811222167.7A CN201811222167A CN109289070A CN 109289070 A CN109289070 A CN 109289070A CN 201811222167 A CN201811222167 A CN 201811222167A CN 109289070 A CN109289070 A CN 109289070A
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- goldleaf
- volatile
- particle
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- air freshener
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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Abstract
The invention discloses a kind of volatile-type liquid air freshener of suspension goldleaf particle, the component including following mass fraction: deionized water 30%~50%, ethyl alcohol 10%~30%, dipropylene glycol methyl ether 15%~35%, solubilizer 1%~10%, essence 1%~10%, acrylic acid crosslinked resin 0.1%~2%, triethanolamine 0.1%~2%, preservative 0.1%~1%, goldleaf particle 0.01%~0.1%.Invention additionally discloses the preparation methods of the volatile-type liquid air freshener of the suspension goldleaf particle.Goldleaf can be steadily suspended in wherein air freshener provided by the invention in use, without being influenced by volatile component volatilization.
Description
Technical field
The present invention relates to a kind of liquid air fresheners and preparation method thereof, more particularly, to a kind of suspension goldleaf particle
Volatile-type liquid air freshener and preparation method thereof.
Background technique
Currently, most of volatile liquid air freshener on the market, abbreviation champignon volatilizees liquid or rattan volatilizees liquid, with rattan
The media such as item, ceramics are assisted fragrance emissions into air.As champignon volatilization liquid is in the universal of American-European air freshener market,
Consumer generates great interest and demand, such as addition goldleaf for the novelty of product appearance to assign product luxury
Appearance.However, the solvent-borne formulation of rattan volatilization liquid influences greatly the suspension stability of goldleaf, while liquid in volatilization process
The continuous of yield value changes the suspension time that also will affect goldleaf.Therefore, it is necessary to study a in volatilization and use process
The volatile liquid air freshener for keeping goldleaf particle to suspend.
Summary of the invention
It is an object of the present invention to provide a kind of volatile-type liquid air freshener of suspension goldleaf particle, the air is clear
Goldleaf can be steadily suspended in wherein in use for new agent, without being influenced by volatile component volatilization.
An object of the present invention is achieved through the following technical solutions: a kind of volatile-type liquid-containing air of suspension goldleaf particle
Gas freshener, the component including following mass fraction:
Deionized water 30%~50%
Ethyl alcohol 10%~30%
Dipropylene glycol methyl ether 15%~35%
Solubilizer 1%~10%
Essence 1%~10%
Acrylic acid crosslinked resin 0.1%~2%
Triethanolamine 0.1%~2%
Preservative 0.1%~1%
Goldleaf particle 0.01%~0.1%.
Transparent thick liquid after acrylic acid crosslinked resin and triethanolamine neutralize in the present invention, forms transparent adhesive tape plastid
System has the function of thickening, suspends, and suitable goldleaf particle can be steadily suspended in wherein, not volatilized by volatile component
It influences and settles.
In the present invention, the viscosity of acrylic acid crosslinked resin will affect the dispersion of goldleaf and other components, and selected
The resin viscosity selected is too big, is unfavorable for volatile component volatilization, can not play the role of air freshener, is event present invention selection
The acrylic acid crosslinked resin of colloid systems of the viscosity lower than 10000Cps can be obtained.Further, the present invention preferably has anti-
The acrylic acid crosslinked resin of electrostatic capacity, including but not limited to polyacrylate cross-linked polymer -6 etc..Due to these acrylic acid
Crosslinked resin has antistatic effect, the electrolyte being able to bear in system, such as ethyl alcohol, dipropylene glycol methyl ether, solubilizer, essence
The electrostatic charge of equal generations, avoids the aggregation of goldleaf from settling, therefore, so that whole system suspendability is maintained.
The preservative selects liquid preservative agent, and including but not limited to liquid is outstanding beautiful (Plus).
The solubilizer includes but is not limited to one of Cremophor RH40 and polysorbas20 (Tween-20) or two
The combination of kind.
The size of the goldleaf particle is 0.2cm × 0.2cm × 0.12 μm.
The second object of the present invention is to provide the preparation side of the volatile-type liquid air freshener of above-mentioned suspension goldleaf particle
Method.
The second object of the present invention is achieved through the following technical solutions: a kind of volatile-type liquid-containing air of suspension goldleaf particle
The preparation method of gas freshener, comprising the following steps:
(1) acrylic acid crosslinked resin is dissolved in part ion water, obtains acrylic acid crosslinked resin aqueous solution；
(2) remaining deionized water dilution triethanolamine is taken to obtain triethanolamine solution, then with acrylic acid crosslinked resin water
Solution mixing, stirring to acrylic acid crosslinked resin and triethanolamine sufficiently neutralize and system pH is 7.0-7.5, obtain clear viscous
Liquid；
(3) ethyl alcohol is added to the resulting clear viscous liquids of step (2) and preservative is uniformly mixed, obtain mixed liquor；
(4) it takes essence, solubilizer and dipropylene glycol methyl ether to be added in the mixed liquor after mixing, stirs evenly；
(5) goldleaf particle is added, stirs evenly, defoams.
Compared with prior art, the invention has the following beneficial effects:
1. the present invention, which is reacted with acrylic acid crosslinked resin with triethanolamine, generates the transparent suitable colloid systems of viscosity, gold
Foil steadily suspends wherein, is not influenced by volatilizing in volatile component.
2. air freshener provided by the invention stands January in 45 DEG C of baking ovens, goldleaf is not settled, and is not assembled.
3.100 grams of goldleaf volatile-type liquid air fresheners are inserted into 6 fibre cores (distribution medium, long 30cm, diameters
3mm), service life is 4~6 months, and allowing maximum residue limit is 15%, and goldleaf does not settle, do not assemble in use process.
Specific embodiment
Invention is further described in detail combined with specific embodiments below, but protection scope of the present invention be not limited to
Under embodiment.
Embodiment 1
Formula: deionized water 40%, ethyl alcohol 15%, dipropylene glycol methyl ether 34%, Cremophor RH40 5%, essence
5%, polyacrylate cross-linked polymer -6 0.2%, triethanolamine 0.5%, liquid outstanding person beauty (Plus) 0.25%, goldleaf particle
(0.2cm × 0.2cm × 0.12 μm) 0.05%.
Preparation method:
(1) polyacrylate cross-linked polymer -6 is dissolved in part ion water, obtains polyacrylate cross-linked polymer -6
Aqueous solution.
(2) it takes remaining deionized water dilution triethanolamine to obtain triethanolamine solution, while stirring adds triethanolamine solution
Enter in -6 aqueous solution of the third polyacrylate cross-linked polymer, continuing stirring makes polyacrylate cross-linked polymer -6 and triethanolamine
It sufficiently neutralizes, system pH is 7.0-7.5, obtains clear viscous liquids.
(3) ethyl alcohol is added to the resulting clear viscous liquids of step (2) and the outstanding beauty of liquid is uniformly mixed, obtain mixed liquor.
(4) essence, Cremophor RH40 and dipropylene glycol methyl ether is taken to be added in the mixed liquor after mixing,
It stirs evenly.
(5) goldleaf particle is added, stirs evenly, defoams.
The volatilization liquid of goldleaf made from the formula passes through 45 DEG C of 1 month baking oven tests；100 grams of goldleaf volatile-type liquia airs
Freshener is inserted into 6 fibre cores (distribution medium, long 30cm, diameter 3mm), and service life is about 6 months, and residual quantity is
10%, goldleaf does not settle, does not assemble in use process.
Embodiment 2
Unlike embodiment one:
Formula: deionized water 35%, ethyl alcohol 25%, dipropylene glycol methyl ether 35%, Cremophor RH40 2%, essence
1%, polyacrylate cross-linked polymer -6 1%, triethanolamine 0.89%, liquid outstanding person beauty (Plus) 0.1%, goldleaf particle
(0.2cm × 0.2cm × 0.12 μm) 0.01%.
The volatilization liquid of goldleaf made from the formula passes through 45 DEG C of 1 month baking oven tests；100 grams of goldleaf volatile-type liquia airs
Freshener is inserted into 6 fibre cores (distribution medium, long 30cm, diameter 3mm), and service life is about 4 months, residual quantity 7%,
Goldleaf does not settle, does not assemble in use process.
Embodiment 3
Unlike embodiment one:
Formula: deionized water 30%, ethyl alcohol 30%, dipropylene glycol methyl ether 20%, Cremophor RH40 10%, essence
5%, polyacrylate cross-linked polymer -6 2%, triethanolamine 1.9%, liquid outstanding person's beauty (Plus) 1%, goldleaf particle (0.2cm
× 0.2cm × 0.12 μm) 0.1%.
The volatilization liquid of goldleaf made from the formula passes through 45 DEG C of 1 month baking oven tests；100 grams of goldleaf volatile-type liquia airs
Freshener is inserted into 6 fibre cores (distribution medium, long 30cm, diameter 3mm), and service life is about 6 months, and residual quantity is
15%, goldleaf does not settle, does not assemble in use process.
Embodiment 4
Unlike embodiment one:
Formula: deionized water 50%, ethyl alcohol 10%, dipropylene glycol methyl ether 35%, Cremophor RH40 1%, essence
2%, polyacrylate cross-linked polymer -6 0.5%, triethanolamine 0.9%, liquid outstanding person beauty (Plus) 0.5%, goldleaf particle
(0.2cm × 0.2cm × 0.12 μm) 0.1%.
The volatilization liquid of goldleaf made from the formula passes through 45 DEG C of 1 month baking oven tests；100 grams of goldleaf volatile-type liquia airs
Freshener is inserted into 6 fibre cores (distribution medium, long 30cm, diameter 3mm), and service life is about 5 months, residual quantity 9%,
Goldleaf does not settle, does not assemble in use process.
Embodiment 5
Unlike embodiment one:
Formula: deionized water 50%, ethyl alcohol 20%, dipropylene glycol methyl ether 15%, Cremophor RH40 6%, essence
4%, polyacrylate cross-linked polymer -6 1.9%, triethanolamine 2%, liquid outstanding person's beauty (Plus) 1%, goldleaf particle (0.2cm
× 0.2cm × 0.12 μm) 0.1%.
The volatilization liquid of goldleaf made from the formula passes through 45 DEG C of 1 month baking oven tests；100 grams of goldleaf volatile-type liquia airs
Freshener is inserted into 6 fibre cores (distribution medium, long 30cm, diameter 3mm), and service life is about 6 months, and residual quantity is
15%, goldleaf does not settle, does not assemble in use process.
Embodiment 6
Formula: deionized water 50%, ethyl alcohol 20%, dipropylene glycol methyl ether 15%, Cremophor RH40 3%, tween
20 3%, essence 4%, polyacrylate cross-linked polymer -6 1.9%, triethanolamine 2%, liquid outstanding person beauty (Plus) 1%, gold
Foil particle (0.2cm × 0.2cm × 0.12 μm) 0.1%.
Preparation method:
(1) polyacrylate cross-linked polymer -6 is dissolved in part ion water, obtains polyacrylate cross-linked polymer -6
Aqueous solution.
(2) it takes remaining deionized water dilution triethanolamine to obtain triethanolamine solution, while stirring adds triethanolamine solution
Enter in -6 aqueous solution of the third polyacrylate cross-linked polymer, continuing stirring makes polyacrylate cross-linked polymer -6 and triethanolamine
It sufficiently neutralizes, system pH is 7.0-7.5, obtains clear viscous liquids.
(3) ethyl alcohol is added to the resulting clear viscous liquids of step (2) and the outstanding beauty of liquid is uniformly mixed, obtain mixed liquor.
(4) essence, Cremophor RH40, polysorbas20 and dipropylene glycol methyl ether is taken to be added to after mixing described mixed
It closes in liquid, stirs evenly.
(5) goldleaf particle is added, stirs evenly, defoams.
The volatilization liquid of goldleaf made from the formula passes through 45 DEG C of 1 month baking oven tests；100 grams of goldleaf volatile-type liquia airs
Freshener is inserted into 6 fibre cores (distribution medium, long 30cm, diameter 3mm), and service life is about 6 months, and residual quantity is
15%, goldleaf does not settle, does not assemble in use process.
Embodiment 7
Formula: deionized water 50%, ethyl alcohol 20%, dipropylene glycol methyl ether 15%, polysorbas20 6%, essence 4%, polypropylene
Acid esters cross-linked polymer -6 1.9%, triethanolamine 2%, liquid outstanding person beauty (Plus) 1%, goldleaf particle (0.2cm × 0.2cm ×
0.12 μm) 0.1%.
Preparation method:
(1) polyacrylate cross-linked polymer -6 is dissolved in part ion water, obtains polyacrylate cross-linked polymer -6
Aqueous solution.
(2) it takes remaining deionized water dilution triethanolamine to obtain triethanolamine solution, while stirring adds triethanolamine solution
Enter in -6 aqueous solution of the third polyacrylate cross-linked polymer, continuing stirring makes polyacrylate cross-linked polymer -6 and triethanolamine
It sufficiently neutralizes, system pH is 7.0-7.5, obtains clear viscous liquids.
(3) ethyl alcohol is added to the resulting clear viscous liquids of step (2) and the outstanding beauty of liquid is uniformly mixed, obtain mixed liquor.
(4) it takes essence, polysorbas20 and dipropylene glycol methyl ether to be added in the mixed liquor after mixing, stirs evenly.
(5) goldleaf particle is added, stirs evenly, defoams.
The volatilization liquid of goldleaf made from the formula passes through 45 DEG C of 1 month baking oven tests；100 grams of goldleaf volatile-type liquia airs
Freshener is inserted into 6 fibre cores (distribution medium, long 30cm, diameter 3mm), and service life is about 6 months, and residual quantity is
15%, goldleaf does not settle, does not assemble in use process.
Comparative example 1
Formula: deionized water 64%, ethyl alcohol 10%, dipropylene glycol methyl ether 10%, Cremophor RH40 5%, essence
10.5%, polyacrylate cross-linked polymer -6 0.05%, triethanolamine 0.05%, liquid outstanding person beauty (Plus) 0.25%, goldleaf
Particle (0.2cm × 0.2cm × 0.12 μm) 0.15%.
Preparation method:
(1) polyacrylate cross-linked polymer -6 is dissolved in part ion water, obtains polyacrylate cross-linked polymer -6
Aqueous solution
(2) it takes remaining deionized water dilution triethanolamine to obtain triethanolamine solution, while stirring adds triethanolamine solution
Enter in -6 aqueous solution of the third polyacrylate cross-linked polymer, continuing stirring makes polyacrylate cross-linked polymer -6 and triethanolamine
It sufficiently neutralizes, system pH is 7.0-7.5, obtains clear viscous liquids.
(3) ethyl alcohol is added to the resulting clear viscous liquids of step (2) and the outstanding beauty of liquid is uniformly mixed, obtain mixed liquor.
(4) essence, Cremophor RH40 and dipropylene glycol methyl ether is taken to be added in the mixed liquor after mixing,
It stirs evenly.
(5) goldleaf particle is added, stirs evenly, defoams.
Goldleaf made from the formula volatilizees, and liquid is muddy, and goldleaf settles.
Comparative example 2
Unlike comparative example one:
Formula: deionized water 20%, ethyl alcohol 20%, dipropylene glycol methyl ether 10%, Cremophor RH40 33.5% are fragrant
Essence 15%, polyacrylate cross-linked polymer -6 0.5%, triethanolamine 0.5%, liquid outstanding person beauty (Plus) 0.3%, goldleaf
Grain (0.2cm × 0.2cm × 0.12 μm) 0.2%.
The volatilization liquid of goldleaf made from the formula is muddy, floccule, goldleaf sedimentation occurs.
Comparative example 3
| Component | It is formulated A | It is formulated B |
| Polyacrylate cross-linked polymer -6 | 0.5% | — |
| C10-13 alkylol acrylamide acid esters cross-linked polymer | — | 0.5% |
| Triethanolamine | 0.5% | 0.5% |
| Water | 99% | 99% |
Using the test method in national standard GB/T 22235-2008 --- 53921 surfactant of DIN is glued with rotary
Degree meter measurement mobility, used instrument are U.S.'s Brookfield DVS+ Rotary Viscosimeter, final result: formula A
Viscosity is 4000Cps, and formula B viscosity is 23000Cps, it can be seen that, the viscosity for being formulated A is more much lower than formula B, i.e. polypropylene
The influence ratio C10-13 alkylol acrylamide acid esters cross-linked polymer of -6 pairs of system viscosities of acid esters cross-linked polymer is low, to volatile component
Volatile performance influence it is also relatively small.
Claims (8)
1. a kind of volatile-type liquid air freshener of suspension goldleaf particle, characterized in that the component including following mass fraction:
Deionized water 30%~50%
Ethyl alcohol 10%~30%
Dipropylene glycol methyl ether 15%~35%
Solubilizer 1%~10%
Essence 1%~10%
Acrylic acid crosslinked resin 0.1%~2%
Triethanolamine 0.1%~2%
Preservative 0.1%~1%
Goldleaf particle 0.01%~0.1%.
2. the volatile-type liquid air freshener of suspension goldleaf particle according to claim 1, characterized in that the propylene
Sour crosslinked resin selection is capable of forming the acrylic acid crosslinked resin of colloid systems of the viscosity lower than 10000Cps.
3. the volatile-type liquid air freshener of suspension goldleaf particle according to claim 1 or 2, characterized in that described
The selection of acrylic acid crosslinked resin has the acrylic acid crosslinked resin of antistatic effect.
4. the volatile-type liquid air freshener of suspension goldleaf particle according to claim 3, characterized in that described to have
The acrylic acid crosslinked resin of antistatic effect includes but is not limited to polyacrylate cross-linked polymer -6.
5. the volatile-type liquid air freshener of suspension goldleaf particle according to claim 1, characterized in that the anti-corrosion
Agent includes but is not limited to the outstanding beauty of liquid.
6. the volatile-type liquid air freshener of suspension goldleaf particle according to claim 1, characterized in that the solubilising
Agent includes but is not limited to the combination of one or both of Cremophor RH40 and polysorbas20.
7. the volatile-type liquid air freshener of suspension goldleaf particle according to claim 1, characterized in that the goldleaf
The size of particle is 0.2cm × 0.2cm × 0.12 μm.
8. a kind of preparation side of the volatile-type liquid air freshener of the described in any item suspension goldleaf particles of claim 1-7
Method, characterized in that the following steps are included:
(1) acrylic acid crosslinked resin is dissolved in part ion water, obtains acrylic acid crosslinked resin aqueous solution；
(2) remaining deionized water dilution triethanolamine is taken to obtain triethanolamine solution, then with acrylic acid crosslinked resin aqueous solution
Mixing, stirring to acrylic acid crosslinked resin and triethanolamine sufficiently neutralize and system pH is 7.0-7.5, obtain clear viscous liquid
Body；
(3) ethyl alcohol is added to the resulting clear viscous liquids of step (2) and preservative is uniformly mixed, obtain mixed liquor；
(4) it takes essence, solubilizer and dipropylene glycol methyl ether to be added in the mixed liquor after mixing, stirs evenly；
(5) goldleaf particle is added, stirs evenly, defoams.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811222167.7A CN109289070B (en) | 2018-10-19 | 2018-10-19 | Volatile liquid air freshener with suspended gold foil particles and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811222167.7A CN109289070B (en) | 2018-10-19 | 2018-10-19 | Volatile liquid air freshener with suspended gold foil particles and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN109289070A true CN109289070A (en) | 2019-02-01 |
| CN109289070B CN109289070B (en) | 2021-06-04 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1491191A (en) * | 2001-02-27 | 2004-04-21 | ����³�عɷ�����˾ | Method and device for manufacturing advanced water containing ultra-fine gold particles |
| CN1784210A (en) * | 2003-05-07 | 2006-06-07 | 弗门尼舍有限公司 | Sprayable perfume with an improved tenacity |
| GB2487298A (en) * | 2011-01-13 | 2012-07-18 | Anthony Clive Umfreville Fisher | A composition for controlling malodours comprising enzyme producing bacteria |
| CN105168018A (en) * | 2015-10-13 | 2015-12-23 | 吕亚楠 | Oxygen ion suspension nanometer gold foil stock solution and preparation method of oxygen ion suspension nanometer gold foil stock solution |
| CN108324983A (en) * | 2018-02-27 | 2018-07-27 | 洛娃日化(江苏)股份有限公司 | A kind of air freshener and preparation method thereof |
-
2018
- 2018-10-19 CN CN201811222167.7A patent/CN109289070B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1491191A (en) * | 2001-02-27 | 2004-04-21 | ����³�عɷ�����˾ | Method and device for manufacturing advanced water containing ultra-fine gold particles |
| CN1784210A (en) * | 2003-05-07 | 2006-06-07 | 弗门尼舍有限公司 | Sprayable perfume with an improved tenacity |
| GB2487298A (en) * | 2011-01-13 | 2012-07-18 | Anthony Clive Umfreville Fisher | A composition for controlling malodours comprising enzyme producing bacteria |
| CN105168018A (en) * | 2015-10-13 | 2015-12-23 | 吕亚楠 | Oxygen ion suspension nanometer gold foil stock solution and preparation method of oxygen ion suspension nanometer gold foil stock solution |
| CN108324983A (en) * | 2018-02-27 | 2018-07-27 | 洛娃日化(江苏)股份有限公司 | A kind of air freshener and preparation method thereof |
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|---|---|
| CN109289070B (en) | 2021-06-04 |
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Address after: No. 66, Hongjing Road, East District, Guangzhou Economic and Technological Development Zone, Guangzhou, Guangdong 510000 Patentee after: Chi Hua ton flavor and fragrance (Guangzhou) Co.,Ltd. Address before: No. 66, Hongjing Road, East District, Guangzhou Economic and Technological Development Zone, Guangzhou, Guangdong 510000 Patentee before: DROM FRAGRANCES (GUANGZHOU) Co.,Ltd. |