CN109281647A - A kind of acidization tool of carbonate reservoir horizontal well - Google Patents

A kind of acidization tool of carbonate reservoir horizontal well Download PDF

Info

Publication number
CN109281647A
CN109281647A CN201811433820.4A CN201811433820A CN109281647A CN 109281647 A CN109281647 A CN 109281647A CN 201811433820 A CN201811433820 A CN 201811433820A CN 109281647 A CN109281647 A CN 109281647A
Authority
CN
China
Prior art keywords
acid
acidization tool
horizontal well
tool according
acidization
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811433820.4A
Other languages
Chinese (zh)
Inventor
张路锋
周福建
张士诚
王晋
王月纯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China University of Petroleum Beijing
Original Assignee
China University of Petroleum Beijing
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China University of Petroleum Beijing filed Critical China University of Petroleum Beijing
Priority to CN201811433820.4A priority Critical patent/CN109281647A/en
Publication of CN109281647A publication Critical patent/CN109281647A/en
Pending legal-status Critical Current

Links

Classifications

    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B43/00Methods or apparatus for obtaining oil, gas, water, soluble or meltable materials or a slurry of minerals from wells
    • E21B43/25Methods for stimulating production
    • E21B43/26Methods for stimulating production by forming crevices or fractures

Abstract

The present invention provides a kind of acidization tools of carbonate reservoir horizontal well.The acidization tool includes: step 1: acid solution is injected into horizontal well, injection flow is 0.5m3/m‑3m3/m;Step 2: injection fibrous foam base VES acid, injection flow are 0.3m3/m‑1.5m3/m;According to the length of horizontal well, the horizontal well horizontal section length circulation primary step 1 of every 60m-100m completes the acidification to carbonate reservoir horizontal well to step 2.Acidization tool of the invention can significantly improve the acidizing effect of horizontal well, and to reservoir fanout free region.

Description

A kind of acidization tool of carbonate reservoir horizontal well
Technical field
The present invention relates to a kind of acidization tool more particularly to a kind of acidization tools of the horizontal well of Carbonate Reservoir, belong to Technical field of petroleum extraction.
Background technique
Carbonate acidizing, which refers to, reacts acidic fluid with carbonate reservoir, to release nearly pit shaft area pollution or change It is apt to the method for such reservoir permeability.During Carbonate acidizing, acid preferentially seeps that condition is preferable or natural fracture hole is sent out with hole The stratum contact educated, and the permeability in such region is further increased, these layers are then proceeded to, journey is employed in low porosity permeability region It spends lower, it is difficult to realize homogeneous acidification.To realize the homogeneous acidification to heterogeneity carbonate reservoir, it is necessary to keep acid low in It seeps with more haptoreactions in hole.
Mechanical coupling segment steering and chemistry diversion acidification transformation, but current technology can be used in carbonate reservoir homogeneous acidification It is primarily present following deficiency:
(1) packer steering construction is complicated, time-consuming, at high cost, and the not applicable longer horizontal well of horizontal segment;
(2) it blocks up ball to turn to due to Horizontal Well segment length, injection discharge capacity is low, and stifled ball sets difficulty;
(3) the temporary stall of foamed acid is to since foam temperature tolerance is poor and high permeability formation leak-off (filtering feature of drilling fluid) is tight Weight, thus application range is limited;
(4) diverting agent turns to mainly by forming the filter cake of hyposmosis in high permeability formation, but Carbonate acidizing can generate Earthworm hole, and the filter cake formed around diverting agent, turning efficiency are bad;
(5) VES turns to acid and is controlled thickening by pH value, but rheological characteristic is poor, therefore uniform acid distribution effect is limited.
Summary of the invention
In order to solve the above-mentioned technical problem, collect viscosity, foam, temporarily stifled shunting in one the purpose of the present invention is to provide a kind of The homogeneous acidification method of body can significantly improve the acidizing effect of horizontal well, and to reservoir fanout free region.
In order to achieve the above technical purposes, the present invention provides a kind of acidization tools of carbonate reservoir horizontal well, should Acidization tool the following steps are included:
Step 1: injecting acid solution into horizontal well, and injection flow is 0.5m3/m-3m3/m;
Step 2: injection fibrous foam base VES acid, injection flow are 0.3m3/m-1.5m3/m;
According to the length cycles above-mentioned steps one and step 2 of horizontal well, in the every 60m-100m circulation primary of horizontal section length Step 1 and step 2 are stated, the acidification to carbonate reservoir horizontal well is completed.
In acidization tool of the invention, it is initially injected conventional acid solution, high permeability formation is acidified;Reinject fibrous foam Base VES acid is temporarily blocked up and is shunted from viscosity building characteristic and fiber winding accumulation using the Jamin effect of foam, VES, carries out to high permeability formation High permeability formation (temporarily being blocked up to high permeability formation) is blocked while deep acidizing;Finally by the conventional acid solution of alternately injection and fibrous foam Base VES acid, realizes the transformation of horizontal well multistage homogeneous acidification.
In acidization tool of the invention, the injection rate in step 1 and step 2 is determined on the basis of reservoir thickness 's.For example, injection rate when injecting acid solution in step 1 is 0.5m3/m-3m3/ m refers to every meter of reservoir thickness injection acid solution 0.5m3-3m3
In acidization tool of the invention, it is preferable that the sum of the mass percent with each raw material of fibrous foam base VES acid is 100% meter, the raw material composition of the fibrous foam base VES acid of use are as follows: the acid of 5%-28%, the diversion agent of 6%-8%, 1%- 2% corrosion inhibiter, the ferrous stability of 1%-2%, the clay stabilizer of 1%-2%, the fiber of 0.5%-2% and surplus Water.
In acidization tool of the invention, specifically, carrier occurs by foam of nitrogen.
More specifically, the foam volume score of fibrous foam base VES acid can be 80%-95%.
Specific embodiment according to the present invention, the fibrous foam base VES acid are injected by foam maker, such as can be with Using foam maker as shown in Figure 1, gas is injected along the first pipeline 1, and the raw material of fibrous foam base VES acid is by the second pipeline 2 injections ultimately form fibrous foam base VES acid through foam maker.
In acidization tool of the invention, the acid in the raw material of fibrous foam base VES acid can link up storage with corrosion rock Layer.Specifically, the acid used is the combination of one or more of hydrochloric acid, hydrofluoric acid, formic acid, acetic acid, citric acid and glycolic.
In acidization tool of the invention, the diversion agent in the raw material of fibrous foam base VES acid plays temporarily stifled high permeability formation, The effect of even cloth acid.
Specifically, the diversion agent used is betaines amphoteric surfactant;Further, the diversion agent used can be with For the DCA-1 type VES diversion agent produced by Beijing KeMaiShi Oil Field Chemical regent Technology Co., Ltd.
In acidization tool of the invention, specifically, the corrosion inhibiter of use is compound by organic amine derivatives and alkynol Into what is obtained;Further, the corrosion inhibiter used (is had for DCA-6 type corrosion inhibiter by Beijing Ke Maishi Oilfield Chemicals technology Limit company production).
In acidization tool of the invention, the ferrous stability in the raw material of fibrous foam base VES acid can be with Complexing Iron Ion prevents iron gel precipitation from damaging to reservoir.
Specifically, the ferrous stability used is organic phosphate.Further, the ferrous stability used is can With the DCA-F sections ion stabilizer to be produced by Beijing KeMaiShi Oil Field Chemical regent Technology Co., Ltd.
In acidization tool of the invention, the clay stabilizer in the raw material of fibrous foam base VES acid can stablize clay Mineral prevent clay mineral water swelling, injury of the dispersion migration clay mineral to reservoir.
Specifically, the clay stabilizer used can be the pure potassium chloride of analysis.
In acidization tool of the invention, the fiber in the raw material of fibrous foam base VES acid plays bridge formation temporarily stifled high permeability formation, Diversion agent is cooperateed with to realize the effect of uniform acid distribution.
Specifically, the fiber used is fine for hydroxypropyl methyl cellulose, hydroxypropyl cellulose, hydroxyethyl cellulose or polyester Dimension.Further, the fiber used is degradable for the DCF-1 type produced by Beijing KeMaiShi Oil Field Chemical regent Technology Co., Ltd Polyester fiber.
In acidization tool of the invention, in step 1, the acid solution of injection can be the conventional acid solution of this field, to adopting Conventional acid solution does not have particular/special requirement.
Specifically, in step 1, the acid solution used is in hydrochloric acid, hydrofluoric acid, formic acid, acetic acid, citric acid and glycolic One or more of combinations.
Acidization tool of the invention is used in the case where being lower than formation fracture pressure, utmostly to improve reservoir.
Acidization tool of the invention is suitable for the acidification of carbonate reservoir horizontal well, is particularly suitable for long well section horizontal well Uniform acid distribution.
There is the acidization tool of carbonate reservoir horizontal well of the invention foam separation capacity, VES to divide from viscosity is viscosified The synergistic combination of the temporary stifled separation capacity three of stream ability and foam accumulation, shunted with individual foam, from viscosify viscosity shunt or Fiber accumulations are temporarily blocked up separate system and are compared, and integrate viscosity, foam, temporarily block up the acid fluid system shunted to Uniform Horizontal Well acidification Effect is more effective;It solves the problems, such as the acidification of long well section Uniform Horizontal Well, is provided for strong Heterogeneous reservoir acid stimulation Effective acidization tool.
The acidization tool of carbonate reservoir horizontal well of the invention integrates viscosity, foam, temporarily stifled shunting, has good Shunting effect well can effectively reduce construction cost, be easy to operate, and difficulty of construction is low, and to reservoir fanout free region.
Detailed description of the invention
Fig. 1 is the structure chart of foam maker of the invention.
Main Reference symbol description
1 first pipeline, 2 second pipeline
Specific embodiment
In order to which technical characteristic of the invention, purpose and beneficial effect are more clearly understood, now to skill of the invention Art scheme carries out described further below, but should not be understood as that limiting the scope of the invention.
Embodiment 1
Present embodiments provide a kind of acidization tool applied to Tarim Basin Donghe oilfield X well comprising following step It is rapid:
East River X well location is constructed in East River 1, well depth 5700m, reservoir thickness 40m, is acidified the long 480m of purpose well section, well logging Explain weighted average porosity 17.4%, oil saturation 73%.Naturally it goes into operation within the well on 2 20th, 2016, initial stage day oil-producing 45.16t, until on 2 2nd, 2017, day oil-producing 18t.The condition of production before being acidified: liquid level is low, and feed flow is insufficient, goes out liquid.The well water Flat section is longer, considers uniform acid distribution, intends being transformed with fibrous foam base VES acid acid fracturing.
Step 1: conventional acid acid 60m is injected into horizontal well3(injection flow is 1.5m3/m);
Step 2: continue to inject fibrous foam base VES acid 12m3(injection flow is 0.3m3/m);
Step 3: horizontal section length 480m, every 80m are repeated once, and recycle above-mentioned steps one and step 26 times, complete Paired parallel horizontal wells carries out the acidification transformation of multistage uniform acid distribution.
After X well acidizing pressing crack construction, liquid is produced daily by 22t and increases to 84t, wherein day oil-producing increases to 54t, acid stimulation by 18t Correctional effect is obvious.
Embodiment 2
Based on laboratory core flow device, rock core flowing experiment is carried out using Haffa Asia A well rock core, tests fibrous foam base The injury situation to reservoir of VES acid, experimental procedure are as follows:
1. connecting equipment, hunts leak, measure its permeability using normal saline solution.
2. under the charge velocity of the minimum critical flow velocity lower than rock core, by the residual of fibrous foam base VES acid after breaking gel 3 times of pore volumes of sour inverse injection rock core.
3. reusing normal saline solution, measurement determines residual acid protection reservoir performance by the permeability of rock core after residual acid pollution.
Experimental result: table 1 gives the reservoir core flowing experiment result of residual acid after breaking gel.
The evaluation result of 1 fibrous foam base VES acid breaking glue solution of table damage reservoir
By the experimental result in table 1 it can be seen that the residual acid solution of fibrous foam base VES acid after breaking gel is to the infiltrations of three blocks of rock cores Saturating rate recovery value is all very high, and up to 100%, minimum also to reach 98.43%, mean permeability recovery value reaches 99.21%, The permeability damage rate of rock core is averagely only 0.79%, illustrates that the permeability of rock core is not damaged substantially.Fibrous foam base VES acid Breaking glue solution damages core permeability very little, and protection reservoir effect is good.

Claims (10)

1. a kind of acidization tool of carbonate reservoir horizontal well, which is characterized in that the acidization tool the following steps are included:
Step 1: injecting acid solution into horizontal well, and injection flow is 0.5m3/m-3m3/m;
Step 2: injection fibrous foam base VES acid, injection flow are 0.3m3/m-1.5m3/m;
According to the length of horizontal well, the every 60m-100m circulation primary step 1 of horizontal section length and step 2 are completed to carbonate The acidification of rock reservoir-level well.
2. acidization tool according to claim 1, which is characterized in that with the matter of each raw material of the fibrous foam base VES acid The sum of percentage is measured as 100% meter, the raw material of the fibrous foam base VES acid forms are as follows: the acid of 5%-28%, 6%-8%'s Diversion agent, the corrosion inhibiter of 1%-2%, the ferrous stability of 1%-2%, the clay stabilizer of 1%-2%, 0.5%-2%'s The water of fiber and surplus.
3. acidization tool according to claim 1 or 2, which is characterized in that carrier occurs by foam of nitrogen;Preferably, The foam volume score of the fibrous foam base VES acid is 80%-95%.
4. acidization tool according to claim 2, which is characterized in that the corrosion inhibiter is by organic amine derivatives and alkynes What alcohol was combined;Preferably, the corrosion inhibiter is DCA-6 type corrosion inhibiter.
5. acidization tool according to claim 2, which is characterized in that the ferrous stability is organic phosphate;It is excellent Selection of land, the ferrous stability are DCA-F sections ion stabilizer.
6. acidization tool according to claim 2, which is characterized in that the diversion agent is beet alkali ampholytic surface active Agent;Preferably, the diversion agent is DCA-1 type VES diversion agent.
7. acidization tool according to claim 2, which is characterized in that the clay stabilizer is to analyze pure potassium chloride.
8. acidization tool according to claim 2, which is characterized in that the fiber is hydroxypropyl methyl cellulose, hydroxypropyl Base cellulose, hydroxyethyl cellulose or polyester fiber;Preferably, the fiber is DCF-1 type biodegradable polyester fiber.
9. acidization tool according to claim 2, which is characterized in that the acid is hydrochloric acid, hydrofluoric acid, formic acid, acetic acid, lemon The combination of one or more of lemon acid and glycolic.
10. acidization tool according to claim 1, which is characterized in that in step 1, the acid solution is hydrochloric acid, hydrogen fluorine The combination of one or more of acid, formic acid, acetic acid, citric acid and glycolic.
CN201811433820.4A 2018-11-28 2018-11-28 A kind of acidization tool of carbonate reservoir horizontal well Pending CN109281647A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811433820.4A CN109281647A (en) 2018-11-28 2018-11-28 A kind of acidization tool of carbonate reservoir horizontal well

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811433820.4A CN109281647A (en) 2018-11-28 2018-11-28 A kind of acidization tool of carbonate reservoir horizontal well

Publications (1)

Publication Number Publication Date
CN109281647A true CN109281647A (en) 2019-01-29

Family

ID=65173932

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201811433820.4A Pending CN109281647A (en) 2018-11-28 2018-11-28 A kind of acidization tool of carbonate reservoir horizontal well

Country Status (1)

Country Link
CN (1) CN109281647A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090272534A1 (en) * 2007-03-21 2009-11-05 Baker Hughes Incorporated Methods of using viscoeleastic surfactant gelled fluids to pre-saturate underground formations
CN102443386A (en) * 2011-12-13 2012-05-09 中国石油集团川庆钻探工程有限公司井下作业公司 Energy enhancing steering acid liquid system
US20120305246A1 (en) * 2009-10-28 2012-12-06 Yiyan Chen Shear-activated viscoelastic surfactant fluid and method
CN105041289A (en) * 2015-07-13 2015-11-11 中国石油大学(北京) Method for forming multiple fractures by forced planar diverting of fracture opening being temporarily plugged
CN105041288A (en) * 2015-07-13 2015-11-11 中国石油大学(北京) Fractural diverting acid-fracturing method for carbonate oil-gas reservoirs
CN105089603A (en) * 2015-07-13 2015-11-25 中国石油大学(北京) Reservoir modifying method through forming crack network by temporary plugging turning in cracks

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090272534A1 (en) * 2007-03-21 2009-11-05 Baker Hughes Incorporated Methods of using viscoeleastic surfactant gelled fluids to pre-saturate underground formations
US20120305246A1 (en) * 2009-10-28 2012-12-06 Yiyan Chen Shear-activated viscoelastic surfactant fluid and method
CN102443386A (en) * 2011-12-13 2012-05-09 中国石油集团川庆钻探工程有限公司井下作业公司 Energy enhancing steering acid liquid system
CN105041289A (en) * 2015-07-13 2015-11-11 中国石油大学(北京) Method for forming multiple fractures by forced planar diverting of fracture opening being temporarily plugged
CN105041288A (en) * 2015-07-13 2015-11-11 中国石油大学(北京) Fractural diverting acid-fracturing method for carbonate oil-gas reservoirs
CN105089603A (en) * 2015-07-13 2015-11-25 中国石油大学(北京) Reservoir modifying method through forming crack network by temporary plugging turning in cracks

Similar Documents

Publication Publication Date Title
CN106050213B (en) A kind of sandstone reservoir low damage distributary acid method
CN106194145B (en) Multistage temporary plugging deep network acid fracturing method
CN101353958B (en) Acid fracturing process of oil gas well mining temperature control various mucic acid
CN105505360B (en) A kind of fluoboric acid de-plugging agent and acidification method for removing blockage
CN104109528B (en) Acidifying liquid capable of sand stabilization and plug removal, and preparation method thereof
CN105089600B (en) The method that temporarily stifled diverting material auxiliary water horizontal well carries out drawing type water-jet transformation
CN109267985B (en) Control method for using amount of temporary plugging agent for temporary plugging steering fracturing
CN110273671B (en) Micro-acid-pressure composite injection increasing method for high-pore high-permeability reservoir on sea
CN110591685B (en) In-situ self-generated microfoam steering acidizing fluid, acidizing steering method and application
CN106337676A (en) Method of fracturing coal-bed gas reservoir
CN115288647B (en) Composite capacity expansion method for improving recovery ratio of oil well
CN106958437B (en) A kind of wellfracturing raising recovery ratio new method
CN108457633B (en) Intralayer selective fracturing method
CN106014401B (en) A kind of experimental method of simulation oil well fracturing fracture extension and fracturing fluid leak process
CN113027418A (en) Oil field water injection well pollution blockage removal experiment testing device and testing effect evaluation method
CN109281647A (en) A kind of acidization tool of carbonate reservoir horizontal well
CN110791279A (en) High-viscosity strong-corrosion acid liquor system for low-permeability sandstone oil reservoir
CN107882544A (en) A kind of mixing heat release method for removing blockage for carbonate cementation molding sand rock heavy oil wells
CN113356826B (en) Moderate sand adding and pressure increasing acid fracturing method for improving fracture-cavity reservoir transformation effect
CN110511735B (en) High-viscosity strong-corrosion acid liquor system for tight oil reservoir
CN114607313A (en) Solid-phase-free gel plugging method
CN104449622B (en) High temperature resistance high pressure organic composite type Oil layer protective solution and preparation method thereof
CN106223912A (en) The augmented injection method of LOW PERMEABILITY RESERVOIR water injection well
CN112709561A (en) Low-pressure compact marlite reservoir transformation method
CN112443306A (en) Pressure-control fracturing method for increasing fracture complexity of deep shale gas well

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20190129

RJ01 Rejection of invention patent application after publication