CN109266190A - A kind of organic fluorescent pigment color protection film and its application method - Google Patents
A kind of organic fluorescent pigment color protection film and its application method Download PDFInfo
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- CN109266190A CN109266190A CN201810982504.6A CN201810982504A CN109266190A CN 109266190 A CN109266190 A CN 109266190A CN 201810982504 A CN201810982504 A CN 201810982504A CN 109266190 A CN109266190 A CN 109266190A
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- Prior art keywords
- fluorescent pigment
- protection film
- organic fluorescent
- pigment color
- color protection
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D123/00—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers
- C09D123/02—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
- C09D123/04—Homopolymers or copolymers of ethene
- C09D123/08—Copolymers of ethene
- C09D123/0846—Copolymers of ethene with unsaturated hydrocarbons containing other atoms than carbon or hydrogen atoms
- C09D123/0853—Vinylacetate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09D133/10—Homopolymers or copolymers of methacrylic acid esters
- C09D133/12—Homopolymers or copolymers of methyl methacrylate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/22—Luminous paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/32—Radiation-absorbing paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
Abstract
The invention discloses a kind of organic fluorescent pigment color protection film and its application methods, by following components and quality percentage composition: optical clear resin 87 ~ 99.7%, light stabilizer 0.1 ~ 2%, antioxidant 0.1 ~ 1%, light absorber 0.1 ~ 10%.Organic fluorescent pigment color protection film of the invention contains light absorber, can effectively absorb the ultraviolet and blue light for generating the specific wavelength of discoloration to fluorescent pigment color, protect the color of fluorescent pigment.Organic fluorescent pigment color protection film composition of the invention is easy to use; after only need to mixing by protection film composition, stir, be uniformly dissolved, colour band surface made of the organic fluorescent pigment coated on required protection can form protective film after vacuum drying solidification; process is simple, at low cost.
Description
Technical field
The invention belongs to organic fluorescent pigment technical fields, and in particular to organic fluorescent pigment color protection film and its use
Method.
Background technique
Organic fluorescence toner yellow, toner is red, and the orange pigment of toner has stronger absorption at 280 and 450nm, because
And they are commonly used in the blue-light absorbers of anti-blue light technical field.When as pigment applications for the fields such as clothes and footwear material
When, cause them to have an opportunity to absorb the purple in sunlight since wearing process is inevitably exposed to for a long time in sun luminous environment
Outer and blue light and gradually lose original color.In general, when making these clothes and footwear material fluorescence color colour band, in formula
Addition antiager and blue-light absorbers are mixed together in fluorescent pigment to prevent pigment from fading.But since addition cannot excessive (mistake
Then easily there is bloom phenomenon in amount), the part being really coated on around pigment after being dispersed is seldom, thus prevents the effect faded non-
It is often limited.
Summary of the invention
The technical problem to be solved by the present invention is to a kind of protective film for preventing organic fluorescent pigment color from changing colour and its make
Use method.
Organic fluorescent pigment color protection film composition of the present invention is by following components and quality percentage composition: optics
Transparent resin 87 ~ 99.7%, light stabilizer 0.1 ~ 2%, antioxidant 0.1 ~ 1% and light absorber 0.1 ~ 10%.
Preferred organic fluorescent pigment color protection film composition is by following components and quality percentage composition: optical lens ming tree
Rouge 88.7 ~ 93.6%, light stabilizer 1 ~ 1.5%, antioxidant 0.4 ~ 0.8% and light absorber 5 ~ 9%.
Optimal organic fluorescent pigment color protection film composition is by following components and quality percentage composition: optical lens ming tree
Rouge 90.2%, light stabilizer 1.2%, antioxidant 0.6% and light absorber 8%.
The optical clear resin is thermoplastic polyurethane (TPU), polymethyl methacrylate (PMMA), ethylene-vinegar
Sour ethylene copolymer (EVA) or colorless and transparent organic siliconresin.
The light stabilizer is bis- (2,2,6,6- tetramethyl -4- piperidyl) sebacates, poly-succinic (4- hydroxyl -
2,2,6,6- tetramethyl -1- piperidine ethanols) ester or 4- benzoyloxy -2,2,6,6- tetramethyl piperidines.
The antioxidant is 4,4'- thiobis (6- tert-butyl-m-cresol), four [β-(3,5- di-t-butyl -4- hydroxy benzenes
Base) propionic acid] pentaerythritol ester, dilauryl thiodipropionate or thio-2 acid 2 stearyl ester.
The light absorber is selected from absorbing wavelength range in 250 ~ 500nm, and maximum absorption wavelength range is in 400 ~ 500nm
Absorbent.The light absorber is commercially available outstanding the LQ01, outstanding the BL1227 or steady moral TM46 in Europe that is full of of being full of.
The application method of organic fluorescent pigment color discoloration protective film of the present invention, including the following steps: will be above-mentioned
Organic fluorescent pigment color protection film composition after mixing, is dissolved, composition with solvent benzol, toluene, dimethylbenzene or chloroform
Mass ratio with solvent is 1:3 ~ 5:4, after stirring and dissolving is uniform, is coated on organic fluorescent pigment colour band, vacuum drying solidification,
After solidification, organic fluorescent pigment color protection film can be obtained.
Advantages of the present invention: 1. organic fluorescent pigment color protection film composition of the invention contains light absorber, can have
The absorption of effect generates the ultraviolet and blue light of the specific wavelength of discoloration to organic fluorescent pigment color, protects it in solarization
Under it is non-discolouring.2. organic fluorescent pigment color protection film composition of the invention is easy to use, protection film composition need to only be mixed
It after closing, stir, being uniformly dissolved, is coated on organic fluorescence color belt, vacuum drying solidification, process is simple, at low cost.
Specific embodiment
Below in conjunction with specific embodiment, present invention is further described in detail.
Embodiment 1
The component and quality of the present embodiment fluorescent pigment color protection film composition are as follows: BASF TPU S85A 9.4g, bis- (2,
2,6,6- tetramethyl -4- piperidyls) sebacate 0.05g, 4,4'- thiobis (6- tert-butyl-m-cresol) 0.15g, it is commercially available
Outstanding the LQ01 0.4g that is full of.
Embodiment 2
The component and quality of the present embodiment fluorescent pigment color protection film composition are as follows: BASF TPU 1185A 10U 9.0g,
Bis- (2,2,6,6- tetramethyl -4- piperidyl) sebacate 0.05g, 4,4'- thiobis (6- tert-butyl-m-cresol) 0.15g,
Commercially available outstanding the LQ01 0.8g that is full of.
Embodiment 3
The component and quality of the present embodiment fluorescent pigment color protection film composition are as follows: 12577 transparent silicone resin of DOW CORNING
9.2g, poly-succinic (4- hydroxyl -2,2,6,6- tetramethyl -1- piperidine ethanols) ester 0.05g, four [β-(3,5- bis- tertiary fourths
Base -4- hydroxy phenyl) propionic acid] pentaerythritol ester 0.15g, the steady moral TM46 0.8g in Europe.
Embodiment 4
The component and quality of the present embodiment fluorescent pigment color protection film composition are as follows: the beautiful sun IRD-70 PMMA 9.1g of Mitsubishi,
4- benzoyloxy -2,2,6,6- tetramethyl piperidine 0.05g, dilauryl thiodipropionate 0.15g are commercially available outstanding
It is full of BL1227 0.8g.
Embodiment 5
The component and quality of the present embodiment fluorescent pigment color protection film composition are as follows: Bayer TPU 3690AU 9.1g, polybutadiene
Acid (4- hydroxyl -2,2,6,6- tetramethyl -1- piperidine ethanols) ester 0.05g, thio-2 acid 2 stearyl ester 0.15g, city
Outstanding the LQ01 0.8g that is full of sold.
Embodiment 6
The component and quality of the present embodiment fluorescent pigment color protection film composition are as follows: Mitsui Chemicals 40LX EVA 9.1g, poly- fourth
Diacid (4- hydroxyl -2,2,6,6- tetramethyl -1- piperidine ethanols) ester 0.05g, thio-2 acid 2 stearyl ester 0.15g,
The steady moral TM46 0.7g in Europe.
The protection film composition of the various embodiments described above is mixed, with solvent benzol, toluene, dimethylbenzene or chloroform etc. are stirred molten
After solving substantially uniformity, it is respectively coated on red organic fluorescence, yellow and rose-pink color bands with bar spreader, vacuum drying 12 is small
Shi Jinhang solidification, the protection film thickness after solidification is about 50 μm.After color inhibition is tested, tested by national standard GB/T 250-2008
Its color fastness.Measuring color fastness is respectively 3,5,5,5,5,4.
Protection film composition of the invention compared with prior art, uses organic fluorescent pigment colour band made of this technology
Color fastness greatly improves, and keeps iridescent band colour-fast in solarization condition.
The present invention is not limited to the above embodiments, and the present invention can also without departing from the spirit and scope of the present invention
There are various changes and modifications, these changes and improvements all fall within the protetion scope of the claimed invention.
Claims (9)
1. a kind of organic fluorescent pigment color protection film composition, it is characterised in that by following components and quality percentage composition: light
Learn transparent resin 87 ~ 99.7%, light stabilizer 0.1 ~ 2%, antioxidant 0.1 ~ 1% and light absorber 0.1 ~ 10%.
2. organic fluorescent pigment color protection film composition according to claim 1, it is characterised in that by following components and
Quality percentage composition: optical clear resin 88.7 ~ 93.6%, light stabilizer 1 ~ 1.5%, antioxidant 0.4 ~ 0.8% and light absorber 5 ~
9%。
3. organic fluorescent pigment color protection film composition according to claim 1 or 2, it is characterised in that by following components
And quality percentage composition: optical clear resin 90.2%, light stabilizer 1.2%, antioxidant 0.6% and light absorber 8%.
4. organic fluorescent pigment color protection film composition according to claim 1, it is characterised in that the light is transparent
Resin is thermoplastic polyurethane, polymethyl methacrylate, ethylene-vinyl acetate copolymer or colorless and transparent organosilicon tree
Rouge.
5. organic fluorescent pigment color protection film composition according to claim 1, it is characterised in that the light is stablized
Agent is bis- (2,2,6,6- tetramethyl -4- piperidyl) sebacates, poly-succinic (4- hydroxyl -2,2,6,6- tetramethyl -1-
Piperidine ethanol) ester or 4- benzoyloxy -2,2,6,6- tetramethyl piperidines.
6. organic fluorescent pigment color protection film composition according to claim 1, it is characterised in that the antioxidant
For 4,4'- thiobis (6- tert-butyl-m-cresol), four [β-(3,5- di-tert-butyl-hydroxy phenyl) propionic acid] pentaerythritol esters,
Dilauryl thiodipropionate or thio-2 acid 2 stearyl ester.
7. organic fluorescent pigment color protection film composition according to claim 1, it is characterised in that the light absorption
Agent is selected from absorbing wavelength range in 250 ~ 500nm, absorbent of the maximum absorption wavelength range in 400 ~ 500nm.
8. organic fluorescent pigment color protection film composition according to claim 1 or claim 7, it is characterised in that the blue light
Absorbent is commercially available outstanding the LQ01, outstanding the BL1227 or steady moral TM46 in Europe that is full of of being full of.
9. the application method of organic fluorescent pigment color protection film described in claim 1, including the following steps: will be above-mentioned organic
Fluorescent pigment color protection film composition after mixing, with solvent benzol, toluene, dimethylbenzene or chloroform dissolution, composition with it is molten
The mass ratio of agent is 1:3 ~ 5:4, after stirring and dissolving is uniform, is coated on organic fluorescent pigment colour band, vacuum drying solidification, solidification
Afterwards, organic fluorescent pigment color protection film can be obtained.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810982504.6A CN109266190B (en) | 2018-08-27 | 2018-08-27 | Organic fluorescent pigment color protection film and use method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810982504.6A CN109266190B (en) | 2018-08-27 | 2018-08-27 | Organic fluorescent pigment color protection film and use method thereof |
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| CN109266190A true CN109266190A (en) | 2019-01-25 |
| CN109266190B CN109266190B (en) | 2020-11-10 |
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| CN103756286A (en) * | 2014-01-16 | 2014-04-30 | 珠海汉胜科技股份有限公司 | Thermoplastic polyurethane cable sheath material and preparation method |
| CN102775939B (en) * | 2012-08-21 | 2015-02-18 | 东方电气集团东方汽轮机有限公司 | Solar battery encapsulation adhesive film |
| KR20160095647A (en) * | 2016-07-11 | 2016-08-11 | 현대모비스 주식회사 | Uv-curable composition for hard-coat paining |
| CN106543915A (en) * | 2016-11-26 | 2017-03-29 | 马益元 | The mobile phone screen surface protection film that a kind of low temperature environment is suitable for |
| CN106590484A (en) * | 2016-11-24 | 2017-04-26 | 南京汇鑫光电材料有限公司 | Acrylate OCA optical adhesive film, and preparation method and application thereof |
| WO2018055010A1 (en) * | 2016-09-20 | 2018-03-29 | Essilor International | Polycarbonate resin compositions with consistent color and stable blue-cut performance |
-
2018
- 2018-08-27 CN CN201810982504.6A patent/CN109266190B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102775939B (en) * | 2012-08-21 | 2015-02-18 | 东方电气集团东方汽轮机有限公司 | Solar battery encapsulation adhesive film |
| CN103448312A (en) * | 2013-09-10 | 2013-12-18 | 温志光 | Screen protection film capable of filtering blue light and preparation method of screen protection film |
| CN103756286A (en) * | 2014-01-16 | 2014-04-30 | 珠海汉胜科技股份有限公司 | Thermoplastic polyurethane cable sheath material and preparation method |
| KR20160095647A (en) * | 2016-07-11 | 2016-08-11 | 현대모비스 주식회사 | Uv-curable composition for hard-coat paining |
| WO2018055010A1 (en) * | 2016-09-20 | 2018-03-29 | Essilor International | Polycarbonate resin compositions with consistent color and stable blue-cut performance |
| CN106590484A (en) * | 2016-11-24 | 2017-04-26 | 南京汇鑫光电材料有限公司 | Acrylate OCA optical adhesive film, and preparation method and application thereof |
| CN106543915A (en) * | 2016-11-26 | 2017-03-29 | 马益元 | The mobile phone screen surface protection film that a kind of low temperature environment is suitable for |
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| CN109266190B (en) | 2020-11-10 |
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Address after: 510000 No. 363, Changxin Road, Guangzhou, Guangdong, Tianhe District Patentee after: Institute of rare metals, Guangdong Academy of Sciences Address before: 510000 No. 363, Changxin Road, Guangzhou, Guangdong, Tianhe District Patentee before: GUANGDONG INSTITUTE OF RARE METALS |
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Effective date of registration: 20230403 Address after: 510651 No. 363, Changxin Road, Guangzhou, Guangdong, Tianhe District Patentee after: Institute of resource utilization and rare earth development, Guangdong Academy of Sciences Address before: 510000 363 Changxin Road, Tianhe District, Guangzhou, Guangdong. Patentee before: Institute of rare metals, Guangdong Academy of Sciences |
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