CN109264072A - The subpackage apparatus and method of gallium liquid - Google Patents
The subpackage apparatus and method of gallium liquid Download PDFInfo
- Publication number
- CN109264072A CN109264072A CN201810867398.7A CN201810867398A CN109264072A CN 109264072 A CN109264072 A CN 109264072A CN 201810867398 A CN201810867398 A CN 201810867398A CN 109264072 A CN109264072 A CN 109264072A
- Authority
- CN
- China
- Prior art keywords
- glove box
- gallium liquid
- pump
- packaging bottle
- transitional storehouse
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B31/00—Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
- B65B31/02—Filling, closing, or filling and closing, containers or wrappers in chambers maintained under vacuum or superatmospheric pressure or containing a special atmosphere, e.g. of inert gas
- B65B31/025—Filling, closing, or filling and closing, containers or wrappers in chambers maintained under vacuum or superatmospheric pressure or containing a special atmosphere, e.g. of inert gas specially adapted for rigid or semi-rigid containers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B3/00—Packaging plastic material, semiliquids, liquids or mixed solids and liquids, in individual containers or receptacles, e.g. bags, sacks, boxes, cartons, cans, or jars
- B65B3/04—Methods of, or means for, filling the material into the containers or receptacles
- B65B3/10—Methods of, or means for, filling the material into the containers or receptacles by application of pressure to material
- B65B3/12—Methods of, or means for, filling the material into the containers or receptacles by application of pressure to material mechanically, e.g. by pistons or pumps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B3/00—Packaging plastic material, semiliquids, liquids or mixed solids and liquids, in individual containers or receptacles, e.g. bags, sacks, boxes, cartons, cans, or jars
- B65B3/26—Methods or devices for controlling the quantity of the material fed or filled
- B65B3/28—Methods or devices for controlling the quantity of the material fed or filled by weighing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B63/00—Auxiliary devices, not otherwise provided for, for operating on articles or materials to be packaged
- B65B63/08—Auxiliary devices, not otherwise provided for, for operating on articles or materials to be packaged for heating or cooling articles or materials to facilitate packaging
Abstract
The present invention relates to a kind of subpackage apparatuses of gallium liquid, the device includes a glove box, the transitional storehouse being bordered by with glove box, the device further includes the electronic scale being built in glove box, several Packaging Bottles, one lifting device, the device further includes the device processed outside glove box, one metering pump, the device processed, metering pump is connected by pump line, and pump line extends to right above the Packaging Bottle in glove box, the Packaging Bottle is placed on electronic scale, and lifting device is fixed on the surface of Packaging Bottle, the transitional storehouse is built-in with a carriage, the glove box and transitional storehouse pass through tracheae and gas cylinder, vacuum pump connection.The subpackage apparatus and method of this gallium liquid in the closed environment provided by glove box, under the atmosphere of protective gas, dispense high purity gallium liquid, while keeping gallium liquid purity, its oxygen content can be made to be less than 3ppm, so that the economic value of gallium liquid is maintained.
Description
Technical field
The present invention relates to material post-processing field more particularly to a kind of subpackage apparatuses and method of gallium liquid.
Background technique
Ultra-pure gallium (purity is 7N or more) is a kind of important semiconductor basis material, with its series compound arsenic
Change gallium, gallium phosphide, gallium aluminum arsenide etc. to be widely applied in the fields such as high speed integrated circuit, LED, light-sensitive element, the city of ultra-pure gallium
Field demand increases sharply.Currently, ultra-pure gallium mainly passes through electrorefining, zone refining, crystal-pulling, fractional crystallization and true
Several combinations in material purifications refining techniques such as sky distillation are directly made.The oxygen content of ultra-pure gallium after purification
It is a key factor in its performance indicator, however, being easy in the last handling process of high purity gallium, such as during packing
It is mixed into oxygen, lead to the too high oxygen level in high purity gallium and seriously affects the performance of end product.
Therefore, it is necessary to design the subpackage apparatus and method of a kind of gallium liquid for being able to maintain extremely low oxygen content.
Summary of the invention
The purpose of the present invention is to provide the subpackage apparatuses and method of a kind of gallium liquid for being able to maintain extremely low oxygen content.
To realize foregoing purpose, the present invention adopts the following technical scheme: a kind of subpackage apparatus of gallium liquid, which includes one
Glove box, the transitional storehouse being bordered by with glove box, which further includes the electronic scale being built in glove box, several packagings
Bottle, a lifting device, the device further include a device processed, a metering pump outside the glove box, and the device processed, metering pump are logical
Pump line connection is crossed, and pump line extends to right above the Packaging Bottle in glove box, the Packaging Bottle is placed on electronic scale, and goes up and down dress
The surface for being fixed on Packaging Bottle is set, the transitional storehouse is built-in with a carriage, and the glove box and transitional storehouse pass through gas
Pipe is connect with gas cylinder, vacuum pump.
As a further improvement of the present invention, the device processed, metering pump, the pump line between glove box are both provided with valve
Door.
As a further improvement of the present invention, the transitional storehouse is provided with a transition door, when opening transition door, hand
Casing is connected to transitional storehouse；When closing transition door, glove box and transitional storehouse, which mutually completely cut off, to be opened.
As a further improvement of the present invention, the glove box is built-in with heat source.
As a further improvement of the present invention, the heat source uses infrared heat source.
The present invention proposes a kind of method for filling of gallium liquid simultaneously, using the subpackage apparatus of above-mentioned gallium liquid comprising as follows
Step:
S1,7N high purity gallium liquid pump is entered to device processed, the set temperature of device processed is 35 DEG C -55 DEG C, starts the stirring of constant temperature constant speed；
S2, glove box and transitional storehouse are vacuumized by vacuum pump first, and protection gas is then passed through into glove box and transitional storehouse
Body, opens the heat source of glove box, and 50-80 DEG C of constant temperature, until the oxygen content in glove box and transitional storehouse is lower than 0.1 ppm；
S3, transition door is opened, Packaging Bottle is transferred in glove box by carriage；Insert pump tube into packagings for lifting device
In bottle, metering switch pump is opened, is pumped into quantitative gallium liquid in Packaging Bottle from device processed according to setting program average rate；
S4, after having dispensed, pump line is detached Packaging Bottle by lifting device, and electronic balance is by weight data synchronous transfer to computer table
In lattice, then pass through one section of intermittent time；
S5, the Packaging Bottle for having dispensed gallium liquid is placed on carriage within the intermittent time, transports transitional storehouse back；
S6, repetition S3-S5 carry out packing operation, until packing finishes.
As a further improvement of the present invention, the setting program in S3 specifically: metering pump in 10-30s by 2500g gallium
In liquid pump to Packaging Bottle.
As a further improvement of the present invention, in S1, the range of speeds of stirring is 20-35 rpm.
As a further improvement of the present invention, in S4, intermittent time 60S-120S.
As a further improvement of the present invention, protective gas is 5N or the above high purity inert gas.
The subpackage apparatus and method of this gallium liquid, in the closed environment provided by glove box, under the atmosphere of protective gas,
High purity gallium liquid is dispensed, while keeping gallium liquid purity, its oxygen content can be made to be less than 3ppm, so that the economic valence of gallium liquid
Value is maintained.
Detailed description of the invention
Fig. 1 is the overall structure diagram of the embodiment of the subpackage apparatus of gallium liquid of the present invention.
Specific embodiment
Technical solution is clearly and completely described below in conjunction with the embodiment of the present invention, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Referring to Fig. 1, the present invention proposes a kind of subpackage apparatus 100 of gallium liquid, the device 100 include a glove box 110, with
The transitional storehouse 120 that glove box 110 is bordered by, which further includes the electronic scale 130 being built in glove box 110, several
Packaging Bottle 140, a lifting device 150, the device 100 further include a device 160 processed, a metering pump outside the glove box 110
170, device 160 processed, metering pump 170 are connected by pump line 180, and pump line 180 extends to the Packaging Bottle 140 in glove box 110
Surface, Packaging Bottle 140 is placed on electronic scale 130, and lifting device 150 is fixed on the surface of Packaging Bottle 140, transitional storehouse
120 are built-in with a carriage 121, and glove box 110 and transitional storehouse 120 are connected by tracheae 192 and gas cylinder 190, vacuum pump 191
It connects.
Glove box 110 provides confined space for the packing of gallium liquid；Glove box 110 is built-in with heat source, it is preferable that heat source uses
Infrared heat source can provide required isoperibol for the packing of gallium liquid.
Transitional storehouse 120 is bordered by with glove box 110, and transitional storehouse 120 is in Packaging Bottle 140 and the gallium liquid dispensed
Turn, transitional storehouse 120 is prepared using metal material that is nonmetallic or not polluting gallium material.It is sliding that transitional storehouse 120 is built-in with one
Dynamic device 121, carriage 121 are used to for empty package bottle 140 being transferred in glove box 110 and gallium liquid are housed by what packing finished
Packaging Bottle 140 be transferred to transitional storehouse 120, carriage 121 uses metal material system that is nonmetallic or not polluting gallium material
It is standby to form.
Electronic scale 130 is for weighing and sending data to computer record.
Packaging Bottle 140 is prepared for containing gallium liquid, Packaging Bottle 140 using high-purity nonmetallic materials, it is preferable that packaging
Bottle 140 is prepared using PE material.
Lifting device 150 is finished for the pump line 180 of metering pump 170 to be inserted into Packaging Bottle 140 before packing in packing
Pump line 180 is detached into Packaging Bottle 140 afterwards.
Device 160 processed is used to hold and high purity gallium liquid processed, and device 160 processed is prepared using high-purity nonmetallic materials,
Gallium will not be polluted；Device 160 processed has heated constant temperature function, it is ensured that gallium liquid temperature is between 30 ~ 60 DEG C；Device 160 processed is also
Has agitating function, it is ensured that gallium liquid ingredient is uniform.
Metering pump 170 can at regular time and quantity enter gallium liquid pump in Packaging Bottle 140.
Device 160 processed, metering pump 170, the pump line 180 between glove box 110 are both provided with valve 181.
Gas cylinder 190 be built-in with 5N or more than protective gas-high purity inert gas, the protective gas in gas cylinder 190 passes through
Tracheae 192 is passed through glove box 110 and transitional storehouse 120.
Vacuum pump 191 is for vacuumizing, using oilless vacuum pump, it is ensured that does not have oil vapour pollution.
The present invention proposes a kind of method for filling of gallium liquid simultaneously, using the subpackage apparatus of above-mentioned gallium liquid comprising as follows
Step:
S1,7N high purity gallium liquid pump is entered to device processed, the set temperature of device processed is 35 DEG C -55 DEG C, starts the stirring of constant temperature constant speed；
S2, glove box and transitional storehouse are vacuumized by vacuum pump first, and protection gas is then passed through into glove box and transitional storehouse
Body, opens the heat source of glove box, and 50-80 DEG C of constant temperature, until the oxygen content in glove box and transitional storehouse is lower than 0.1 ppm；
S3, transition door is opened, Packaging Bottle is transferred in glove box by carriage；Insert pump tube into packagings for lifting device
In bottle, metering switch pump is opened, is pumped into quantitative gallium liquid in Packaging Bottle from device processed according to setting program average rate；
S4, after having dispensed, pump line is detached Packaging Bottle by lifting device, and electronic balance is by weight data synchronous transfer to computer table
In lattice, then pass through one section of intermittent time；
S5, the Packaging Bottle for having dispensed gallium liquid is placed on carriage within the intermittent time, transports transitional storehouse back；
S6, repetition S3-S5 carry out packing operation, until packing finishes.
In certain embodiments of the present invention, the setting program in S3 specifically: metering pump in 10-30s by 2500g gallium
In liquid pump to Packaging Bottle.
In certain embodiments of the present invention, in S1, the range of speeds of stirring is 20-35 rpm.
In certain embodiments of the present invention, in S4, intermittent time 60S-120S.
In certain embodiments of the present invention, protective gas is 5N or the above high purity inert gas.
Embodiment 1.
Using the subpackage apparatus of gallium liquid, the high purity gallium liquid pump that 200KG purity is 7N is entered into device processed, the setting of device processed
Temperature is 35 DEG C, and speed of agitator is 20 rpm, starts the stirring of constant temperature constant speed；Heat source in unlatching glove box, 50 DEG C of constant temperature, until
Oxygen content in glove box and transitional storehouse is lower than 0.1 ppm；Transition door is opened, is shifted Packaging Bottle by carriage in one's hands
In casing；Lifting device opens metering switch pump insert pump tube into Packaging Bottle, according to setting program average rate by 2500g gallium liquid
It is pumped into Packaging Bottle in 10s；After having dispensed, pump line is detached Packaging Bottle by lifting device, and weight data is synchronized and passed by electronic balance
It is defeated into computer table, then pass through 60S intermittent time；The Packaging Bottle for having dispensed gallium liquid is placed in cunning within the intermittent time
It on dynamic device, transports transitional storehouse back, repeats above-mentioned packing operation, until packing finishes.It is detected, the superelevation dispensed
The purity of pure gallium liquid is still 7N, and wherein oxygen content is less than 1ppm.
Embodiment 2.
Using the subpackage apparatus of gallium liquid, the high purity gallium liquid pump that 300KG purity is 7N is entered into device processed, the setting of device processed
Temperature is 45 DEG C, and speed of agitator is 30 rpm, starts the stirring of constant temperature constant speed；Heat source in unlatching glove box, 70 DEG C of constant temperature, until
Oxygen content in glove box and transitional storehouse is lower than 0.1 ppm；Transition door is opened, is shifted Packaging Bottle by carriage in one's hands
In casing；Lifting device opens metering switch pump insert pump tube into Packaging Bottle, according to setting program average rate by 2500g gallium liquid
It is pumped into Packaging Bottle in 20s；After having dispensed, pump line is detached Packaging Bottle by lifting device, and weight data is synchronized and passed by electronic balance
It is defeated into computer table, then pass through 90S intermittent time；The Packaging Bottle for having dispensed gallium liquid is placed in cunning within the intermittent time
It on dynamic device, transports transitional storehouse back, repeats above-mentioned packing operation, until packing finishes.It is detected, the superelevation dispensed
The purity of pure gallium liquid is still 7N, and wherein oxygen content is less than 2.5ppm.
Embodiment 3.
Using the subpackage apparatus of gallium liquid, the high purity gallium liquid pump that 100KG purity is 7N is entered into device processed, the setting of device processed
Temperature is 55 DEG C, and speed of agitator is 35 rpm, starts the stirring of constant temperature constant speed；Heat source in unlatching glove box, 50 DEG C of constant temperature, until
Oxygen content in glove box and transitional storehouse is lower than 0.1 ppm；Transition door is opened, is shifted Packaging Bottle by carriage in one's hands
In casing；Lifting device opens metering switch pump insert pump tube into Packaging Bottle, according to setting program average rate by 2500g gallium liquid
It is pumped into Packaging Bottle in 10s；After having dispensed, pump line is detached Packaging Bottle by lifting device, and weight data is synchronized and passed by electronic balance
It is defeated into computer table, then pass through 120S intermittent time；The Packaging Bottle for having dispensed gallium liquid is placed in cunning in the intermittent time
It on dynamic device, transports transitional storehouse back, repeats above-mentioned packing operation, until packing finishes.It is detected, the superelevation dispensed
The purity of pure gallium liquid is still 7N, and wherein oxygen content is less than 3ppm.
The subpackage apparatus and method of this gallium liquid, in the closed environment provided by glove box, under the atmosphere of protective gas,
High purity gallium liquid is dispensed, while keeping gallium liquid purity, its oxygen content can be made to be less than 3ppm, so that the economic valence of gallium liquid
Value is maintained.
Although for illustrative purposes, the preferred embodiment of the present invention is had been disclosed, but the ordinary skill people of this field
Member will realize without departing from the scope and spirit of the invention as disclosed by the appended claims, various to change
Into, increase and replace be possible.
Claims (10)
1. a kind of subpackage apparatus of gallium liquid, it is characterised in that: the device includes the transition that a glove box and glove box are bordered by
Storehouse, the device further include the electronic scale being built in glove box, several Packaging Bottles, a lifting device, which further includes position
In the device processed of one outside glove box, a metering pump, the device processed, metering pump are connected by pump line, and pump line extends to gloves
Right above Packaging Bottle in case, the Packaging Bottle is placed on electronic scale, and lifting device is fixed on the surface of Packaging Bottle, described
Transitional storehouse is built-in with a carriage, and the glove box and transitional storehouse pass through tracheae and connect with gas cylinder, vacuum pump.
2. the subpackage apparatus of the gallium liquid according to claim 1, it is characterised in that: the device processed, metering pump, glove box
Between pump line be both provided with valve.
3. the subpackage apparatus of gallium liquid according to claim 2, it is characterised in that: the transitional storehouse is provided with a transitional storehouse
Door, when opening transition door, glove box is connected to transitional storehouse；When closing transition door, glove box and transitional storehouse mutually every
It opens absolutely.
4. the subpackage apparatus of gallium liquid according to claim 3, it is characterised in that: the glove box is built-in with heat source.
5. the subpackage apparatus of gallium liquid according to claim 4, it is characterised in that: the heat source uses infrared heat source.
6. a kind of method for filling of gallium liquid, it is characterised in that: using the subpackage apparatus of the gallium liquid described in claim 5 comprising
Following steps:
S1,7N high purity gallium liquid pump is entered to device processed, the set temperature of device processed is 35 DEG C -55 DEG C, starts the stirring of constant temperature constant speed；
S2, glove box and transitional storehouse are vacuumized by vacuum pump first, and protection gas is then passed through into glove box and transitional storehouse
Body, opens the heat source of glove box, and 50-80 DEG C of constant temperature, until the oxygen content in glove box and transitional storehouse is lower than 0.1 ppm；
S3, transition door is opened, Packaging Bottle is transferred in glove box by carriage；Insert pump tube into packagings for lifting device
In bottle, metering switch pump is opened, is pumped into quantitative gallium liquid in Packaging Bottle from device processed according to setting program average rate；
S4, after having dispensed, pump line is detached Packaging Bottle by lifting device, and electronic balance is by weight data synchronous transfer to computer table
In lattice, then pass through one section of intermittent time；
S5, the Packaging Bottle for having dispensed gallium liquid is placed on carriage within the intermittent time, transports transitional storehouse back；
S6, repetition S3-S5 carry out packing operation, until packing finishes.
7. the method for filling of gallium liquid according to claim 6, it is characterised in that: the setting program in S3 specifically: metering
It pumps in will be in 2500g gallium liquid pump to Packaging Bottle in 10-30s.
8. the method for filling of gallium liquid according to claim 6, it is characterised in that: in S1, the range of speeds of stirring is 20-
35 rpm。
9. the method for filling of gallium liquid according to claim 6, it is characterised in that: in S4, intermittent time 60S-120S.
10. the method for filling of gallium liquid according to claim 6, it is characterised in that: protective gas be 5N or more than it is high-purity lazy
Property gas.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810867398.7A CN109264072A (en) | 2018-08-02 | 2018-08-02 | The subpackage apparatus and method of gallium liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810867398.7A CN109264072A (en) | 2018-08-02 | 2018-08-02 | The subpackage apparatus and method of gallium liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109264072A true CN109264072A (en) | 2019-01-25 |
Family
ID=65148251
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810867398.7A Pending CN109264072A (en) | 2018-08-02 | 2018-08-02 | The subpackage apparatus and method of gallium liquid |
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| Country | Link |
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| CN (1) | CN109264072A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112030050A (en) * | 2019-06-03 | 2020-12-04 | 常州大学 | Continuous preparation method of gallium-based liquid alloy |
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| CN205984664U (en) * | 2016-08-12 | 2017-02-22 | 山西德益科技有限公司 | Super capacitor annotates liquid equipment |
| CN207275071U (en) * | 2018-01-24 | 2018-04-27 | 成都优材科技有限公司 | The packaging facilities of refining metallic powder |
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2018
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|---|---|---|---|---|
| CN202474087U (en) * | 2011-11-30 | 2012-10-03 | 凯迈（江苏）机电有限公司 | Glove box for lithium battery sealing and injecting |
| CN103545479A (en) * | 2013-08-02 | 2014-01-29 | 奇瑞汽车股份有限公司 | Glove box device |
| CN106184885A (en) * | 2015-04-30 | 2016-12-07 | 飞而康快速制造科技有限责任公司 | The security protection packing method of aviation-grade titanium alloy powder |
| CN205738178U (en) * | 2016-05-11 | 2016-11-30 | 安徽慧创科技有限公司 | A kind of protected against explosion automatic filling device |
| CN205984664U (en) * | 2016-08-12 | 2017-02-22 | 山西德益科技有限公司 | Super capacitor annotates liquid equipment |
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