CN109259740A - A kind of anti-low temperature scald skin temperature Indicator Paper - Google Patents
A kind of anti-low temperature scald skin temperature Indicator Paper Download PDFInfo
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- CN109259740A CN109259740A CN201811236426.1A CN201811236426A CN109259740A CN 109259740 A CN109259740 A CN 109259740A CN 201811236426 A CN201811236426 A CN 201811236426A CN 109259740 A CN109259740 A CN 109259740A
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- temperature indicator
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- low temperature
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B5/00—Measuring for diagnostic purposes; Identification of persons
- A61B5/01—Measuring temperature of body parts ; Diagnostic temperature sensing, e.g. for malignant or inflamed tissue
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01K—MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
- G01K11/00—Measuring temperature based upon physical or chemical changes not covered by groups G01K3/00, G01K5/00, G01K7/00 or G01K9/00
- G01K11/12—Measuring temperature based upon physical or chemical changes not covered by groups G01K3/00, G01K5/00, G01K7/00 or G01K9/00 using changes in colour, translucency or reflectance
- G01K11/14—Measuring temperature based upon physical or chemical changes not covered by groups G01K3/00, G01K5/00, G01K7/00 or G01K9/00 using changes in colour, translucency or reflectance of inorganic materials
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- Heart & Thoracic Surgery (AREA)
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- General Health & Medical Sciences (AREA)
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- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
Abstract
The invention discloses a kind of anti-low temperature to scald skin temperature Indicator Paper, including following component: acetic acid cloth, temperature indicator, adhesive and release paper；The adhesive is attached to the side of acetic acid cloth, is bonded release paper on the outside of adhesive.The temperature indicating test paper mainly using cobalt chloride it is hygroscopic and it is heated lose water when the changed property of color, the color change point of traditional CoCL2 6H2O is 50 DEG C and 70 DEG C, in order to control its color variation range and improve sensitivity, mixed ligand is added in the present invention in temperature indicator, form cobalt chloride complex solution, temperature indicating test paper is finally reached that 0 DEG C -41 DEG C colourless, 42 DEG C of -59 DEG C of light reds, the variation range of 60 DEG C or more purples.
Description
Technical field
The present invention relates to fields more particularly to a kind of anti-low temperature to scald skin temperature Indicator Paper.
Background technique
When carrying out the treatment of moxa-moxibustion or similar physical therapy, the heating of certain temperature can be carried out to skin, due to heating temperature
It is not high or patient when feeling more blunt, easily there is low temperature scald.Common skin temperature detector can only be to the temperature of a point
Degree is monitored, and can not carry out the monitoring temperature of large area.
It is affixed on the skin being heated, the heat object that 70 DEG C of skin contact continues one minute, or nearly 60 DEG C of the temperature of contact
Degree is when continuing 5 minutes or more, it is possible to cause low temperature to scald, it is minimum 45 DEG C of skin contacts be more than will also result within 2 hours it is low
Temperature scald.
The present invention in order to prevent scald by physical therapy, provides a kind of anti-low temperature scald skin temperature Indicator Paper, should be with temperature
The test paper material of degree indicator has significant metachromasia on one side, so as to medical staff's observation, and adjusts in time.
Summary of the invention
Technical problems based on background technology, the invention proposes a kind of anti-low temperature scald skin temperature instruction examinations
Paper.
Technical scheme is as follows:
A kind of anti-low temperature scalds skin temperature Indicator Paper, including following component: acetic acid cloth, temperature indicator, adhesive and from
Type paper；The adhesive is attached to the side of acetic acid cloth, is bonded release paper on the outside of adhesive.
The acetic acid cloth with a thickness of 20-30mil, adhesive with a thickness of 8-15mil.
Preferably, the anti-low temperature scalds skin temperature Indicator Paper, by following weight percent at being grouped as: vinegar
Sour cloth 18-25%, temperature indicator 2-6%, adhesive 30-40% and release paper surplus.
Preferably, the main component of the temperature indicator is cobalt chloride complex solution.
The adhesive is harmless aqueous medical acrylate adhesive.
Preferably, the preparation method of anti-low temperature scald skin temperature Indicator Paper, comprising the following steps:
A, temperature indicator is configured as requested；
B, acetic acid cloth is immersed in temperature indicator after impregnating 30-60s and is taken out, naturally dry；
C, in the side coating binder of acetic acid cloth；
D, it is bonded release paper on the outside of adhesive, crimps, cut, pack.
Preferably, the preparation method of the temperature indicator, comprising the following steps:
Step 1: sodium metaaluminate and sodium hydroxide are dissolved in deionized water and are configured to solution A；
Step 2: magnesium chloride is dissolved in deionized water and is configured to solution B；It is prepared being poured into B after cobalt chloride diluted hydrochloric acid dissolution
At solution C；
Step 3: mixed serum D is configured in odium stearate by mixed ligand is miscible；
Step 4: under strong stirring or ultrasonic wave effect, while solution A is added dropwise in mixed serum D with solution C and is prepared
At mixed serum E, temperature indicator can be obtained.
Preferably, the cobalt chloride is 0.15-0.2mol/L in the content of mixed serum E.
Preferably, the mixed ligand is mixed by ligand one and ligand two；The ligand is first is that thenoyl
It is any one in trifluoroacetone (TTA), benzoyltrifluoroacetone (BTA), benzoyl acetone (BA) or acetylacetone,2,4-pentanedione (acac)
Kind；The ligand two is 2,2- bipyridyl (2,2-biby) or 1,10- phenanthroline (o-phen).
The invention has the beneficial effects that: anti-low temperature of the invention scalds skin temperature Indicator Paper, mainly utilizes chlorine
Change that cobalt is hygroscopic and heated color changed property when losing water, the color change point of traditional CoCL2 6H2O is 50 DEG C
With 70 DEG C, in order to control its color variation range, mixed ligand is added in the present invention in temperature indicator, forms cobalt chloride and matches
Polymer solution, temperature indicating test paper are finally reached that 0 DEG C -41 DEG C colourless, the change of 42 DEG C of -59 DEG C of light reds, 60 DEG C or more purples
Change range.
Specific embodiment
Embodiment 1:
A kind of anti-low temperature scalds skin temperature Indicator Paper, by following weight percent at being grouped as: acetic acid cloth 22%, temperature
Indicator 4.5%, adhesive 35% and release paper surplus.
The main component of the temperature indicator is cobalt chloride complex solution.
The adhesive is harmless aqueous medical acrylate adhesive.
The preparation method of the anti-low temperature scald skin temperature Indicator Paper, comprising the following steps:
A, temperature indicator is configured as requested；
B, acetic acid cloth is immersed in temperature indicator after impregnating 45s and is taken out, naturally dry；
C, in the side coating binder of acetic acid cloth；
D, it is bonded release paper on the outside of adhesive, crimps, cut, pack.
The preparation method of the temperature indicator, comprising the following steps:
Step 1: sodium metaaluminate and sodium hydroxide are dissolved in deionized water and are configured to solution A；
Step 2: magnesium chloride is dissolved in deionized water and is configured to solution B；It is prepared being poured into B after cobalt chloride diluted hydrochloric acid dissolution
At solution C；
Step 3: mixed serum D is configured in odium stearate by mixed ligand is miscible；
Step 4: under strong stirring or ultrasonic wave effect, while solution A is added dropwise in mixed serum D with solution C and is prepared
At mixed serum E, temperature indicator can be obtained.
In the solution A, sodium metaaluminate mass percent accounts for 18%, and sodium hydroxide mass percent accounts for 11%.
The molar ratio of the solution B and solution A, Mg element therein and Al element is 1:0.35.
In the solution C, the molar ratio of Mg element and Al element is 1:0.018.
The solution C and mixed serum D, magnesium ion therein: the molar ratio of odium stearate is 1:0.22.
The cobalt chloride is 0.17mol/L in the content of mixed serum E.
The mixed ligand is mixed by ligand one and ligand two；The ligand is first is that thioyl trifluoroacetone
(TTA)；The ligand two is 2,2- bipyridyl (2,2-biby).
Embodiment 2:
A kind of anti-low temperature scalds skin temperature Indicator Paper, by following weight percent at being grouped as: acetic acid cloth 25%, temperature
Indicator 2%, adhesive 40% and release paper surplus.
The main component of the temperature indicator is cobalt chloride complex solution.
The adhesive is harmless aqueous medical acrylate adhesive.
The preparation method of the anti-low temperature scald skin temperature Indicator Paper, comprising the following steps:
A, temperature indicator is configured as requested；
B, acetic acid cloth is immersed in temperature indicator after impregnating 30s and is taken out, naturally dry；
C, in the side coating binder of acetic acid cloth；
D, it is bonded release paper on the outside of adhesive, crimps, cut, pack.
The preparation method of the temperature indicator, comprising the following steps:
Step 1: sodium metaaluminate and sodium hydroxide are dissolved in deionized water and are configured to solution A；
Step 2: magnesium chloride is dissolved in deionized water and is configured to solution B；It is prepared being poured into B after cobalt chloride diluted hydrochloric acid dissolution
At solution C；
Step 3: mixed serum D is configured in odium stearate by mixed ligand is miscible；
Step 4: under strong stirring or ultrasonic wave effect, while solution A is added dropwise in mixed serum D with solution C and is prepared
At mixed serum E, temperature indicator can be obtained.
In the solution A, sodium metaaluminate mass percent accounts for 20%, and sodium hydroxide mass percent accounts for 8.5%.
The molar ratio of the solution B and solution A, Mg element therein and Al element is 1:0.25.
In the solution C, the molar ratio of Mg element and Al element is 1:0.025.
The solution C and mixed serum D, magnesium ion therein: the molar ratio of odium stearate is 1:0.15.
The cobalt chloride is 0.2mol/L in the content of mixed serum E.
The mixed ligand is mixed by ligand one and ligand two；The ligand is first is that benzoyl acetone (BA)；
The ligand two is 1,10- phenanthroline (o-phen).
Embodiment 3:
A kind of anti-low temperature scalds skin temperature Indicator Paper, by following weight percent at being grouped as: acetic acid cloth 18%, temperature
Indicator 6%, adhesive 30% and release paper surplus.
The main component of the temperature indicator is cobalt chloride complex solution.
The adhesive is harmless aqueous medical acrylate adhesive.
The preparation method of the anti-low temperature scald skin temperature Indicator Paper, comprising the following steps:
A, temperature indicator is configured as requested；
B, acetic acid cloth is immersed in temperature indicator after impregnating 60s and is taken out, naturally dry；
C, in the side coating binder of acetic acid cloth；
D, it is bonded release paper on the outside of adhesive, crimps, cut, pack.
The preparation method of the temperature indicator, comprising the following steps:
Step 1: sodium metaaluminate and sodium hydroxide are dissolved in deionized water and are configured to solution A；
Step 2: magnesium chloride is dissolved in deionized water and is configured to solution B；It is prepared being poured into B after cobalt chloride diluted hydrochloric acid dissolution
At solution C；
Step 3: mixed serum D is configured in odium stearate by mixed ligand is miscible；
Step 4: under strong stirring or ultrasonic wave effect, while solution A is added dropwise in mixed serum D with solution C and is prepared
At mixed serum E, temperature indicator can be obtained.
In the solution A, sodium metaaluminate mass percent accounts for 16%, and sodium hydroxide mass percent accounts for 12%.
The molar ratio of the solution B and solution A, Mg element therein and Al element is 1:0.4.
In the solution C, the molar ratio of Mg element and Al element is 1:0.012.
The solution C and mixed serum D, magnesium ion therein: the molar ratio of odium stearate is 1:0.28.
The cobalt chloride is 0.15mol/L in the content of mixed serum E.
The mixed ligand is mixed by ligand one and ligand two；The ligand is first is that benzoyltrifluoroacetone
(BTA)；The ligand two is 2,2- bipyridyl (2,2-biby).
Comparative example 1
By the mixed ligand removal in embodiment 1.
The temperature indicating test paper of embodiment 1-3 is detected, and finds the detection time in 42 DEG C -59 DEG C pale red color ranges
For 10-15s；The detection time of 60 DEG C or more purples is 4-6s.
And the sample in comparative example 1 to 50 DEG C and 70 DEG C of detection time more than 1min.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (8)
1. a kind of anti-low temperature scalds skin temperature Indicator Paper, which is characterized in that including following component: acetic acid cloth, temperature instruction
Agent, adhesive and release paper；The adhesive is attached to the side of acetic acid cloth, is bonded release paper on the outside of adhesive.
2. anti-low temperature as described in claim 1 scalds skin temperature Indicator Paper, which is characterized in that by following weight percent
At being grouped as: acetic acid cloth 18-25%, temperature indicator 2-6%, adhesive 30-40% and release paper surplus.
3. anti-low temperature as described in claim 1 scalds skin temperature Indicator Paper, which is characterized in that the temperature indicator
Main component be cobalt chloride complex solution.
4. anti-low temperature as described in claim 1 scalds skin temperature Indicator Paper, which is characterized in that the adhesive is to people
The harmless aqueous medical acrylate adhesive of body.
5. anti-low temperature as described in claim 1 scalds skin temperature Indicator Paper, which is characterized in that the anti-low temperature scald
The preparation method of skin temperature Indicator Paper, comprising the following steps:
A, temperature indicator is configured as requested；
B, acetic acid cloth is immersed in temperature indicator after impregnating 30-60s and is taken out, naturally dry；
C, in the side coating binder of acetic acid cloth；
D, it is bonded release paper on the outside of adhesive, crimps, cut, pack.
6. anti-low temperature as claimed in claim 5 scalds skin temperature Indicator Paper, which is characterized in that the temperature indicator
Preparation method, comprising the following steps:
Step 1: sodium metaaluminate and sodium hydroxide are dissolved in deionized water and are configured to solution A；
Step 2: magnesium chloride is dissolved in deionized water and is configured to solution B；It is prepared being poured into B after cobalt chloride diluted hydrochloric acid dissolution
At solution C；
Step 3: mixed serum D is configured in odium stearate by mixed ligand is miscible；
Step 4: under strong stirring or ultrasonic wave effect, while solution A is added dropwise in mixed serum D with solution C and is prepared
At mixed serum E, temperature indicator can be obtained.
7. anti-low temperature as claimed in claim 6 scalds skin temperature Indicator Paper, which is characterized in that the cobalt chloride is mixed
The content for closing slurries E is 0.15-0.2mol/L.
8. anti-low temperature as claimed in claim 6 scalds skin temperature Indicator Paper, which is characterized in that the mixed ligand by
Ligand one and ligand two mix；The ligand is first is that thioyl trifluoroacetone, benzoyltrifluoroacetone, benzoyl third
Any one in ketone or acetylacetone,2,4-pentanedione；The ligand two is 2,2- bipyridyl or 1,10- phenanthroline.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811236426.1A CN109259740B (en) | 2018-10-23 | 2018-10-23 | Skin temperature indicating test paper for preventing low-temperature scald |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811236426.1A CN109259740B (en) | 2018-10-23 | 2018-10-23 | Skin temperature indicating test paper for preventing low-temperature scald |
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| Publication Number | Publication Date |
|---|---|
| CN109259740A true CN109259740A (en) | 2019-01-25 |
| CN109259740B CN109259740B (en) | 2021-12-10 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811236426.1A Active CN109259740B (en) | 2018-10-23 | 2018-10-23 | Skin temperature indicating test paper for preventing low-temperature scald |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111982339A (en) * | 2020-08-26 | 2020-11-24 | 中国烟草总公司郑州烟草研究院 | Detection test paper loaded with temperature-sensitive marker, preparation method and application |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN86209663U (en) * | 1986-11-29 | 1987-10-31 | 潘国治 | Colour moisture meter |
| CN1385555A (en) * | 2002-03-21 | 2002-12-18 | 李建起 | Electrolytic pole board insulated covering edge and protective method |
| CN101250409A (en) * | 2007-12-14 | 2008-08-27 | 福建师范大学 | Rear earth containing hydrotalcite having high fluorescence and preparation method thereof |
| CN102796216A (en) * | 2012-08-09 | 2012-11-28 | 福建师范大学 | Preparation method of rare earth hydrotalcite-like compound/polymer nanocomposite |
| CN102795657A (en) * | 2012-08-09 | 2012-11-28 | 福建师范大学 | Preparation method of white hydrotalcite-like compound |
| CN103364096A (en) * | 2013-07-08 | 2013-10-23 | 吴江龙纺纺织有限公司 | Temperature test paper with thermosensitive gauze |
| CN103408682A (en) * | 2013-07-23 | 2013-11-27 | 福建师范大学 | White-light-type hydrotalcite nano composite material and application thereof for LED light source |
| CN204176727U (en) * | 2014-10-03 | 2015-02-25 | 北京中科联众科技股份有限公司 | A kind of infrared induction heater of changeable colour |
| WO2017169109A1 (en) * | 2016-03-30 | 2017-10-05 | 日東電工株式会社 | Temperature sensor |
-
2018
- 2018-10-23 CN CN201811236426.1A patent/CN109259740B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN86209663U (en) * | 1986-11-29 | 1987-10-31 | 潘国治 | Colour moisture meter |
| CN1385555A (en) * | 2002-03-21 | 2002-12-18 | 李建起 | Electrolytic pole board insulated covering edge and protective method |
| CN101250409A (en) * | 2007-12-14 | 2008-08-27 | 福建师范大学 | Rear earth containing hydrotalcite having high fluorescence and preparation method thereof |
| CN102796216A (en) * | 2012-08-09 | 2012-11-28 | 福建师范大学 | Preparation method of rare earth hydrotalcite-like compound/polymer nanocomposite |
| CN102795657A (en) * | 2012-08-09 | 2012-11-28 | 福建师范大学 | Preparation method of white hydrotalcite-like compound |
| CN103364096A (en) * | 2013-07-08 | 2013-10-23 | 吴江龙纺纺织有限公司 | Temperature test paper with thermosensitive gauze |
| CN103408682A (en) * | 2013-07-23 | 2013-11-27 | 福建师范大学 | White-light-type hydrotalcite nano composite material and application thereof for LED light source |
| CN204176727U (en) * | 2014-10-03 | 2015-02-25 | 北京中科联众科技股份有限公司 | A kind of infrared induction heater of changeable colour |
| WO2017169109A1 (en) * | 2016-03-30 | 2017-10-05 | 日東電工株式会社 | Temperature sensor |
Non-Patent Citations (1)
| Title |
|---|
| 王海滨: "无机热致变色材料的研究及应用进展", 《中国陶瓷》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111982339A (en) * | 2020-08-26 | 2020-11-24 | 中国烟草总公司郑州烟草研究院 | Detection test paper loaded with temperature-sensitive marker, preparation method and application |
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| CN109259740B (en) | 2021-12-10 |
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