CN109231403A - A kind of preparation method of subset alkalinity hydrogen-rich water - Google Patents

A kind of preparation method of subset alkalinity hydrogen-rich water Download PDF

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Publication number
CN109231403A
CN109231403A CN201810939844.0A CN201810939844A CN109231403A CN 109231403 A CN109231403 A CN 109231403A CN 201810939844 A CN201810939844 A CN 201810939844A CN 109231403 A CN109231403 A CN 109231403A
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China
Prior art keywords
hydrogen
rich water
preparation
subset
water
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Pending
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CN201810939844.0A
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Chinese (zh)
Inventor
陈木成
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Heng Tian Quantum (xiamen) Technology Co Ltd
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Heng Tian Quantum (xiamen) Technology Co Ltd
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Priority to CN201810939844.0A priority Critical patent/CN109231403A/en
Publication of CN109231403A publication Critical patent/CN109231403A/en
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/68Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • General Preparation And Processing Of Foods (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention belongs to drinking water production technical fields, disclose a kind of preparation method of subset alkalinity hydrogen-rich water, comprise the steps of: step 1, by emulsifier and hydrogen storage filler ground and mixed, obtaining surfactant and hydrogen storage filler mixture;Step 2, it feeds the mixture into small-micelle water and simultaneously low temperature ultrasonic refinement is sufficiently stirred, obtain suspension;Step 3, suspension beneath be covered in the closed container of hydride is placed in react;Step 4, acid-base modifier is added into container and adjusts PH to 7.5-8.5;Step 5, solution after reaction is stirred at low speed into placement a period of time, takes suspension.This method can solve the problems, such as hydrogen storage in hydrogen-rich water under certain technique, the formula can utilize the powerful adsorption effect of hydrogen storage filler, by hydrogen adsorption in filler, it is suspended into water by the package of emulsifier again, the mode that original hydrogen-rich water is dissolved in water by hydrogen is sufficiently changed, the content of hydrogen is improved.

Description

A kind of preparation method of subset alkalinity hydrogen-rich water
Technical field
The invention belongs to drinking water production technical field more particularly to a kind of preparation sides of subset alkalinity hydrogen-rich water Method.
Background technique
Small-micelle water is that 5-6 water molecules form, and traditional drinking water is that macromolecular mass water is by 10 or more water Molecule is formed through Hydrogenbond, and macromolecular mass cannot be needed by cell membrane through intestinal absorption since molecule is larger, and small point Son rolls into a ball the cell membrane that can directly shuttle, and can keep the skin wet in time for cell, and cell is more effectively discharged and generates waste;
It is that hydrogen is dissolved in the water that hydrogen-rich water, which is also known as water element water, can be reduced in vivo by drinking or injecting hydrogen-rich water The amount of active oxygen reduces free radical, has good effect to salubrity and to some diseases treatment.At present for the system of hydrogen-rich water Standby mainly have chemical hydrogen manufacturing: active metal react with water prepare hydrogen or by electrolysis water by way of prepare hydrogen, then Hydrogen is dissolved into preparation hydrogen-rich water in water, another kind is directly to inject hydrogen and water dissolution preparation hydrogen-rich water by hydrogen cylinder, this Although two ways can prepare hydrogen-rich water but the compatible prepared hydrogen-rich water hydrogen of the simple mixing by hydrogen and water contains Measure it is low, and hydrogen be not easy storage be easily separated from water influence hydrogen-rich water practicability.
Hydrogen agent and water are tied up in a kind of method use for inexpensively preparing long-acting hydrogen-rich water of Chinese invention patent 201410211336.2 Mixing prepares hydrogen-rich water by way of being passed through hydrogen again, although can temporarily store hydrogen using hydrogen agent package hydrogen is tied up, It is that hydrogen molecule is small, storage hydrogen that merely can not be permanently effective by tiing up hydrogen agent.
A kind of hydrogen-rich water of Chinese invention patent 201610823677.4 or the preparation method of hydrogen-rich beverage use calcium hydride It is reacted with water, is surface-treated by the package to calcium hydride and the effect of auxiliary agent slows down so that hydrogen slowly produces, to reach The solute effect of hydrogen and water;The method although slows down the generation speed of hydrogen but not can solve hydrogen property compatible with water poor The problem of, gained hydrogen-rich water hydrogen content is low.
In conclusion problem of the existing technology is: hydrogen and water solvability are limited in hydrogen-rich water, gained hydrogen-rich water Hydrogen content is lower, and the higher hydrogen-rich water of density of hydrogen can not be obtained and cannot protect for a long time by being mixed by hydrogen with water merely Hold hydrogen content in hydrogen-rich water.
Summary of the invention
(1) the technical issues of solving
In view of the deficiencies of the prior art, the present invention provides a kind of preparation methods of subset alkalinity hydrogen-rich water, solve Hydrogen and water solvability are limited in hydrogen-rich water, and gained hydrogen-rich water hydrogen content is lower, are mixed simultaneously by hydrogen with water merely The problem of cannot obtaining the higher hydrogen-rich water of density of hydrogen and hydrogen content in hydrogen-rich water cannot be kept for a long time.
(2) technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs: a kind of subset alkalinity hydrogen-rich water Preparation method, steps are as follows for the preparation method of the subset alkalinity hydrogen-rich water:
Emulsifier and hydrogen storage filler ground and mixed are obtained surfactant and hydrogen storage filler mixture by step 1;
Step 2 feeds the mixture into small-micelle water and simultaneously low temperature ultrasonic refinement is sufficiently stirred, obtains suspension;
Suspension is placed in beneath be covered in the closed container of hydride and reacted by step 3;
Acid-base modifier is added into container and adjusts PH to 7.5-8.5 by step 4;
Solution after reaction is stirred at low speed placement a period of time, takes suspension by step 5.
Preferably, the emulsifier is food grade emulsifier.
Preferably, the hydrogen storage filler is food grade bamboo charcoal powder or other edible high ratios with high-specific surface area Area carbon based material.
Preferably, the ultrasonic cryogenic refinement, ultrasonic power < 350W, ultrasonic time 0.5-2h, temperature control is 10- 20℃。
Preferably, the hydride is sodium hydride and calcium hydride.
Preferably, the acid-base modifier is sodium bicarbonate.
Preferably, the hydrogen storage filler specific surface area is 500-2000m2/ g, having a size of nanoscale.
(3) beneficial effect
The present invention provides a kind of preparation method of subset alkalinity hydrogen-rich water, have it is following the utility model has the advantages that
The present invention can solve the problems, such as hydrogen storage in hydrogen-rich water under certain technique, utilize the powerful absorption of hydrogen storage filler Effect by hydrogen adsorption in filler, then is suspended into water by the package of emulsifier, and it is logical sufficiently to change original hydrogen-rich water The mode that hydrogen is dissolved in water is crossed, the content of hydrogen is improved, while the storage problem of hydrogen-rich water can be solved, uses small molecule Group's water can quickly absorb moisture and the moisture supplement of cell and waste is promoted to exclude, and promote health.
Detailed description of the invention
Fig. 1 is the preparation process flow chart of the preparation method of subset alkalinity hydrogen-rich water provided in an embodiment of the present invention;
Fig. 2 is the schematic diagram of the preparation method of subset alkalinity hydrogen-rich water provided in an embodiment of the present invention.
In figure: step 1 S101;Step 2 S102;Step 3 S103;Step 4 S104;Step 5 S105.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
The present invention provides a kind of technical solution referring to FIG. 1-2: a kind of preparation method of subset alkalinity hydrogen-rich water, Steps are as follows for preparation method:
S101: by emulsifier and hydrogen storage filler ground and mixed, surfactant and hydrogen storage filler mixture are obtained;
S102: it feeds the mixture into small-micelle water and simultaneously low temperature ultrasonic refinement is sufficiently stirred, obtain suspension;
S103: suspension is placed in beneath be covered in the closed container of hydride and is reacted;
S104: acid-base modifier is added into container and adjusts PH to 7.5-8.5;
S105: solution after reaction is stirred at low speed into placement a period of time, takes suspension.
As the preferred embodiment of the present invention, the emulsifier is food grade emulsifier.
As the preferred embodiment of the present invention, the hydrogen storage filler be food grade bamboo charcoal powder with high-specific surface area or Other edible high-specific surface area carbon-based materials.
As the preferred embodiment of the present invention, the ultrasonic cryogenic refinement, ultrasonic power < 350W, ultrasonic time 0.5- 2h, temperature control are 10-20 DEG C.
As the preferred embodiment of the present invention, the hydride is sodium hydride and calcium hydride.
As the preferred embodiment of the present invention, the acid-base modifier is sodium bicarbonate.
As the preferred embodiment of the present invention, the hydrogen storage filler specific surface area is 500-2000m2/g, having a size of receiving Meter level.
Application principle of the invention is further described combined with specific embodiments below.
Embodiment 1:
A kind of preparation method of subset alkalinity hydrogen-rich water
Key step are as follows:
(1) by emulsifier and hydrogen storage filler ground and mixed, surfactant and hydrogen storage filler mixture are obtained;
(2) it feeds the mixture into small-micelle water and simultaneously low temperature ultrasonic refinement is sufficiently stirred, obtain suspension;
(3) suspension beneath be covered in the closed container of hydride is placed in react;
(4) acid-base modifier is added into container and adjusts PH to 7.5-8.5;
(5) solution after reaction is stirred at low speed into placement a period of time, takes suspension.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
In conclusion the present invention can solve the problems, such as hydrogen storage in hydrogen-rich water under certain technique, hydrogen storage filler is utilized Powerful adsorption effect, by hydrogen adsorption in filler, then be suspended into water by the package of emulsifier, sufficiently change original The mode for having hydrogen-rich water to be dissolved in water by hydrogen improves the content of hydrogen, while can solve the storage problem of hydrogen-rich water, Moisture, which can quickly be absorbed, using small-micelle water promotes the moisture supplement of cell and waste to exclude, and promotes health.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (7)

1. a kind of preparation method of subset alkalinity hydrogen-rich water, feature exist, the preparation of the subset alkalinity hydrogen-rich water Method and step is as follows:
Emulsifier and hydrogen storage filler ground and mixed are obtained surfactant and hydrogen storage filler mixture by step 1;
Step 2 feeds the mixture into small-micelle water and simultaneously low temperature ultrasonic refinement is sufficiently stirred, obtains suspension;
Suspension is placed in beneath be covered in the closed container of hydride and reacted by step 3;
Acid-base modifier is added into container and adjusts PH to 7.5-8.5 by step 4;
Solution after reaction is stirred at low speed placement a period of time, takes suspension by step 5.
2. a kind of preparation method of subset alkalinity hydrogen-rich water according to claim 1, it is characterised in that: the emulsification Agent is food grade emulsifier.
3. a kind of preparation method of subset alkalinity hydrogen-rich water according to claim 1, it is characterised in that: the hydrogen storage Filler is food grade bamboo charcoal powder or other edible high-specific surface area carbon-based materials with high-specific surface area.
4. a kind of preparation method of subset alkalinity hydrogen-rich water according to claim 1, it is characterised in that: the ultrasound Low temperature refining, ultrasonic power < 350W, ultrasonic time 0.5-2h, temperature control is 10-20 DEG C.
5. a kind of preparation method of subset alkalinity hydrogen-rich water according to claim 1, it is characterised in that: the hydrogenation Object is sodium hydride and calcium hydride.
6. a kind of preparation method of subset alkalinity hydrogen-rich water according to claim 1, it is characterised in that: the soda acid Regulator is sodium bicarbonate.
7. a kind of preparation method of subset alkalinity hydrogen-rich water according to claim 1, it is characterised in that: the hydrogen storage Filler specific surface area is 500-2000m2/ g, having a size of nanoscale.
CN201810939844.0A 2018-08-17 2018-08-17 A kind of preparation method of subset alkalinity hydrogen-rich water Pending CN109231403A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110357183A (en) * 2019-08-09 2019-10-22 珠海品源绿色健康产业发展有限公司 A kind of synthetic method of hydrogen-rich water ceramic element
CN114258998A (en) * 2021-12-14 2022-04-01 湖南中榜生物科技有限公司 Hydrogen-rich beverage and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050121399A1 (en) * 2003-12-03 2005-06-09 Hidemitsu Hayashi Method of producing hydrogen rich water and hydrogen rich water generator
CN104016471A (en) * 2014-05-19 2014-09-03 西安交通大学 Method for cheaply preparing long-acting hydrogen-rich water
CN105668894A (en) * 2016-02-29 2016-06-15 朱上翔 Preparation process of small molecular group weakly alkaline negative-hydrogen healthy water
CN105923733A (en) * 2016-06-16 2016-09-07 杭州氢源科技有限公司 Portable hydrogen-rich water preparation device and method

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050121399A1 (en) * 2003-12-03 2005-06-09 Hidemitsu Hayashi Method of producing hydrogen rich water and hydrogen rich water generator
CN104016471A (en) * 2014-05-19 2014-09-03 西安交通大学 Method for cheaply preparing long-acting hydrogen-rich water
CN105668894A (en) * 2016-02-29 2016-06-15 朱上翔 Preparation process of small molecular group weakly alkaline negative-hydrogen healthy water
CN105923733A (en) * 2016-06-16 2016-09-07 杭州氢源科技有限公司 Portable hydrogen-rich water preparation device and method

Non-Patent Citations (2)

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Title
刘建国: "《可再生能源导论》", 28 February 2017, 中国轻工业出版社 *
左振素 等: "《饮水决定健康》", 31 January 2007, 吉林科学技术出版社 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110357183A (en) * 2019-08-09 2019-10-22 珠海品源绿色健康产业发展有限公司 A kind of synthetic method of hydrogen-rich water ceramic element
CN110357183B (en) * 2019-08-09 2021-11-23 珠海品源绿色健康产业发展有限公司 Synthesis method of hydrogen-rich water ceramic filter element
CN114258998A (en) * 2021-12-14 2022-04-01 湖南中榜生物科技有限公司 Hydrogen-rich beverage and preparation method thereof
CN114258998B (en) * 2021-12-14 2024-02-09 湖南中榜生物科技有限公司 Hydrogen-enriched beverage and preparation method thereof

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