CN101268997A - Complexing form wash and bath liquid of natural mineral matter and micro-element, and preparation method - Google Patents
Complexing form wash and bath liquid of natural mineral matter and micro-element, and preparation method Download PDFInfo
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- CN101268997A CN101268997A CNA2008103000915A CN200810300091A CN101268997A CN 101268997 A CN101268997 A CN 101268997A CN A2008103000915 A CNA2008103000915 A CN A2008103000915A CN 200810300091 A CN200810300091 A CN 200810300091A CN 101268997 A CN101268997 A CN 101268997A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/02—Non-contaminated water, e.g. for industrial water supply
- C02F2103/026—Treating water for medical or cosmetic purposes
Abstract
A complex bath foam with natural mineral composition and microelements contains natural mineral composition activating concentrated solution, sea water activating concentrated solution , oyster shell whiting, complexing agent, acidifying or alkalizing agent and purified water; wherein, the ratio by weight of the natural mineral composition activating concentrated solution and the sea water activating concentrated solution is 1:1 to 50, the adding quantity of the purified water is 0 to 50 percent of the total weight of the mixed liquid of the natural mineral composition activating concentrated solution and the sea water activating concentrated solution, the adding quantity of the oyster shell whiting is 0 to 30 percent of the total weight of the mixed liquid, the pH value of the bath foam is 5.5 to 7.5 and the specific gravity is 1.1 to 1.8. The natural mineral composition activating concentrated solution is prepared by mineral flour and solution, wherein, the mineral flour contains zinc mineral flour, mica powder, vermiculite powder and magnesium mineral flour. The bath foam contains a variety of mineral compositions and microelements which are beneficial to the health of human body, and has stable floating effect and the functions of entertainment, hairdressing and body-building.
Description
(1) technical field
The present invention relates to a kind of bath lotion and compound method thereof, particularly a kind ofly contain natural mineral matter and trace element, and can allow the buoyant complex state bath lotion of human body.
(2) background technology
Along with the raising of people's living standard, variation has taken place in the idea that people wash whole body to a basin clear water, and bathing requires culture, pursues leisure, amusement, health care or the like in the past.As everyone knows, " Dead Sea " of Israel is famous tourist attraction, Middle East, because Israel " Dead Sea " has the dual-use function of " floating " and " disease curing and body-building ", therefore, reach the millions of people to the visitor that Israel " Dead Sea " plays every year all over the world, brought huge income for the tourist industry of Israel.Along with the approval to Israel " Dead Sea ", various places have occurred in succession various " the artificial Dead Seas ", and still, there are following many fatal shortcomings in existing " the artificial Dead Sea " bath lotion:
(1), formulation analysis: prescription originally lacks science, reasonability.Because, only be purpose with the levitating, modulate with single salt and form, so, cause the liquid component prepared too single, it is all multi-functional to bring into play leisure, health care etc.Owing to be subjected to the restriction of the dissolubility of single salt, make bath lotion proportion on the low side, though can make human body floating reluctantly, but, always give the insecurity of a kind of sinking of people, make the experiencer not reach whole body and loosen, can not get due impression, can't reach the purpose such as real leisure, amusement, medical treatment, health care of expection.
(2) novelty analysis: because the deficiency of above-mentioned prescription causes in the past " the artificial Dead Sea " only to possess buoyant characteristics, and lacks multifunctionalities such as health care such as physical therapy, body-building, performance is too dull, does not have novelty, lacks economic development value.
(3) bath lotion performance evaluation: because the unicity of synthetic liquid component causes the variation sensitivity of liquid to ambient temperature, along with the variation of ambient temperature, phenomenon is separated out in the crystallization that salinity can occur, proportion descends, and floating ability instability needs heating constantly, guarantee not separating out of salinity with the temperature that improves liquid, it is too high to lead temperature like this, makes the experiencer feel overheated uncomfortable, has influenced the bathing effect, simultaneously, the problems referred to above have brought inconvenience for bathing out of doors.
(4) modulation process and effect analysis: " the artificial Dead Sea " or the floating bath of preparation in the past, because composition is single, be subjected to the restriction of problems such as dissolubility, make the adjustable range of bath lotion too small, aspect the acid-base value of bath lotion, also be difficult for adjusting, pH value is crossed low or too high, cause bath lotion to be peracidity or parlkaline, like this, people are in floating or bathing process, and bath lotion can be to the skin of human body, wound, face etc. produce twinge, calcination etc., produce uncomfortable feeling, and abnormal response or drying etc. appear in skin after the bathing, do not reach original bathing purpose.
(5) analysis of composition: " the artificial Dead Sea " of preparation in the past often selects cheap magnesium sulfate salt or sodium salt aspect dissolving salt, these two kinds of salt are medically all belonging to cathartic.Because proportion is lower, people can not fully loosen still in tension in floating or bathing process, so experiencer's water phenomenon that is easy to out choke is as drinking accidentally in the abdomen, can cause diarrhoea very soon, and, cause very big injury to human body owing to be that impurity is more.
(3) summary of the invention
The purpose of this invention is to provide a kind of natural mineral matter and trace element complex state bath lotion and compound method thereof, solve single, the floating effect problem of unstable of existing bath lotion prescription.
For achieving the above object, the present invention adopts following technical scheme:
A kind of natural mineral matter and trace element complex state bath lotion is characterized in that: this bath lotion contains natural mineral matter activation concentrated solution, sea water activation concentrated solution, conch meal, chelating agent, acid-base modifier and pure water; Wherein the weight ratio of natural mineral matter activation concentrated solution and sea water activation concentrated solution is 1: 1～50, the addition of pure water is 0～50% of natural mineral matter activation concentrated solution and a sea water activation concentrated solution mixed liquor gross weight, the conch meal addition is 0～30% of a mixed liquor gross weight, the pH value of bath lotion is 5.5～7.5, and proportion is 1.1～1.8;
Above-mentioned natural mineral matter activation concentrated solution is formulated with mineral powder and lysate, in the mineral powder gross weight is 100, and the zinc ore powder content is 20～50%, mica powder content is 10～20%, vermiculite power content is 10～20%, the magnesium ore powder content is 20～50%; The content of lysate is 1～3 times of mineral powder cumulative volume.
Above-mentioned lysate is inorganic lysate, organic lysate or both mixed liquors; Above-mentioned inorganic lysate is one or more the mixture in sulphuric acid, hydrochloric acid, phosphoric acid, the carbonic acid, and above-mentioned organic lysate is one or more the mixture in formic acid, acetic acid, oxalic acid, the ethanedioic acid.
Above-mentioned chelating agent is inorganic complexing agent or organic complexing agent, wherein inorganic complexing agent is one or more the mixture in ammonia, sodium carbonate, chloride, iodide or the sodium bicarbonate, and organic complexing agent is one or more mixture in amine or the carboxylic acids.
Above-mentioned acid-base modifier is one or more the alkaline solution in sodium hydroxide, sodium carbonate, sodium bicarbonate or the bubble flower alkali, the perhaps acid solution of one or more in hydrochloric acid, phosphoric acid, formic acid, the acetic acid.
The compound method of a kind of natural mineral matter and trace element complex state bath lotion is characterized in that preparation steps is as follows:
Step 1, that the natural mineral matter for preparing activation concentrated solution and sea water are activated concentrated solution is even by 1: 1～50 mixed, natural mineral matter activation concentrated solution and sea water activation concentrated solution add in the pure water by 1～50% of pure water volume, the pH value that makes mixed liquor is 1.0～5.0, add conch meal and regulate the proportion of mixed liquor, make it to reach 1.2～2.0;
Step 2, adding chelating agent are that 5～10MHz, intensity are 10～15W/cm with frequency
2Ultrasonic Treatment 0.5～1 hour, make metal ion form stable complex state;
Step 3, adding acid-base modifier, pure water, the pH value that makes mixed liquor is 5.5～7.5, proportion is 1.1～1.8;
Step 4, sterilization, sterilization, and with the microfilter filtration of 0.2～5 μ m;
Step 5, usefulness activator activation processing 1～3 hour promptly obtain natural mineral matter and trace element complex state bath lotion.
The preparation steps of above-mentioned natural mineral matter activation concentrated solution is:
Step a is that 50～200 purpose zinc ore stone powders, mica powder, vermiculite power, magnesium ore powder take by weighing in proportion with granularity, soaks 0.5～1 hour with pure water, and dehydration is to half-dried;
Step b will soak, dehydrated raw material adds capping in the pressurized tank, be heated to 150～300 ℃, be pressurized to 1～5kg/cm
2In time, left standstill 0.5～1 hour, reduces to room temperature, normal pressure afterwards fast;
Step c will handle material and move in the dissolving tank, add the acid dissoluting liquid of 1～3 times of mineral powder volume again, soaked at normal temperatures and pressures 2～7 hours, and be that 5～10MHz, intensity are 10～15W/cm with frequency simultaneously
2Ultrasonic Treatment, be dipped into beginnings in 2 hours solution in dissolving tank and send into oxygen, filter through the microfilter of 1～5 μ m again;
Steps d adds the chelating agent mixing with filtrate, uses activator activation processing 1～8 hour, obtains natural mineral matter activation concentrated solution.
As the further optimized technical scheme of the present invention: the filtrate behind the above-mentioned steps c keeps, and gets the acid dissoluting liquid that residue adds 1～3 times of mineral powder volume again and soaks 1～5 hour down at 40～80 ℃, use supersound process, through the microfilter filtration of 1～5 μ m.
The preparation steps of above-mentioned conch meal is:
Step I selects the shell of free of contamination ocean shell biology;
Step II is broken into fine powder more than 90 orders with conch meal;
Step II I is with conch meal ashing at high temperature;
Powder after step IV, the high temperature ashing is conch meal.
The preparation steps of above-mentioned sea water activation concentrated solution is:
Steps A, extracting seawater is injected hold-up tank;
Step B filters;
Step C, sterilization, sterilization;
Step D concentrates;
Step e, activation processing obtains sea water activation concentrated solution.
The combination of one or more in above-mentioned sterilization, sterilisation step employing ozone, ultraviolet, chlorine dioxide, the sodium hypochlorite sterilization method.
Compared with prior art the present invention has following characteristics and beneficial effect:
The present invention has overcome tradition " artificial the Dead Sea " the existing defective of bath lotion, provide a kind of contain multiple to useful mineral of health and trace element, can make human body floating, bathing, have the bath lotion and a preparation method of functions such as amusement and recreation, cosmetology and health again.
The present invention has adopted several natural crystals, utilize advanced production technology, health useful mineral and trace element are extracted repeatedly, mix activation processing, make natural mineral matter activation concentrated solution, underground deep layer sea water activation concentrated solution with pure natural is mixed in proportion again, makes and is rich in tens kinds of natural mineral matters such as K, Na, Ca, Mg, Sr, Zn, Se, Li, Cu, Fe, Al, Mn, Mo, Ni, Ti, Si, Ge, F, Cl, Br, I, P, B, V and trace element in the water.
The enough floating human body of liquid adds chelating agent, and the reuse acid-base modifier is regulated the pH value of bath lotion, near neutral, carries out activation processing at last again.
Natural crystal composition and effect that the present invention adopts are as follows:
Zinc ore, main component is a zinc sulfide, contains mineral and trace element such as a large amount of zinc, ferrum, gallium, indium, thallium.Adopting purpose is in order to increase the content of zinc in the mineral activating solution.
Muscovitum, main component is an aluminosilicate, contains macroelement and trace element such as a large amount of potassium, sodium, magnesium, ferrum, aluminum, titanium, lithium, silicon.Adopting purpose is in order to enrich the content of elements such as potassium, sodium, calcium, magnesium, ferrum, aluminum, lithium, silicon in the mineral activating solution.
Vermiculitum is the femic aluminosilicate, contains natural mineral matters such as a large amount of ferrum, magnesium, aluminum, silicon.Adopting purpose is in order to increase the content of elements such as ferrum, aluminum, magnesium, silicon in the mineral activating solution.
Magnesium ore is Ling Meikuang, and its main component is a magnesium oxide.The compositions such as calcium, silicon, manganese, ferrum that also have other.Adopting purpose is in order to increase the content of magnesium elements in the activating solution.
Sea water of the present invention is the underground sea water of the nature that formed during earth transition before 100000000 years.Wherein contain various trace element compositions such as K, Na, Ca, Mg, Zn, Mn, Al, Sr, Li, B, Ti, Ba, V, Ni, Cu, Si, Co.
With traditional bath lotion contrast, the present invention mainly contains following advantage:
1, main component of the present invention derives from nature Ore and underground sea water, is not general industrial chemicals simple modulation, and the various materials that contained in the solution are natural, are floating, the bath lotion of the health of real pure natural.
2, bath lotion of the present invention contains abundant, isostatic mineral and trace element, and natural mineral matter activation concentrated solution is through activation processing, can significantly improve the activity of water after adding in the entry, make mineral and trace element in the water more help absorption of human body, thereby give multiple functions such as floating bathing health care, cosmetology and health.But blood circulation promoting, promotion human body metabolism, set up fast, can produce mitigation various skin disease, cardiovascular and cerebrovascular disease, diabetes, cervical spondylosis, scapulohumeral periarthritis, arthritis, scapulalgia, muscular soreness, neurasthenia and health and the excessive syndrome that causes of mental pressure.
3, bath lotion of the present invention has adopted the transformation technology of natural salinity, the result who shows is that the whole dissolubility in bath lotion of salt is improved, enough salinities are dissolved in the water, significantly and stably improved the proportion (reaching as high as 1.8) of bath lotion, crystallization (minimum reach subzero 20 degree) can not appear in bath lotion yet under lower temperature, set up large-scale floating outdoor bathing place for the open air and lay a good foundation.Satisfied novelty and practicality, had unique society and economic benefit as the production commodity technology.Simultaneously, be that prerequisite reduces cost to improve the quality of products, in the use of technology and product consumption process, cut down the consumption of energy, reduced operator's cost, for the market-oriented commercialization of technology provides good condition.
4, complex state bath lotion of the present invention is without the industrial chemicals of magnesium sulfate salt or sodium salt, be purely from natural crystal and underground sea water, take out molten concentrating and salinity, be pure natural.Thereby aspect safety, be guaranteed more, bath lotion is strayed in the abdomen, can not cause the diarrhoea poisoning to wait injury to human body yet.
5, bath lotion of the present invention is used the activator activation processing at last, and the material in the mineral solution is paramagnetic in violent vibration processes, and both the zwitterion in the mineral solution became the linear array structure by random arrangement, formed linear condensed state.This structure energy state adds the activity that can significantly improve water in the entry than higher.Test by nuclear magnetic resonance analyser: the wide 55～75Hz of being of nuclear magnetic resoance spectrum half range that adds the water of 0.1% mineral activation concentrated solution, the wide 133Hz of being of nuclear magnetic resoance spectrum half range that does not add the water of mineral activating solution, the nuclear magnetic resoance spectrum half range of water is wide narrow more, and energy is high more, activity is big more.
5, bath lotion pH value of the present invention is 5.5～7.5, thereby can not cause uncomfortable sensation to human body skin, wound, face etc.; Because bath lotion of the present invention can guarantee the floating proportion of using of stable human body, so people needn't wear with complicated protective device such as bolster when floating or bathing, have reduced many unnecessary troubles, easily experience is floating, bathing joyful.
(4) description of drawings
The present invention is further detailed explanation below in conjunction with accompanying drawing.
Fig. 1 is the flow chart of compound method of the present invention.
(5) specific embodiment
Embodiment: a kind of natural mineral matter and trace element complex state bath lotion is characterized in that: this bath lotion contains natural mineral matter activation concentrated solution, sea water activation concentrated solution, conch meal, chelating agent, acid-base modifier and pure water; Wherein the weight ratio of natural mineral matter activation concentrated solution and sea water activation concentrated solution is 1: 10,1: 20,1: 30,1: 40 or 1: 50, the addition of pure water is 1～50% of natural mineral matter activation concentrated solution and a sea water activation concentrated solution mixed liquor gross weight, the conch meal addition is 1～5% of a mixed liquor gross weight, the pH value of bath lotion is 5.5～7.5, and proportion is 1.1～1.8.
Above-mentioned natural mineral matter activation concentrated solution is formulated with mineral powder and lysate, in the mineral powder gross weight is 100, and the zinc ore powder content is 30～40%, mica powder content is 10～20%, vermiculite power content is 10～20%, the magnesium ore powder content is 30～40%; The content of lysate is 1～3 times of mineral powder cumulative volume.
Mineral powder proportioning embodiment:
| Material name | Mineral powder embodiment one | Mineral powder embodiment two | Mineral powder embodiment three |
| Relieving fatigue | Beauty and skin care | Health-care physical therapy | |
| The zinc ore stone powder | 30-40％ | 40-50％ | 35-40％ |
| Mica powder | 10-20％ | 5-10％ | 5-10％ |
| Vermiculite power | 10-20％ | 1-5％ | 1-5％ |
| The magnesium ore powder | 30-40％ | 40-50％ | 40-50％ |
Above-mentioned lysate is inorganic lysate, organic lysate or both mixed liquors; Above-mentioned inorganic lysate is one or more the mixture in sulphuric acid, hydrochloric acid, phosphoric acid, the carbonic acid, and above-mentioned organic lysate is one or more the mixture in formic acid, acetic acid, oxalic acid, the ethanedioic acid.
Above-mentioned chelating agent is inorganic complexing agent or organic complexing agent, wherein inorganic complexing agent is one or more the mixture in ammonia, sodium carbonate, chloride, iodide or the sodium bicarbonate, and organic complexing agent is one or more mixture in amine or the carboxylic acids.Its objective is to make the reaction of metal ion dissolved in the Ore and chelating agent form stable complex, to reduce separating out or precipitating of metal ion.
Above-mentioned acid-base modifier is one or more the alkaline solution in sodium hydroxide, sodium carbonate, sodium bicarbonate or the bubble flower alkali, or one or more the acid solution in the hydrochloric acid, phosphoric acid, formic acid, acetic acid.
Referring to shown in Figure 1, the compound method of a kind of natural mineral matter and trace element complex state bath lotion is characterized in that preparation steps is as follows:
Step 1, that the natural mineral matter for preparing activation concentrated solution and sea water are activated concentrated solution is even by 1: 1～50 mixed, add the pure water of mixed liquor gross weight 0～50%, it is an amount of to add conch meal, the conch meal addition is 0～30% of a mixed liquor gross weight, regulate the proportion of mixed liquor, make it to reach 1.1～1.8.
Step 2, adding chelating agent are that 5～10MHz, intensity are 10～15W/cm with frequency
2Ultrasonic Treatment 0.5～1 hour, make metal ion form stable complex state.
Step 3, adding acid-base modifier, pure water, the pH value that makes mixed liquor is 5.5～7.5, proportion is 1.1～1.8.
Step 4, sterilization, sterilization, the combination of one or more in above-mentioned sterilization, sterilisation step employing ozone, ultraviolet, chlorine dioxide, the sodium hypochlorite sterilization method.Microfilter with 0.2～5 μ m filters then.
Step 5, usefulness activator activation processing 1～3 hour promptly obtain natural mineral matter and trace element complex state bath lotion.Above-mentioned activator is a kind ofly material in the mineral solution can be paramagnetic in violent vibration processes, and promptly the zwitterion in the mineral solution becomes the linear array structure by random arrangement, forms the existing device of linear condensed state.
The preparation steps of natural mineral matter activation concentrated solution is:
Step a is that 50～200 purpose zinc ore stone powders, mica powder, vermiculite power, magnesium ore powder take by weighing in proportion with granularity, soaks 0.5～1 hour with pure water, and dehydration is to half-dried.
Step b will soak, dehydrated raw material adds capping in the pressurized tank, be heated to 150～300 ℃, be pressurized to 1～5kg/cm
2In time, left standstill 0.5～1 hour, reduces to room temperature, normal pressure afterwards fast.
Step c will handle material and move in the dissolving tank, add No. 1 acid dissoluting liquid of 1～3 times of mineral powder volume again, soaked at normal temperatures and pressures 2～7 hours, and be that 5～10MHz, intensity are 10～15W/cm with frequency simultaneously
2Ultrasonic Treatment, be dipped into beginnings in 2 hours solution in dissolving tank and send into oxygen, filter through the microfilter of 1～5 μ m again.
No. 1 acid dissoluting liquid: be mixed with 30～80% sulfate liquids with 98% sulphuric acid.No. 1 acid dissoluting liquid is mineral acid or organic acid or its mixed liquor, and described mineral acid comprises one or more mixture in sulphuric acid (concentration 98%), hydrochloric acid (concentration 36%), the phosphoric acid (concentration 90%).
Steps d keeps the filtrate in the step 3, gets No. 2 acid dissoluting liquids that residue adds 1～3 times of mineral powder volume again and soaks 1～5 hour down at 40～80 ℃, continues use above-mentioned supersound process simultaneously, through the microfilter filtration of 1～5 μ m.
No. 2 acid dissoluting liquids: 36% hydrochloric acid mixes with 36% ethanedioic acid at 1: 1.No. 2 acid dissoluting liquids are that organic acid comprises one or more mixture in formic acid (concentration 30%), acetic acid (concentration 36%), the ethanedioic acid (concentration 20%), its objective is that the metal ion that makes in the Ore is dissolved in the lysate to greatest extent.
Step e step 3 and the resulting filtrate mixing of step 4, adds the chelating agent mixing, uses activator activation processing 1～8 hour, obtains natural mineral matter activation concentrated solution.
The preparation steps of above-mentioned sea water activation concentrated solution is:
Steps A, it is standby to extract natural underground sea water injection hold-up tank.
Step B is through 0.2～1 μ m filter element filtering.
Step C, sterilization, sterilization, the combination of one or more in above-mentioned sterilization, sterilisation step employing ozone, ultraviolet, chlorine dioxide, the sodium hypochlorite sterilization method.
Step D is transported in the thickener and concentrates 1～10 hour.
Step e is used activator activation processing 1～5 hour, obtains underground sea water activation concentrated solution.
The preparation steps of above-mentioned conch meal is:
Step I selects the shell of natural free of contamination shellfish ocean shell class.
Step II is broken into 100 purpose fine powders with conch meal.
Step II I joins conch meal in the ashing furnace, ashing under 500～1000 ℃ temperature.
After step IV, the ashing of collection high temperature, remaining powder is conch meal.
Claims (10)
1. natural mineral matter and trace element complex state bath lotion, it is characterized in that: this bath lotion contains natural mineral matter activation concentrated solution, sea water activation concentrated solution, conch meal, chelating agent, acid-base modifier and pure water; Wherein the weight ratio of natural mineral matter activation concentrated solution and sea water activation concentrated solution is 1: 1～50, the addition of pure water is 0～50% of natural mineral matter activation concentrated solution and a sea water activation concentrated solution mixed liquor gross weight, the conch meal addition is 0～30% of a mixed liquor gross weight, the pH value of bath lotion is 5.5～7.5, and proportion is 1.1～1.8;
Above-mentioned natural mineral matter activation concentrated solution is formulated with mineral powder and lysate, in the mineral powder gross weight is 100, and the zinc ore powder content is 20～50%, mica powder content is 10～20%, vermiculite power content is 10～20%, the magnesium ore powder content is 20～50%; The content of lysate is 1～3 times of mineral powder cumulative volume.
2. natural mineral matter according to claim 1 and trace element complex state bath lotion is characterized in that: above-mentioned lysate is inorganic lysate, organic lysate or both mixed liquors; Above-mentioned inorganic lysate is one or more the mixture in sulphuric acid, hydrochloric acid, phosphoric acid, the carbonic acid, and above-mentioned organic lysate is one or more the mixture in formic acid, acetic acid, oxalic acid, the ethanedioic acid.
3. natural mineral matter according to claim 1 and trace element complex state bath lotion, it is characterized in that: above-mentioned chelating agent is inorganic complexing agent or organic complexing agent, wherein inorganic complexing agent is one or more the mixture in ammonia, sodium carbonate, chloride, iodide or the sodium bicarbonate, and organic complexing agent is one or more mixture in amine or the carboxylic acids.
4. natural mineral matter according to claim 1 and trace element complex state bath lotion, it is characterized in that: above-mentioned acid-base modifier is one or more the alkaline solution in sodium hydroxide, sodium carbonate, sodium bicarbonate or the bubble flower alkali, the perhaps acid solution of one or more in hydrochloric acid, phosphoric acid, formic acid, the acetic acid.
5. the compound method of natural mineral matter and trace element complex state bath lotion is characterized in that preparation steps is as follows:
Step 1, that the natural mineral matter for preparing activation concentrated solution and sea water are activated concentrated solution is even by 1: 1～50 mixed, natural mineral matter activation concentrated solution and sea water activation concentrated solution add in the pure water by 1～50% of pure water volume, the pH value that makes mixed liquor is 1.0～5.0, add conch meal and regulate the proportion of mixed liquor, make it to reach 1.2～2.0;
Step 2, adding chelating agent, is that 5～10MHz, intensity are the ultrasonic Treatment 0.5～1 hour of 10～15W/cm2 with frequency, makes metal ion form stable complex state;
Step 3, adding acid-base modifier, pure water, the pH value that makes mixed liquor is 5.5～7.5, proportion is 1.1～1.8;
Step 4, sterilization, sterilization, and with the microfilter filtration of 0.2～5 μ m;
Step 5, usefulness activator activation processing 1～3 hour promptly obtain natural mineral matter and trace element complex state bath lotion.
6. the compound method of natural mineral matter according to claim 5 and trace element complex state bath lotion is characterized in that: the preparation steps of above-mentioned natural mineral matter activation concentrated solution is:
Step a is that 50～200 purpose zinc ore stone powders, mica powder, vermiculite power, magnesium ore powder take by weighing in proportion with granularity, soaks 0.5～1 hour with pure water, and dehydration is to half-dried;
Step b will soak, dehydrated raw material adds capping in the pressurized tank, is heated to 150～300 ℃, leaves standstill when being pressurized to 1～5,kg/,cm2 0.5～1 hour, reduces to room temperature, normal pressure afterwards fast;
Step c, to handle material moves in the dissolving tank, the acid dissoluting liquid that adds 1～3 times of mineral powder volume again, soaked at normal temperatures and pressures 2～7 hours, be that 5～10MHz, intensity are the ultrasonic Treatment of 10～15W/cm2 with frequency simultaneously, be dipped into beginnings in 2 hours solution in dissolving tank and send into oxygen, the microfilter through 1～5 μ m filters again;
Steps d adds the chelating agent mixing with filtrate, uses activator activation processing 1～8 hour, obtains natural mineral matter activation concentrated solution.
7. the compound method of natural mineral matter according to claim 6 and trace element complex state bath lotion, it is characterized in that: the filtrate behind the above-mentioned steps c keeps, get residue and add the acid dissoluting liquid of 1～3 times of mineral powder volume again 40～80 ℃ of following immersions 1～5 hour, use supersound process, through the microfilter filtration of 1～5 μ m.
8. according to the compound method of claim 6 or 7 described natural mineral matters and trace element complex state bath lotion, it is characterized in that the preparation steps of above-mentioned conch meal is:
Step I selects the shell of free of contamination ocean shell biology;
Step II is broken into fine powder more than 90 orders with conch meal;
Step II I is with conch meal ashing at high temperature;
Powder after step IV, the high temperature ashing is conch meal.
9. according to the compound method of claim 6 or 7 described natural mineral matters and trace element complex state bath lotion, it is characterized in that the preparation steps of above-mentioned sea water activation concentrated solution is:
Steps A, extracting seawater is injected hold-up tank;
Step B filters;
Step C, sterilization, sterilization;
Step D concentrates;
Step e, activation processing obtains sea water activation concentrated solution.
10. the compound method of natural mineral matter according to claim 9 and trace element complex state bath lotion is characterized in that: the combination of one or more in above-mentioned sterilization, sterilisation step employing ozone, ultraviolet, chlorine dioxide, the sodium hypochlorite sterilization method.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
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| CNA2008103000915A CN101268997A (en) | 2008-01-14 | 2008-01-14 | Complexing form wash and bath liquid of natural mineral matter and micro-element, and preparation method |
| PCT/CN2008/073219 WO2009089705A1 (en) | 2008-01-14 | 2008-11-27 | A bath water comprising activated concentrated solution of nature minerals and activated concentrated seawater |
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| CNA2008103000915A CN101268997A (en) | 2008-01-14 | 2008-01-14 | Complexing form wash and bath liquid of natural mineral matter and micro-element, and preparation method |
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| WO (1) | WO2009089705A1 (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009089705A1 (en) * | 2008-01-14 | 2009-07-23 | Jishan Yin | A bath water comprising activated concentrated solution of nature minerals and activated concentrated seawater |
| CN101822403A (en) * | 2010-04-20 | 2010-09-08 | 王衍洲 | Ocean element electrolysis concentrated product and manufacture method thereof |
| CN104313617A (en) * | 2014-11-07 | 2015-01-28 | 合肥大安印刷有限责任公司 | Rust-removing metal surface cleaning agent and preparation method thereof |
| CN105330421A (en) * | 2014-11-15 | 2016-02-17 | 深圳市芭田生态工程股份有限公司 | Method for preparing complex-state mineral element organic liquid fertilizer |
| CN106316552A (en) * | 2015-06-18 | 2017-01-11 | 刘海涛 | Fulvic acid mineral fertilizer and preparation method thereof |
| CN111803518A (en) * | 2020-07-22 | 2020-10-23 | 烟台冠玉生物科技有限公司 | Liquid trace element, preparation method and application |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1117559C (en) * | 2000-04-28 | 2003-08-13 | 北京四博工贸有限公司 | Activated and concentrated liquid containing minerals and race elements and preparing process thereof |
| JP2003246739A (en) * | 2002-02-25 | 2003-09-02 | Hoso Shizai Center:Kk | Health water and its preparation process |
| CN100558651C (en) * | 2005-09-23 | 2009-11-11 | 成都死海盐疗健康馆服务有限公司 | A kind of preparation method of dead sea floated rock salt solution |
| CN1742703A (en) * | 2005-09-23 | 2006-03-08 | 成都死海盐疗健康馆服务有限公司 | Dead-sea floatation salt-therapy bathing solution |
| CN101268997A (en) * | 2008-01-14 | 2008-09-24 | 尹吉山 | Complexing form wash and bath liquid of natural mineral matter and micro-element, and preparation method |
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2008
- 2008-01-14 CN CNA2008103000915A patent/CN101268997A/en active Pending
- 2008-11-27 WO PCT/CN2008/073219 patent/WO2009089705A1/en active Application Filing
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009089705A1 (en) * | 2008-01-14 | 2009-07-23 | Jishan Yin | A bath water comprising activated concentrated solution of nature minerals and activated concentrated seawater |
| CN101822403A (en) * | 2010-04-20 | 2010-09-08 | 王衍洲 | Ocean element electrolysis concentrated product and manufacture method thereof |
| CN101822403B (en) * | 2010-04-20 | 2012-12-26 | 王衍洲 | Ocean element electrolysis concentrated product and manufacture method thereof |
| CN104313617A (en) * | 2014-11-07 | 2015-01-28 | 合肥大安印刷有限责任公司 | Rust-removing metal surface cleaning agent and preparation method thereof |
| CN105330421A (en) * | 2014-11-15 | 2016-02-17 | 深圳市芭田生态工程股份有限公司 | Method for preparing complex-state mineral element organic liquid fertilizer |
| CN106316552A (en) * | 2015-06-18 | 2017-01-11 | 刘海涛 | Fulvic acid mineral fertilizer and preparation method thereof |
| CN111803518A (en) * | 2020-07-22 | 2020-10-23 | 烟台冠玉生物科技有限公司 | Liquid trace element, preparation method and application |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2009089705A1 (en) | 2009-07-23 |
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