CN109221177A - Composite plant immunity inducing agent and preparation method thereof - Google Patents
Composite plant immunity inducing agent and preparation method thereof Download PDFInfo
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- CN109221177A CN109221177A CN201811372778.XA CN201811372778A CN109221177A CN 109221177 A CN109221177 A CN 109221177A CN 201811372778 A CN201811372778 A CN 201811372778A CN 109221177 A CN109221177 A CN 109221177A
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- 239000002131 composite material Substances 0.000 title claims abstract description 41
- 238000002360 preparation method Methods 0.000 title abstract description 9
- 230000036039 immunity Effects 0.000 title abstract description 5
- 230000001939 inductive effect Effects 0.000 title 1
- 239000000411 inducer Substances 0.000 claims abstract description 32
- -1 alginate oligosaccharide Chemical class 0.000 claims abstract description 20
- 230000000694 effects Effects 0.000 claims abstract description 17
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 16
- WHHIPMZEDGBUCC-UHFFFAOYSA-N probenazole Chemical compound C1=CC=C2C(OCC=C)=NS(=O)(=O)C2=C1 WHHIPMZEDGBUCC-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 239000000463 material Substances 0.000 claims abstract description 13
- 229920001491 Lentinan Polymers 0.000 claims abstract description 9
- 229940115286 lentinan Drugs 0.000 claims abstract description 9
- 239000011552 falling film Substances 0.000 claims abstract description 6
- 229920001542 oligosaccharide Polymers 0.000 claims abstract 2
- 238000000034 method Methods 0.000 claims description 17
- OQEBBZSWEGYTPG-UHFFFAOYSA-N 3-aminobutanoic acid Chemical compound CC(N)CC(O)=O OQEBBZSWEGYTPG-UHFFFAOYSA-N 0.000 claims description 16
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 16
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 14
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 13
- 229940024606 amino acid Drugs 0.000 claims description 13
- 239000011593 sulfur Substances 0.000 claims description 12
- 229910052717 sulfur Inorganic materials 0.000 claims description 12
- 238000001704 evaporation Methods 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000004475 Arginine Substances 0.000 claims description 8
- KZSNJWFQEVHDMF-BYPYZUCNSA-N L-valine Chemical compound CC(C)[C@H](N)C(O)=O KZSNJWFQEVHDMF-BYPYZUCNSA-N 0.000 claims description 8
- KZSNJWFQEVHDMF-UHFFFAOYSA-N Valine Natural products CC(C)C(N)C(O)=O KZSNJWFQEVHDMF-UHFFFAOYSA-N 0.000 claims description 8
- ODKSFYDXXFIFQN-UHFFFAOYSA-N arginine Natural products OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 claims description 8
- RUTXIHLAWFEWGM-UHFFFAOYSA-H iron(3+) sulfate Chemical compound [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 claims description 8
- 229910000360 iron(III) sulfate Inorganic materials 0.000 claims description 8
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 8
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 8
- 108010064470 polyaspartate Proteins 0.000 claims description 8
- 239000004474 valine Substances 0.000 claims description 8
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims description 8
- 229960001763 zinc sulfate Drugs 0.000 claims description 8
- 229910000368 zinc sulfate Inorganic materials 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- WZCQRUWWHSTZEM-UHFFFAOYSA-N 1,3-phenylenediamine Chemical compound NC1=CC=CC(N)=C1 WZCQRUWWHSTZEM-UHFFFAOYSA-N 0.000 claims description 4
- 229940018564 m-phenylenediamine Drugs 0.000 claims description 4
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 3
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 3
- QSJXEFYPDANLFS-UHFFFAOYSA-N Diacetyl Chemical group CC(=O)C(C)=O QSJXEFYPDANLFS-UHFFFAOYSA-N 0.000 claims description 3
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 3
- 229920001213 Polysorbate 20 Polymers 0.000 claims description 3
- ZSBOMYJPSRFZAL-JLHYYAGUSA-N [(2e)-3,7-dimethylocta-2,6-dienyl] butanoate Chemical compound CCCC(=O)OC\C=C(/C)CCC=C(C)C ZSBOMYJPSRFZAL-JLHYYAGUSA-N 0.000 claims description 3
- 239000002253 acid Substances 0.000 claims description 3
- 125000001931 aliphatic group Chemical group 0.000 claims description 3
- 239000004359 castor oil Substances 0.000 claims description 3
- 235000019438 castor oil Nutrition 0.000 claims description 3
- NHCQMVNKPJAQJZ-UHFFFAOYSA-N geranyl n-butyrate Natural products CCCCOCC=C(C)CCC=C(C)C NHCQMVNKPJAQJZ-UHFFFAOYSA-N 0.000 claims description 3
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 3
- OOCMUZJPDXYRFD-UHFFFAOYSA-L calcium;2-dodecylbenzenesulfonate Chemical compound [Ca+2].CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O.CCCCCCCCCCCCC1=CC=CC=C1S([O-])(=O)=O OOCMUZJPDXYRFD-UHFFFAOYSA-L 0.000 claims description 2
- DWNBOPVKNPVNQG-LURJTMIESA-N (2s)-4-hydroxy-2-(propylamino)butanoic acid Chemical compound CCCN[C@H](C(O)=O)CCO DWNBOPVKNPVNQG-LURJTMIESA-N 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 150000002191 fatty alcohols Chemical class 0.000 claims 1
- 150000002482 oligosaccharides Chemical class 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 abstract description 41
- 241000209140 Triticum Species 0.000 abstract description 27
- 235000021307 Triticum Nutrition 0.000 abstract description 25
- 230000008901 benefit Effects 0.000 abstract description 6
- 229940072056 alginate Drugs 0.000 abstract 1
- 235000010443 alginic acid Nutrition 0.000 abstract 1
- 229920000615 alginic acid Polymers 0.000 abstract 1
- 244000144972 livestock Species 0.000 abstract 1
- 230000009044 synergistic interaction Effects 0.000 abstract 1
- 238000005507 spraying Methods 0.000 description 18
- 235000001014 amino acid Nutrition 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 8
- ODKSFYDXXFIFQN-BYPYZUCNSA-P L-argininium(2+) Chemical compound NC(=[NH2+])NCCC[C@H]([NH3+])C(O)=O ODKSFYDXXFIFQN-BYPYZUCNSA-P 0.000 description 6
- 235000018417 cysteine Nutrition 0.000 description 6
- XUJNEKJLAYXESH-UHFFFAOYSA-N cysteine Natural products SCC(N)C(O)=O XUJNEKJLAYXESH-UHFFFAOYSA-N 0.000 description 6
- 201000010099 disease Diseases 0.000 description 6
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 241001530056 Athelia rolfsii Species 0.000 description 5
- 244000052769 pathogen Species 0.000 description 5
- 230000001717 pathogenic effect Effects 0.000 description 5
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 3
- XUJNEKJLAYXESH-REOHCLBHSA-N L-Cysteine Chemical compound SC[C@H](N)C(O)=O XUJNEKJLAYXESH-REOHCLBHSA-N 0.000 description 3
- 238000003723 Smelting Methods 0.000 description 3
- 229920002472 Starch Polymers 0.000 description 3
- 150000004676 glycans Chemical class 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 239000002304 perfume Substances 0.000 description 3
- 229920001282 polysaccharide Polymers 0.000 description 3
- 239000005017 polysaccharide Substances 0.000 description 3
- 230000002265 prevention Effects 0.000 description 3
- 235000019698 starch Nutrition 0.000 description 3
- 239000008107 starch Substances 0.000 description 3
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 2
- 102000030523 Catechol oxidase Human genes 0.000 description 2
- 108010031396 Catechol oxidase Proteins 0.000 description 2
- 208000035240 Disease Resistance Diseases 0.000 description 2
- 206010059866 Drug resistance Diseases 0.000 description 2
- 102000003992 Peroxidases Human genes 0.000 description 2
- 241000813090 Rhizoctonia solani Species 0.000 description 2
- 230000004913 activation Effects 0.000 description 2
- 239000003905 agrochemical Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 230000001965 increasing effect Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 108040007629 peroxidase activity proteins Proteins 0.000 description 2
- 239000000447 pesticide residue Substances 0.000 description 2
- 235000018102 proteins Nutrition 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- CSNIZNHTOVFARY-UHFFFAOYSA-N 1,2-benzothiazole Chemical group C1=CC=C2C=NSC2=C1 CSNIZNHTOVFARY-UHFFFAOYSA-N 0.000 description 1
- 102100036601 Aggrecan core protein Human genes 0.000 description 1
- 239000004382 Amylase Substances 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 241001290235 Ceratobasidium cereale Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 241001272567 Hominoidea Species 0.000 description 1
- 102000004882 Lipase Human genes 0.000 description 1
- 239000004367 Lipase Substances 0.000 description 1
- 108090001060 Lipase Proteins 0.000 description 1
- 102000004317 Lyases Human genes 0.000 description 1
- 108090000856 Lyases Proteins 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 108091005804 Peptidases Proteins 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004365 Protease Substances 0.000 description 1
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 1
- 108091006419 SLC25A12 Proteins 0.000 description 1
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- CGIHPACLZJDCBQ-UHFFFAOYSA-N acibenzolar Chemical compound SC(=O)C1=CC=CC2=C1SN=N2 CGIHPACLZJDCBQ-UHFFFAOYSA-N 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000003872 anastomosis Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 238000009360 aquaculture Methods 0.000 description 1
- 244000144974 aquaculture Species 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000000853 biopesticidal effect Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 230000007123 defense Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000012010 growth Effects 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 230000007124 immune defense Effects 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 231100001231 less toxic Toxicity 0.000 description 1
- 235000019421 lipase Nutrition 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000000618 nitrogen fertilizer Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000001575 pathological effect Effects 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 239000005962 plant activator Substances 0.000 description 1
- 230000008121 plant development Effects 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 230000011664 signaling Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 229960005486 vaccine Drugs 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
- A01N37/46—N-acyl derivatives
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
- A01N47/42—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=CX2 groups, e.g. isothiourea
- A01N47/44—Guanidine; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
Landscapes
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a composite plant immunity inducer and a preparation method thereof, wherein the composite plant immunity inducer comprises the following raw material components in parts by weight: 10-15 parts of brown alginate oligosaccharide, 18-22 parts of probenazole, 8-14 parts of lentinan, 8-19 parts of compound amino acid, 5-8 parts of compound sulfate and 1-3 parts of emulsifier. The raw materials are treated and mixed, then a double-effect falling film evaporator is adopted for concentration, and the concentrated mixed material is spray-dried to obtain the composite material. The composite plant immunity inducer provided by the invention has reasonable components, has synergistic interaction among the components, not only has good control effect on wheat sharp eyespot, improves the yield of wheat, but also can improve the quality of wheat, is harmless to people and livestock after being applied, does not pollute the environment, and has good economic benefit and ecological benefit.
Description
Technical field
The present invention relates to a kind of composite plants, and inducer and preparation method thereof is immunized, and belongs to technical field of pesticide.
Technical background
Wheat sharp eyespot is also known as wheat point eye spot disease, and just there is morbidity at the beginning of the seventies in last century in China.In recent years, due to gas
Reasons, the wheat lines such as time warms, the raising of chemical fertilizer especially amount of application of nitrogen fertilizer and times shift to an earlier date, application rate increases are withered
Disease is in a increasing trend year by year, and seriously threatens the stable high yield of wheat.Wheat sharp eyespot is by Rhizoctonia cerealis
(4 mycelia anastomosis groups such as CAG-1, CAG-3, CAG-6 and AGC1) and Rhizoctonia solani Kuhn (AG4 and AG5 merge group) cause, wheat
There is significant linear correlation, the every raising level-one of severity, yield between production loss and banded sclerotial blight severity rank
Loss increases about 10%~20% or so.Beginning recovers morning, and morbidity is heavier, and corresponding production loss is bigger.It falls ill before boot stage,
Production loss 25%~40% is fallen ill after beginning fringe, and production loss is generally less than 20%.Studies have shown that wheat sharp eyespot not only shadow
The yield of wheat is rung, and has an effect on rice quality.
Prevention and control for the disease are prevented and treated using the single chemical agent of such as jinggangmeisu always, but jinggangmeisu
Generated apparent drug resistance, every season times for spraying from 2 times before 20 years 3~5 times increased till now, dosage also from
1.5kg/hm2Increase to 4.5~6.0kg/hm2.Agro-chemicals control not only pollutes environment, but also there are at high cost, pesticide residue and productions
The problems such as raw drug resistance, while control efficiency is also by inside even from weather such as rainfall, humidity.
Plant immune inducer is also known as plant vaccine, is a kind of novel biopesticide, and plant immune inducer passes through activation
The immune system of plant and the metabolism for adjusting plant, improve the nutrient situation of plant, and enhancing is resisted pathogen ability and resisted
Inverse ability, to achieve the purpose that disease resistance.Brown alga oligose be it is a kind of have height physiological activity plant it is immune lure it is anti-
Agent can be used as the regulation activity that signaling molecule participates in plant growth and development, can also be expressed with the intracorporal hormone of activated plant seedling,
Adjust plant endo-amylase, lipase and protease vigor, accelerate endosperm starch hydrolytic process, promote seed sprout and
The growth of root, bud；Meanwhile brown alga oligose can also induce plant generation resisting substance to cause to damage to alleviate adverse circumstance to plant.
Brown alga oligose is from a wealth of sources, and has many advantages, such as to be therefore widely used in green agriculture to no toxic biological, efficient, low-residual
The industries such as industry, aquaculture, food and medicine.
Probenazole is benzo isothiazole Plant activator also known as allyl isothiazole, probenazole itself
There is no direct bactericidal activity, but the potential of plant can be excited, performance is similar with the Acibenzolar of Syngenta, also known as disease-resistant activation
Agent (or anti pathologic immunity activator).Phenylalanine lyase (PAL), peroxidase (POD) and polyphenol oxidase (PPO) are small
The intracorporal significant defense enzyme of wheat plant is influenced by probenazole induction, and the activity of this 3 kinds of defensive ferments improves, to promote
By the lignification of pathogen infection tissue, penetrating further into and infecting for pathogen is prevented, this lignifying reaction is to plant
Object resists pathogen and invades most effective means, to make plant performance disease resistance.It lives to pathogen without directly effect
Property, therefore selection pressure is not generated, germ is not easy to generate resistance to it；Nonpathogenic bacteria with direct or indirect influence do not occur,
Be conducive to protect beneficial microbe population.Therefore, probenazole safety, to people and animals, environment and non-target close friend, is expected to become
A kind of important tool of wheat diseases prevention and treatment, be develop green agriculture and nuisanceless and green food the ideal chose of production it
One.
Summary of the invention
It is an object of the invention to: a kind of immune inducer of composite plant that preventing and treating wheat sharp eyespot is provided, it is of the invention
Another object is to provide the vegetation method that inducer is immunized in above-mentioned composite plant, and said preparation not only has well wheat sharp eyespot
Control efficiency improves wheat yield, moreover it is possible to improve the quality of wheat, while small to environmental hazard.
The present invention is achieved by the following technical solutions: a kind of immune inducer of composite plant, it is characterised in that: it is former
Material component and each component parts by weight be respectively as follows: 10~15 parts of brown alga oligose, 18~22 parts of probenazole, lentinan 8~
14 parts, 8~19 parts of compound amino acid, 5~8 parts of composite sulfur hydrochlorate, 1~3 part of emulsifier.
It is preferred that the compound amino acid includes the raw material of following parts by weight: 3~6 parts of poly-aspartate, beta-aminobutyric acid 2
~4 parts, 1~3 part of arginine, 1~3 part of valine, 1~3 part of cysteine.
It is preferred that the composite sulfur hydrochlorate is the raw material for including following parts by weight: 1~2 part of ferric sulfate, 2~3 parts of magnesium sulfate,
2~3 parts of zinc sulfate.
It is preferred that the emulsifier are as follows: m-phenylene diamine (MPD), diacetyl tartarate monoglyceride, geranyl butyrate, castor oil are poly-
Ethylene oxide ether, APES sulfosuccinate, polyoxyethylene 20 sorbitan monolaurate, detergent alkylate
Sulfoacid calcium and one of aliphatic acid polyethenoxy ether or polyoxyethylene aliphatic alcohol ether are a variety of.
The present invention also provides the methods for preparing the immune inducer of above-mentioned composite plant, the specific steps of which are as follows:
(1) brown alga oligose, probenazole and lentinan are proportionally accurately weighed, mixture is uniformly mixing to obtain,
Mixture is fully ground, 40~70 meshes is crossed, obtains component A；
(2) to weigh compound amino acid according to aforementioned proportion soluble in water, obtains component B；
(3) proportionally accurately weigh composite sulfur hydrochlorate, put into furnace heats fusing, add temperature be 48~
52 DEG C of deionized water stirs 15~20min and is chelated, and natural cooling room temperature obtains component C；
(4) component A, B and C obtained above are uniformly mixed, emulsifier is added, is placed in high pressure homogenizer, is heated to
55~65 DEG C, pressure condition is 18~22MPa；
(5) mixed material in (4) is warming up to 60~70 DEG C, is concentrated using double-effect falling film evaporator, will be concentrated
Mixed material afterwards is spray-dried.
The temperature that furnace heats melt in preferred steps (3) is 120~145 DEG C, and the time is 220~240s.
The first effect vacuum degree is 25~30kPa in preferred steps (5), and evaporating temperature is 65~75 DEG C；Second effect vacuum degree
For 55~60kPa, evaporating temperature is 35~45 DEG C.
The method of administration of inducer is immunized in the composite plant are as follows: from tillering stage to boot stage every 15 days with spraying pipeline spraying
Inducer is immunized in the composite plant that concentration is 104~110mg/L, and the amount of spraying is 18~22kg/ mus, every 20 after boot stage
Inducer is immunized with the composite plant that concentration of pipeline spraying is 68~70mg/L is sprayed in it, and the amount of spraying is 14~16kg/ mus.
The utility model has the advantages that
All material used in this preparation is all less toxic or non-toxic components, environmentally friendly, is not remained to crop exceeded
Danger；The present invention is aided with a variety of amino acid and sulphur using brown alga oligose, probenazole and lentinan as bacteriostatic active ingredients
Hydrochlorate, effectively can excite or activate the immune defense function of wheat itself, and enhancing wheat Rhizoctonia solani itself resists energy
Power.The composite plant is immunized inducer and is up to 95% or more to the resistance of wheat sharp eyespot, which has a extensive future,
With good economy and ecological benefits.
Specific embodiment
Below with reference to embodiment to the present invention make further in detail explanation, but case study on implementation the present invention is not done it is any
The restriction of form.
Embodiment 1:
The raw material that inducer includes following parts by weight: 10 parts of brown alga oligose, 20 parts of probenazole, perfume is immunized in composite plant
12 parts of mushroom polysaccharide, 14 parts of compound amino acid, 6 parts of composite sulfur hydrochlorate, 2 parts of emulsifier.
Wherein compound amino acid includes the raw material of following weight point: 6 parts of poly-aspartate, 3 parts of beta-aminobutyric acid, arginine
1.5 parts, 1.5 parts of valine, Cys2 part.
Wherein composite sulfur hydrochlorate is the raw material for including following weight point: 1 part of ferric sulfate, 3 parts of magnesium sulfate, 2 parts of zinc sulfate.
Emulsifier are as follows: castor oil polyoxyethylene ether and polyoxyethylene 20 sorbitan monolaurate, each half of ratio.
The preparation method of inducer is immunized in composite plant, includes the following steps:
(1) brown alga oligose, probenazole and lentinan are accurately weighed according to aforementioned proportion, is uniformly mixing to obtain mixing
Mixture is fully ground by object, is crossed 40 meshes, is obtained component A.
(2) poly-aspartate, beta-aminobutyric acid, arginine, valine and cysteine are weighed in strict accordance with aforementioned proportion,
It is soluble in water, obtain component B.
(3) ferric sulfate, magnesium sulfate, zinc sulfate are proportionally accurately weighed, the smelting furnace which puts into 125 DEG C is added
It is hot-melted 220s, the deionized water stirring 15min that temperature is 50 DEG C is added and is chelated, natural cooling room temperature obtains component
C。
(4) component A, B and C obtained above are uniformly mixed, emulsifier is added, is placed in high pressure homogenizer, is heated to
57 DEG C, pressure condition 18MPa.
(5) mixed material in (4) is warming up to 65 DEG C, is concentrated using double-effect falling film evaporator, the first effect vacuum
Degree is 25kPa, and evaporating temperature is 72 DEG C；Second effect vacuum degree is 55kPa, evaporating temperature is 35 DEG C, by the mixture after concentration
Material is spray-dried.
Method of administration are as follows: every 15 days are answering for 105mg/L with concentration of pipeline spraying is sprayed from tillering stage to boot stage
Plant immune inducer is closed, the amount of spraying is 22kg/ mus, is with concentration of pipeline spraying is sprayed within every 20 days after boot stage
Inducer is immunized in the composite plant of 68mg/L, and the amount of spraying is 14kg/ mus.
Embodiment 2:
The raw material that inducer includes following parts by weight: 13 parts of brown alga oligose, 22 parts of probenazole, perfume is immunized in composite plant
8 parts of mushroom polysaccharide, 9 parts of compound amino acid, 8 parts of composite sulfur hydrochlorate, 2.5 parts of emulsifier.
Wherein compound amino acid includes the raw material of following weight point: 3 parts of poly-aspartate, 2 parts of beta-aminobutyric acid, arginine
2 parts, 1 part of valine, 1 part of cysteine.
Wherein composite sulfur hydrochlorate is the raw material for including following weight point: 2 parts of ferric sulfate, 3 parts of magnesium sulfate, 3 parts of zinc sulfate.
Emulsifier uses geranyl butyrate, polyoxyethylene aliphatic alcohol ether, diacetyl tartarate monoglyceride, and ratio respectively accounts for
1/3。
The preparation method of inducer is immunized in composite plant, includes the following steps:
(1) brown alga oligose, probenazole and lentinan are accurately weighed according to aforementioned proportion, is uniformly mixing to obtain mixing
Mixture is fully ground by object, is crossed 55 meshes, is obtained component A.
(2) poly-aspartate, beta-aminobutyric acid, arginine, valine and cysteine are weighed in strict accordance with aforementioned proportion,
It is soluble in water, obtain component B.
(3) ferric sulfate, magnesium sulfate, zinc sulfate are proportionally accurately weighed, the smelting furnace which puts into 145 DEG C is added
It is hot-melted 230s, the deionized water stirring 20min that temperature is 48 DEG C is added and is chelated, natural cooling room temperature obtains component
C。
(4) component A, B and C obtained above are uniformly mixed, emulsifier is added, is placed in high pressure homogenizer, is heated to
63 DEG C, pressure condition 22MPa.
(5) mixed material in (4) is warming up to 70 DEG C, is concentrated using double-effect falling film evaporator, the first effect vacuum
Degree is 30kPa, evaporating temperature is 65 DEG C；Second effect vacuum degree is 58kPa, evaporating temperature is 37 DEG C, by the mixing after concentration
Material is spray-dried.
Method of administration are as follows: every 15 days are answering for 110mg/L with concentration of pipeline spraying is sprayed from tillering stage to boot stage
Plant immune inducer is closed, the amount of spraying is 21kg/ mus, is with concentration of pipeline spraying is sprayed within every 20 days after boot stage
Inducer is immunized in the composite plant of 69mg/L, and the amount of spraying is 16kg/ mus.
Embodiment 3:
The raw material that inducer includes following parts by weight: 10 parts of brown alga oligose, 20 parts of probenazole, perfume is immunized in composite plant
12 parts of mushroom polysaccharide, amino acid compound 18 part, 5 parts of composite sulfur hydrochlorate, 3 parts of emulsifier.
Wherein compound amino acid includes the raw material of following weight point: 6 parts of poly-aspartate, 3 parts of beta-aminobutyric acid, arginine
3 parts, 3 parts of valine, 3 parts of cysteine.
Wherein composite sulfur hydrochlorate is the raw material for including following weight point: 1 part of ferric sulfate, 2 parts of magnesium sulfate, 2 parts of zinc sulfate.
Emulsifier are as follows: calcium dodecyl benzene sulfonate and aliphatic acid polyethenoxy ether.
The preparation method of inducer is immunized in composite plant, includes the following steps:
(1) brown alga oligose, probenazole and lentinan are accurately weighed according to aforementioned proportion, is uniformly mixing to obtain mixing
Mixture is fully ground by object, is crossed 50 meshes, is obtained component A.
(2) poly-aspartate, beta-aminobutyric acid, arginine, valine and cysteine are weighed in strict accordance with aforementioned proportion,
It is soluble in water, obtain component B.
(3) ferric sulfate, magnesium sulfate, zinc sulfate are proportionally accurately weighed, the smelting furnace which puts into 130 DEG C is added
It is hot-melted 240s, the deionized water stirring 18min that temperature is 52 DEG C is added and is chelated, natural cooling room temperature obtains component
C。
(4) component A, B and C obtained above are uniformly mixed, emulsifier is added, is placed in high pressure homogenizer, is heated to
55 DEG C, pressure condition 20MPa.
(5) mixed material in (4) is warming up to 62 DEG C, is concentrated using double-effect falling film evaporator, the first effect vacuum
Degree is 28kPa, evaporating temperature is 75 DEG C；Second effect vacuum degree is 60kPa, evaporating temperature is 40 DEG C, by the mixing after concentration
Material is spray-dried.
Method of administration are as follows: every 15 days are answering for 108mg/L with concentration of pipeline spraying is sprayed from tillering stage to boot stage
Plant immune inducer is closed, the amount of spraying is 20kg/ mus, is with concentration of pipeline spraying is sprayed within every 20 days after boot stage
Inducer is immunized in the composite plant of 70mg/L, and the amount of spraying is 15kg/ mus.
Comparative example:
Control method of the jinggangmeisu to wheat sharp eyespot.
The measurement of embodiment and comparative example control method indices:
In areal, carried out at prevention according to wheat of the control method of embodiment and comparative example to same breed respectively
Reason counts the disease incidence of banded sclerotial blight and inspection respectively in the banded sclerotial blight wheat plant of the field of embodiment and comparative example plantation equivalent
Its control efficiency is surveyed, embodiment and comparative example control method indices measurement result is shown in Table 1.
Table 1: the measurement of embodiment and comparative example control method indices
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example |
| Banded sclerotial blight rate/(%) | 3 | 2 | 3 | 17 |
| Pesticide residue | It is not detected | It is not detected | It is not detected | Detection |
| Plant height (cm) | 105 | 106 | 106 | 95 |
| Setting percentage/(%) | 94.8 | 95.2 | 95.0 | 89.5 |
| Protein/(%) | 14.75 | 14.56 | 14.33 | 13.52 |
| Oil/(%) | 2.68 | 2.83 | 2.70 | 1.91 |
| Starch/(%) | 68.5 | 66.7 | 67.3 | 64.8 |
| Bulk density/(gL-1) | 793 | 789 | 783 | 769 |
| Save the cost/(%) | 12.3 | 12.7 | 12.5 | — |
Table 1 the result shows that, the control method effect of embodiment wheat sharp eyespot is than using traditional jinggangmeisu to prevent and treat
Effect is good, and the obvious relative scale of banded sclerotial blight rate is low, non agricultural chemical residuum, the plant height and wheat quality, that is, setting percentage, protein of wheat
Content, oil content and content of starch and bulk density have apparent advantage compared with comparative example, compared with embodiment more save the cost, say
The control method of bright wheat sharp eyespot provided by the invention has significant control efficiency.
Claims (7)
1. inducer is immunized in a kind of composite plant, it is characterised in that: the parts by weight of its raw material components and each component are respectively as follows: brown alga
10~15 parts of oligosaccharides, 18~22 parts of probenazole, 8~14 parts of lentinan, 8~19 parts of compound amino acid, composite sulfur hydrochlorate 5
~8 parts, 1~3 part of emulsifier.
2. inducer is immunized in composite plant according to claim 1, it is characterized in that: the compound amino acid includes following
The raw material of parts by weight: 3~6 parts of poly-aspartate, 2~4 parts of beta-aminobutyric acid, 1~3 part of arginine, 1~3 part of valine, half Guang
1~3 part of propylhomoserin.
3. inducer is immunized in composite plant according to claim 1, it is characterized in that: the composite sulfur hydrochlorate be include with
The raw material of lower parts by weight: 1~2 part of ferric sulfate, 2~3 parts of magnesium sulfate, 2~3 parts of zinc sulfate.
4. inducer is immunized in composite plant according to claim 1, it is characterized in that: the emulsifier are as follows: m-phenylene diamine (MPD),
Diacetyl tartarate monoglyceride, geranyl butyrate, castor oil polyoxyethylene ether, alkyl phenol polyoxyethylene ether sulfosuccinic acid
Ester, polyoxyethylene 20 sorbitan monolaurate, calcium dodecyl benzene sulfonate and aliphatic acid polyethenoxy ether or polyoxyethylene
One of fatty alcohol ether is a variety of.
5. a kind of method for preparing composite plant as described in claim 1 and inducer being immunized, the specific steps of which are as follows:
(1) brown alga oligose, probenazole and lentinan are proportionally accurately weighed, mixture is uniformly mixing to obtain, will be mixed
It closes object to be fully ground, crosses 40~70 meshes, obtain component A；
(2) to weigh compound amino acid according to aforementioned proportion soluble in water, obtains component B；
(3) composite sulfur hydrochlorate is proportionally accurately weighed, furnace heats fusing is put into, adding temperature is 48~52 DEG C
Deionized water stir 15~20min chelated, natural cooling obtains component C；
(4) component A, B and C obtained above are uniformly mixed, emulsifier is added, is placed in high pressure homogenizer, it is heated to 55~
65 DEG C, pressure condition is 18~22MPa；
(5) mixed material in (4) is warming up to 60~70 DEG C, is concentrated using double-effect falling film evaporator, after concentration
Mixed material is spray-dried.
6. according to the method described in claim 5, it is characterized in that the temperature that furnace heats melt in step (3) is 120~145
DEG C, the time is 220~240s.
7. according to the method described in claim 5, it is characterized in that the first effect vacuum degree is 25~30kPa, evaporation in step (5)
Temperature is 65~75 DEG C；Second effect vacuum degree is 55~60kPa, evaporating temperature is 35~45 DEG C.
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