CN109207249A - The physics cold pressing process of rapeseed oil - Google Patents

The physics cold pressing process of rapeseed oil Download PDF

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Publication number
CN109207249A
CN109207249A CN201710540952.6A CN201710540952A CN109207249A CN 109207249 A CN109207249 A CN 109207249A CN 201710540952 A CN201710540952 A CN 201710540952A CN 109207249 A CN109207249 A CN 109207249A
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CN
China
Prior art keywords
oil
rape oil
rape
temperature
vegetable seed
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Pending
Application number
CN201710540952.6A
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Chinese (zh)
Inventor
王元银
王维
王超
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Wangmo Buyiwang Grease Co Ltd
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Wangmo Buyiwang Grease Co Ltd
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Priority to CN201710540952.6A priority Critical patent/CN109207249A/en
Publication of CN109207249A publication Critical patent/CN109207249A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/06Production of fats or fatty oils from raw materials by pressing
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/008Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Microbiology (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses a kind of physics cold pressing process of rapeseed oil, method includes the following steps: the vegetable seed of acquisition is dried, promote vegetable seed after-ripening;The vegetable seed of after-ripening is carried out to the crude oil obtained after cleaning removes using cold press process squeezing rapeseed;In temperature it is 30 DEG C by crude oil, is filtered using 50 mesh or 60 mesh filter clothes and obtains semi-finished product rape oil with brilliant growing the grain;Semi-finished product rape oil is introduced into the warm bucket that temperature is 280 DEG C -380 DEG C, adjusting revolving speed is 30/min, semi-finished product rape oil is disposably decolourized, depickling, degumming, deodorization, is filtered to obtain rape oil using 100 mesh, rape oil is introduced into the insulation barrel that temperature is 50 DEG C, pure rape oil must be refined by multiple filtration.The present invention is simple and easy to do, does not lose the nutrition in oil in expressing process, does not generate secondary pollution in refining process, and the limpid appearance luster of rapeseed oil true qualities is presented in obtained squeezing rape oil.

Description

The physics cold pressing process of rapeseed oil
Technical field
The present invention relates to the processing technique fields of rapeseed oil, relate in particular to a kind of physics cold pressing process of rapeseed oil.
Background technique
Currently, people pay attention to edible oil it is healthy and safe it is more be tea-seed oil and rapeseed oil.Rapeseed oil is using rape Seed squeezing processing after obtained oil, also known as rape oil, generally conventional rape oil processing method is to dry the vegetable seed after acquisition, Steaming fries, rolls embryo, squeezing, Dip goes out, the processes production such as addition active matter carclazyte is oily in refining process,
The method of existing rape oil expression, which is still in, will pass through the stage of steaming and frying technique in vegetable seed, and steams the high temperature fried and hold The nutritional ingredient in oil is easily lost, affects fragrance and the shelf-life of active material and rape itself, traditional refinery practice is also The crude oil come of squeezing out is dried in vacuo, add the chemical components such as carclazyte, alkali, salt, water, vacuum decoloration, high temperature high vacuum The process flows such as deodorization processing, equally can be to palmitinic acid C16:0, linoleic acid C18:2, the erucic acid C22:1, wood tar in hair rape oil The effective ingredients such as sour C24:0 cause largely to lose, in addition, containing more impurity, vegetable seed scurf, phosphatide, trip in hair rape oil From fatty acid, carbohydrate, moisture content, protein and their degradation product, oxide, the appearance luster of oil is not only affected, Also directly second of pollution of contact oil, influences the interior quality of oil, it is therefore desirable to remove from office to existing rape oil squeezing process Newly.
Summary of the invention
It the purpose of the present invention is overcoming above-mentioned technological deficiency, provides a kind of simple and easy to do, is not lost in oil in expressing process Nutrition, do not generate secondary pollution in refining process, the limpid appearance color of rapeseed oil true qualities is presented in obtained squeezing rape oil Rape oil mark is squeezed better than DB53/T 288-2009, GB/T23373-2009, GB/T22460-2008, GB/T 5530-2005 in pool The physics cold pressing process of quasi- rapeseed oil.
Realize the physics cold pressing process the technical solution of the present invention is as follows: a kind of rapeseed oil, method includes the following steps:
(1) vegetable seed of acquisition is dried, the biochemical basis acted on using seed afterripening promotes vegetable seed after-ripening;
(2) vegetable seed of after-ripening is subjected to cleaning removal of impurities, rapeseed is squeezed using cold press process;
(3) crude oil and rape cake that the vegetable seed after squeezing is collected;
(4) it is 30 DEG C in temperature by crude oil, is filtered using 50 mesh or 60 mesh filter clothes and obtains semi-finished product rape oil with brilliant growing the grain;
(5) semi-finished product rape oil is introduced into the warm bucket that temperature is 280 DEG C -380 DEG C, adjusting revolving speed is 30/min, by semi-finished product Rape oil disposably decolourizes, depickling, degumming, deodorization, is filtered to obtain rape oil using 100 mesh, and it is 50 DEG C that rape oil, which is introduced temperature, Insulation barrel must refine pure rape oil by multiple filtration.
It preferably, further include drying vegetable seed to be placed on 0 DEG C -20 DEG C of low temperature environment and store to dish in the step (1) Seed after-ripening.
Preferably, vegetable seed after-ripening to aridity is 80-85% in the step (1).
Preferably, the temperature of cold press process described in the step (2) is 18-33 DEG C.
Preferably, semi-finished product rape oil is introduced into the warm bucket that temperature is 380 DEG C in the step (5), adjusting revolving speed is 30/ Semi-finished product rape oil is disposably decolourized, depickling, degumming, deodorization, is filtered to obtain rape oil using 100 mesh, rape oil is introduced by min The insulation barrel that temperature is 50 DEG C, must refine pure rape oil by multiple filtration.
The invention also discloses a kind of rapeseed oils, it is to process to obtain by the physics cold pressing process of any of the above-described kind of rapeseed oil 's.
Compared with prior art, the beneficial effects of the present invention are: 1, by the way that vegetable seed is dried, utilize seed afterripening effect Biochemical basis promotes vegetable seed after-ripening, improves raw material vegetable seed quality, ensure that material quality;2, the vegetable seed bits shadow in dark pool is avoided Ring product color;3, the inferior vegetable seed raw material of mildew is avoided to enter in production technology, ensure that squeezing crude oil quality and Mitigate cost of investment;4, rapeseed oil color depth and burning are avoided, ensure that rapeseed oil intrinsic smell and flavour;5, disposable 280 DEG C of -380 DEG C of high temperature, 50 DEG C of filter at low temperature refining techniques avoid caustic soda in normal refinery activities, salt depickling, carclazyte activity The pollution that chemical substance caused by water decolorization technique is directly contacted with rapeseed oil, at the same also avoid the vacuum drying in tradition, The distortion of vegetable seed incense oil taste when vacuum decoloration, high-temperature vacuum deodorization, be effectively retained the following fatty acid of 14 carbon in rapeseed oil, Palmitinic acid C16:0, palm monoenoic acid C16:1, lignoceric acid C24:0 erucic acid C22:1, stearic acid C18:0, oleic acid C18:1 etc. have Imitate composition;The limpid appearance luster of rapeseed oil true qualities is presented in squeezing rape oil through examining the present invention to obtain, is better than DB53/T 288- 2009, GB/T23373-2009, GB/T22460-2008, GB/T 5530-2005 squeeze rape oil standard.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention.Based on the implementation in the present invention Example, those skilled in the art's every other embodiment obtained without making creative work, belongs to this hair The range of bright protection.
Embodiment 1:
1, the vegetable seed for acquiring 100 kilograms dries, and stores through 0 DEG C -20 DEG C of low temperature environments, utilizes vegetable seeds afterripening Biochemical basis promote rapeseed after-ripening to aridity be 80%;
2, after the rapeseed of after-ripening being carried out cleaning removal of impurities, under conditions of temperature is 18-33 DEG C, cold press process pressure is utilized Hot pickled mustard tuber seed;
3, the vegetable seed after squeezing carries out the crude oil and rape cake that separate collection obtains;
4, will be 30 DEG C in temperature, using the filter cloth of 50 mesh be filtered with brilliant growing the grain, obtain semi-finished product hair rape oil;
5, by semi-finished product hair rape oil introduce temperature be 380 DEG C of temperature control buckets, adjust revolving speed 30/min rape oil is disposably decolourized, Depickling, deodorization are filtered to obtain rape oil using 100 mesh, and rape oil is then introduced the insulation barrel that temperature is 50 DEG C and carries out multilayer mistake Filter to obtain the pure rape oil of refining.
Embodiment 2:
1, the vegetable seed for acquiring 100 kilograms dries, and after removal of impurities, stores through 0 DEG C -20 DEG C of low temperature environments, utilizes vegetable seeds It is 82% that the biochemical basis of afterripening, which promotes rapeseed after-ripening to aridity,;
2, after the rapeseed of after-ripening being carried out cleaning removal of impurities, under conditions of temperature is 18-33 DEG C, cold press process pressure is utilized Hot pickled mustard tuber seed;
3, the vegetable seed after squeezing carries out the crude oil and rape cake that separate collection obtains;
4, will be 30 DEG C in temperature, using the filter cloth of 60 mesh be filtered with brilliant growing the grain, obtain semi-finished product hair rape oil;
5, semi-finished product hair rape oil is introduced temperature is 280 DEG C of temperature control buckets, setting speed 30/min disposably decolourizes rape oil, Depickling, deodorization are filtered to obtain rape oil using 100 mesh, after by rape oil introduce temperature be 50 DEG C insulation barrel carry out multiple filtration Pure rape oil must be refined.
Embodiment 3:
1, the vegetable seed for acquiring 100 kilograms dries, and after removal of impurities, stores through 0 DEG C -20 DEG C of low temperature environments, utilizes vegetable seeds It is 85% that the biochemical basis of afterripening, which promotes rapeseed after-ripening to aridity,;
2, after the rapeseed of after-ripening being carried out cleaning removal of impurities, under conditions of temperature is 18-33 DEG C, cold press process pressure is utilized Hot pickled mustard tuber seed;
3, the vegetable seed after squeezing carries out the crude oil and rape cake that separate collection obtains;
4, will be 30 DEG C in temperature, using the filter cloth of 60 mesh be filtered with brilliant growing the grain, obtain semi-finished product hair rape oil;
5, semi-finished product hair rape oil is introduced temperature is 300 DEG C of temperature control buckets, setting speed 30/min disposably decolourizes rape oil, Depickling, deodorization are filtered to obtain rape oil using 100 mesh, after by rape oil introduce temperature be 50 DEG C insulation barrel carry out multiple filtration Pure rape oil must be refined.
Embodiment 4:
1, the vegetable seed for acquiring 100 kilograms dries;Promote rapeseed after-ripening using the biochemical basis of vegetable seeds afterripening;
2, after the rapeseed of after-ripening being carried out cleaning removal of impurities, vegetable seed is squeezed according to conventional cold press process;
3, the vegetable seed after squeezing carries out the crude oil and rape cake that separate collection obtains;
4, will be 30 DEG C in temperature, using the filter cloth of 60 mesh be filtered with brilliant growing the grain, obtain semi-finished product hair rape oil;
5, semi-finished product hair rape oil is introduced temperature is 260 DEG C of temperature control buckets, setting speed 30/min disposably decolourizes rape oil, Depickling, deodorization are filtered to obtain rape oil using 100 mesh, after by rape oil introduce temperature be 50 DEG C insulation barrel carry out multiple filtration Pure rape oil must be refined.
Embodiment 5:
1, the vegetable seed for acquiring 100 kilograms dries;
2, after rapeseed being carried out cleaning removal of impurities, vegetable seed is squeezed according to conventional cold press process;
3, the vegetable seed after squeezing carries out the crude oil and rape cake that separate collection obtains;
4, will be 30 DEG C in temperature, using the filter cloth of 50 mesh be filtered with brilliant growing the grain, obtain semi-finished product hair rape oil;
5, semi-finished product hair rape oil is introduced temperature is 400 DEG C of temperature control buckets, setting speed 30/min disposably decolourizes rape oil, Depickling, deodorization are filtered to obtain rape oil using 100 mesh, after by rape oil introduce temperature be 50 DEG C insulation barrel carry out multiple filtration Pure rape oil must be refined.
Finally the rapeseed oil in embodiment 1 to 5 is collected, the oil yield of embodiment 1 to 5 is followed successively by 45%, 43%, 44%, 40%, 36%, it finally randomly selects the pure rape oil obtained after embodiment 1 to 3 refines and tests, as a result such as table 1 and table Shown in 2:
Table 1: the result of rapeseed oil detection;
Table 2: fatty acid forms in rape oil:
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims (6)

1. a kind of physics cold pressing process of rapeseed oil, which is characterized in that method includes the following steps:
(1) vegetable seed of acquisition is dried, the biochemical basis acted on using seed afterripening promotes vegetable seed after-ripening;
(2) vegetable seed of after-ripening is subjected to cleaning removal of impurities, rapeseed is squeezed using cold press process;
(3) crude oil and rape cake that the vegetable seed after squeezing is collected;
(4) it is 30 DEG C in temperature by crude oil, is filtered using 50 mesh or 60 mesh filter clothes and obtains semi-finished product rape oil with brilliant growing the grain;
(5) semi-finished product rape oil is introduced into the warm bucket that temperature is 280 DEG C -380 DEG C, adjusting revolving speed is 30/min, by semi-finished product rape oil Disposable decoloration, depickling, degumming, deodorization, are filtered to obtain rape oil using 100 mesh, and rape oil is introduced the heat preservation that temperature is 50 DEG C Bucket, must refine pure rape oil by multiple filtration.
2. the physics cold pressing process of rapeseed oil according to claim 1, it is characterised in that: further include in the step (1) by Vegetable seed, which dries, to be placed on 0 DEG C -20 DEG C of low temperature environment and stores to vegetable seed after-ripening.
3. the physics cold pressing process of rapeseed oil according to claim 1 or claim 2, it is characterised in that: in the step (1) after vegetable seed It is ripe to aridity be 80-85%.
4. the physics cold pressing process of rapeseed oil according to claim 3, it is characterised in that: cold press described in the step (2) The temperature of process is 18-33 DEG C.
5. the physics cold pressing process of rapeseed oil according to claim 3, it is characterised in that: by semi-finished product in the step (5) It is 380 DEG C of warm bucket that rape oil, which introduces temperature, and adjustings revolving speed is 30/min, semi-finished product rape oil is disposably decolourized, depickling, degumming, Deodorization, is filtered to obtain rape oil using 100 mesh, and rape oil is introduced the insulation barrel that temperature is 50 DEG C, must be refined by multiple filtration Pure rape oil.
6. a kind of rapeseed oil, which is characterized in that it is the physics cold pressing process processing by any one of claim 1 to 5 rapeseed oil It obtains.
CN201710540952.6A 2017-07-05 2017-07-05 The physics cold pressing process of rapeseed oil Pending CN109207249A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110903900A (en) * 2019-12-17 2020-03-24 湖南林邑新能源有限公司 Method for refining tung oil

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1827754A (en) * 2006-03-27 2006-09-06 郴州邦尔泰苏仙油脂有限公司 Physical low-temperature cold-squeezing process for tea-seed oil
CN103666749A (en) * 2013-12-31 2014-03-26 贵州省黎平县侗乡米业有限公司 Processing process for rapeseed oil

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1827754A (en) * 2006-03-27 2006-09-06 郴州邦尔泰苏仙油脂有限公司 Physical low-temperature cold-squeezing process for tea-seed oil
CN103666749A (en) * 2013-12-31 2014-03-26 贵州省黎平县侗乡米业有限公司 Processing process for rapeseed oil

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
朱文鑫 等: "油菜籽直接冷榨制油工艺的研究与应用", 《中国油脂》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110903900A (en) * 2019-12-17 2020-03-24 湖南林邑新能源有限公司 Method for refining tung oil

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Application publication date: 20190115