CN109206235A - A kind of humic acid Macroelement water-soluble fertilizer and preparation method thereof - Google Patents
A kind of humic acid Macroelement water-soluble fertilizer and preparation method thereof Download PDFInfo
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- CN109206235A CN109206235A CN201811262432.4A CN201811262432A CN109206235A CN 109206235 A CN109206235 A CN 109206235A CN 201811262432 A CN201811262432 A CN 201811262432A CN 109206235 A CN109206235 A CN 109206235A
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- humic acid
- water
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- soluble fertilizer
- potassium
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
Present invention relates particularly to a kind of humic acid Macroelement water-soluble fertilizers and preparation method thereof, belong to technical field of fertilizers, technical problem to be solved is good to provide a kind of stability, high water solubility, the high humic acid Macroelement water-soluble fertilizer and preparation method thereof of fertilizer efficiency, a kind of technical solution of use are as follows: humic acid Macroelement water-soluble fertilizer, raw material including following parts by weight: 6~10 parts of humic acid potassium, 30~45 parts of dipotassium hydrogen phosphate, 4~6 parts of potassium chloride, 8~10 parts of microelement, 0.6~1 part of synergist, 1.8~2.5 parts of plant modifying agent, 25.5~50 parts of water；The microelement is eight Boratex of ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt and four water；The present invention is used to provide required nutriment for crop, can improve soil texture, increases crop yield, improves crops quality, and good water solubility, fertilizer efficiency are high.
Description
Technical field
The present invention relates to technical field of fertilizers, and in particular to a kind of humic acid Macroelement water-soluble fertilizer and its preparation side
Method.
Background technique
Humic acid water-soluble fertilizer is a kind of novel and multifunctional fertilizer containing humic acid substance, recently as ecology
Agricultural and the yield and demand of the humic acid water-soluble fertilizer of one of environmental friend fertilizer kind increase year by year, existing humic acid
Although water-soluble fertilizer has improvement soil texture, improves salinized soil, reduce perniciousness harm, improve crop anti-adversity, increase yield
And the advantages that improving crops quality, but poorly water-soluble, fertilizer efficiency are low.
Summary of the invention
The high corruption of good, high water solubility that the invention overcomes the deficiencies of the prior art, and provides a kind of stability, fertilizer efficiency
Phytic acid Macroelement water-soluble fertilizer and preparation method thereof.
In order to solve the above-mentioned technical problem, a kind of the technical solution adopted by the present invention are as follows: humic acid Macroelement water-soluble
Fertilizer, the raw material including following parts by weight:
6~10 parts of humic acid potassium, 30~45 parts of dipotassium hydrogen phosphate, 4~6 parts of potassium chloride, 8~10 parts of microelement, synergist 0.6
~1 part, 1.8~2.5 parts of plant modifying agent, 25.5~50 parts of water.
The microelement is eight Boratex of ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt and four water.
The synergist is sodium salicylate.
The plant modifying agent is brassin lactones, α-Nafusaku and compound sodium nitrophenolate.
The humic acid potassium is mineral resources fulvic acid potassium, humic acid >=50.0%, potassium oxide >=10.0%.
The microelement ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt, four water, eight Boratex weight ratio be
3:5:2。
The plant modifying agent is 0.1% brassin lactones, 98% α-Nafusaku and 98% compound sodium nitrophenolate.
A kind of preparation method of humic acid Macroelement water-soluble fertilizer, comprising the following steps:
1) it by the humic acid potassium and water addition reactor tank after weighing, dissolves by heating, dipotassium hydrogen phosphate is added under agitation, protect
60~70 DEG C of temperature are held, reaction to dissolution of raw material；
2) above-mentioned steps 1 are added in potassium chloride and synergist) solution in, kept for 60~70 DEG C of temperature, reaction to dissolution of raw material；
3) under conditions of continuous heating and stirring, by microelement be added above-mentioned steps 2) solution in, react it is molten to raw material
Solution；
4) plant modifying agent is added in warm water and will be dissolved, above-mentioned steps 3 are then added) in resulting solution, persistently stir 0.5~
It 1.5 hours, is cooled to room temperature later to get humic acid Macroelement water-soluble fertilizer.
The present invention has the advantages that compared with prior art.
One, water soluble fertilizer prepared by the present invention is not only containing elements such as nitrogen, phosphorus needed for plant, potassium, zinc, manganese and boron,
And mineral resources potassium fulvate and plant growth regulator with chelation, absorb fast, efficient, high-quality, water-saving and volume increase effect
Fruit is significant.
Two, water soluble fertilizer prepared by the present invention can satisfy demand of the fruit growth period to various nutrition, solve crop
Later period is de- fertile and lacks malnutrition and teratogenesis caused by nutrient, and flower and fruit protecting, swollen fruit is hyperchromic, increases sugared deacidification, mentions
Early ripe improves commodity rate.
Three, water soluble fertilizer cold-resistant drought resisting prepared by the present invention, hot-dry wind tolerance, anti-continuous cropping ability is strong, promotes crop root
Growth enhances crop photosynthesis, is conducive to crop growth, can reduce the infection probability of crop disease and insect.
Four, water soluble fertilizer prepared by the present invention is in Chelating state, can be to avoid due to soil acidity or alkalinity, water content and micro-
The influence of biology and be fixed, and avoid leaching, improve fertilizer efficiency.
Five, water soluble fertilizer utilization rate prepared by the present invention is high, can foliage-spray, punching applies, and disappear fillings, reduces investment, increase
Output improves crop quality, increases economic efficiency.
Specific embodiment
Below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
A kind of humic acid Macroelement water-soluble fertilizer, the raw material including following parts by weight:
6 parts of humic acid potassium, 30 parts of dipotassium hydrogen phosphate, 4 parts of potassium chloride, 8 parts of microelement, 0.6 part of synergist, plant modifying agent
1.8 parts, 50 parts of water.
The microelement is eight Boratex of ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt and four water.
The synergist is sodium salicylate.
The plant modifying agent is brassin lactones, α-Nafusaku and compound sodium nitrophenolate.
The humic acid potassium is mineral resources fulvic acid potassium, humic acid >=50.0%, potassium oxide >=10.0%.
The microelement ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt, four water, eight Boratex weight ratio be
3:5:2。
The plant modifying agent is 0.1% brassin lactones, 98% α-Nafusaku and 98% compound sodium nitrophenolate.
A kind of preparation method of humic acid Macroelement water-soluble fertilizer, comprising the following steps:
1) it by the humic acid potassium and water addition reactor tank after weighing, dissolves by heating, dipotassium hydrogen phosphate is added under agitation, protect
60~70 DEG C of temperature are held, reaction to dissolution of raw material；
2) above-mentioned steps 1 are added in potassium chloride and synergist) solution in, kept for 60~70 DEG C of temperature, reaction to dissolution of raw material；
3) under conditions of continuous heating and stirring, by microelement be added above-mentioned steps 2) solution in, react it is molten to raw material
Solution；
4) plant modifying agent is added in warm water and will be dissolved, above-mentioned steps 3 are then added) in resulting solution, it is small persistently to stir 0.5
When, it is cooled to room temperature later to get humic acid Macroelement water-soluble fertilizer.
Embodiment 2
A kind of humic acid Macroelement water-soluble fertilizer, the raw material including following parts by weight:
10 parts of humic acid potassium, 45 parts of dipotassium hydrogen phosphate, 6 parts of potassium chloride, 10 parts of microelement, 1 part of synergist, plant modifying agent
2.5 parts, 25.5 parts of water.
The microelement is eight Boratex of ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt and four water.
The synergist is sodium salicylate.
The plant modifying agent is brassin lactones, α-Nafusaku and compound sodium nitrophenolate.
The humic acid potassium is mineral resources fulvic acid potassium, humic acid >=50.0%, potassium oxide >=10.0%.
The microelement ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt, four water, eight Boratex weight ratio be
3:5:2。
The plant modifying agent is 0.1% brassin lactones, 98% α-Nafusaku and 98% compound sodium nitrophenolate.
A kind of preparation method of humic acid Macroelement water-soluble fertilizer, comprising the following steps:
1) it by the humic acid potassium and water addition reactor tank after weighing, dissolves by heating, dipotassium hydrogen phosphate is added under agitation, protect
60~70 DEG C of temperature are held, reaction to dissolution of raw material；
2) above-mentioned steps 1 are added in potassium chloride and synergist) solution in, kept for 60~70 DEG C of temperature, reaction to dissolution of raw material；
3) under conditions of continuous heating and stirring, by microelement be added above-mentioned steps 2) solution in, react it is molten to raw material
Solution；
4) plant modifying agent is added in warm water and will be dissolved, above-mentioned steps 3 are then added) in resulting solution, it is small persistently to stir 1
When, it is cooled to room temperature later to get humic acid Macroelement water-soluble fertilizer.
Embodiment 3
A kind of humic acid Macroelement water-soluble fertilizer, the raw material including following parts by weight:
7 parts of humic acid potassium, 32 parts of dipotassium hydrogen phosphate, 5 parts of potassium chloride, 9 parts of microelement, 0.7 part of synergist, plant modifying agent
2.0 parts, 44.5 parts of water.
The microelement is eight Boratex of ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt and four water.
The synergist is sodium salicylate.
The plant modifying agent is brassin lactones, α-Nafusaku and compound sodium nitrophenolate.
The humic acid potassium is mineral resources fulvic acid potassium, humic acid >=50.0%, potassium oxide >=10.0%.
The microelement ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt, four water, eight Boratex weight ratio be
3:5:2。
The plant modifying agent is 0.1% brassin lactones, 98% α-Nafusaku and 98% compound sodium nitrophenolate.
A kind of preparation method of humic acid Macroelement water-soluble fertilizer, comprising the following steps:
1) it by the humic acid potassium and water addition reactor tank after weighing, dissolves by heating, dipotassium hydrogen phosphate is added under agitation, protect
60~70 DEG C of temperature are held, reaction to dissolution of raw material；
2) above-mentioned steps 1 are added in potassium chloride and synergist) solution in, kept for 60~70 DEG C of temperature, reaction to dissolution of raw material；
3) under conditions of continuous heating and stirring, by microelement be added above-mentioned steps 2) solution in, react it is molten to raw material
Solution；
4) plant modifying agent is added in warm water and will be dissolved, above-mentioned steps 3 are then added) in resulting solution, it is small persistently to stir 1.5
When, it is cooled to room temperature later to get humic acid Macroelement water-soluble fertilizer.
Embodiment 4
A kind of humic acid Macroelement water-soluble fertilizer, the raw material including following parts by weight:
8 parts of humic acid potassium, 36 parts of dipotassium hydrogen phosphate, 4 parts of potassium chloride, 8 parts of microelement, 0.8 part of synergist, plant modifying agent
2.2 parts, 41 parts of water.
The microelement is eight Boratex of ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt and four water.
The synergist is sodium salicylate.
The plant modifying agent is brassin lactones, α-Nafusaku and compound sodium nitrophenolate.
The humic acid potassium is mineral resources fulvic acid potassium, humic acid >=50.0%, potassium oxide >=10.0%.
The microelement ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt, four water, eight Boratex weight ratio be
3:5:2。
The plant modifying agent is 0.1% brassin lactones, 98% α-Nafusaku and 98% compound sodium nitrophenolate.
Embodiment 5
A kind of humic acid Macroelement water-soluble fertilizer, the raw material including following parts by weight:
9 parts of humic acid potassium, 40 parts of dipotassium hydrogen phosphate, 6 parts of potassium chloride, 9 parts of microelement, 0.9 part of synergist, plant modifying agent
2.4 parts, 50 parts of water.
The microelement is eight Boratex of ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt and four water.
The synergist is sodium salicylate.
The plant modifying agent is brassin lactones, α-Nafusaku and compound sodium nitrophenolate.
The humic acid potassium is mineral resources fulvic acid potassium, humic acid >=50.0%, potassium oxide >=10.0%.
The microelement ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt, four water, eight Boratex weight ratio be
3:5:2。
The plant modifying agent is 0.1% brassin lactones, 98% α-Nafusaku and 98% compound sodium nitrophenolate.
Embodiment 6
Field trial:
It is 5 years Sheng Kelunsheng grapes for studying object, is humic acid Macroelement water-soluble fertilizer prepared by the present invention for examination fertilizer；
Experimental field select: certain large-scale grape-planting regions, the plot topography is flat, and fertility is uniform, and experimental field soil is middle loamy texture
Black earth soil, soil physico-chemical property: alkali-hydrolyzable nitrogen 30mg/kg, available potassium 183mg/kg, organic matter 4.1g/kg, pH value 8.4.
Test group 1: local habits fertilization+application humic acid Macroelement water-soluble fertilizer prepared by the present invention, humic acid
Macroelement water-soluble fertilizer ampoule is 100g/ mus, dilutes 500 times of liquid, blade face uniformly sprays, is repeated 3 times, test group 1
Area 30m2；
Control group 1: local habits fertilization+foliage-spray clear water, clear water ampoule are 100g/ mus, are repeated 3 times, 1 face of control group
Product 30m2；
Test group 2: applying humic acid Macroelement water-soluble fertilizer prepared by the present invention, and usage amount is 10Kg/ mus, trickle irrigation, weight
It is 3 times multiple, 2 area 30m of test group2。
Control group 2: application clear water, usage amount are 10Kg/ mus, and trickle irrigation is repeated 3 times, 2 area 30m of control group2。
Test group and control group use equivalent water and fertilizer management measure and equivalent pest control method.
| Control project | Grain number per spike | Simple grain weight | Spike weight amount | Strain produces | Pol | Tinctorial yield | Per mu yield |
| Unit | It is a | g | kg | kg | % | % | kg |
| Test group 1 | 166 | 6.8 | 1.13 | 4.52 | 18 | 98 | 5048 |
| Control group 1 | 160 | 6.2 | 0.99 | 3.96 | 16 | 92 | 4513 |
As seen from the above table, using foliage dressing, the grape growing way and quality of test group 1 are better than control group 1, tinctorial yield yield
Higher than control group 1, test group 1 does sth. in advance maturation 3~5 days, and rate of growth is 10% or more.
| Control project | Grain number per spike | Simple grain weight | Spike weight amount | Strain produces | Pol | Tinctorial yield | Per mu yield |
| Unit | It is a | g | kg | kg | % | % | kg |
| Test group 2 | 190 | 7.2 | 1.37 | 5.48 | 20 | 98 | 5160 |
| Control group 2 | 185 | 6.8 | 1.26 | 5.04 | 18 | 94 | 4415 |
As seen from the above table, using fertigation, 2 grape growing way of test group and quality are substantially better than control group 2, tinctorial yield,
Sugar content, yield is obviously higher than control group 2, and test group 2 does sth. in advance 7~10 days mature, 15% or more volume increase.
Above embodiment is merely exemplary to illustrate the principle of the present invention and its effect, and is not intended to limit the present invention.For
Person skilled in the art all without departing from the spirit and scope of the present invention, modifies above-described embodiment or is improved.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by tool usually intellectual in all act technical fields
At all equivalent modifications or change, should be covered by the claims of the present invention.
Claims (8)
1. a kind of humic acid Macroelement water-soluble fertilizer, which is characterized in that the raw material including following parts by weight:
6~10 parts of humic acid potassium, 30~45 parts of dipotassium hydrogen phosphate, 4~6 parts of potassium chloride, 8~10 parts of microelement, synergist 0.6
~1 part, 1.8~2.5 parts of plant modifying agent, 25.5~50 parts of water.
2. a kind of humic acid Macroelement water-soluble fertilizer according to claim 1, which is characterized in that the microelement
For eight Boratex of ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt and four water.
3. a kind of humic acid Macroelement water-soluble fertilizer according to claim 1, which is characterized in that the synergist is
Sodium salicylate.
4. a kind of humic acid Macroelement water-soluble fertilizer according to claim 1, which is characterized in that the plant is adjusted
Agent is brassin lactones, α-Nafusaku and compound sodium nitrophenolate.
5. a kind of humic acid Macroelement water-soluble fertilizer according to claim 1, which is characterized in that the humic acid potassium
For mineral resources fulvic acid potassium, humic acid >=50.0%, potassium oxide >=10.0%.
6. a kind of humic acid Macroelement water-soluble fertilizer according to claim 1 or 2, which is characterized in that described micro-
Secondary element ethylenediamine tetra-acetic acid manganese salt, ethylenediamine tetra-acetic acid zinc salt, four water, eight Boratex weight ratio be 3:5:2.
7. according to claim 1 or a kind of humic acid Macroelement water-soluble fertilizer described in 4, which is characterized in that the plant
Object regulator is 0.1% brassin lactones, 98% α-Nafusaku and 98% compound sodium nitrophenolate.
8. a kind of preparation side of humic acid Macroelement water-soluble fertilizer according to any one of claims 1 to 5
Method, which comprises the following steps:
1) it by the humic acid potassium and water addition reactor tank after weighing, dissolves by heating, dipotassium hydrogen phosphate is added under agitation, protect
60~70 DEG C of temperature are held, reaction to dissolution of raw material；
2) above-mentioned steps 1 are added in potassium chloride and synergist) solution in, kept for 60~70 DEG C of temperature, reaction to dissolution of raw material；
3) under conditions of continuous heating and stirring, by microelement be added above-mentioned steps 2) solution in, react it is molten to raw material
Solution；
4) plant modifying agent is added in warm water and will be dissolved, above-mentioned steps 3 are then added) in resulting solution, persistently stir 0.5~
It 1.5 hours, is cooled to room temperature, is packed up to humic acid Macroelement water-soluble fertilizer later.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811262432.4A CN109206235A (en) | 2018-10-27 | 2018-10-27 | A kind of humic acid Macroelement water-soluble fertilizer and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811262432.4A CN109206235A (en) | 2018-10-27 | 2018-10-27 | A kind of humic acid Macroelement water-soluble fertilizer and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110240518A (en) * | 2019-06-24 | 2019-09-17 | 戴斌 | A kind of high-efficiency multi-function plant leaf surface sprays hyperconcetration fertilizer and preparation method thereof |
| CN111328816A (en) * | 2020-04-10 | 2020-06-26 | 雷晓芳 | Fulic acid water-retaining plant seed growth additive and preparation method thereof |
| CN114213183A (en) * | 2022-01-05 | 2022-03-22 | 深圳市芭田生态工程股份有限公司 | Fertilizer and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101798246A (en) * | 2010-03-16 | 2010-08-11 | 陕西鼎华慧农生物科技有限公司 | Water-soluble fertilizer by complexing humic acid with plurality of nutrient elements and preparation method thereof |
| CN106518407A (en) * | 2016-11-20 | 2017-03-22 | 曲沃县万乡红肥业有限公司 | High-stability and high-concentration humic-acid-containing water-soluble fertilizer and production method thereof |
-
2018
- 2018-10-27 CN CN201811262432.4A patent/CN109206235A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101798246A (en) * | 2010-03-16 | 2010-08-11 | 陕西鼎华慧农生物科技有限公司 | Water-soluble fertilizer by complexing humic acid with plurality of nutrient elements and preparation method thereof |
| CN106518407A (en) * | 2016-11-20 | 2017-03-22 | 曲沃县万乡红肥业有限公司 | High-stability and high-concentration humic-acid-containing water-soluble fertilizer and production method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110240518A (en) * | 2019-06-24 | 2019-09-17 | 戴斌 | A kind of high-efficiency multi-function plant leaf surface sprays hyperconcetration fertilizer and preparation method thereof |
| CN111328816A (en) * | 2020-04-10 | 2020-06-26 | 雷晓芳 | Fulic acid water-retaining plant seed growth additive and preparation method thereof |
| CN114213183A (en) * | 2022-01-05 | 2022-03-22 | 深圳市芭田生态工程股份有限公司 | Fertilizer and preparation method and application thereof |
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