CN109173954A - Intelligent rapid digestion device - Google Patents
Intelligent rapid digestion device Download PDFInfo
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- CN109173954A CN109173954A CN201811286317.0A CN201811286317A CN109173954A CN 109173954 A CN109173954 A CN 109173954A CN 201811286317 A CN201811286317 A CN 201811286317A CN 109173954 A CN109173954 A CN 109173954A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/002—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by condensation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00054—Controlling or regulating the heat exchange system
- B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
- B01J2219/00058—Temperature measurement
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Abstract
The present invention relates to a kind of intelligent rapid digestion devices, it is characterised in that: slaking apparatus is connected with cooling device；Lifting device is located at slaking apparatus and cooling device middle upper part is fixed on the rear side of slaking apparatus；There is air duct between the digestion furnace body and shell of slaking apparatus, blower fan is fixedly connected in the air duct of outer casing inner wall；Above the interlayer that the shell of the cooling bath of cooling device and cooling bath are formed or setting has fan on wall side wall inside the shell, and cooling bath inner wall is equipped with air holes, and the lifting column of lifting device is fixedly connected on rear side of slaking apparatus, and rotating arm is connected on lifting column.Its rotating arm can automatic lifting, rotation, save manual operation；And realize air-cooled and water cooling in the same area and alternately cool down, save cooling time；Digest tube carries out recirculated water cooling using cooling water；The temperature fall time of furnace body is shortened, digest tube and waste discharge, which are provide with, sets frosted mouth, and it is excessive to reduce exhaust gas.
Description
Technical field
The present invention relates to a kind of intelligent rapid digestion devices, belong to chemical equipment technical field.
Background technique
Thermophilic digestion device mainly clears up organic matter samples under the conditions of high-temperature strong acid is converted into inorganic matter, after being used for
Continuous analysis detection.This device is widely used in the basic science experimental study such as agricultural, biology, medicine, industry and protein is surveyed
Digestion process before fixed.It, need to be under high-temperature strong acid environment such as the measurement of the content of nitrogen and phosphorous in field of ecology soil or plant sample
Inorganic nitrogen, phosphorus are converted by organic nitrogen, phosphorus.For another example common Kjeldahl nitrogen determination protein content in food, also needs the dress
Resolution is set, the concentrated sulfuric acid is reacted with the nitrogen in food for ammonium sulfate under 420 DEG C of hot environments.Currently, existing device is all
It does not take measures to digestion furnace body cooling, usually natural cooling, and it is fast to digest heating rate, but cooling rate is very slow,
Limit the process of next group treatments of the sample, widely used tradition slaking apparatus digesting protein content in measurement food
When, it needs to be arranged temperature and reaches 420 DEG C of high temperature, then furnace body cooling and digest tube can be very slow by natural cooling speed, when waiting
Between it is long, cumbersome, the degree of automation is not high, to seriously affect working efficiency；Usual digesting cools to 150 from 380 DEG C
It DEG C needs to spend 90 minutes or so, in addition, the exhaust gas that generates of digestion process by draught cupboard is directly discharged into air or by water band gas
It is discharged into sewer, causes environmental pollution and water resource waste.It is usually directed to a large amount of samples in scientific research and food inspection
Measurement, the above deficiency of traditional slaking apparatus seriously limit digestion rate and entirely test process, reduce working efficiency, and
Serious pollution is caused to atmosphere.Therefore, it is necessary to research and develop a kind of slaking apparatus of high-efficiency environment friendly.
Summary of the invention
In view of the above-mentioned problems, being equipped with lifting dress the purpose of the present invention is to provide a kind of intelligent rapid digestion device
Set, rotating arm can automatic lifting, rotation, save manual operation；And air-cooled and water cooling is realized alternately in the same area
It is cooling, save cooling time；Digest tube carries out water cooling using cooling water, and cooling water is Ke Xunhuanliyong；Shorten the drop of furnace body
Warm time, digest tube and waste discharge, which are provide with, sets frosted mouth, and it is excessive to reduce exhaust gas.
To achieve the goals above, the technical scheme is that being achieved: a kind of intelligence rapid digestion device, packet
Include slaking apparatus, cooling device, lifting device, cooling water tank, lye tank (vat)；It is characterized by: slaking apparatus and cooling device phase
Even；Lifting device is located at slaking apparatus and cooling device middle upper part is fixed on the rear side of slaking apparatus；
Slaking apparatus includes digestion furnace body, air-cooled interlayer, shell, control unit；Wherein, shell is wrapped in the outer of digestion furnace body
Layer digests and forms cavity between furnace body and shell, and cavity is the air duct of air-cooled interlayer, and air duct one end is equipped with closed guard, air duct
The exhaust vent of the other end be located at the rear side of shell, control unit is located at digesting body case surface, and blower fan is fixedly connected on
In the air duct of outer casing inner wall, it is equipped with heating metal pipe in the lower end of digestion furnace body, temp probe is mounted on digestion lower portion of furnace body.
Be above the air-cooled interlayer it is closed, the width of air-cooled interlayer is 6-10cm.
The blower fan is that 2-4 is mounted in housing back wall or rear wall and side wall, wind form up time along air-cooled interlayer
Needle annular fluid.
The blower fan and shell wall is arranged to 15-30 degree angle along clockwise.
The heating metal pipe takes aluminium ingot integrally to heat, and the temperature difference is small, and treatments of the sample is uniform, and in-furnace temperature continuously may be used
It adjusts, stable temperature control and precision height.
It is more than 70 DEG C that control unit, which includes power key, function key and LED bi-colour LED i.e. furnace body temperature equipped with keyboard,
It is displayed in red, is displayed in blue no more than 70 DEG C.
Cooling device includes cooling bath, the shell of cooling bath, fan, digestion pipe support, wherein digestion pipe support is placed in cooling
In slot, above the interlayer that fan is located at the shell of cooling bath and cooling bath is formed or it is arranged on wall side wall inside the shell, cooling bath
Inner wall is equipped with air holes, and air holes is inward slant aperture, and cooling bath inner wall is provided with inlet and outlet, and water inlet is located at cooling bath
Forward right side bottom, water outlet are located at the 2/3 of cooling bath left rear side, the outlet pipe of cooling water tank and the water inlet phase on cooling bath
Even, the water inlet pipe of cooling water tank is connected with the water outlet of cooling bath, and water pump, cooling water tank are connected on the outlet pipe of cooling water tank
Water inlet pipe and outlet pipe controlled by valve.
The outlet pipe of the cooling water tank passes through interlayer air duct and is directly entered cooling by the water inlet of cooling bath inner wall
Slot.
It is each that front side, left side and right side is distributed in the interlayer that the shell that the fan is located at cooling bath is formed with cooling bath
3, totally 9 fan air blast simultaneously, wind are dried through the air holes on inner wall to oblique lower section.
The angle that baffle in the cooling bath inner wall air holes is opened is 10-15 degree, and wind is made to disappear towards digestion bottom of the tube
It blows the position for changing liquid.
The digestion pipe support is placed in cooling bath middle position, and there is stabilizer blade in digestion pipe support bottom, has prevented ponding, caused
Test tube is burst.
The water inlet of the cooling bath is also evacuation port, and cooling water is derived from cooling water tank, the water inlet pipe of cooling water tank and
Outlet pipe passes through interlayer and is connected to water outlet and water inlet on cooling bath inner wall, and water outlet is arranged at cooling bath rear.
The lifting device includes lifting column, rotating arm, waste discharge cover, aspiration pump and exhaust tube；Wherein aspiration pump
It is arranged on the flow-guiding mouth in waste discharge cover, aspiration pump is connect with exhaust tube, and exhaust tube is connected with waste discharge cover；Rotating arm is fixed to be connected
It is connected to waste discharge cover, digest tube is fixed in the digest tube pipe clamp of waste discharge cover, and lifting column is fixedly connected on rear side of slaking apparatus,
Rotating arm connects on lifting column.
The exhaust tube is connect with waste discharge cover and lye tank (vat) respectively, and exhaust tube is forbidden to be bent in operation or be turned round
Knot avoids liquid from accumulating and air is hindered to flow.
The digest tube nozzle and waste discharge cover corresponding position is set as frosted mouth, reduces digestion process exhaust gas and overflows.
The waste discharge cover is fixed on lifting column, can axially be rotated, and lifting column is moved between three positions
Dynamic, when digesting low level, a cooling high position and not working middle position, is equipped with motor, motor passes through vertical in lifting column
It is risen or fallen to screw drive lifting column, horizontal screw bolt drives rotating arm rotation, waste discharge cover and digest tube synchronizing moving.
Filter screen is installed, water pump is arranged in the water outlet of cooling water tank at the outlet pipe and water inlet pipe of the cooling water tank
At pipe.
The lifting column can be moved between three positions: when digesting low level, a cooling high position and not working
Middle position.Motor drives lifting column to rise or fall by longitudinal screw, horizontal screw bolt driving digestion pipe clamp rotation branch
Arm rotation, if load too high, motor can be automatically stopped；Waste discharge cover is with digest tube synchronizing moving.
The positive effect of the present invention is: slaking apparatus apoplexy circularizes fluid along air-cooled sandwich shape, increases and digesting
The contact area of body improves digestion furnace body rate of temperature fall；The wind deflector of setting flows wind according to clockwise direction along air-cooled interlayer
It is dynamic；If the air outlet of housing back wall is exhaust outlet, gas is discharged by rear, guarantees experiment safety；Air-cooled interlayer to digestion furnace body and
Control unit can be effectively heat-insulated, extends LCD control panel service life；Control unit can effectively keep out from digestion furnace body and transmit
High heat, meanwhile, it avoids and the contact for the liquid that may be leaked from broken digest tube.Cooling device combines air-cooled and water cooling,
Save the time for waiting digestive juice cooling；It after digest tube digests, is moved it in cooling device by lifting device, fan is certainly
It is dynamic to open, 100 DEG C are cooled to temperature, fan is automatically closed, and the baffle of cooling bath blocks aperture, and cooling water tank synchronizes to be opened automatically
It opens, digest tube is cooled to room temperature；Aperture obliquely on cooling bath, ensure that wind is blown toward obliquely downward, wind faces digest tube
In liquid, improve air-cooled efficiency；Cooling water is derived from cooling water tank, realizes that water is recycled, improves water use efficiency；Cooling water tank
Outlet pipe be set to bottom, effectively prevent the short stream of water.Digestion pipe support is placed in cooling bath middle position, and certain altitude is arranged at bottom
Stabilizer blade, prevent having ponding in cooling bath, digest tube caused to burst, digest pipe holder and slaking apparatus it is mating.
Detailed description of the invention
Fig. 1 is the structural diagram of the present invention.
Fig. 2 is perspective view of the present invention.
Fig. 3 is cooling bath inner wall air holes and flapper closure state diagram of the invention.
Fig. 4 is cooling bath inner wall air holes of the invention and baffle open state figure.
Specific embodiment
The present invention will be further described with reference to the accompanying drawings and examples: as shown in Figs 1-4, a kind of intelligent quick
Slaking apparatus, including slaking apparatus 1, cooling device 2, lifting device 3, cooling water tank 4；It is characterized by: slaking apparatus 1 with it is cold
But device 2 is connected；Lifting device 3 is located at slaking apparatus 1 and 2 middle upper part of cooling device is fixed on the rear side of slaking apparatus 1；
Slaking apparatus 1 includes digestion furnace body 1-1, air-cooled interlayer 1-2, shell 1-3, control unit 1-4；Wherein, shell 1-3 is wrapped up
In the outer layer of digestion furnace body 1-1, digesting and form cavity between furnace body 1-1 and shell 1-3, cavity is the air duct of air-cooled interlayer 1-2,
Air duct one end is equipped with closed guard 1-6, and the exhaust vent of the other end in air duct is located at the rear side of shell, and control unit 1-4, which is located at, to disappear
Change furnace body 1-1 case surface, blower fan 1-5 is fixedly connected on the inner wall of shell 1-3；
It is equipped with heating metal pipe in the lower end of digestion furnace body 1-1, temp probe is mounted on the digestion lower part furnace body 1-1,
It is closed air duct above the air-cooled interlayer 1-2, the width in air duct is 6-10cm.
The blower fan is that 2-4 is mounted on shell 1-3 rear wall or rear wall and side wall, and wind is along air-cooled interlayer 1-2 shape
It is discharged at fluid clockwise by exhaust vent.
The blower fan 1-5 and shell wall is arranged to 15-30 degree angle along clockwise.
The heating metal pipe takes aluminium ingot integrally to heat, and the temperature difference is small, and treatments of the sample is uniform, and in-furnace temperature continuously may be used
It adjusts, stable temperature control and precision height.
It is more than 70 DEG C that control unit, which includes power key, function key and LED bi-colour LED i.e. furnace body temperature equipped with keyboard,
It is displayed in red, is displayed in blue no more than 70 DEG C.
Cooling device 2 includes cooling bath 2-1, the shell 2-2 of cooling bath, fan, digestion pipe support, wherein digestion pipe support is placed
In cooling bath 2-1, above the interlayer that the shell 2-2 and cooling bath 2-1 that fan is located at cooling bath are formed or it is arranged inside the shell
On wall side wall, cooling bath 2-1 inner wall is equipped with air holes 2-3, and air holes 2-3 is inward slant aperture, and air holes 2-3 is equipped with flapper closure
Cooling bath and interlayer is isolated in air holes, and cooling bath 2-1 inner wall is provided with water inlet 2-5 and water outlet 2-4, and water inlet 2-5 is located at cold
But slot 2-1 forward right side bottom, water outlet 2-4 are located at the left rear side 2/3 of cooling bath 2-1, the outlet pipe of cooling water tank and cooling
Water inlet on slot 2-1 is connected, and the water inlet pipe of cooling water tank is connected with the water outlet of cooling bath 2-1, the outlet pipe of cooling water tank
On be connected with water pump, the water inlet pipe and outlet pipe of cooling water tank are controlled by valve.
The outlet pipe of the cooling water tank passes through interlayer air duct and is directly entered cooling by the water inlet of cooling bath inner wall
Slot.
The fan be located at cooling bath shell 2-2 and cooling bath 2-1 formed interlayer in be distributed in front side, left side and
Each 3 of right side, totally 9 fan air blast simultaneously, wind are dried through the air holes on inner wall to oblique lower section.
The angle that baffle in the cooling bath inner wall air holes is opened is 10-15 degree, and wind is made to disappear towards digestion bottom of the tube
It blows the position for changing liquid.
In conjunction with air-cooled and water cooling, the time for waiting digestion solution cooling in experiment is saved.After digest tube digests, by rising
Falling unit 3 moves it on the digestion pipe support in cooling bath 2-1, opens fan, and cold wind is blown by the air holes 2-3 on slot inner wall
The test tube on pipe support is digested, 100 degree or so is cooled to the digestive juice temperature in test tube, closes fan, while in cooling water tank 4
Outlet pipe valve opening, cooling water, which is injected into cooling bath 2-1, is cooled to room temperature digest tube.
The digestion pipe support is placed in the middle position cooling bath 2-1, and there is stabilizer blade in digestion pipe support bottom, prevents cooling bath 2-
There is ponding in 1, test tube is caused to burst.
The water inlet 2-5 of the cooling bath is also evacuation port, and cooling water is derived from cooling water tank 4, the water outlet of cooling water tank
Pipe and water inlet pipe pass through interlayer and are connected to water inlet 2-5 and water outlet 2-4 on cooling bath inner wall, and water outlet 2-4 is arranged cold
But the rear slot 2-1.
The lifting device 3 includes lifting column 3-1, rotating arm 3-2, waste discharge cover 3-3 and exhaust tube 3-4；Wherein
Exhaust tube 3-4 is connected with waste discharge cover 3-3；Rotating arm 3-2 is fixedly connected with waste discharge cover 3-3, and digest tube is fixed on waste discharge cover 3-3
Digest tube pipe clamp on, lifting column 3-1 is fixedly connected on the rear side of slaking apparatus 1, rotating arm 3-2 connection lifting column 3-
On 1；
The exhaust tube 3-4 is connect with waste discharge cover 3-3 and lye tank (vat) 5 respectively, and exhaust tube 3-4 forbids to be bent in operation
Or kink, avoid liquid from accumulating and air is hindered to flow.
The digest tube nozzle and the corresponding position waste discharge cover 3-3 is set as frosted mouth, reduces digestion process exhaust gas and overflows.
The waste discharge cover 3-3 is fixed on lifting column 3-1, can axially be rotated, and lifting column 3-1 is three positions
Between moved, digestion low level, cooling high-order and when not working middle position are equipped with motor in lifting column 3-1,
Motor drives lifting column 3-1 to rise or fall by longitudinal screw, and horizontal screw bolt drives rotating arm 3-2 rotation, waste discharge cover
3-3 and digest tube synchronizing moving.
Filter screen is installed, water pump is arranged in the water outlet of cooling water tank at the outlet pipe and water inlet pipe of the cooling water tank
At pipe.
The cooling water of recycling need to be filtered processing by filter screen；When the cooling water of cooling device is opened, water pump
The water of cooling water tank 4 is entered in cooling bath 4 by cooling water tank outlet pipe, water-cooled process is realized, by cooling bath water outlet
The cooling water of 2-4 discharge is recycled along the water inlet pipe of cooling water tank 4, at the filtering for carrying out recycle-water by filter screen on the way
Reason, guarantees that the water of cooling water tank completely can be used.When digestive juice is cooled to 25 DEG C, water pump is automatically closed.Manually opened water cooling plant
It is vented valve, the water in water cooling plant is discharged into cooling water tank, the water inside cooling water tank can continue as next group
The water cooling water of sample, Reusability are prepared for next digestion process.
The lifting column 3-1 can be moved between three positions: digestion low level, cooling is high-order and does not work
When middle position.Motor drives lifting column 3-1 to rise or fall by longitudinal screw, horizontal screw bolt driving digestion pipe clamp rotation
Turn support arm 3-2 rotation, if load too high, motor can be automatically stopped；Waste discharge cover 3-3 is with digest tube synchronizing moving.
Specific step is as follows: 1, will add sample and various reagents in mating digest tube, and digest tube is placed on digestion
On furnace body 1-1, waste discharge cover 3-3 is covered above digest tube, digest tube nozzle is fixed on waste discharge cover 3-3 by digesting pipe clip
It is interior, meanwhile, the condensing cover in waste discharge cover 3-3 is docked with digest tube nozzle frosted interface, is prevented exhaust leak in digestion process, is beaten
Switch power supply, temperature and time needed for sample digestion is set by control unit function key；
2, the exhaust gas flow-guiding mouth in waste discharge cover 3-3 is connected with aspiration pump, and in digestion process, aspiration pump is in working condition, and will disappear
The exhaust gas generated during changing imports lye tank (vat) along exhaust tube and carries out neutralization reaction；
3, after the completion of digestion reaction, control unit stops digestion furnace body 1-1 heating, while opening air cooling equipment, to digesting
Body 1-1 implements cooling, prepares for next group digestion (because reagent added by digest tube is usually therefore explosive dangerous material add
The digest tube of sample digestion and reagent need to be 100 DEG C arranged below in digestion furnace body 1-1 temperature, such as to soil or plant sample into
Row resolution, surveys its content of tatal phosphorus, because institute's reagent adding is strong oxidizer perchloric acid, easily makes quick-fried, burst point is 130 DEG C, therefore, need to be
130 DEG C of digest tubes arranged below) simultaneously, the lifting column 3-1 and rotating arm 3-2 in lifting device 3 are operated, digestion is complete
Digest tube together with waste discharge cover 3-3 global transfer on digestion pipe holder into cooling device cooling bath 2-1, digestion pipe holder is set
Stabilizer blade is set, 2-3 centimetres of support foot hight, thermophilic digestion tube bottom is avoided to touch the remaining cooling water of cooling bath 2-1 and lead to digest tube
It bursts.
4, lifting column 3-1 send digest tube to cooling bath 2-1, opens cooling blower fan from top to bottom or from side
The inside air blast of wall makes to be covered with wind in the air duct that cooling bath 2-1 inner wall and shell are constituted, and wind is offseted by air holes 2-3 in the diagonal
It is air-cooled to change pipe progress.
5, temperature is controlled through the probe in cooling device, digest tube is hard glass, when being lower than 100 DEG C, closes wind
Device for cooling opens digestion pipe clip, removes waste discharge cover 3-3, and waste discharge cover 3-3 moves to left side, prepares for next group digestion, can
To carry out the digestion heating of second round by above-mentioned steps.Water cooling plant is opened simultaneously, opens water pump for the water pump of cooling water tank 4
Enter cooling bath 2-1 and make the cooling water level in cooling bath not less than digestion liquid level, the air duct cooling bath 2-1 rear side outer wall is provided
The setting height of mouth of a river 2-4, water outlet 2-4 are at cooling bath 2-1 high 2/3, higher than the 1/3(of digest tube because of usual digest tube
Interior liquid height is 1/3, and cooling water need to not cross this liquid height), while it is excessive to avoid cooling water.
6, cooling water is discharged into cooling water tank 4 by the strainer of cooling water tank water inlet pipe from water outlet 2-4, and filter screen is to prevent
Cooling device endoparticle object enters cooling water tank 4, damages to cooling water pump.It can be closed when cooling device reaches cooling temperature
Water cooling work is closed, water is vented after filter screen filtration into cooling water tank 4 by cooling water intake 2-5 as drain at this time.
After water cooling works, use digestion pipe support by digest tube collection to subsequent experiment by testing crew.
Claims (10)
1. a kind of intelligence rapid digestion device, including slaking apparatus, cooling device, lifting device, cooling water tank；Its feature exists
In: slaking apparatus is connected with cooling device；Lifting device is located at slaking apparatus and cooling device middle upper part is fixed on digestion dress
The rear side set；
Slaking apparatus includes digestion furnace body, air-cooled interlayer, shell, control unit；Wherein, shell is wrapped in the outer of digestion furnace body
Layer digests and forms cavity between furnace body and shell, and cavity is the air duct of air-cooled interlayer, and air duct one end is equipped with closed guard, air duct
The exhaust vent of the other end be located at the rear side of shell, control unit is located at digesting body case surface, and blower fan is fixedly connected on
In the air duct of outer casing inner wall, it is equipped with heating metal pipe in the lower end of digestion furnace body, temp probe is mounted on digestion lower portion of furnace body；
Cooling device includes cooling bath, the shell of cooling bath, fan, digestion pipe support, wherein digestion pipe support is placed in cooling bath,
Above the interlayer that fan is located at the shell of cooling bath and cooling bath is formed or it is arranged on wall side wall inside the shell, cooling bath inner wall is set
There is air holes, air holes is inward slant aperture, and cooling bath inner wall is provided with inlet and outlet, and water inlet is located at cooling bath forward right side
Bottom, water outlet are located at the 2/3 of cooling bath left rear side, and the outlet pipe of cooling water tank is connected with the water inlet on cooling bath, cold
But the water inlet pipe of water tank is connected with the water outlet of cooling bath, is connected with water pump on the outlet pipe of cooling water tank, cooling water tank into
Water pipe and outlet pipe are controlled by valve；
Lifting device includes lifting column, rotating arm, waste discharge cover, aspiration pump and exhaust tube；Wherein aspiration pump is arranged in waste discharge
On flow-guiding mouth in cover, aspiration pump is connect with exhaust tube, and exhaust tube is connected with waste discharge cover；Rotating arm is fixedly connected with waste discharge
Cover, digest tube are fixed in the digest tube pipe clamp of waste discharge cover, and lifting column is fixedly connected on rear side of slaking apparatus, rotating arm
It is connected on lifting column.
2. a kind of intelligent rapid digestion device according to claim 1, it is characterised in that above the air-cooled interlayer
Be it is closed, the width of air-cooled interlayer is 6-10cm.
3. a kind of intelligent rapid digestion device according to claim 1, it is characterised in that the blower fan is 2-4
It is mounted in housing back wall or rear wall and side wall, wind forms fluid clockwise along air-cooled interlayer.
4. a kind of intelligent rapid digestion device according to claim 1, it is characterised in that the blower fan and shell
Wall is arranged to 15-30 degree angle along clockwise.
5. a kind of intelligent rapid digestion device according to claim 1, it is characterised in that the fan is located at cooling
It is distributed in each 3 of front side, left side and right side in the interlayer that the shell and cooling bath of slot are formed, totally 9 fan air blast simultaneously, wind are saturating
The air holes crossed on inner wall is dried to oblique lower section.
6. a kind of intelligent rapid digestion device according to claim 1, it is characterised in that the cooling bath inner wall wind
The angle that baffle on hole is opened is 10-15 degree, blows wind towards the position of digestion bottom of the tube digestive juice.
7. a kind of intelligent rapid digestion device according to claim 1, it is characterised in that the water inlet of the cooling bath
Mouth is also evacuation port, and cooling water is derived from cooling water tank, and the water inlet pipe and outlet pipe of cooling water tank pass through interlayer and be connected to cooling bath
Water outlet and water inlet on inner wall, water outlet are arranged at cooling bath rear.
8. a kind of intelligent rapid digestion device according to claim 1, it is characterised in that the exhaust tube respectively with
Waste discharge cover is connected with lye tank (vat), and waste discharge cover is fixed on lifting column, can axially be rotated, lifting column between three positions into
Row movement, middle position when digesting low level, a cooling high position and not working, is equipped with motor, motor is logical in lifting column
It crosses longitudinal screw driving lifting column to rise or fall, horizontal screw bolt drives rotating arm rotation, and waste discharge cover is synchronous with digest tube
It is mobile.
9. a kind of intelligent rapid digestion device according to claim 1, it is characterised in that the digest tube nozzle with
Waste discharge cover corresponding position is set as frosted mouth.
10. a kind of intelligent rapid digestion device according to claim 1, it is characterised in that the cooling water tank goes out
Water pipe passes through interlayer air duct and is directly entered cooling bath by the water inlet of cooling bath inner wall.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811286317.0A CN109173954A (en) | 2018-10-31 | 2018-10-31 | Intelligent rapid digestion device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811286317.0A CN109173954A (en) | 2018-10-31 | 2018-10-31 | Intelligent rapid digestion device |
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| Publication Number | Publication Date |
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| CN109173954A true CN109173954A (en) | 2019-01-11 |
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| CN201811286317.0A Pending CN109173954A (en) | 2018-10-31 | 2018-10-31 | Intelligent rapid digestion device |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112056384A (en) * | 2020-09-03 | 2020-12-11 | 余姚谷满仓食品有限公司 | HACCP-based cleome gynandra quick-freezing method and blanching and cooling water machine thereof |
| CN113351146A (en) * | 2021-05-14 | 2021-09-07 | 南阳师范学院 | Special rotatory high temperature vulcanizer of rare earth sulfide synthesis |
Citations (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3020130A (en) * | 1959-08-06 | 1962-02-06 | Technicon Instr | Digestion apparatus and method |
| US3178265A (en) * | 1961-05-25 | 1965-04-13 | Technicon Instr | Digestion and analysis apparatus and method |
| US5215715A (en) * | 1991-07-10 | 1993-06-01 | Cem Corporation | Microwave heated digesting system for digesting materials to be analyzed |
| US5415847A (en) * | 1993-06-22 | 1995-05-16 | Gem, Inc. | Treatment of pit waste containing chromated copper arsenate |
| CN2226762Y (en) * | 1994-09-28 | 1996-05-08 | 黄庭国 | Enclosed microwave pressure liquor sample pot |
| KR100827418B1 (en) * | 2007-11-30 | 2008-05-06 | 주식회사 위드텍 | A sampling system and method for acidic gases using a cooling and alkaline absorbing solution and a monitoring system |
| CN201375832Y (en) * | 2009-03-02 | 2010-01-06 | 河南农大迅捷测试技术有限公司 | Portable acid gas or acid mist condensing and absorbing device |
| CN201389459Y (en) * | 2008-08-05 | 2010-01-27 | 奥罗达(佛山)科技有限公司 | Microwave digestion system |
| CN101900663A (en) * | 2009-05-27 | 2010-12-01 | 宝山钢铁股份有限公司 | High-temperature cyclic oxidation corrosion simulating test device |
| CN103792130A (en) * | 2014-01-14 | 2014-05-14 | 陕西师范大学 | Efficient environment-friendly digestion device |
| CN203705251U (en) * | 2014-01-14 | 2014-07-09 | 耿佃刚 | Heating digestion thermostat device for measuring chemical oxygen demand in water |
| CN104226664A (en) * | 2013-06-08 | 2014-12-24 | 上海纤检仪器有限公司 | Digestion device exhaust emission device and method |
| CN104297044A (en) * | 2014-11-07 | 2015-01-21 | 中山出入境检验检疫局 | Acid gas processing device for graphite digestion system |
| CN204261554U (en) * | 2014-11-25 | 2015-04-15 | 南京农业大学 | One is exempted from fume hood and to be disappeared boiler |
| CN209155808U (en) * | 2018-10-31 | 2019-07-26 | 东北师范大学 | Intelligent rapid digestion device |
-
2018
- 2018-10-31 CN CN201811286317.0A patent/CN109173954A/en active Pending
Patent Citations (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3020130A (en) * | 1959-08-06 | 1962-02-06 | Technicon Instr | Digestion apparatus and method |
| US3178265A (en) * | 1961-05-25 | 1965-04-13 | Technicon Instr | Digestion and analysis apparatus and method |
| US5215715A (en) * | 1991-07-10 | 1993-06-01 | Cem Corporation | Microwave heated digesting system for digesting materials to be analyzed |
| US5415847A (en) * | 1993-06-22 | 1995-05-16 | Gem, Inc. | Treatment of pit waste containing chromated copper arsenate |
| CN2226762Y (en) * | 1994-09-28 | 1996-05-08 | 黄庭国 | Enclosed microwave pressure liquor sample pot |
| KR100827418B1 (en) * | 2007-11-30 | 2008-05-06 | 주식회사 위드텍 | A sampling system and method for acidic gases using a cooling and alkaline absorbing solution and a monitoring system |
| CN201389459Y (en) * | 2008-08-05 | 2010-01-27 | 奥罗达(佛山)科技有限公司 | Microwave digestion system |
| CN201375832Y (en) * | 2009-03-02 | 2010-01-06 | 河南农大迅捷测试技术有限公司 | Portable acid gas or acid mist condensing and absorbing device |
| CN101900663A (en) * | 2009-05-27 | 2010-12-01 | 宝山钢铁股份有限公司 | High-temperature cyclic oxidation corrosion simulating test device |
| CN104226664A (en) * | 2013-06-08 | 2014-12-24 | 上海纤检仪器有限公司 | Digestion device exhaust emission device and method |
| CN103792130A (en) * | 2014-01-14 | 2014-05-14 | 陕西师范大学 | Efficient environment-friendly digestion device |
| CN203705251U (en) * | 2014-01-14 | 2014-07-09 | 耿佃刚 | Heating digestion thermostat device for measuring chemical oxygen demand in water |
| CN104297044A (en) * | 2014-11-07 | 2015-01-21 | 中山出入境检验检疫局 | Acid gas processing device for graphite digestion system |
| CN204261554U (en) * | 2014-11-25 | 2015-04-15 | 南京农业大学 | One is exempted from fume hood and to be disappeared boiler |
| CN209155808U (en) * | 2018-10-31 | 2019-07-26 | 东北师范大学 | Intelligent rapid digestion device |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112056384A (en) * | 2020-09-03 | 2020-12-11 | 余姚谷满仓食品有限公司 | HACCP-based cleome gynandra quick-freezing method and blanching and cooling water machine thereof |
| CN113351146A (en) * | 2021-05-14 | 2021-09-07 | 南阳师范学院 | Special rotatory high temperature vulcanizer of rare earth sulfide synthesis |
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