CN109173948A - A kind of slow-release microcapsule material and its preparation method and application discharging fragrance - Google Patents
A kind of slow-release microcapsule material and its preparation method and application discharging fragrance Download PDFInfo
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- CN109173948A CN109173948A CN201811128239.1A CN201811128239A CN109173948A CN 109173948 A CN109173948 A CN 109173948A CN 201811128239 A CN201811128239 A CN 201811128239A CN 109173948 A CN109173948 A CN 109173948A
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- Prior art keywords
- fragrance
- slow
- cigarette
- release
- release microcapsule
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
- B01J13/043—Drying and spraying
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Fats And Perfumes (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a kind of slow-release microcapsule materials for discharging fragrance, and the microencapsulation material includes following raw material components and parts by weight: 10 parts of fragrance, 10-60 parts of microcapsule wall material, 10-50 parts of emulsifier.When microencapsulation material of the invention is in cigarette, there is slow releasing function, the flavor component in capsule can be slowly released, validity period is long；Can according to the size of cigarette package, region, fragrance, adjust on demand microencapsulation material number or region；When external force or external environment change, can accelerated release in vitro fragrance, when such as finger friction cigarette paper, so that it may make the cigarette paper release fragrance for being added to microencapsulation material of the invention；Or in smoking process, finger friction cigarette paper promotes the release of fragrance, or promotes to add the filter tip release fragrance of microencapsulation material of the present invention.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to it is a kind of discharge fragrance slow-release microcapsule material and its preparation side
Method and purposes.
Background technique
Microcapsules technology is the technology that micro substance is wrapped in thin polymer film, is a kind of store solids, liquid, gas
Microdisplay package technology.In recent years in the fields such as food industry, bio-pharmaceuticals extensive application.Microcapsules technology has protrusion
The advantages of: reaction of the active material to outside environmental elements (such as light, oxygen, water) can be effectively reduced；Heartwood is reduced to environment
Diffusion and evaporation；The release for controlling heartwood, the special breath for sheltering heartwood, physical property (including the color, shape for changing heartwood
Shape, density, dispersion performance), chemical property etc..
In the correlative study of tobacco and tobacco product, there is document report that microcapsules are applied in cigarette filter, utilizes
The flavor component wrapped up in microcapsules can be released, achievees the effect that increase peat-reek.But existing research is by micro- glue
Capsule is added in cigarette filter rod or pipe tobacco and filter stick contact jaw, gradually discharges wherein substance by the slow-release function of microcapsules,
Its fragrance keeping period is generally two to three months, and when suction, and fragrance release is uneven, and suction experience effect is bad.Moreover, because existing
There is the fragrance keeping period in research unsmooth therefore not lasting enough there are the holding time, it is more difficult to which the time for meeting cigarette storage and transport is wanted
The problems such as asking.
Summary of the invention
In view of the foregoing deficiencies of prior art, the purpose of the present invention is to provide a kind of micro- glue of sustained release for discharging fragrance
Capsule material and its preparation method and application, overcome the cigarette products fragrance holding time existing in the prior art not persistently, storage
Or haulage time requires the problems such as stringent.
To achieve the goals above or other purposes, the present invention is achieved by the following technical solutions.
A kind of slow-release microcapsule material discharging fragrance, the slow-release microcapsule material includes following raw material components and weight
Number: 10 parts of fragrance, 10~60 parts of microcapsule wall material, 10~50 parts of emulsifier.
Further, the fragrance is cigarette synthetic perfume or natural perfume for cigarette.
Further, the fragrance is selected from one of menthol, fennel oil, caryophyllus oil, orange oil.
Further, the microcapsule wall material in maltodextrin, gelatin, Arabic gum, cyclodextrin, rosin one
Kind.
Preferably, the microcapsule wall material is selected from maltodextrin, the DE value < 15 of the maltodextrin.
Further, the emulsifier is selected from Tween 80.
Second aspect of the present invention provides a kind of preparation method of the slow-release microcapsule material of release fragrance described above, packet
Include following steps:
(1) microcapsule wall material is added in ethanol water, microcapsule wall material solution is made in stirring homogenizing；
(2) ethanol solution of fragrance is added into microcapsule wall material solution obtained by step (1), stirs evenly；
(3) emulsifier is added into mixed solution obtained by step (2), after mixing evenly, microcapsules material is made in spray drying
Material.
Further, the volume ratio of ethyl alcohol and water is (1:2)~(2:1) in ethanol water.
Further, the content of microcapsule wall material is 12%~20% in microcapsule wall material solution.
Further, mixing speed is 1000~1300rpm in step (1), and homogenization speed is 8000~10000rpm,
The change time is 5~20min.
Further, the mass volume ratio of fragrance and ethyl alcohol is 1:20g/ml in the ethanol solution of fragrance.
Further, the partial size of the slow-release microcapsule material is 0.5~1 μm.
Third aspect present invention provides a kind of purposes of the slow-release microcapsule material of above-mentioned release fragrance in cigarette.
The cigarette includes filter tip, cigarette sticks and the tipping paper for being hinged with the filter tip and the cigarette sticks, the filter
Mouth includes filter stick and the forming paper for wrapping up the filter stick, and the cigarette sticks include pipe tobacco and the volume for coating the pipe tobacco
Cigarette paper.
When the slow-release microcapsule material is used in cigarette, which can be added in ink and be printed
To cigarette paper or cigarette tipping paper surface, or it is directly appended in filter stick.On the other hand, the slow-release microcapsule material can add
The outer packing of cigarette product, i.e. cigarette wrapping paper surface are printed into ink.
Preferably, slow-release microcapsule material is added in ink, by the way of silk-screen printing, is printed onto cigarette package
Paper, cigarette paper or cigarette tipping paper surface.
Preferably, the ink is natural plant gum through the fully emulsified obtained colloidal solution of colloid mill.The natural plant gum is Chinese scholartree
The mixture of bean gum, guar gum and tragacanth, the mass ratio of locust bean gum, guar gum and tragacanth are 1:1:1.
Preferably, the coating weight of ink is 2-20g/m2。
Preferably, slow-release microcapsule material is 5%~30% relative to the addition weight ratio of cigarette paper or cigarette tipping paper.
Preferably, slow-release microcapsule material can be directly appended in filter stick, weight of the slow-release microcapsule material relative to filter stick
Amount is than being 1%-30%.
A kind of slow-release microcapsule material discharging fragrance provided by the invention, slow-release microcapsule material is printable, coating or
Make an addition to cigarette packaging material, may be added in cigarette filter, by all external force such as pressure, friction, heating or illumination or
External environment changes accelerated release in vitro, and fragrance rate of release is variable, and scent duration is long.Microencapsulation material of the invention is in cigarette
In storage or transportational process, be in stable state, can slow release fragrance, but store 1 year its fragrance under room temperature without obvious change
Change；When friction or temperature increase, wall material is destroyed, and the fragrance wrapped up can discharge fragrance, and microcapsules material of the invention
Material is spansule material, has certain slow-release function, is able to extend fragrance demurrage, avoids cigarette in aspiration procedure
Occur starting fragrance foot and the phenomenon that back segment aroma fades.
In short, there is slow releasing function, can slowly release in capsule when microencapsulation material of the invention is in cigarette
Flavor component, validity period is long；Can according to the size of cigarette package, region, fragrance, adjust on demand microencapsulation material number or
Region；When external force or external environment change, can accelerated release in vitro fragrance, when such as finger friction cigarette paper, so that it may make to be added to this
The cigarette paper of the microencapsulation material of invention discharges fragrance；Or in smoking process, finger friction cigarette paper promotes the release of fragrance, or
The filter tip for adding microencapsulation material of the present invention is promoted to discharge fragrance.
Specific embodiment
Embodiments of the present invention are illustrated by particular specific embodiment below, those skilled in the art can be by this explanation
Content disclosed by book is understood other advantages and efficacy of the present invention easily.
Before further describing the specific embodiments of the present invention, it should be appreciated that protection scope of the present invention is not limited to down
State specific specific embodiment；It is also understood that term used in the embodiment of the present invention is specific specific in order to describe
Embodiment, rather than limiting the scope of protection of the present invention.The test method of actual conditions is not specified in the following example,
Usually according to normal condition, or according to condition proposed by each manufacturer.
When embodiment provides numberical range, it should be appreciated that except non-present invention is otherwise noted, two ends of each numberical range
Any one numerical value can be selected between point and two endpoints.Unless otherwise defined, the present invention used in all technologies and
Scientific term is identical as the normally understood meaning of those skilled in the art of the present technique.Except specific method, equipment used in embodiment,
Outside material, grasp and record of the invention according to those skilled in the art to the prior art can also be used and this
Any method, equipment and the material of the similar or equivalent prior art of method described in inventive embodiments, equipment, material come real
The existing present invention.
Embodiment 1
A kind of slow-release microcapsule material, including 10 parts of menthol, 10 parts of beta-cyclodextrin, 50 parts of Tween 80.
(1) beta-cyclodextrin is added in ethanol water (volume ratio of ethyl alcohol and water is 1:2) solution, is stirred under 1300rpm speed
It mixes, is homogenized 10min under 10000rpm, beta-cyclodextrin solution is made, beta-cyclodextrin content is 20%,；
(2) ethanol solution of menthol is added into beta-cyclodextrin solution obtained by step (1), is stirred evenly under room temperature；
(3) emulsifier tween 80 is added into mixed solution obtained by step (2), after mixing evenly, spray drying is made micro-
Capsule material.
Embodiment 2
A kind of slow-release microcapsule material, including 10 parts of orange oil, 30 parts of maltodextrin, 40 parts of Tween 80.
(1) maltodextrin is added in water (volume ratio of ethyl alcohol and water is 1:2) solution, is stirred under 1000rpm speed,
It is homogenized 10min under 9000rpm, maltodextrin solution, gelatine content 20% is made；
(2) ethanol solution of orange oil is added into maltodextrin solution obtained by step (1), is stirred evenly under room temperature；
(3) emulsifier tween 80 is added into mixed solution obtained by step (2), after mixing evenly, spray drying is made micro-
Capsule material.
Embodiment 3
A kind of slow-release microcapsule material, including 10 parts of caryophyllus oil, 10 parts of Arabic gum, 50 parts of Tween 80.
(1) Arabic gum is added in water (volume ratio of ethyl alcohol and water is 2:1) solution, is stirred under 1200rpm speed,
It is homogenized 5min under 8000rpm, gumwater is made, Arabic gum content is 20%；
(2) ethanol solution of caryophyllus oil is added into beta-cyclodextrin solution obtained by step (1), is stirred evenly under room temperature；
(3) emulsifier tween 80 is added into mixed solution obtained by step (2), after mixing evenly, spray drying is made micro-
Capsule material.
Comparative example 1
The present embodiment is as a comparison case, wherein microencapsulation material includes 10 parts of menthol, 10 parts of beta-cyclodextrin；
The preparation method comprises the following steps: beta-cyclodextrin is added to the water by (1), beta-cyclodextrin solution is made, beta-cyclodextrin content is 20%；
(2) menthol is added into beta-cyclodextrin solution obtained by step (1), is stirred evenly under room temperature；Spray drying, obtains micro-
Encapsulated materials.
Comparative example 2
The present embodiment is as a comparison case, wherein the component and part of microencapsulation material is different from embodiment 1, still
Preparation method is different, for investigating the different influences to microencapsulation material effect of preparation method.
The preparation method comprises the following steps: (1) beta-cyclodextrin is added in ethanol solution, stirred under 1500rpm speed, under 15000rpm
To change 10min, beta-cyclodextrin solution is made, beta-cyclodextrin content is 20%,；
(2) ethanol solution of menthol is added into beta-cyclodextrin solution obtained by step (1), is stirred evenly under room temperature；
(3) emulsifier tween 80 is added into mixed solution obtained by step (2), after mixing evenly, spray drying is made micro-
Capsule material.
Application examples 1
Microencapsulation material made from embodiment 1 is added in ink, cigarette wrapping paper is printed in, microencapsulation material is opposite
It is 10% in the addition weight ratio of cigarette wrapping paper, finished cigarettes package paper is made.It is found in use process, cigarette package can
Fragrance is distributed, after handling friction or heating, flavor component accelerated release in vitro distributes more rich fragrance.It is placed under room temperature, the cigarette
Wrapping paper fragrance can be distributed slowly 1 year or more.
Application examples 2
Microencapsulation material made from embodiment 1-3, comparative example 1 is added in cigarette filter rod respectively, institute's adding proportion are as follows:
Microencapsulation material is 5% relative to the weight ratio of filter stick.Wherein, the pipe tobacco of cigarette is identical, only adds in filter stick different
Microencapsulation material.And carry out test of smokeing panel test respectively by 10 members of smoking, test index include fragrance before aspirating (be divided into nothing, have,
Slightly fragrance), (0-10 points, 9-10 defends oneself, and bright fragrance is sufficient, and 6-8 illustrates that perfume quantity is more sufficient, and 0-6 is said for perfume quantity in aspiration procedure
Bright perfume quantity is insufficient), fragrance last (0-10 points, when 9-10 defends oneself that bright perfume substantiation is very long, 6-8 illustrates fragrance last
Between it is slightly long, 0-6 illustrates that perfume substantiation is shorter), overall organoleptic etc., the scoring results of evaluation are the flat of 10 member of smokings' marking
Mean value, evaluation results are shown in Table 1.
Table 1 is smoked panel test test result
To sum up, it is used in cigarette using microencapsulation material provided by the invention, releasable fragrance, through external force or external environment
When variation, fragrance can be accelerated to discharge, release process is a sustained release process, and release time is lasting, and fragrance release is uniform, suction effect
Fruit is preferable.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology all without departing from the spirit and scope of the present invention, carries out modifications and changes to above-described embodiment.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should be covered by the claims of the present invention.
Claims (10)
1. a kind of slow-release microcapsule material for discharging fragrance, which is characterized in that the slow-release microcapsule material includes following raw material
Component and part: 10 parts of fragrance, 10~60 parts of microcapsule wall material, 10~50 parts of emulsifier.
2. slow-release microcapsule material as described in claim 1, which is characterized in that the fragrance is cigarette synthetic perfume or cigarette day
Right fragrance.
3. slow-release microcapsule material as claimed in claim 2, which is characterized in that the fragrance is selected from menthol, fennel oil, cloves
One of oil, orange oil.
4. slow-release microcapsule material as described in claim 1, which is characterized in that the microcapsule wall material is selected from maltodextrin, bright
One of glue, Arabic gum, cyclodextrin, oligosaccharide, starch.
5. slow-release microcapsule material as described in claim 1, which is characterized in that the emulsifier is selected from Tween 80.
6. discharging the preparation method of the slow-release microcapsule material of fragrance as described in any one of claim 1 to 5, which is characterized in that
The following steps are included:
(1) microcapsule wall material is added in ethanol water, microcapsule wall material solution is made in stirring homogenizing；
(2) ethanol solution of fragrance is added into microcapsule wall material solution obtained by step (1), stirs evenly；
(3) emulsifier is added into mixed solution obtained by step (2), after mixing evenly, microencapsulation material is made in spray drying.
7. preparation method as claimed in claim 6, which is characterized in that any one or multinomial including following technical characteristic:
The volume ratio of ethyl alcohol and water is (1:2)~(2:1) in ethanol water；
In step (1) mixing speed be 1000~1300rpm, homogenization speed be 8000~10000rpm, homogenising time be 5~
20min。
8. discharging purposes of the slow-release microcapsule material of fragrance in cigarette as described in any one of claim 1 to 5.
9. purposes as claimed in claim 8, which is characterized in that slow-release microcapsule material is added in ink, using screen printing
The mode of brush is printed onto cigarette wrapping paper, cigarette paper or cigarette tipping paper surface.
10. purposes as claimed in claim 9, which is characterized in that slow-release microcapsule material relative to cigarette wrapping paper, cigarette paper or
The addition weight ratio of cigarette tipping paper is 5%~30%.
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| CN201811128239.1A CN109173948A (en) | 2018-09-27 | 2018-09-27 | A kind of slow-release microcapsule material and its preparation method and application discharging fragrance |
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| CN201811128239.1A CN109173948A (en) | 2018-09-27 | 2018-09-27 | A kind of slow-release microcapsule material and its preparation method and application discharging fragrance |
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| CN110013806A (en) * | 2019-04-17 | 2019-07-16 | 云南中烟工业有限责任公司 | A kind of porous complex microsphere of graphene-plant and the preparation method and application thereof |
| CN110172866A (en) * | 2019-06-26 | 2019-08-27 | 红云红河烟草(集团)有限责任公司 | A kind of perfuming type cigarette paper |
| CN110537730A (en) * | 2019-09-20 | 2019-12-06 | 安徽坤大生物工程技术有限公司 | mint taste puffed bead for cigarettes and preparation method thereof |
| CN110982620A (en) * | 2019-11-26 | 2020-04-10 | 云南中烟工业有限责任公司 | Porous starch-loaded molecular capsule, and preparation method and application thereof |
| CN111074674A (en) * | 2020-01-08 | 2020-04-28 | 云南恩典科技产业发展有限公司 | Slow-release essence forming paper |
| CN111484766A (en) * | 2020-04-28 | 2020-08-04 | 安徽集友纸业包装有限公司 | Gloss oil with slow-release fragrance, cigarette tipping paper, filter element and smoking product |
| CN112316862A (en) * | 2020-11-25 | 2021-02-05 | 江西中烟工业有限责任公司 | Preparation method of stevia rebaudiana enzyme microcapsule and application of stevia rebaudiana enzyme microcapsule in cigarettes |
| CN112826122A (en) * | 2021-03-02 | 2021-05-25 | 云南中烟工业有限责任公司 | Three-section cigarette, preparation method and application thereof |
| CN113025425A (en) * | 2019-12-24 | 2021-06-25 | 深圳波顿香料有限公司 | Perfuming microcapsule particle for cigarette, preparation method thereof and application of perfuming microcapsule particle in cigarette |
| CN113068395A (en) * | 2019-10-30 | 2021-07-02 | 韩国烟草人参公社 | Tipping paper suitable for finger smoke smell reducing technology, smoking article comprising tipping paper and preparation method of tipping paper |
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| CN114775333A (en) * | 2022-04-13 | 2022-07-22 | 江苏卫星新材料股份有限公司 | Sweetener tipping paper and preparation method thereof |
| CN116236983A (en) * | 2023-03-14 | 2023-06-09 | 福建中烟工业有限责任公司 | Fat-soluble essence slow-release double-layer microcapsule for cigarettes and preparation method thereof |
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| CN110537730A (en) * | 2019-09-20 | 2019-12-06 | 安徽坤大生物工程技术有限公司 | mint taste puffed bead for cigarettes and preparation method thereof |
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Application publication date: 20190111 |