CN109173317A - A kind of Chemical Manufacture distillation still - Google Patents
A kind of Chemical Manufacture distillation still Download PDFInfo
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- CN109173317A CN109173317A CN201811207291.6A CN201811207291A CN109173317A CN 109173317 A CN109173317 A CN 109173317A CN 201811207291 A CN201811207291 A CN 201811207291A CN 109173317 A CN109173317 A CN 109173317A
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- tank body
- cooling dome
- separation chamber
- wall
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The present invention relates to chemical industry technical field of processing equipment, specifically a kind of Chemical Manufacture distillation still, including heating mechanism, tank body, the second-order separation mechanism, level-one separating mechanism, water supply mechanism, drainage mechanism, the first cooling dome and the second cooling dome；Fluid present invention is circulated in the second-order separation room after level-one separation chamber is distilled, and recirculation is realized and chemical liquid quick segmentation is distilled, whole process carries out in tank body, rapid without transfer, circulation to three-level separation chamber after the second-order separation room is distilled；It can be realized the cooling for the second-order separation room, level-one separation chamber by the cooperation of cooling dome and water supply mechanism, drainage mechanism, so that each separation chamber can reach required temperature；Supporting plate can be collected final remaining material, and when staff opens sealing mechanism, supporting plate rotation can be driven under traction rope effect, and material skids off automatically, is convenient for feeding.
Description
Technical field
The present invention relates to chemical industry technical field of processing equipment, specifically a kind of Chemical Manufacture distillation still.
Background technique
Distillation still be related to distilling in a kind of Chemical Manufacture used in kettle；It is mainly the existing distillation still of solution in life
It is designed when need to be interrupted maintenance cleaning containing decorating film and when high boiling product in material the problem of during production.
Temperature in current distillation still is relatively more fixed, when needing stepwise distillation to process, needs respectively to convey liquid
In to different distillation equipments, so that entire processing line is longer；It is relatively difficult in feeding, it is surplus without quickly, thoroughly taking out
Excess material.In consideration of it, being had the following characteristics that the present invention provides a kind of Chemical Manufacture distillation still
(1) a kind of Chemical Manufacture distillation still of the present invention, be from top to bottom successively arranged in tank body level-one separation chamber,
The second-order separation room and three-level separation chamber, since the intracorporal temperature of tank from top to bottom gradually rises, the distillation of level-one separation chamber is finished
After be circulated in the second-order separation room, recirculation is realized fast for chemical liquid to three-level separation chamber after the second-order separation room is distilled
Fast stepwise distillation, whole process carry out in tank body, rapid without transfer, circulation.
(2) a kind of Chemical Manufacture distillation still of the present invention is matched by cooling dome and water supply mechanism, drainage mechanism
The cooling that can be realized for the second-order separation room, level-one separation chamber is closed, so that each separation chamber can reach required temperature.
(3) a kind of Chemical Manufacture distillation still of the present invention, supporting plate can be collected final remaining material,
When staff opens sealing mechanism, supporting plate rotation can be driven under traction rope effect, material skids off automatically, convenient for taking
Material.
Summary of the invention
For the problems of the prior art, the present invention provides a kind of Chemical Manufacture distillation stills, in tank body by up to
Under be successively arranged level-one separation chamber, the second-order separation room and three-level separation chamber, since the intracorporal temperature of tank from top to bottom gradually rises
Height, level-one separation chamber are circulated in the second-order separation room after distilling, and recirculation is to three fractions after the second-order separation room is distilled
It from room, realizes and chemical liquid quick segmentation is distilled, whole process carries out in tank body, rapid without transfer, circulation；Pass through
The cooperation of cooling dome and water supply mechanism, drainage mechanism can be realized the cooling for the second-order separation room, level-one separation chamber, so that often
A separation chamber can reach required temperature；Supporting plate can be collected final remaining material, when staff opens
When sealing mechanism, supporting plate rotation can be driven under traction rope effect, material skids off automatically, is convenient for feeding.
The technical solution adopted by the present invention to solve the technical problems is: a kind of Chemical Manufacture distillation still, including heating
Mechanism, tank body, the second-order separation mechanism, level-one separating mechanism, water supply mechanism, drainage mechanism, the first cooling dome and second are cooling
Cover；The top of the heating mechanism is equipped with the tank body, and the heating mechanism is to heat the tank body；The tank body
Inner top layer be equipped with the level-one separating mechanism, the level-one separating mechanism to liquid carry out level-one distillation；Described one
The bottom of grade separating mechanism is equipped with the second-order separation mechanism, and the second-order separation mechanism is to carry out secondary distillation to liquid；
The inner wall of the level-one separating mechanism is equipped with first cooling dome, and it is cold that the inner wall of the second-order separation mechanism is equipped with described second
But it covers, first cooling dome, second cooling dome are to cool down；First cooling dome, second cooling dome are equal
It is communicated with the water supply mechanism, the drainage mechanism, the water supply mechanism, the drainage mechanism are to supply water and drain.
Specifically, the tank body is the cylindrical structure of bottom end semicircle shape, the top of the tank body is equipped with feeding port, described
The interior bottom portion of tank body is three-level separation chamber, and the inner wall of the three-level separation chamber is closely fitted with the supporting plate of semicircle shape, the support
One end of plate is equipped with bail, the inner wall of the hinged three-level separation chamber of the other end of the supporting plate, the outer wall of the tank body with
Sealing mechanism is equipped at three-level separation chamber relative position.
Specifically, the sealing mechanism includes traction rope, sealing plate and handle, described in one end connection of the traction rope
Bail, for the traction rope through the tank body, the other end of the traction rope is fixedly connected with the inner wall top of the sealing plate
The outer wall in portion, the outer wall of the hinged tank body in the bottom of the sealing plate, the sealing plate is equipped with the handle.
Specifically, the heating mechanism includes pedestal and electrical bar, the bottom end of the tank body is embedded in the interior of the pedestal
Portion, the inside of the pedestal are fixed with the electrical bar, and the electrical bar semicircular in shape array distribution is in the bottom of the tank body.
Specifically, the level-one separating mechanism includes level-one separation chamber, the second agitating paddle, the second lower hopper and the second electricity
The top enclosed space of magnet valve, the inside of the tank body and second lower hopper is the level-one separation chamber, a fraction
Second lower hopper is equipped with from the bottom of room, the outlet end of second lower hopper is equipped with the second solenoid valve, and described one
Second agitating paddle is equipped at the center of grade separation chamber, it is cooling that the inner wall of the level-one separation chamber is equipped with cricoid described first
Cover.
Specifically, the second-order separation mechanism includes the second-order separation room, the first lower hopper, the first agitating paddle and the first electricity
Magnet valve, region between first lower hopper and second lower hopper are the second-order separation room, in the second-order separation room
First agitating paddle is equipped at the heart, the outlet end of first lower hopper is equipped with first solenoid valve, the second-order separation
The inner wall of room is equipped with cricoid second cooling dome, and second cooling dome is identical as the described first cooling cover structure, described
Bulge-structure is distributed in the inner wall of first cooling dome.
Specifically, the water supply mechanism includes water inlet supervisor, the first water inlet is in charge of and the second water inlet is in charge of, described first
Water inlet is in charge of to be connected to the input end of first cooling dome, and the input end with second cooling dome is in charge of in second water inlet
Connection, first water inlet is in charge of, the top and bottom end for being connected to the water inlet supervisor are in charge of in second water inlet.
Specifically, the drainage mechanism includes drain header, first row moisture pipe, the first check valve, second row moisture pipe
And second one-way valve, the outlet end of the first row moisture pipe and first cooling dome are interconnected, second draining
It is in charge of and is interconnected with the outlet end of second cooling dome, the first row moisture pipe, the second row moisture pipe connects respectively
Passing to the top and bottom end of the drain header, the outer wall of the first row moisture pipe is equipped with first check valve, and described the
The outer wall that two drainings are in charge of is equipped with the second one-way valve.
Specifically, the water inlet supervisor is connected to suction pump by conduit, the suction pump and cold water storage cistern are interconnected, institute
It states drain header and the cold water storage cistern is connected to by conduit.
Specifically, the outer wall of the tank body is separated with the level-one separation chamber, the second-order separation room and the three-level
Room is separately installed with exhaust valve and thermometer at relative position.
Beneficial effects of the present invention:
(1) a kind of Chemical Manufacture distillation still of the present invention, be from top to bottom successively arranged in tank body level-one separation chamber,
The second-order separation room and three-level separation chamber, since the intracorporal temperature of tank from top to bottom gradually rises, the distillation of level-one separation chamber is finished
After be circulated in the second-order separation room, recirculation is realized fast for chemical liquid to three-level separation chamber after the second-order separation room is distilled
Fast stepwise distillation, whole process carry out in tank body, rapid without transfer, circulation.
(2) a kind of Chemical Manufacture distillation still of the present invention is matched by cooling dome and water supply mechanism, drainage mechanism
The cooling that can be realized for the second-order separation room, level-one separation chamber is closed, so that each separation chamber can reach required temperature.
(3) a kind of Chemical Manufacture distillation still of the present invention, supporting plate can be collected final remaining material,
When staff opens sealing mechanism, supporting plate rotation can be driven under traction rope effect, material skids off automatically, convenient for taking
Material.
Detailed description of the invention
Present invention will be further explained below with reference to the attached drawings and examples.
Fig. 1 is a kind of structural schematic diagram of preferred embodiment of Chemical Manufacture distillation still provided by the invention；
Fig. 2 is tank body integral outer structural schematic diagram shown in FIG. 1；
Fig. 3 is sealing mechanism attachment structure schematic diagram shown in Fig. 2；
Fig. 4 is cooling dome structural schematic diagram shown in FIG. 1.
In figure: 1, heating mechanism, 11, pedestal, 12, electrical bar, 2, tank body, 21, feeding port, 22, sealing mechanism, 221, lead
Messenger, 222, sealing plate, 223, handle, 23, supporting plate, 231, bail, 24, three-level separation chamber, 3, the second-order separation mechanism, 31,
The second-order separation room, the 32, first lower hopper, the 33, first agitating paddle, the 34, first solenoid valve, 4, level-one separating mechanism, 41, one fraction
From room, the 41, second agitating paddle, the 43, second lower hopper, 44, second solenoid valve, 5, water supply mechanism, 51, water inlet supervisor, 52, first
Water inlet is in charge of, and the 53, second water inlet is in charge of, 6, drainage mechanism, 61, drain header, 62, first row moisture pipe, and 63, first is unidirectional
Valve, 64, second row moisture pipe, 65, second one-way valve, the 7, first cooling dome, the 8, second cooling dome, 9, exhaust valve, 9a, temperature
Meter, 9b, cold water storage cistern, 91b, suction pump.
Specific embodiment
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
As Figure 1-Figure 4, a kind of Chemical Manufacture distillation still of the present invention, including heating mechanism 1, tank body 2, two
Grade separating mechanism 3, level-one separating mechanism 4, water supply mechanism 5, drainage mechanism 6, the first cooling dome 7 and the second cooling dome 8；It is described
The top of heating mechanism 1 is equipped with the tank body 2, and the heating mechanism 1 is to heat the tank body 2；The tank body 2
Inner top layer is equipped with the level-one separating mechanism 4, and the level-one separating mechanism 4 is to carry out level-one distillation to liquid；Described one
The bottom of grade separating mechanism 4 is equipped with the second-order separation mechanism 3, and the second-order separation mechanism 3 is to carry out second level steaming to liquid
It evaporates；The inner wall of the level-one separating mechanism 4 is equipped with first cooling dome 7, and the inner wall of the second-order separation mechanism 3 is equipped with described
Second cooling dome 8, first cooling dome 7, second cooling dome 8 are to cool down；First cooling dome 7, described
Two cooling domes 8 are communicated with the water supply mechanism 5, the drainage mechanism 6, the water supply mechanism 5, the drainage mechanism 6 to
It supplies water and drains.
Specifically, the tank body 2 is the cylindrical structure of bottom end semicircle shape, the tank as shown in Figure 1, Figure 2 and shown in Fig. 3
The top of body 2 is equipped with feeding port 21, and the interior bottom portion of the tank body 2 is three-level separation chamber 24, the three-level separation chamber 24 it is interior
Wall is closely fitted with the supporting plate 23 of semicircle shape, and one end of the supporting plate 23 is equipped with bail 231, and the other end of the supporting plate 23 is cut with scissors
The inner wall of the three-level separation chamber 24 is connect, is equipped with sealing at the outer wall of the tank body 2 and 24 relative position of three-level separation chamber
Mechanism 22；Last evaporation separation can be carried out to liquid by three-level separation chamber 24, supporting plate 23 can receive residue
It receives.
Specifically, as shown in figure 3, the sealing mechanism 22 includes traction rope 221, sealing plate 222 and handle 223, institute
The one end for stating traction rope 221 connects the bail 231, and the traction rope 221 is through the tank body 2, the traction rope 221
The other end be fixedly connected at the top of the inner wall of the sealing plate 222, the hinged tank body 2 in the bottom of the sealing plate 222 it is outer
The outer wall of wall, the sealing plate 222 is equipped with the handle 223；Tank body 2 can be sealed by sealing plate 222, and energy
It is enough that supporting plate 23 can be pulled to rotate when opening.
Specifically, the bottom end of the tank body 2 is embedding as shown in Figure 1, the heating mechanism 1 includes pedestal 11 and electrical bar 12
Enter the inside of the pedestal 11, the inside of the pedestal 11 is fixed with the electrical bar 12,12 semicircular in shape of electrical bar
Array distribution is in the bottom of the tank body 2；Enable to heating surface more identical with tank body 2 by the electrical bar 12 of semicircle shape,
So that heating is more abundant.
Specifically, as shown in Figure 1, the level-one separating mechanism 4 includes level-one separation chamber 41, the second agitating paddle 42, second
The top enclosed space of lower hopper 43 and second solenoid valve 44, the inside of the tank body 2 and second lower hopper 43 is institute
Level-one separation chamber 41 is stated, the bottom of the level-one separation chamber 41 is equipped with second lower hopper 43, second lower hopper 43
Outlet end is equipped with the second solenoid valve 44, and second agitating paddle 42 is equipped at the center of the level-one separation chamber 41, described
The inner wall of level-one separation chamber 41 is equipped with cricoid first cooling dome 7；The second-order separation mechanism 3 includes the second-order separation room
31, the first lower hopper 32, the first agitating paddle 33 and the first solenoid valve 34, first lower hopper 32 and second lower hopper
Region between 43 is the second-order separation room 31, and first agitating paddle 33 is equipped at the center of the second-order separation room 31, described
The outlet end of first lower hopper 32 is equipped with first solenoid valve 34, and the inner wall of the second-order separation room 31 is equipped with cricoid described
Second cooling dome 8, second cooling dome 8 is identical as 7 structure of the first cooling dome, the inner wall point of first cooling dome 7
It is furnished with bulge-structure；It is processed by the distillation that level-one separating mechanism 4, the second-order separation mechanism 3 can carry out different phase to liquid,
So that entire processing line is more smooth, continuous, processing efficiency is higher.
Specifically, as shown in Figure 1, the water supply mechanism 5 include water inlet supervisor 51, first water inlet be in charge of 52 and second into
Moisture pipe 53, first water inlet are in charge of 52 and be connected tos with the input end of first cooling dome 7, described second intakes be in charge of 53 and
The input end of second cooling dome 8 is connected to, first water inlet be in charge of 52, second water inlet be in charge of 53 be connected to it is described into
The top and bottom end of water supervisor 51；Cooling can be evacuated in each cooling dome by water supply mechanism 5, realization cools.
Specifically, as shown in Figure 1, the drainage mechanism 6 is unidirectional including drain header 61, first row moisture pipe 62, first
Valve 63, second row moisture pipe 64 and second one-way valve 65, the outlet of the first row moisture pipe 62 and first cooling dome 7
End is interconnected, and the outlet end of the second row moisture pipe 64 and second cooling dome 8 is interconnected, the first row moisture
Pipe 62, the second row moisture pipe 64 are respectively communicated to the top and bottom end of the drain header 61, the first row moisture pipe
62 outer wall is equipped with first check valve 63, and the outer wall of the second row moisture pipe 64 is equipped with the second one-way valve 65；
Circularly cooling can be carried out by the water being heated again water conservancy diversion recovery tank by drainage mechanism 6, and can also adjust circulation speed
Degree, to control cooling velocity.
Specifically, as shown in Figure 1, water inlet supervisor 51 is connected to suction pump 91b, the suction pump 91b by conduit
It is interconnected with cold water storage cistern 9b, the drain header 61 is connected to the cold water storage cistern 9b by conduit；Cooler bin 9b is to provide
Required cold water.
Specifically, as shown in Figure 1, the outer wall of the tank body 2 and the level-one separation chamber 41, the second-order separation room 31 with
And exhaust valve 9 and thermometer 9a are separately installed at 24 relative position of three-level separation chamber；It can be arranged in time by exhaust valve 9
Steam out, thermometer 9a is to observe the indoor temperature of each separation.
Level-one separation chamber 41, the second-order separation room 31 and three-level separation chamber 24 are from top to bottom successively arranged in tank body 2, by
It from top to bottom being gradually risen in the temperature in tank body 2, level-one separation chamber 41 is circulated in the second-order separation room 31 after distilling, and two
Recirculation is realized to three-level separation chamber 24 for the distillation of chemical liquid quick segmentation, whole process after grade separation chamber 31 is distilled
Carried out in tank body 2, it is rapid without transfer, circulation；It can be real by the cooperation of cooling dome and water supply mechanism 5, drainage mechanism 6
Referring now to the cooling of the second-order separation room 31, level-one separation chamber 41, so that each separation chamber can reach required temperature；Supporting plate
23 can be collected final remaining material, when staff opens sealing mechanism 22, can act in traction rope 221
Lower drive supporting plate 23 rotates, and material skids off automatically, is convenient for feeding.Specifically have:
(1) before processing, each solenoid valve, exhaust valve 9 are in off state, and starting electrical bar 12 adds tank body 2
Heat, judges to be classified indoor temperature by thermometer 9a corresponding to each grading room, then adjust again each separation chamber to
Then required temperature starts suction pump when the opening and closing that the temperature of three-level separation chamber 24 can control electrical bar 12 keeps this temperature
Cooling water is pumped into drain header 51 by 91b, then cooling water be in charge of by the first water inlet 52 enter in the first cooling dome 7,
It is in charge of 53 by the second water inlet to enter in the second cooling dome 8, then the indoor heat of cooling water absorption and separation, so that separation chamber
After being reduced to required temperature, cooling to say heat absorption drain header can be entered by first row moisture pipe 62, second row moisture pipe 64
It in 61, is then flowed into tank body 2 again, the circulation temperature lowering for the second-order separation room 31, level-one separation chamber 41 is realized, in order to guarantee
The temperature of the second-order separation room 31 is greater than level-one separation chamber 41, and it is big can to adjust the first check valve 63, the discharge capacity of second one-way valve 65
It is small, so that the discharge capacity of second one-way valve 65 is less than the first check valve 63, to can slow down the cold water circulation in the second cooling dome 8
Speed reduces its refrigeration effect, realizes that the temperature of the second-order separation room 31 is greater than level-one separation chamber 41；Check valve also can avoid draining
The reversed crossfire of water in supervisor 61；
(2) when each temperature reaches desirable value, chemical liquid is discharged into level-one separation chamber 41 by feeding port 21, in height
Under temperature effect, gasification temperature meets the liquid of temperature in level-one separation chamber 41, will gasification separation at first, open level-one separation chamber
Gas discharge is collected separately 41 corresponding exhaust valves 9, and the second agitating paddle 41 is able to drive liquid rotation, accelerates gasification rate；
After separating to level-one separation chamber 41, second solenoid valve 44 is opened, liquid is flowed into the second-order separation room 31, and gasification temperature is full
The liquid of temperature in sufficient the second-order separation room 31, will gasification separation, open the corresponding exhaust valve 9 in the second-order separation room 31 gas is arranged
It is collected separately out, the first agitating paddle 33 can accelerate gasification rate；After the second-order separation room 31 separates, the first solenoid valve is opened
34, so that remaining liq enters on the supporting plate 23 in three-level separation chamber 24, it is needed to be separated all under the action of the highest temperature
Gas will be isolated and is collected separately by the discharge of corresponding exhaust valve 9, and final required solid matter can be stored in supporting plate
On 23；
(3) after completion of processing, staff opens sealing plate 222, during 222 rotating opening of sealing plate, can incite somebody to action
Traction rope 221 pulls out, and traction rope 221 drives supporting plate 23 to be rotated up by bail 231, and the solid matter in supporting plate 23
Can be along supporting plate 23 to one Slideslip of opening of sealing plate 222, when sealing plate 222 fully opens, solid matter will be skidded off,
The present invention is from top to bottom successively arranged level-one separation chamber 41, the second-order separation room 31 and three-level separation in tank body 2
Room 24, since the temperature in tank body 2 from top to bottom gradually rises, level-one separation chamber 41 is circulated to the second-order separation room after distilling
In 31, for recirculation to three-level separation chamber 24, chemical liquid quick segmentation is distilled in realization, whole after the second-order separation room 31 is distilled
A process carries out in tank body 2, rapid without transfer, circulation；Pass through the cooperation of cooling dome and water supply mechanism 5, drainage mechanism 6
It can be realized the cooling for the second-order separation room 31, level-one separation chamber 41, so that each separation chamber can reach required temperature
Degree；Supporting plate 23 can be collected final remaining material, can be in traction rope when staff opens sealing mechanism 22
221 effects are lower to drive supporting plate 23 to rotate, and material skids off automatically, is convenient for feeding.
The basic principles, main features and advantages of the invention have been shown and described above.The technical staff of the industry should
Understand, the present invention is not limited to the above embodiments, and the description in above embodiment and specification only illustrates the present invention
Principle, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these variation and
Improvement is both fallen in the scope of protection of present invention.The claimed scope of the invention is by appended claims and its equivalent
Object defines.
Claims (10)
1. a kind of Chemical Manufacture distillation still, it is characterised in that: including heating mechanism (1), tank body (2), the second-order separation mechanism
(3), level-one separating mechanism (4), water supply mechanism (5), drainage mechanism (6), the first cooling dome (7) and the second cooling dome (8)；Institute
The top for stating heating mechanism (1) is equipped with the tank body (2), and the heating mechanism (1) is to heat the tank body (2)；
The inner top layer of the tank body (2) be equipped with the level-one separating mechanism (4), the level-one separating mechanism (4) to liquid into
The distillation of row level-one；The bottom of the level-one separating mechanism (4) is equipped with the second-order separation mechanism (3), the second-order separation mechanism
(3) to carry out secondary distillation to liquid；The inner wall of the level-one separating mechanism (4) is equipped with first cooling dome (7), described
The inner wall of the second-order separation mechanism (3) is equipped with second cooling dome (8), first cooling dome (7), second cooling dome
(8) to cool down；First cooling dome (7), second cooling dome (8) are communicated with the water supply mechanism (5), described
Drainage mechanism (6), the water supply mechanism (5), the drainage mechanism (6) are to supply water and drain.
2. a kind of Chemical Manufacture distillation still according to claim 1, it is characterised in that: the tank body (2) is bottom end half
The top of the cylindrical structure of round shape, the tank body (2) is equipped with feeding port (21), and the interior bottom portion of the tank body (2) is three-level
Separation chamber (24), the inner wall of the three-level separation chamber (24) are closely fitted with the supporting plate (23) of semicircle shape, the supporting plate (23)
One end is equipped with bail (231), the inner wall of the hinged three-level separation chamber (24) of the other end of the supporting plate (23), the tank body
(2) outer wall is equipped with sealing mechanism (22) at three-level separation chamber (24) relative position.
3. a kind of Chemical Manufacture distillation still according to claim 2, it is characterised in that: the sealing mechanism (22) includes
One end of traction rope (221), sealing plate (222) and handle (223), the traction rope (221) connects the bail
(231), the traction rope (221) is fixedly connected described close through the tank body (2), the other end of the traction rope (221)
At the top of the inner wall of sealing plate (222), the outer wall of the hinged tank body (2) in the bottom of the sealing plate (222), the sealing plate
(222) outer wall is equipped with the handle (223).
4. a kind of Chemical Manufacture distillation still according to claim 1, it is characterised in that: the heating mechanism (1) includes
Pedestal (11) and electrical bar (12), the bottom end of the tank body (2) are embedded in the inside of the pedestal (11), the pedestal (11)
Inside is fixed with the electrical bar (12), and electrical bar (12) the semicircular in shape array distribution is in the bottom of the tank body (2).
5. a kind of Chemical Manufacture distillation still according to claim 2, it is characterised in that: the level-one separating mechanism (4)
Including level-one separation chamber (41), the second agitating paddle (42), the second lower hopper (43) and second solenoid valve (44), the tank body
(2) the top enclosed space of inside and second lower hopper (43) is the level-one separation chamber (41), the level-one separation
The bottom of room (41) is equipped with second lower hopper (43), and the outlet end of second lower hopper (43) is equipped with second electromagnetism
Valve (44) is equipped with second agitating paddle (42) at the center of the level-one separation chamber (41), the level-one separation chamber (41)
Inner wall is equipped with cricoid first cooling dome (7).
6. a kind of Chemical Manufacture distillation still according to claim 5, it is characterised in that: the second-order separation mechanism (3)
Including the second-order separation room (31), the first lower hopper (32), the first agitating paddle (33) and the first solenoid valve (34), under described first
Region between hopper (32) and second lower hopper (43) is the second-order separation room (31), in the second-order separation room (31)
First agitating paddle (33) is equipped at the heart, the outlet end of first lower hopper (32) is equipped with first solenoid valve (34),
The inner wall of the second-order separation room (31) is equipped with cricoid second cooling dome (8), second cooling dome (8) and described the
One cooling dome (7) structure is identical, and bulge-structure is distributed in the inner wall of first cooling dome (7).
7. a kind of Chemical Manufacture distillation still according to claim 1, it is characterised in that: the water supply mechanism (5) includes
Water inlet supervisor (51), first water inlet be in charge of (52) and second water inlet be in charge of (53), it is described first water inlet be in charge of (52) with it is described
The input end of first cooling dome (7) is connected to, and (53) are in charge of in second water inlet and the input end of second cooling dome (8) connects
Logical, (52) are in charge of in first water inlet, top and bottom that (53) are connected to the water inlet supervisor (51) are in charge of in second water inlet
End.
8. a kind of Chemical Manufacture distillation still according to claim 7, it is characterised in that: the drainage mechanism (6) includes
Drain header (61), first row moisture pipe (62), the first check valve (63), second row moisture pipe (64) and second one-way valve
(65), the outlet end of the first row moisture pipe (62) and first cooling dome (7) is interconnected, the second row moisture pipe
(64) it is interconnected with the outlet end of second cooling dome (8), the first row moisture pipe (62), the second row moisture pipe
(64) it is respectively communicated to the top and bottom end of the drain header (61), the outer wall of the first row moisture pipe (62) is equipped with described
The outer wall of first check valve (63), the second row moisture pipe (64) is equipped with the second one-way valve (65).
9. a kind of Chemical Manufacture distillation still according to claim 8, it is characterised in that: the water inlet supervisor (51) passes through
Conduit is connected to suction pump (91b), and the suction pump (91b) and cold water storage cistern (9b) are interconnected, and the drain header (61) is logical
It crosses conduit and is connected to the cold water storage cistern (9b).
10. a kind of Chemical Manufacture distillation still according to claim 6, it is characterised in that: the outer wall of the tank body (2) with
It is installed respectively at the level-one separation chamber (41), the second-order separation room (31) and the three-level separation chamber (24) relative position
There are exhaust valve (9) and thermometer (9a).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811207291.6A CN109173317B (en) | 2018-10-17 | 2018-10-17 | Distillation still for chemical production |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114405044A (en) * | 2022-03-28 | 2022-04-29 | 博润生物科技南通有限公司 | Adjustable distillation device for benzaldehyde production |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3933574A (en) * | 1973-08-07 | 1976-01-20 | Alexandr Fedorovich Zinoviev | Method of and device for isolation of rubber-like polymers from hydrocarbon solutions |
| DE3245556A1 (en) * | 1982-10-22 | 1984-04-26 | Albert Dipl Ing Moegli | Column device for carrying out matter exchange processes or the like |
| CN205205954U (en) * | 2015-10-31 | 2016-05-04 | 重庆丰兴源生态农业发展有限公司 | Eluriate device convenient to vegetables are collected |
| CN205516576U (en) * | 2016-02-19 | 2016-08-31 | 宁波大学 | Washing type stills is exempted from in saving |
| CN206508583U (en) * | 2016-12-30 | 2017-09-22 | 河北野田农用化学有限公司 | Cyclopentadiene rectifying tower top temperature control control equipment |
| CN206965317U (en) * | 2017-07-06 | 2018-02-06 | 江苏天成纸业有限公司 | Papermaking wastewater filter |
| CN207253787U (en) * | 2017-07-27 | 2018-04-20 | 新昌县羽林街道达康机械厂 | A kind of chemical industry distilling apparatus |
-
2018
- 2018-10-17 CN CN201811207291.6A patent/CN109173317B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3933574A (en) * | 1973-08-07 | 1976-01-20 | Alexandr Fedorovich Zinoviev | Method of and device for isolation of rubber-like polymers from hydrocarbon solutions |
| DE3245556A1 (en) * | 1982-10-22 | 1984-04-26 | Albert Dipl Ing Moegli | Column device for carrying out matter exchange processes or the like |
| CN205205954U (en) * | 2015-10-31 | 2016-05-04 | 重庆丰兴源生态农业发展有限公司 | Eluriate device convenient to vegetables are collected |
| CN205516576U (en) * | 2016-02-19 | 2016-08-31 | 宁波大学 | Washing type stills is exempted from in saving |
| CN206508583U (en) * | 2016-12-30 | 2017-09-22 | 河北野田农用化学有限公司 | Cyclopentadiene rectifying tower top temperature control control equipment |
| CN206965317U (en) * | 2017-07-06 | 2018-02-06 | 江苏天成纸业有限公司 | Papermaking wastewater filter |
| CN207253787U (en) * | 2017-07-27 | 2018-04-20 | 新昌县羽林街道达康机械厂 | A kind of chemical industry distilling apparatus |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114405044A (en) * | 2022-03-28 | 2022-04-29 | 博润生物科技南通有限公司 | Adjustable distillation device for benzaldehyde production |
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| CN109173317B (en) | 2021-01-15 |
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