CN109172632A - A kind of shoulder neck is releived Essence and preparation method thereof - Google Patents

A kind of shoulder neck is releived Essence and preparation method thereof Download PDF

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CN109172632A
CN109172632A CN201811191416.0A CN201811191416A CN109172632A CN 109172632 A CN109172632 A CN 109172632A CN 201811191416 A CN201811191416 A CN 201811191416A CN 109172632 A CN109172632 A CN 109172632A
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essence
extract
releived
shoulder neck
preparation
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黄丽仙
阮莉姣
陈小玲
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Guangzhou Liweina Biotechnology Co Ltd
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Guangzhou Liweina Biotechnology Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/488—Pueraria (kudzu)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
    • A61K36/232—Angelica
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    • A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/36—Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
    • A61K47/38—Cellulose; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/0012—Galenical forms characterised by the site of application
    • A61K9/0014—Skin, i.e. galenical aspects of topical compositions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30—Extraction of the material
    • A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction

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Abstract

It releives the components such as Essence, including water, glycerol, propylene glycol, hydroxyethyl cellulose, xanthan gum, releives the preparation method of Essence the invention also discloses a kind of shoulder neck, preparation method is simple, at low cost the invention discloses a kind of shoulder neck；A kind of shoulder neck of the present invention is releived Essence, easy to use, using pure natural Chinese herbal medicine and plants essential oil component, it is not necessary that chemical addition agent is added, external application reduces the intake of human harmful substance, color is limpid, transparent, safe and non-stimulating, has and alleviates DOMS, it feels run-down, the effect to mind at rest, and preparation method is simple, is produced without large scale equipment, entire production environment guarantee is nontoxic sterile, and the quality of finished product Essence is effectively guaranteed.

Description

A kind of shoulder neck is releived Essence and preparation method thereof
Technical field
It releives product the present invention relates to a kind of shoulder neck, specifically a kind of shoulder neck is releived Essence and preparation method thereof.
Background technique
The rhythm of life of modern is fast, and pressure is big, in addition some unsound life styles, such as long-term against computer, long Sit motionless, the problems such as staying up late for work etc. makes body ache, out of strength, lassitude, Essence currently on the market is usually It is deployed by chemical substance, lubrication can only be played the role of for effect, often, cannot not only bring health, also Chemical side effect can be brought, does not have the effect of shoulder neck is releived.
Summary of the invention
It releives Essence and preparation method thereof the purpose of the present invention is to provide a kind of shoulder neck, to solve above-mentioned background technique The problem of middle proposition.
To achieve the above object, the present invention provides the following technical solutions,
A kind of shoulder neck is releived Essence, including following component by weight percentage:
Water 25.97%-63.19%, glycerol 3%-6%, propylene glycol 3%-6%, hydroxyethyl cellulose 0.1%-0.4%, Xanthan gum 0.1%-0.3%, allantoin 0.1%-0.3%, vanillyl butyl ether 0.1%-0.3%, kudzu root extract 10%- 20%, angelica extract 10%-20%, Notogineng Extract 10%-20%, Phenoxyethanol 0.3%-0.5%, decoyl hydroximic acid The bromo- 2- nitropropane -1,3- glycol 0.01%-0.03% of 0.1%-0.2%, 2-；
A kind of shoulder neck is releived the preparation method of Essence, specifically includes the following steps:
S1, prepare emulsion pot, and emulsion pot main cooker, oil cauldron are cleaned up, carry out disinfection to emulsion pot saucepan and oil cauldron；
S2, the extraction for carrying out kudzu root extract, angelica extract, Notogineng Extract, and prepare each group by weight percentage Divide material；
Main cooker is added in S3, Jiang Shui, glycerol, propylene glycol and allantoin, heats to main cooker, after being heated to target temperature, Start to stir homogeneous, hydroxyethyl cellulose and xanthan gum are added in homogenizing process, the material homogeneous of addition is equal to material dispersion Until even no particle clustering phenomena；
After the completion of S4, homogeneous, main cooker held for some time carries out cooling water temperature after heat preservation；
S5, when being cooled to 45 DEG C, vanillyl butyl ether, kudzu root extract, angelica extract, Radix Notoginseng is added in main cooker and mentions Object and Phenoxyethanol are taken, continues to stir homogeneous, stirring certain time keeps material dispersion uniform, continues after homogeneous Cooling water temperature；
S6, when being cooled to 42 DEG C, close cooling water, stop cooling, toward main cooker in addition decoyl hydroximic acid and the bromo- 2- nitre of 2- Base propane -1,3- glycol continues to stir homogeneous；
S7, standing are cooled to room temperature, and sampling inspection declaration detection discharges after detection is qualified, obtains target product semi-finished product；
S8, packaging coding obtain finished product, storage storage.
Further, in the step S1, disinfection way is matched using high temperature and high pressure steam disinfection and ultraviolet radiation disinfection Conjunction carries out disinfection.
Further, in the step S2, the extracting method of kudzu root extract are as follows: appropriate pueraria lobata pulverizing medicinal materials, sieving are taken, Powder is obtained, the NaOH aqueous solution that concentration is 0.2mo1/L is added, is the mixing of 1:10 ratio in solid-to-liquid ratio, hot dipping mentions at 80 DEG C 2h is taken, is repeated 2 times, is filtered, it is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, under the revolving speed of 4000r/min Centrifuge separation, goes supernatant to obtain sediment, as kudzu root extract；
The extracting method of angelica extract is；Appropriate Radix Angelicae Sinensis pulverizing medicinal materials, sieving are taken, powder is obtained, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as angelica extract；
The extracting method of Notogineng Extract are as follows: take appropriate pseudo-ginseng to crush, sieving, obtain powder, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as Notogineng Extract.
Further, in the step S3, heating method uses steam heating method, and heating target temperature is 80-85 DEG C, Mixing speed is specially 25r/min.
Further, in the step S4, soaking time is specially 20min.
Further, in the step S5, mixing time 5min, speed of agitator 25r/min.
Further, in the step S6, mixing time is specially 10min, mixing speed 40r/min.
A kind of shoulder neck is releived the application method of Essence, and shoulder neck Essence of releiving is coated on shoulder and skin of neck table Face, massage 10-20min absorb.
Compared with prior art, the invention has the advantages that
A kind of shoulder neck of the present invention is releived Essence, using pure natural Chinese herbal medicine and plants essential oil component, it is not necessary that chemistry is added Additive, external application reduce the intake of human harmful substance, and color is limpid, transparent, safe and non-stimulating, have and alleviate DOMS, It feels run-down, the effect to mind at rest, and preparation method is simple, is produced without large scale equipment, entire production environment Guarantee nontoxic sterile, the quality of finished product Essence is effectively guaranteed.
Specific embodiment
In order to deepen the understanding of the present invention, the present invention will be described in further detail with reference to the examples below, implements below Example for explaining only the invention, is not intended to limit the scope of the present invention..
Embodiment 1
A kind of shoulder neck is releived Essence, including following component by weight percentage:
Water 25.97%, glycerol 6%, propylene glycol 6%, hydroxyethyl cellulose 0.4%, xanthan gum 0.3%, allantoin 0.3%, vanillyl butyl ether 0.3%, kudzu root extract 20%, angelica extract 20%, Notogineng Extract 20%, Phenoxyethanol 0.5%, the bromo- 2- nitropropane -1,3- glycol 0.03% of decoyl hydroximic acid 0.2%, 2-.
A kind of shoulder neck is releived the preparation method of Essence, specifically includes the following steps:
S1, prepare emulsion pot, and emulsion pot main cooker, oil cauldron are cleaned up, carry out disinfection to emulsion pot saucepan and oil cauldron；
S2, the extraction for carrying out kudzu root extract, angelica extract, Notogineng Extract, and prepare each group by weight percentage Divide material；
Main cooker is added in S3, Jiang Shui, glycerol, propylene glycol and allantoin, heats to main cooker, after being heated to target temperature, Start to stir homogeneous, hydroxyethyl cellulose and xanthan gum are added in homogenizing process, the material homogeneous of addition is equal to material dispersion Until even no particle clustering phenomena；
After the completion of S4, homogeneous, main cooker held for some time carries out cooling water temperature after heat preservation；
S5, when being cooled to 45 DEG C, vanillyl butyl ether, kudzu root extract, angelica extract, Radix Notoginseng is added in main cooker and mentions Object and Phenoxyethanol are taken, continues to stir homogeneous, stirring certain time keeps material dispersion uniform, continues after homogeneous Cooling water temperature；
S6, when being cooled to 42 DEG C, close cooling water, stop cooling, toward main cooker in addition decoyl hydroximic acid and the bromo- 2- nitre of 2- Base propane -1,3- glycol continues to stir homogeneous；
S7, standing are cooled to room temperature, and sampling inspection declaration detection discharges after detection is qualified, obtains target product semi-finished product；
S8, packaging coding obtain finished product, storage storage；
In the step S1, disinfection way is disappeared using high temperature and high pressure steam disinfection and ultraviolet radiation disinfection cooperation Poison；
In the step S2, the extracting method of kudzu root extract are as follows: appropriate pueraria lobata pulverizing medicinal materials, sieving are taken, powder is obtained, The NaOH aqueous solution that concentration is 0.2mo1/L is added, is the mixing of 1:10 ratio in solid-to-liquid ratio, 2h is extracted in hot dipping at 80 DEG C, is repeated It 2 times, filtering, the hydrochloric acid tune pH value that addition mass concentration is 3% in filtrate to 7 is centrifugated under the revolving speed of 4000r/min, Supernatant is gone to obtain sediment, as kudzu root extract；
The extracting method of angelica extract is；Appropriate Radix Angelicae Sinensis pulverizing medicinal materials, sieving are taken, powder is obtained, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as angelica extract；
The extracting method of Notogineng Extract are as follows: take appropriate pseudo-ginseng to crush, sieving, obtain powder, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as Notogineng Extract；
In the step S3, heating method uses steam heating method, and heating target temperature is 80 DEG C, and mixing speed is specific For 25r/min；
In the step S4, soaking time is specially 20min；
In the step S5, mixing time 5min, speed of agitator 25r/min；
In the step S6, mixing time is specially 10min, mixing speed 40r/min.
The shoulder neck prepared in the present embodiment is releived Essence, is suitable for neutral skin crowd and is used, will not generate to skin Stimulation, and good absorption effect.
Embodiment 2
A kind of shoulder neck is releived Essence, including following component by weight percentage:
Water 53.88%, glycerol 3.75%, propylene glycol 3.75%, hydroxyethyl cellulose 0.175%, xanthan gum 0.15%, urine Bursin 0.15%, vanillyl butyl ether 0.15%, kudzu root extract 12.5%, angelica extract 12.5%, Notogineng Extract 12.5%, the bromo- 2- nitropropane -1,3- glycol 0.02% of Phenoxyethanol 0.35%, decoyl hydroximic acid 0.125%, 2-.
A kind of shoulder neck is releived the preparation method of Essence, specifically includes the following steps:
S1, prepare emulsion pot, and emulsion pot main cooker, oil cauldron are cleaned up, carry out disinfection to emulsion pot saucepan and oil cauldron；
S2, the extraction for carrying out kudzu root extract, angelica extract, Notogineng Extract, and prepare each group by weight percentage Divide material；
Main cooker is added in S3, Jiang Shui, glycerol, propylene glycol and allantoin, heats to main cooker, after being heated to target temperature, Start to stir homogeneous, hydroxyethyl cellulose and xanthan gum are added in homogenizing process, the material homogeneous of addition is equal to material dispersion Until even no particle clustering phenomena；
After the completion of S4, homogeneous, main cooker held for some time carries out cooling water temperature after heat preservation；
S5, when being cooled to 45 DEG C, vanillyl butyl ether, kudzu root extract, angelica extract, Radix Notoginseng is added in main cooker and mentions Object and Phenoxyethanol are taken, continues to stir homogeneous, stirring certain time keeps material dispersion uniform, continues after homogeneous Cooling water temperature；
S6, when being cooled to 42 DEG C, close cooling water, stop cooling, toward main cooker in addition decoyl hydroximic acid and the bromo- 2- nitre of 2- Base propane -1,3- glycol continues to stir homogeneous；
S7, standing are cooled to room temperature, and sampling inspection declaration detection discharges after detection is qualified, obtains target product semi-finished product；
S8, packaging coding obtain finished product, storage storage；
In the step S1, disinfection way is disappeared using high temperature and high pressure steam disinfection and ultraviolet radiation disinfection cooperation Poison；
In the step S2, the extracting method of kudzu root extract are as follows: appropriate pueraria lobata pulverizing medicinal materials, sieving are taken, powder is obtained, The NaOH aqueous solution that concentration is 0.2mo1/L is added, is the mixing of 1:10 ratio in solid-to-liquid ratio, 2h is extracted in hot dipping at 80 DEG C, is repeated It 2 times, filtering, the hydrochloric acid tune pH value that addition mass concentration is 3% in filtrate to 7 is centrifugated under the revolving speed of 4000r/min, Supernatant is gone to obtain sediment, as kudzu root extract；
The extracting method of angelica extract is；Appropriate Radix Angelicae Sinensis pulverizing medicinal materials, sieving are taken, powder is obtained, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as angelica extract；
The extracting method of Notogineng Extract are as follows: take appropriate pseudo-ginseng to crush, sieving, obtain powder, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as Notogineng Extract；
In the step S3, heating method uses steam heating method, and heating target temperature is 82 DEG C, and mixing speed is specific For 25r/min；
In the step S4, soaking time is specially 20min；
In the step S5, mixing time 5min, speed of agitator 25r/min；
In the step S6, mixing time is specially 10min, mixing speed 40r/min.
The shoulder neck prepared in the present embodiment is releived Essence, is suitable for Oily crowd and is used, will not generate to skin Stimulation, and good absorption effect.
Embodiment 3
A kind of shoulder neck is releived Essence, including following component by weight percentage:
Water 44.58%, glycerol 4.5%, propylene glycol 4.5%, hydroxyethyl cellulose 0.25%, xanthan gum 0.2%, allantoin 0.2%, vanillyl butyl ether 0.2%, kudzu root extract 15%, angelica extract 15%, Notogineng Extract 15%, Phenoxyethanol 0.4%, the bromo- 2- nitropropane -1,3- glycol 0.02% of decoyl hydroximic acid 0.15%, 2-；
A kind of shoulder neck is releived the preparation method of Essence, specifically includes the following steps:
S1, prepare emulsion pot, and emulsion pot main cooker, oil cauldron are cleaned up, carry out disinfection to emulsion pot saucepan and oil cauldron；
S2, the extraction for carrying out kudzu root extract, angelica extract, Notogineng Extract, and prepare each group by weight percentage Divide material；
Main cooker is added in S3, Jiang Shui, glycerol, propylene glycol and allantoin, heats to main cooker, after being heated to target temperature, Start to stir homogeneous, hydroxyethyl cellulose and xanthan gum are added in homogenizing process, the material homogeneous of addition is equal to material dispersion Until even no particle clustering phenomena；
After the completion of S4, homogeneous, main cooker held for some time carries out cooling water temperature after heat preservation；
S5, when being cooled to 45 DEG C, vanillyl butyl ether, kudzu root extract, angelica extract, Radix Notoginseng is added in main cooker and mentions Object and Phenoxyethanol are taken, continues to stir homogeneous, stirring certain time keeps material dispersion uniform, continues after homogeneous Cooling water temperature；
S6, when being cooled to 42 DEG C, close cooling water, stop cooling, toward main cooker in addition decoyl hydroximic acid and the bromo- 2- nitre of 2- Base propane -1,3- glycol continues to stir homogeneous；
S7, standing are cooled to room temperature, and sampling inspection declaration detection discharges after detection is qualified, obtains target product semi-finished product；
S8, packaging coding obtain finished product, storage storage；
In the step S1, disinfection way is disappeared using high temperature and high pressure steam disinfection and ultraviolet radiation disinfection cooperation Poison；
In the step S2, the extracting method of kudzu root extract are as follows: appropriate pueraria lobata pulverizing medicinal materials, sieving are taken, powder is obtained, The NaOH aqueous solution that concentration is 0.2mo1/L is added, is the mixing of 1:10 ratio in solid-to-liquid ratio, 2h is extracted in hot dipping at 80 DEG C, is repeated It 2 times, filtering, the hydrochloric acid tune pH value that addition mass concentration is 3% in filtrate to 7 is centrifugated under the revolving speed of 4000r/min, Supernatant is gone to obtain sediment, as kudzu root extract；
The extracting method of angelica extract is；Appropriate Radix Angelicae Sinensis pulverizing medicinal materials, sieving are taken, powder is obtained, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as angelica extract；
The extracting method of Notogineng Extract are as follows: take appropriate pseudo-ginseng to crush, sieving, obtain powder, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as Notogineng Extract；
In the step S3, heating method uses steam heating method, and heating target temperature is 83 DEG C, and mixing speed is specific For 25r/min；
In the step S4, soaking time is specially 20min；
In the step S5, mixing time 5min, speed of agitator 25r/min；
In the step S6, mixing time is specially 10min, mixing speed 40r/min.
The shoulder neck prepared in the present embodiment is releived Essence, is suitable for dry skin crowd and is used, will not generate to skin Stimulation, and good absorption effect.
Embodiment 4
A kind of shoulder neck is releived Essence, including following component by weight percentage:
Water 35.27%, glycerol 5.25%, propylene glycol 5.25%, hydroxyethyl cellulose 0.33%, xanthan gum 0.25%, urine Bursin 0.25%, vanillyl butyl ether 0.25%, kudzu root extract 17.5%, angelica extract 17.5%, Notogineng Extract 17.5%, the bromo- 2- nitropropane -1,3- glycol 0.025% of Phenoxyethanol 0.45%, decoyl hydroximic acid 0.175%, 2-.
A kind of shoulder neck is releived the preparation method of Essence, specifically includes the following steps:
S1, prepare emulsion pot, and emulsion pot main cooker, oil cauldron are cleaned up, carry out disinfection to emulsion pot saucepan and oil cauldron；
S2, the extraction for carrying out kudzu root extract, angelica extract, Notogineng Extract, and prepare each group by weight percentage Divide material；
Main cooker is added in S3, Jiang Shui, glycerol, propylene glycol and allantoin, heats to main cooker, after being heated to target temperature, Start to stir homogeneous, hydroxyethyl cellulose and xanthan gum are added in homogenizing process, the material homogeneous of addition is equal to material dispersion Until even no particle clustering phenomena；
After the completion of S4, homogeneous, main cooker held for some time carries out cooling water temperature after heat preservation；
S5, when being cooled to 45 DEG C, vanillyl butyl ether, kudzu root extract, angelica extract, Radix Notoginseng is added in main cooker and mentions Object and Phenoxyethanol are taken, continues to stir homogeneous, stirring certain time keeps material dispersion uniform, continues after homogeneous Cooling water temperature；
S6, when being cooled to 42 DEG C, close cooling water, stop cooling, toward main cooker in addition decoyl hydroximic acid and the bromo- 2- nitre of 2- Base propane -1,3- glycol continues to stir homogeneous；
S7, standing are cooled to room temperature, and sampling inspection declaration detection discharges after detection is qualified, obtains target product semi-finished product；
S8, packaging coding obtain finished product, storage storage；
In the step S1, disinfection way is disappeared using high temperature and high pressure steam disinfection and ultraviolet radiation disinfection cooperation Poison；
In the step S2, the extracting method of kudzu root extract are as follows: appropriate pueraria lobata pulverizing medicinal materials, sieving are taken, powder is obtained, The NaOH aqueous solution that concentration is 0.2mo1/L is added, is the mixing of 1:10 ratio in solid-to-liquid ratio, 2h is extracted in hot dipping at 80 DEG C, is repeated It 2 times, filtering, the hydrochloric acid tune pH value that addition mass concentration is 3% in filtrate to 7 is centrifugated under the revolving speed of 4000r/min, Supernatant is gone to obtain sediment, as kudzu root extract；
The extracting method of angelica extract is；Appropriate Radix Angelicae Sinensis pulverizing medicinal materials, sieving are taken, powder is obtained, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as angelica extract；
The extracting method of Notogineng Extract are as follows: take appropriate pseudo-ginseng to crush, sieving, obtain powder, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as Notogineng Extract；
In the step S3, heating method uses steam heating method, and heating target temperature is 84 DEG C, and mixing speed is specific For 25r/min；
In the step S4, soaking time is specially 20min；
In the step S5, mixing time 5min, speed of agitator 25r/min；
In the step S6, mixing time is specially 10min, mixing speed 40r/min.
The shoulder neck prepared in the present embodiment is releived Essence, is suitable for combination crowd and is used, will not produce to skin Raw stimulation, and good absorption effect.
Embodiment 5
A kind of shoulder neck is releived Essence, including following component by weight percentage:
Water 63.19%%, glycerol 3%, propylene glycol 3%, hydroxyethyl cellulose 0.1%, xanthan gum 0.1%, allantoin 0.1%, vanillyl butyl ether 0.1%, kudzu root extract 10%, angelica extract 10%-, Notogineng Extract 10%, benzene oxygen second The bromo- 2- nitropropane -1,3- glycol 0.01% of alcohol 0.3%, decoyl hydroximic acid 0.1%, 2-.
A kind of shoulder neck is releived the preparation method of Essence, specifically includes the following steps:
S1, prepare emulsion pot, and emulsion pot main cooker, oil cauldron are cleaned up, carry out disinfection to emulsion pot saucepan and oil cauldron；
S2, the extraction for carrying out kudzu root extract, angelica extract, Notogineng Extract, and prepare each group by weight percentage Divide material；
Main cooker is added in S3, Jiang Shui, glycerol, propylene glycol and allantoin, heats to main cooker, after being heated to target temperature, Start to stir homogeneous, hydroxyethyl cellulose and xanthan gum are added in homogenizing process, the material homogeneous of addition is equal to material dispersion Until even no particle clustering phenomena；
After the completion of S4, homogeneous, main cooker held for some time carries out cooling water temperature after heat preservation；
S5, when being cooled to 45 DEG C, vanillyl butyl ether, kudzu root extract, angelica extract, Radix Notoginseng is added in main cooker and mentions Object and Phenoxyethanol are taken, continues to stir homogeneous, stirring certain time keeps material dispersion uniform, continues after homogeneous Cooling water temperature；
S6, when being cooled to 42 DEG C, close cooling water, stop cooling, toward main cooker in addition decoyl hydroximic acid and the bromo- 2- nitre of 2- Base propane -1,3- glycol continues to stir homogeneous；
S7, standing are cooled to room temperature, and sampling inspection declaration detection discharges after detection is qualified, obtains target product semi-finished product；
S8, packaging coding obtain finished product, storage storage；
In the step S1, disinfection way is disappeared using high temperature and high pressure steam disinfection and ultraviolet radiation disinfection cooperation Poison；
In the step S2, the extracting method of kudzu root extract are as follows: appropriate pueraria lobata pulverizing medicinal materials, sieving are taken, powder is obtained, The NaOH aqueous solution that concentration is 0.2mo1/L is added, is the mixing of 1:10 ratio in solid-to-liquid ratio, 2h is extracted in hot dipping at 80 DEG C, is repeated It 2 times, filtering, the hydrochloric acid tune pH value that addition mass concentration is 3% in filtrate to 7 is centrifugated under the revolving speed of 4000r/min, Supernatant is gone to obtain sediment, as kudzu root extract；
The extracting method of angelica extract is；Appropriate Radix Angelicae Sinensis pulverizing medicinal materials, sieving are taken, powder is obtained, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as angelica extract；
The extracting method of Notogineng Extract are as follows: take appropriate pseudo-ginseng to crush, sieving, obtain powder, concentration, which is added, is The NaOH aqueous solution of 0.2mo1/L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, It is 3% hydrochloric acid tune pH value to 7 that mass concentration is added in filtrate, is centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain Sediment, as Notogineng Extract；
In the step S3, heating method uses steam heating method, and heating target temperature is 85 DEG C, and mixing speed is specific For 25r/min；
In the step S4, soaking time is specially 20min；
In the step S5, mixing time 5min, speed of agitator 25r/min；
In the step S6, mixing time is specially 10min, mixing speed 40r/min.
The shoulder neck prepared in the present embodiment is releived Essence, is suitable for sensitive crowd and is used, will not produce to skin Raw stimulation, and good absorption effect.
A kind of shoulder neck of the present invention is releived Essence, when in use, shoulder neck Essence of releiving is applied to shoulder and neck skin Skin surface, massage 10-20min absorb.
A kind of shoulder neck of the present invention is releived Essence, using pure natural Chinese herbal medicine and plants essential oil component, it is not necessary that chemistry is added Additive, external application reduce the intake of human harmful substance, and color is limpid, transparent, safe and non-stimulating, have and alleviate DOMS, It feels run-down, the effect to mind at rest, and preparation method is simple, is produced without large scale equipment, entire production environment Guarantee nontoxic sterile, the quality of finished product Essence is effectively guaranteed.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and what is described in the above embodiment and the description is only the present invention Principle, various changes and improvements may be made to the invention without departing from the spirit and scope of the present invention, these variation and Improvement is both fallen in the range of claimed invention.The present invention claims protection scope by appended claims and its Equivalent defines.

Claims (10)

  1. The Essence 1. a kind of shoulder neck is releived, which is characterized in that including following component by weight percentage:
    Water 25.97-63.19%%, glycerol 3%-6%, propylene glycol 3%-6%, hydroxyethyl cellulose 0.1%-0.4%, xanthan Glue 0.1%-0.3%, allantoin 0.1%-0.3%, vanillyl butyl ether 0.1%-0.3%, kudzu root extract 10%-20%, Angelica extract 10%-20%, Notogineng Extract 10%-20%, Phenoxyethanol 0.3%-0.5%, decoyl hydroximic acid 0.1%- 0.2%, the bromo- 2- nitropropane -1,3- glycol 0.01%-0.03% of 2-.
  2. The Essence 2. a kind of shoulder neck according to claim 1 is releived, which is characterized in that including it is following by weight percentage Component:
    Water 44.58%, glycerol 4.5%, propylene glycol 4.5%, hydroxyethyl cellulose 0.25%, xanthan gum 0.2%, allantoin 0.2%, vanillyl butyl ether 0.2%, kudzu root extract 15%, angelica extract 15%, Notogineng Extract 15%, Phenoxyethanol 0.4%, the bromo- 2- nitropropane -1,3- glycol 0.02% of decoyl hydroximic acid 0.15%, 2-.
  3. The preparation method of Essence 3. a kind of shoulder neck is releived, which is characterized in that specifically includes the following steps:
    S1, prepare emulsion pot, and emulsion pot main cooker, oil cauldron are cleaned up, carry out disinfection to emulsion pot saucepan and oil cauldron；
    S2, the extraction for carrying out kudzu root extract, angelica extract, Notogineng Extract, and prepare each component material by weight percentage Material；
    Main cooker is added in S3, Jiang Shui, glycerol, propylene glycol and allantoin, heats to main cooker, after being heated to target temperature, starts Homogeneous is stirred, hydroxyethyl cellulose and xanthan gum is added in homogenizing process, by the material homogeneous of addition to the uniform nothing of material dispersion Until particle clustering phenomena；
    After the completion of S4, homogeneous, main cooker held for some time carries out cooling water temperature after heat preservation；
    S5, when being cooled to 45 DEG C, vanillyl butyl ether, kudzu root extract, angelica extract, Notogineng Extract are added in main cooker And Phenoxyethanol, continue to stir homogeneous, stirring certain time keeps material dispersion uniform, continues to cool down after homogeneous Water cooling；
    S6, when being cooled to 42 DEG C, close cooling water, stop cooling, toward main cooker in addition decoyl hydroximic acid and the bromo- 2- nitro third of 2- Alkane -1,3- glycol continues to stir homogeneous；
    S7, standing are cooled to room temperature, and sampling inspection declaration detection discharges after detection is qualified, obtains target product semi-finished product；
    S8, packaging coding obtain finished product, storage storage.
  4. The preparation method of Essence 4. a kind of shoulder neck according to claim 3 is releived, which is characterized in that the step S1 In, disinfection way is carried out disinfection using high temperature and high pressure steam disinfection and ultraviolet radiation disinfection cooperation.
  5. The preparation method of Essence 5. a kind of shoulder neck according to claim 3 is releived, which is characterized in that the step S2 In, the extracting method of kudzu root extract are as follows: take appropriate pueraria lobata pulverizing medicinal materials, sieving, obtain powder, addition concentration is 0.2mo1/L NaOH aqueous solution, be that 1:10 ratio mixes in solid-to-liquid ratio, 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, filter, in filtrate plus Enter the hydrochloric acid tune pH value that mass concentration is 3% to 7, be centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain sediment, As kudzu root extract；
    The extracting method of angelica extract is；Appropriate Radix Angelicae Sinensis pulverizing medicinal materials, sieving are taken, powder is obtained, addition concentration is 0.2mo1/ The NaOH aqueous solution of L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, and is added in filtrate Enter the hydrochloric acid tune pH value that mass concentration is 3% to 7, be centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain sediment, As angelica extract；
    The extracting method of Notogineng Extract are as follows: take appropriate pseudo-ginseng to crush, sieving, obtain powder, addition concentration is 0.2mo1/ The NaOH aqueous solution of L is the mixing of 1:10 ratio in solid-to-liquid ratio, and 2h is extracted in hot dipping at 80 DEG C, is repeated 2 times, and is filtered, and is added in filtrate Enter the hydrochloric acid tune pH value that mass concentration is 3% to 7, be centrifugated under the revolving speed of 4000r/min, supernatant is gone to obtain sediment, As Notogineng Extract.
  6. The preparation method of Essence 6. a kind of shoulder neck according to claim 3 is releived, which is characterized in that the step S3 In, heating method uses steam heating method, and heating target temperature is 80-85 DEG C, and mixing speed is specially 25r/min.
  7. The preparation method of Essence 7. a kind of shoulder neck according to claim 3 is releived, which is characterized in that the step S4 In, soaking time is specially 20min.
  8. The preparation method of Essence 8. a kind of shoulder neck according to claim 3 is releived, which is characterized in that the step S5 In, mixing time 5min, speed of agitator 25r/min.
  9. The preparation method of Essence 9. a kind of shoulder neck according to claim 3 is releived, which is characterized in that the step S6 In, mixing time is specially 10min, mixing speed 40r/min.
  10. The application method of Essence 10. a kind of shoulder neck is releived, which is characterized in that shoulder neck Essence of releiving is coated on shoulder and neck Portion's skin surface, massage 10-20min absorb.
CN201811191416.0A 2018-10-12 2018-10-12 A kind of shoulder neck is releived Essence and preparation method thereof Pending CN109172632A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110123934A (en) * 2019-06-06 2019-08-16 广州市裕朝化妆品有限公司 A kind of shoulder neck, which is releived, raises Essence
CN111450227A (en) * 2020-04-25 2020-07-28 福建百想生物科技有限公司 Plant essential oil for relieving shoulder and neck ache

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CN107261046A (en) * 2017-06-04 2017-10-20 张志杰 Multi-functional traditional Chinese medicine massage oil

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CN202536915U (en) * 2012-04-21 2012-11-21 邵明省 Traditional Chinese medicine health-care pillow with cervical vertebra massaging function
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110123934A (en) * 2019-06-06 2019-08-16 广州市裕朝化妆品有限公司 A kind of shoulder neck, which is releived, raises Essence
CN111450227A (en) * 2020-04-25 2020-07-28 福建百想生物科技有限公司 Plant essential oil for relieving shoulder and neck ache

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Application publication date: 20190111