CN109162092A - A kind of production technology of anti-ultraviolet functional dacron - Google Patents
A kind of production technology of anti-ultraviolet functional dacron Download PDFInfo
- Publication number
- CN109162092A CN109162092A CN201810889849.7A CN201810889849A CN109162092A CN 109162092 A CN109162092 A CN 109162092A CN 201810889849 A CN201810889849 A CN 201810889849A CN 109162092 A CN109162092 A CN 109162092A
- Authority
- CN
- China
- Prior art keywords
- product
- parts
- uvioresistant
- obtains
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000005020 polyethylene terephthalate Substances 0.000 title claims abstract description 31
- 229920004934 Dacron® Polymers 0.000 title claims abstract description 28
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 238000005516 engineering process Methods 0.000 title claims abstract description 15
- 238000002803 maceration Methods 0.000 claims abstract description 30
- 238000001035 drying Methods 0.000 claims abstract description 22
- 238000005096 rolling process Methods 0.000 claims abstract description 5
- 238000002791 soaking Methods 0.000 claims abstract description 5
- 239000000047 product Substances 0.000 claims description 89
- 239000000243 solution Substances 0.000 claims description 32
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 22
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 21
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 18
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- 239000011259 mixed solution Substances 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 11
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 10
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 10
- ZXDDPOHVAMWLBH-UHFFFAOYSA-N 2,4-Dihydroxybenzophenone Chemical compound OC1=CC(O)=CC=C1C(=O)C1=CC=CC=C1 ZXDDPOHVAMWLBH-UHFFFAOYSA-N 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 8
- 239000004816 latex Substances 0.000 claims description 8
- 229920000126 latex Polymers 0.000 claims description 8
- 239000003208 petroleum Substances 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 5
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 239000000084 colloidal system Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- HGWOWDFNMKCVLG-UHFFFAOYSA-N [O--].[O--].[Ti+4].[Ti+4] Chemical compound [O--].[O--].[Ti+4].[Ti+4] HGWOWDFNMKCVLG-UHFFFAOYSA-N 0.000 claims description 2
- 230000035484 reaction time Effects 0.000 claims description 2
- 239000006228 supernatant Substances 0.000 claims description 2
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 claims 1
- 239000011806 microball Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 238000004140 cleaning Methods 0.000 abstract description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 229920004933 Terylene® Polymers 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 1
- 229940123457 Free radical scavenger Drugs 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 230000006750 UV protection Effects 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000004611 light stabiliser Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000004224 protection Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000002516 radical scavenger Substances 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000012209 synthetic fiber Substances 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/328—Amines the amino group being bound to an acyclic or cycloaliphatic carbon atom
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/35—Abrasion, pilling or fibrillation resistance
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of production technologies of anti-ultraviolet functional dacron, comprising the following steps: A, cleaning dacron are simultaneously dried, and a product are obtained；Drying temperature is 50-60 DEG C, time 3-4min；B, a product are put into uvioresistant maceration extract and are impregnated, obtain b product；Bath raio between a product and uvioresistant maceration extract is 1:30, and the temperature of uvioresistant maceration extract is 28-33 DEG C, soaking time 40-45min；C, b product are squeezed, rolling surplus is 95-98%, obtains c product；D, c product are subjected to prebake, obtain d product；The temperature of prebake is 55-65 DEG C, time 3-4min；E, microwave drying processing is carried out to d product, obtains e product；F, e product are cleaned, f1 product are obtained；Using 50-60 DEG C of temperature, by f1 product, drying to constant weight, obtains final finished product.The present invention has the characteristics that UVResistant effect can be effectively improved and improves durability.
Description
Technical field
The present invention relates to a kind for the treatment of process of dacron, especially a kind of production of anti-ultraviolet functional dacron
Technique.
Background technique
Terylene has rapidly become the maximum synthetic fibers of usage amount in daily life since putting goods on the market, but terylene
The uvioresistant ability of fabric is poor, needs to carry out subsequent anti-ultraviolet radiation treatment to dacron.At present both at home and abroad for terylene
The UV resistance method of fabric mainly adds the light stabilizers such as excitation state quencher and free radical scavenger and high molecular material carries out
Blending and modifying, but due to such lesser reason of method molecular weight these small molecule in prolonged use and process
Stabilizer to overflow its durability poor.Therefore, existing technology is bad there is UVResistant effect and durability is poor
Problem.
Summary of the invention
The object of the present invention is to provide a kind of production technologies of anti-ultraviolet functional dacron.The present invention has energy
The characteristics of being enough effectively improved UVResistant effect and improving durability.
A kind of technical solution of the present invention: production technology of anti-ultraviolet functional dacron, comprising the following steps:
A, it cleans dacron and dries, obtain a product；Drying temperature is 50-60 DEG C, time 3-4min；
B, a product are put into uvioresistant maceration extract and are impregnated, obtain b product；Bath raio between a product and uvioresistant maceration extract is 1:
30, the temperature of uvioresistant maceration extract is 28-33 DEG C, soaking time 40-45min；
C, b product are squeezed, rolling surplus is 95-98%, obtains c product；
D, c product are subjected to prebake, obtain d product；The temperature of prebake is 55-65 DEG C, time 3-4min；
E, microwave drying processing is carried out to d product, obtains e product；
F, e product are cleaned, f1 product are obtained；Using 50-60 DEG C of temperature, by f1 product, drying to constant weight, obtains final finished product.
In a kind of production technology of anti-ultraviolet functional dacron above-mentioned, microwave baking is carried out to d product in the step E
Dry-cure method particularly includes: first use microwave output power to heat 20-35s to d product for the power section of 3-4kW, obtain d1 product；
Then, 50-60s is heated to d1 product with the power section that microwave output power is 40-45kW, obtains d2 product；Then it is exported with microwave
The power section that power is 70-80kW heats 10-15s to d2 product, obtains e product.
In a kind of production technology of anti-ultraviolet functional dacron above-mentioned, the uvioresistant maceration extract includes following
The component of parts by weight: 2,4-DihydroxyBenzophenone, 12-15 parts；Triethylamine, 20-22 parts；Ethyl acetate, 1-2 parts；Petroleum ether,
8-16 parts；Sodium bicarbonate solution, 30-35 parts；Dehydrated alcohol, 15-16 parts；Nano-titanium dioxide, 2-3 parts；Monodisperse colloid is micro-
1-2 parts of ball；Water, 10-15 parts.
In a kind of production technology of anti-ultraviolet functional dacron above-mentioned, the preparation side of the uvioresistant maceration extract
Method: 1) dissolving 2,4-DihydroxyBenzophenone and triethylamine in reaction flask, obtains mixed solution a；2) under condition of ice bath,
By ethyl acetate and petroleum ether and mixed solution a hybrid reaction, reaction time 5h obtains mixed solution b；3) sodium bicarbonate is used
After solution and mixed solution B hybrid reaction, 1-2h is stood, supernatant liquid is taken to obtain solution c；4) solution c is evaporated, obtains object
Product d；5), that article d is soluble in water, obtain solution e；6) nano-titanium dioxide and monodisperse latex are mixed with dehydrated alcohol
Close, and 35-40 DEG C at a temperature of stir evenly, obtain mixed liquor f；7), mixed liquor f is mixed with solution e, at 30-35 DEG C
At a temperature of stir evenly, obtain the finished product of uvioresistant maceration extract.
Compared with prior art, the present invention successively carries out washing and drying to dacron, pads uvioresistant maceration extract, preliminary drying
Dry, microwave drying, cleaning and drying processing, and pass through the technological parameter of each step of strict control, so that uvioresistant substance
It can firmly be attached on dacron, the dacron produced has good UVResistant effect and endurance quality,
UV shielding rate >=95%.In addition, the present invention also passes through ingredient, proportion and the production work of strict control uvioresistant maceration extract
Skill, obtained uvioresistant maceration extract can not only effectively improve the LJV protection factors of fabric, and can also make it well
It anchors on dacron, extends the time of dacron uvioresistant；Simultaneously nano silica and monodisperse latex it
Between also will form layer protecting film, a part of ultraviolet light can not only be adsorbed, additionally it is possible to improve the intensity of dacron and wear-resisting
Performance.In conclusion the present invention has the characteristics that UVResistant effect can be effectively improved and improves durability.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated, but is not intended as the foundation limited the present invention.
Embodiment 1.A kind of production technology of anti-ultraviolet functional dacron, comprising the following steps:
A, it cleans dacron and dries, obtain a product；Drying temperature is 50-60 DEG C, time 3-4min；
B, a product are put into uvioresistant maceration extract and are impregnated, obtain b product；Bath raio between a product and uvioresistant maceration extract is 1:
30, the temperature of uvioresistant maceration extract is 28-33 DEG C, soaking time 40-45min；
C, b product are squeezed, rolling surplus is 95-98%, obtains c product；
D, c product are subjected to prebake, obtain d product；The temperature of prebake is 55-65 DEG C, time 3-4min；
E, microwave drying processing is carried out to d product, obtains e product；
F, e product are cleaned, f1 product are obtained；Using 50-60 DEG C of temperature, by f1 product, drying to constant weight, obtains final finished product.
Microwave drying processing is carried out to d product in the step E method particularly includes: first use microwave output power for 3-
The power section of 4kW heats 20-35s to d product, obtains d1 product；Then, the power section for being 40-45kW with microwave output power is to d1
Product heat 50-60s, obtain d2 product；Then 10-15s is heated to d2 product with the power section that microwave output power is 70-80kW, obtained
To e product.
The uvioresistant maceration extract comprises the following components in parts by weight: 2,4-DihydroxyBenzophenone, and 12-15 parts；Three
Ethamine, 20-22 parts；Ethyl acetate, 1-2 parts；Petroleum ether, 8-16 parts；Sodium bicarbonate solution, 30-35 parts；Dehydrated alcohol, 15-16
Part；Nano-titanium dioxide, 2-3 parts；1-2 parts of monodisperse latex；Water, 10-15 parts.
The preparation method of the uvioresistant maceration extract: 1) 2,4 dihydroxyl benzophenone and triethylamine is molten in reaction flask
Solution, obtains mixed solution a；2) under condition of ice bath, by ethyl acetate and petroleum ether and mixed solution a hybrid reaction, when reaction
Between be 5h, obtain mixed solution b；3) with after sodium bicarbonate solution and mixed solution B hybrid reaction, 1-2h is stood, takes upper layer clear
Clear liquid obtains solution c；4) solution c is evaporated, obtains article d；5), that article d is soluble in water, obtain solution e；6) by nanometer two
Titanium oxide and monodisperse latex are mixed with dehydrated alcohol, and 35-40 DEG C at a temperature of stir evenly, obtain mixed liquor f；
7), mixed liquor f is mixed with solution e, 30-35 DEG C at a temperature of stir evenly, obtain the finished product of uvioresistant maceration extract.
Sodium bicarbonate solution is saturated sodium bicarbonate solution.
Monodisperse latex is monodisperse carbon colloid microballoon.
Embodiment 2.A kind of production technology of anti-ultraviolet functional dacron, comprising the following steps:
A, it cleans dacron and dries, obtain a product；Drying temperature is 55 DEG C, time 3.5min；
B, a product are put into uvioresistant maceration extract and are impregnated, obtain b product；Bath raio between a product and uvioresistant maceration extract is 1:
30, the temperature of uvioresistant maceration extract is 30 DEG C, soaking time 42min；
C, b product are squeezed, rolling surplus is 97%, obtains c product；
D, c product are subjected to prebake, obtain d product；The temperature of prebake is 60 DEG C, time 3.5min；
E, microwave drying processing is carried out to d product, obtains e product；
F, e product are cleaned, f1 product are obtained；Using 55 DEG C of temperature, by f1 product, drying to constant weight, obtains final finished product.
Microwave drying processing is carried out to d product in the step E method particularly includes: first use microwave output power for 4kW
Power section to d product heat 30s, obtain d1 product；Then, 55s is heated to d1 product with the power section that microwave output power is 45kW,
Obtain d2 product；Then 12s is heated to d2 product with the power section that microwave output power is 75kW, obtains e product.
The uvioresistant maceration extract comprises the following components in parts by weight: 2,4-DihydroxyBenzophenone, and 13 parts；Three second
Amine, 21 parts；Ethyl acetate, 2 parts；Petroleum ether, 13 parts；Sodium bicarbonate solution, 33 parts；Dehydrated alcohol, 15 parts；Nanometer titanium dioxide
Titanium, 3 parts；2 parts of monodisperse latex；Water, 13 parts.
The preparation method of the uvioresistant maceration extract: 1) 2,4 dihydroxyl benzophenone and triethylamine is molten in reaction flask
Solution, obtains mixed solution a；2) under condition of ice bath, by ethyl acetate and petroleum ether and mixed solution a hybrid reaction, when reaction
Between be 5h, obtain mixed solution b；3) with after sodium bicarbonate solution and mixed solution B hybrid reaction, 2h is stood, upper layer is taken to clarify
Liquid obtains solution c；4) solution c is evaporated, obtains article d；5), that article d is soluble in water, obtain solution e；6) by nano-silica
Change titanium and monodisperse latex to mix with dehydrated alcohol, and 38 DEG C at a temperature of stir evenly, obtain mixed liquor f；7), will
Mixed liquor f is mixed with solution e, 33 DEG C at a temperature of stir evenly, obtain the finished product of uvioresistant maceration extract.
Sodium bicarbonate solution is saturated sodium bicarbonate solution.
Claims (4)
1. a kind of production technology of anti-ultraviolet functional dacron, which comprises the following steps:
A, it cleans dacron and dries, obtain a product；Drying temperature is 50-60 DEG C, time 3-4min；
B, a product are put into uvioresistant maceration extract and are impregnated, obtain b product；Bath raio between a product and uvioresistant maceration extract is 1:30,
The temperature of uvioresistant maceration extract is 28-33 DEG C, soaking time 40-45min；
C, b product are squeezed, rolling surplus is 95-98%, obtains c product；
D, c product are subjected to prebake, obtain d product；The temperature of prebake is 55-65 DEG C, time 3-4min；
E, microwave drying processing is carried out to d product, obtains e product；
F, e product are cleaned, f1 product are obtained；Using 50-60 DEG C of temperature, by f1 product, drying to constant weight, obtains final finished product.
2. a kind of production technology of anti-ultraviolet functional dacron according to claim 1, which is characterized in that the step
Microwave drying processing is carried out to d product in rapid E method particularly includes: first using microwave output power is the power section of 3-4kW to d product
20-35s is heated, d1 product are obtained；Then, 50-60s is heated to d1 product with the power section that microwave output power is 40-45kW, obtained
D2 product；Then 10-15s is heated to d2 product with the power section that microwave output power is 70-80kW, obtains e product.
3. a kind of production technology of anti-ultraviolet functional dacron according to claim 1, which is characterized in that described
Uvioresistant maceration extract comprises the following components in parts by weight: 2,4-DihydroxyBenzophenone, and 12-15 parts；Triethylamine, 20-22 parts；Second
Acetoacetic ester, 1-2 parts；Petroleum ether, 8-16 parts；Sodium bicarbonate solution, 30-35 parts；Dehydrated alcohol, 15-16 parts；Nanometer titanium dioxide
Titanium, 2-3 parts；1-2 parts of monodisperse latex；Water, 10-15 parts.
4. a kind of production technology of anti-ultraviolet functional dacron according to claim 3, which is characterized in that described anti-
The preparation method of ultraviolet maceration extract: 1) dissolving 2,4-DihydroxyBenzophenone and triethylamine in reaction flask, obtains mixing molten
Liquid a；2) under condition of ice bath, by ethyl acetate and petroleum ether and mixed solution a hybrid reaction, reaction time 5h is mixed
Close solution b；3) with after sodium bicarbonate solution and mixed solution B hybrid reaction, 1-2h is stood, supernatant liquid is taken to obtain solution c；
4) solution c is evaporated, obtains article d；5), that article d is soluble in water, obtain solution e；6) by nano-titanium dioxide and monodisperse
Colloid micro ball is mixed with dehydrated alcohol, and 35-40 DEG C at a temperature of stir evenly, obtain mixed liquor f；7), by mixed liquor f with
Solution e mixing, 30-35 DEG C at a temperature of stir evenly, obtain the finished product of uvioresistant maceration extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810889849.7A CN109162092A (en) | 2018-08-07 | 2018-08-07 | A kind of production technology of anti-ultraviolet functional dacron |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810889849.7A CN109162092A (en) | 2018-08-07 | 2018-08-07 | A kind of production technology of anti-ultraviolet functional dacron |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109162092A true CN109162092A (en) | 2019-01-08 |
Family
ID=64895238
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810889849.7A Pending CN109162092A (en) | 2018-08-07 | 2018-08-07 | A kind of production technology of anti-ultraviolet functional dacron |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109162092A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110205810A (en) * | 2019-07-12 | 2019-09-06 | 常熟市新光毛条处理有限公司 | A kind of preparation method of washable non-shrinkable wool item |
| CN114921971A (en) * | 2022-04-14 | 2022-08-19 | 浙江彩蝶实业股份有限公司 | Production process of polyester curtain fabric based on biomass anti-ultraviolet coating |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104727133A (en) * | 2015-03-10 | 2015-06-24 | 西安工程大学 | Preparation method of UVB-resistant finishing agent and UVB-resistant PBO (poly(p-phenylene benzobisoxazole)) fibers |
| CN106120305A (en) * | 2016-07-04 | 2016-11-16 | 伍硕硕 | Sunproof clothes |
-
2018
- 2018-08-07 CN CN201810889849.7A patent/CN109162092A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104727133A (en) * | 2015-03-10 | 2015-06-24 | 西安工程大学 | Preparation method of UVB-resistant finishing agent and UVB-resistant PBO (poly(p-phenylene benzobisoxazole)) fibers |
| CN106120305A (en) * | 2016-07-04 | 2016-11-16 | 伍硕硕 | Sunproof clothes |
Non-Patent Citations (1)
| Title |
|---|
| 董永春: "《纺织助剂化学》", 31 January 2010, 东华大学出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110205810A (en) * | 2019-07-12 | 2019-09-06 | 常熟市新光毛条处理有限公司 | A kind of preparation method of washable non-shrinkable wool item |
| CN114921971A (en) * | 2022-04-14 | 2022-08-19 | 浙江彩蝶实业股份有限公司 | Production process of polyester curtain fabric based on biomass anti-ultraviolet coating |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103981694B (en) | A kind of shitosan/TiO 2the method of composite finishing wool fabric | |
| CN100575595C (en) | Wash-free dyeing method for silk | |
| CN109162092A (en) | A kind of production technology of anti-ultraviolet functional dacron | |
| CN106811959A (en) | A kind of anion finishing technique of Australia's wool top | |
| CN103981702A (en) | Compound finishing method of wool fabric | |
| CN101760970B (en) | Production method of high-density synthetic leather | |
| CN102517919A (en) | Leather production method | |
| CN108393985A (en) | A kind of processing technology of finished wood or finished product | |
| CN106120305B (en) | Sunproof clothes | |
| CN103898750A (en) | Sizing method of low-pollution textile slurry | |
| CN103882709A (en) | Sizing method of environment-friendly textile slurry | |
| CN107662164A (en) | A kind of cloth base for super abrasive fused alumina zirconia abrasive band and preparation method thereof | |
| CN108316027A (en) | A kind of wet steaming technique of dyeing | |
| CN106827141B (en) | Timber drawing pencil softening method | |
| CN107938348A (en) | A kind of uvioresistant finishing process of fabric | |
| CN104441151A (en) | Wood plate antique finishing method | |
| CN107649649A (en) | A kind of surface processing technique of evaporative pattern | |
| CN103898756A (en) | Sizing method of textile slurry for dacron fabrics | |
| CN103882712B (en) | A kind of method for sizing being applicable to sodolin spinning sizing agent | |
| CN103451933A (en) | Production method of nanoparticle-2D resin functional silk fabric | |
| CN108018720A (en) | A kind of durable shiinkproof finish technique of wool fabric | |
| CN110685187A (en) | Internal sizing composition for paper pulp and application method and application thereof | |
| CN106283725A (en) | The colouring method of sheet fabric | |
| CN107956139A (en) | The fabric production method of fragrance can be kept for a long time | |
| CN103898758B (en) | A kind of method for sizing being applicable to real silk fabric spinning sizing agent |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190108 |
|
| RJ01 | Rejection of invention patent application after publication |