CN109136548A - Steam type high-temperature leaching device - Google Patents
Steam type high-temperature leaching device Download PDFInfo
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- CN109136548A CN109136548A CN201811203446.9A CN201811203446A CN109136548A CN 109136548 A CN109136548 A CN 109136548A CN 201811203446 A CN201811203446 A CN 201811203446A CN 109136548 A CN109136548 A CN 109136548A
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- 238000002386 leaching Methods 0.000 title claims abstract description 47
- 238000006243 chemical reaction Methods 0.000 claims abstract description 124
- 239000000463 material Substances 0.000 claims abstract description 56
- 238000010438 heat treatment Methods 0.000 claims abstract description 35
- 230000007246 mechanism Effects 0.000 claims description 30
- 230000005540 biological transmission Effects 0.000 claims description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- 238000005303 weighing Methods 0.000 claims description 12
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims description 11
- 238000007667 floating Methods 0.000 claims description 9
- 230000008676 import Effects 0.000 claims description 3
- 238000009833 condensation Methods 0.000 claims description 2
- 230000005494 condensation Effects 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 11
- 230000007613 environmental effect Effects 0.000 abstract description 5
- 238000007599 discharging Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- 238000009434 installation Methods 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000007790 solid phase Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 238000010924 continuous production Methods 0.000 description 3
- 238000005265 energy consumption Methods 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- 230000003068 static effect Effects 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000000903 blocking effect Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- JMANVNJQNLATNU-UHFFFAOYSA-N oxalonitrile Chemical compound N#CC#N JMANVNJQNLATNU-UHFFFAOYSA-N 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000011343 solid material Substances 0.000 description 2
- 241000208340 Araliaceae Species 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 206010024769 Local reaction Diseases 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 239000005083 Zinc sulfide Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000007259 addition reaction Methods 0.000 description 1
- 208000012826 adjustment disease Diseases 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 238000009854 hydrometallurgy Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000010310 metallurgical process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000009938 salting Methods 0.000 description 1
- 230000011218 segmentation Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 235000010215 titanium dioxide Nutrition 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 238000010977 unit operation Methods 0.000 description 1
- DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/02—Apparatus therefor
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
The invention discloses a steam type high-temperature leaching device, which comprises a reactor and a vibration component connected with the reactor and driving the reactor to vibrate, wherein the reactor is provided with a reaction channel for materials to pass through, the reaction channel is provided with a feeding hole and a discharging hole, and the steam type high-temperature leaching device also comprises a steam type heating component for heating the materials in the reaction channel. The invention has the advantages of high production efficiency, good environmental protection, low production cost, wide application range, high heating speed, more sufficient and uniform material reaction and the like.
Description
Technical field
The present invention relates to hydrometallurgys and chemical engineering to produce equipment technology field, and in particular to a kind of steam-type high temperature leaching
Device out.
Background technique
Leaching is one of unit operation mostly important in metallurgical process, specifically using leaching agent selectivity appropriate
Certain constituent elements or component in dissolved solid material, formed the salting liquid containing the metal, and the component insoluble with other into
The process of row initial gross separation.It will be apparent that the purpose leached is to enter the target constituent element in solid material by chemical reaction
Solution is separated with non-targeted constituent element as far as possible.Leach has very extensive application in metallurgical industry, for example, the cyanogen of gold mine
Change leaching, the ammonia leaching of the pressurized acid leaching of zinc sulphide, nickel ore concentrate, the dilute sulfuric acid leaching of the chlorine leaching of high nickel matte, titanium white mine and tungsten
Caustic soda leaching of concentrate etc..
It usually requires to heat material to increase the rate of Leach reaction, when operating temperature is at or above liquid
When the boiling point of phase, hyperbaric environment can be generated, and then improves the leaching rate of material in the liquid phase, the operating pressure in usual container needs
It is greater than 0.1MPa.Therefore, the requirement to the design of leaching device, material, leakproofness is very high, also results in high temperature and pressure and leaches dress
Set that structure is complicated, equipment manufacturing cost is expensive.Also, traditional technique is difficult to realize continuous behaviour of the material under high temperature and high pressure environment
Make, usually several intermittent high-temperature high-pressure reaction kettles are connected in series together, but it is substantially or intermittent operation.
Meanwhile resistance heating manner is used in traditional leaching device, the disadvantage of resistance heating maximum is exactly thermal conversion efficiency
Rate is not high, needs that there are temperature differences in heat transfer process, and related to the thermal conductivity of material, therefore has and can greatly dissipate
It loses in ambient enviroment.
In addition, existing leaching device is generally the consersion unit of static fixation, by during the reaction to object
Expect that the method for stirring react the contact area between phase, and then the reaction rate between raising two-phase increasing solid phase with other.
But there is the uneven or insufficient phenomenon of stirring in stirring means, or even the phenomenon that stirring dead angle occur.So as to cause reaction
Contact area energy imbalance between the solid phase and liquid phase at each position, causes local reaction incomplete in equipment, and product quality is difficult
To guarantee.
Summary of the invention
The technical problem to be solved in the present invention is to overcome the shortcomings of the prior art, provides a kind of high production efficiency, ring
Guarantor property is good, production cost is low, use scope is wide, heating speed is fast, the more abundant and uniform steam-type of material reaction can be made high
Warm leaching device.
In order to solve the above technical problems, the invention adopts the following technical scheme:
A kind of steam-type high temperature leaching device, the vibration group for being connected including reactor and with reactor and reactor being driven to vibrate
Part, the reaction utensil have the reaction channel for passing through for material, and the reaction channel is equipped with inlet port and outlet port, described
Steam-type high temperature leaching device further includes the steam-type heating component for being heated to material in reaction channel.
As a further improvement of the above technical scheme:
The steam-type heating component includes the annular steam channel being coated on outside reaction channel, the annular steam channel tool
There are steam inlet and steam (vapor) outlet.
The reaction channel is the pipeline for curling up into multi-turn, and gradually downward from reaction channel described in feed inlet to discharge port
Inclination extends.
The steam inlet is located at the discharge outlet close to reaction channel, and the steam (vapor) outlet is located at close to reaction channel
At feed inlet, the annular steam channel is additionally provided with the condensed water discharge outlet for condensed water in annular steam channel to be discharged.
The steam-type heating component includes steam heating cavity, the steam heating cavity have the import that enters for steam with
For the outlet of steam discharge, the reaction channel is set in the steam heating cavity.
The reaction channel be equipped with multiple adjustable relief valves for pressure release, multiple adjustable relief valves along reaction channel successively
Arranged for interval.
The reaction channel is equipped with multiple thermal detectors for being used to detect temperature in reaction channel, and multiple thermal detectors are logical along reaction
Road successively arranged for interval.
The feed inlet and/or discharge port are equipped with the valve that can be opened and closed and be adjustable flow；The steam-type high temperature leaches
Device is additionally provided with for measuring the metering pump from discharge port output mass flow, for weighing from discharge port output weight of material
Weighing apparatus and at least one of pressure gauge for measuring pressure in reaction channel, wherein the metering pump and pressure gauge are set
In on reaction channel, the weighing apparatus is set to and can accept from the position of discharge port output material.
The vibration component includes more than one the vibratory drive mechanism of pedestal and installation on the base, and the reactor is logical
Cross the installation of elastic floating supporting mechanism on the base, the vibratory drive mechanism is connected with the reactor.
The vibratory drive mechanism includes rotary drive, transmission shaft and vibrating shaft, the driving end of the rotary drive
It is connected with the transmission shaft, the transmission shaft is connected by universal joint with vibrating shaft, and the vibrating shaft is equipped with several eccentric blocks,
The vibrating shaft is connected with reactor；The elastic floating supporting mechanism includes several branch being connected between pedestal and reactor
Spring is held, several bearing springs are evenly arranged in the surrounding of more than one vibratory drive mechanism.
Compared with the prior art, the advantages of the present invention are as follows: steam-type high temperature leaching devices of the invention by reaction chamber
Room is set as dynamic stationary state, overcomes the technology prejudice that Leach reaction equipment in the prior art is usually static fixation, is
Reaction chamber provides vibration supporting way, realizes the mass motion of consersion unit chamber.Reaction is driven using vibration component
Device vibration, can make the material in reaction channel constantly be stir-fried, be mixed, the contact of material is more abundant, to make the anti-of material
It should be more full and uniform.Meanwhile continuous production can be realized using the reaction channel of duct type, to greatly improve production effect
Rate, and material is reacted in the reaction channel of relative closure, and the feature of environmental protection might as well.Further, it is heated using steam-type
Component heats the material in reaction channel, can satisfy the temperature requirement of material reaction, has expanded leaching device significantly
The scope of application, and the heating speed of steam-type heating component is fast, can be realized be rapidly heated, the feature of environmental protection is good, easily operated control
System, cost and operating cost are low.Steam-type high temperature leaching device of the invention can be very good to solve existing equipment in solid phase ginseng
It the problem of with the Leach reaction reacted, can not only realize the reaction environment of high temperature and pressure, and can be realized serialization
Production.
Detailed description of the invention
Fig. 1 is that reactor is mounted on the intracorporal structure schematic diagram of fully sheathed case in steam-type high temperature leaching device.
Fig. 2 is the structure schematic diagram that vibration component is connect with heater box in steam-type high temperature leaching device.
Fig. 3 is the schematic perspective view of coiled pipeline.
Fig. 4 is the side structure schematic view of coiled pipeline.
Marginal data:
1, reactor；11, reaction channel；111, feed inlet；112, discharge port；113, valve；2, pedestal；3, rotary drive；
4, transmission shaft；41, the first transmission segment；42, the second transmission segment；43, connecting flange；44, splined shaft；5, vibrating shaft；6, universal joint；
7, eccentric block；9, spring is supported；10, fixed deformation bearing；201, annular steam channel；2011, steam inlet；2012, steam
Outlet；2013, condensed water discharge outlet；202, closed box；203, insulating layer；301, adjustable relief valve；302, thermal detector；303,
Metering pump；304, pressure gauge.
Specific embodiment
The present invention is described in further detail below in conjunction with the drawings and specific embodiments.
As shown in Figures 1 to 4, the steam-type high temperature leaching device of the present embodiment, including reactor 1 and vibration component, vibration
Dynamic component is connected with reactor 1 and reactor 1 is driven to vibrate, and reactor 1 has the reaction channel 11 for passing through for material, instead
Channel 11 is answered to be equipped with feed inlet 111 and discharge port 112, high-temperature steam formula leaching device further includes for object in reaction channel 11
Expect the steam-type heating component heated.When work, reaction channel 11 is added from feed inlet 111 in material, and from discharge port 112
Output, material are reacted during through reaction channel 11.The steam-type high temperature leaching device is set by reaction chamber
It is set to dynamic stationary state, overcomes the technology prejudice that Leach reaction equipment in the prior art is usually static fixation, for reaction
Chamber provides vibration supporting way, realizes the mass motion of consersion unit chamber.Reactor 1 is driven to shake using vibration component
It is dynamic, the material in reaction channel 11 can be made constantly to be stir-fried, be mixed, the contact of material is more abundant, to make the reaction of material
It is more full and uniform.Meanwhile continuous production can be realized using the reaction channel of duct type 11, to greatly improve production effect
Rate, and material is reacted in the reaction channel 11 of relative closure, and the feature of environmental protection might as well.Further, using steam-type plus
Hot component heats the material in reaction channel 11, can satisfy the temperature requirement of material reaction, has expanded leaching significantly
The scope of application of device, and the heating speed of steam-type heating component is fast, can be realized be rapidly heated, the feature of environmental protection is good, the thermal efficiency
High, easily operated control, cost and operating cost are low.Steam-type high temperature leaching device of the invention can be very good to solve existing
Equipment can not only realize the reaction environment of high temperature and pressure, and energy the problem of solid phase participates in the Leach reaction of reaction
Enough realize continuous production.
In the present embodiment, as shown in Figure 1, steam-type heating component includes the annular steam being coated on outside reaction channel 11
Channel 201, annular steam channel 201 have steam inlet 2011 and steam (vapor) outlet 2012.Using the ring in coating reaction channel 11
Shape steam channel 201 heats reaction channel 11, fast to the heating speed of reaction channel 11, high-efficient, and can be improved anti-
The temperature uniformity of material in channel 11 is answered, guarantees material homogeneous reaction.
In other embodiments, other heating methods can also be used in steam-type heating component, for example, steam-type heating group
Part includes steam heating cavity, and steam heating cavity is with the import entered for steam and for the outlet of steam discharge, reaction channel 11
In the steam heating cavity.Reaction channel 11 integrally heats in steam heating cavity, the knot of this kind of steam-type heating component
Structure is simple, at low cost.Steam-type heating component can also be the jet chimney being wrapped in outside reaction channel 11.
In the present embodiment, extension is tilted gradually downward from feed inlet 111 to 112 reaction channel 11 of discharge port, can make material
Automatically it is moved from feed inlet 111 to discharge port 112, feed automatically is formed, conducive to reducing energy consumption and production costs.
In the present embodiment, reaction channel 11 is the pipeline for curling up into multi-turn, 11 occupied space of reaction channel of this kind of form
It is small, structural compactness can be greatly improved.Preferably, the both ends of pipeline are respectively that feed inlet 111 arrives discharge port 112.Pipeline is
Circular pipe, conducive to the full and uniform stir-frying of material, mixing.
It is further preferred that pipeline is the coiled pipeline curled up around a vertical centerline, feed inlet 111 is located at discharge port
112 top, and be gradually increased from feed inlet 111 to the radial spacing of 112 coiled pipeline of discharge port and vertical centerline, it should
Kind pipeline is conducive to material stir-frying, is more fully mixed uniformly, and passes through reaction channel 11 conducive to material is smooth.It is above-mentioned curl up into it is more
The reaction channel 11 of circle can be various shape, such as can also be round perhaps ellipse but be not limited only to round or ellipse
It is round.
In the present embodiment, steam inlet 2011 is located at the discharge port 112 of reaction channel 11, and steam (vapor) outlet 2012
In close to reaction channel 11 feed inlet 111 at namely steam be from close to discharge port 112 position from enter, from close into
It is discharged at the position of material mouth 111.Since material is after the addition reaction channel 11 of feed inlet 111, need to move along reaction channel 11
The reaction temperature of setting can be just gradually risen to after longer period of time by initial temperature, namely arrives discharge port along feed inlet 111
The temperature of 112 materials gradually increases, until reaching the reaction temperature of setting.Above-mentioned steam inlet 2011 and steam (vapor) outlet 2012
Set-up mode, the steam with higher temperature for making the annular steam channel 201 for most starting to be passed through and the temperature close to discharge port 112
Spending has biggish temperature difference between higher material, as steam is moved along annular steam channel 201 to steam (vapor) outlet 2012,
Because heat exchange vapor (steam) temperature can gradually decrease, and the temperature closer to 111 material of feed inlet is also lower, reduces the steam of temperature still
There can be biggish temperature difference between the lower material of temperature of feed inlet 111, it in this way can along entire reaction channel 11
Higher temperature difference is enough kept, efficiency of heating- utilization can be greatly improved.Meanwhile annular steam channel 201 is additionally provided with for being discharged
The condensed water discharge outlet 2013 of condensed water in annular steam channel 201, it is logical that annular steam can be discharged in condensed water discharge outlet 2013
Condensed water in road 201 avoids condensation water slug annular steam channel 201, guarantees progress stable and reliable in work.Preferably, it condenses
Water outlet 2013 is positioned close at the position of steam inlet 2011 namely condensed water discharge outlet 2013 is arranged in annular steam
The lower part in channel 201, excludes in time conducive to condensed water.
In the present embodiment, reaction channel 11 is equipped with multiple adjustable relief valves 301 for pressure release, multiple adjustable relief valves
301 along the successively arranged for interval of reaction channel 11.Adjustable relief valve 301 can carry out release to reaction channel 11 and adjust release
Pressure is in pressure in reaction channel 11 in the range of setting, avoids after heating that pressure increases and shadow in reaction channel 11
It rings material reaction and even results in the rupture of reaction channel 11, guarantee the reliability of device work.In the actual production process by
Pressure in position each in reaction channel 11 may be unbalanced, further, by multiple adjustable relief valves 301 along reaction channel 11
Successively arranged for interval carries out the pressure in reaction channel 11 sectional-regulated, it is ensured that and pressure is balanced in entire reaction channel 11,
Also, the position whether reaction channel 11 blocks and block can be also judged according to each section of pressure condition.
In the present embodiment, reaction channel 11 is equipped with multiple thermal detectors 302 for being used to detect temperature in reaction channel 11, multiple
Thermal detector 302 is along the successively arranged for interval of reaction channel 11.It can be real-time and easily to the temperature in reaction channel 11 by thermal detector 302
Degree is detected, and is controlled convenient for combined heat component the temperature in reaction channel 11.In the actual production process due to
In reaction channel 11 each position temperature may it is unbalanced, further, by multiple thermal detectors 302 along reaction channel 11 successively between
Every arrangement, segmentation detection is carried out to the temperature in reaction channel 11, the temperature conditions at each position of reaction channel 11 can be obtained,
Conducive to the temperature in accurate adjustment reaction channel 11, also, also whether reaction channel 11 can be judged according to each section of temperature conditions
The position of blocking and blocking.
In the present embodiment, discharge port 112, which is equipped with, can be opened and closed and be adjustable the valve 113 of flow, can be with by the valve 113
Discharge port 112 is opened or closed, while can also adjust the flow that material reaction product is flowed out from discharge port 112, thus realization pair
The control of reaction rate substantially increases the controllability and using flexible of steam-type high temperature leaching device.In other embodiments
In, valve 113 only can also be set in feed inlet 111, material is controlled by the valve 113 of feed inlet 111 and enters reaction channel 11
Flow, reaction rate can also be controlled.Also valve 113 can be respectively provided in feed inlet 111 and discharge port 112.
In the present embodiment, steam-type high temperature leaching device can be also equipped with for measuring from 112 outputting material flow of discharge port
Metering pump 303, for weighing from the weighing apparatus of 112 outputting material weight of discharge port and for measuring pressure in reaction channel 11
At least one of pressure gauge 304, wherein metering pump 303 and pressure gauge 304 are set on reaction channel 11, and weighing apparatus is set to
It can accept from the position of 112 outputting material of discharge port.It can be measured by metering pump 303 from 112 outputting material of discharge port
Flow can weigh the quality of 112 outputting material of discharge port by weighing apparatus, can measure reaction channel by pressure gauge 304
Pressure in 11 can easily be acquired relevant information.The present embodiment is specifically provided with above-mentioned metering pump 303 and surveys pressure
Metering pump 303, weighing apparatus and pressure gauge 304 can also be only arranged in table 304, in other embodiments, steam-type high temperature leaching device
In one or two, or be provided with metering pump 303, weighing apparatus and pressure gauge 304 simultaneously.
In the present embodiment, vibration component includes more than one the vibratory drive mechanism of pedestal 2 and installation on the base 2, instead
Device 1 is answered to install on the base 2 by elastic floating supporting mechanism, vibratory drive mechanism is connected with reactor 1.Due to reactor 1
On the base 2 by the installation of elastic floating supporting mechanism, reactor 1 can elastic floating on the base 2, make vibratory drive mechanism
Can drive response device 1 vibrate, and reactor 1 vibrate stability it is good.The structure of this kind of vibration component is simple, at low cost, work
Make reliable and stable.
In the present embodiment, vibration component has altogether there are two vibratory drive mechanism, the vibration frequency of all vibratory drive mechanisms
It is equal with amplitude, good resonance effect can be generated in this way, keeps stirring more violent, and material contact is more abundant, and reaction is more
Add uniformly.Preferably, Liang Ge vibratory drive mechanism is symmetrical relative to the vertical centerline of coiled pipeline, resonance effect
More preferably, the stress of reactor 1 is also more evenly.In other embodiments, the quantity of the had vibratory drive mechanism of vibration component is also
It can be one or three or more, when vibration component tool is there are three the above vibratory drive mechanism, all vibratory drive mechanisms
The vertical centerline of drum tubular conduit is uniformly distributed, and resonance effect can be made more preferable, and the stress of reactor 1 is more evenly.
In the present embodiment, vibratory drive mechanism includes rotary drive 3, transmission shaft 4 and vibrating shaft 5, rotary drive 3
Driving end is connected with transmission shaft 4, and transmission shaft 4 is connected by universal joint 6 with vibrating shaft 5, and vibrating shaft 5 is equipped with several eccentric blocks 7,
Vibrating shaft 5 is connected with reactor 1.When rotary drive 3 drives transmission shaft 4 to rotate, transmission shaft 4 drives vibration by universal joint 6
Axis 5 rotates, and since vibrating shaft 5 is equipped with eccentric block 7, eccentric block 7 can make vibrating shaft 5 generate vibration when rotating with vibrating shaft 5, from
And it is vibrated with reactor 1.The structure of the vibratory drive mechanism is simple, it is at low cost, stable and reliable in work, be easily installed maintenance.
Preferably, it is 500 ~ 6000r/min that rotary drive 3, which drives the revolving speed of transmission shaft 4,.There are two being set on vibrating shaft 5
Between eccentric block 7, two eccentric blocks 7 are divided into the opposite sides of vibrating shaft 5, and two eccentric blocks 7 are on 5 axis direction of vibrating shaft
Every setting.
In the present embodiment, reaction channel 11 and the annular steam channel 201 being coated on outside reaction channel 11 are mounted on one
In closed box 202, the loss of heat can be reduced, saves energy consumption.Preferably, it wraps up and being provided on the side wall of closed box 202
Insulating layer 203 can further save energy consumption.The reactor 1 and closed box 202 of the present embodiment are affixed.Each vibratory drive mechanism
Vibrating shaft 5 connect with closed box 202 namely vibratory drive mechanism is connected by closed box 202 with reactor 1, drive
Closed box 202 and reactor 1 vibrate simultaneously.Vibrating shaft 5 is connect with closed box 202: being sheathed on vibrating shaft 5
A few fixed deformation bearing 10, fixed deformation bearing 10 include the inner ring body and outer ring body of rotation connection, wherein inner ring body set
On vibrating shaft 5, outer ring body is mounted in the installation sleeve being fixedly arranged on closed box 202.
In the present embodiment, transmission shaft 4 includes the first transmission segment 41 and the second transmission segment 42, the driving end of rotary drive 3
It is connected with the first transmission segment 41, the first transmission segment 41 and the second transmission segment 42 are moved and are driven can be axially relative to
Mode connect, the second transmission segment 42 is connected by universal joint 6 with vibrating shaft 5.Due to reactor 1 vibrate when and environment temperature
Can generate axial stress when variation, the first transmission segment 41 and the second transmission segment 42 can relative motion in the axial direction, can play and disappear
Except the effect of the axial stress, the service life of steam-type high temperature leaching device is improved.
In the present embodiment, the first transmission segment 41 is connect by splined shaft 44 with the second transmission segment 42；Rotary drive 3 is electricity
The output shaft of machine, motor is connected by connecting flange 43 with the first transmission segment 41 or the output shaft of motor passes through chain conveyer machine
Structure is connected with the first transmission segment 41.
In the present embodiment, elastic floating supporting mechanism includes several bearing springs being connected between pedestal 2 and reactor 1
9, several bearing springs 9 are evenly arranged in the surrounding of all vibratory drive mechanisms, and the reliable and stable of the vibration of reactor 1 can be improved
Property, and the structure of the elastic floating supporting mechanism it is simple, it is at low cost, be easy to make.
Steam-type high temperature leaching device of the invention can also flow according to material and reaction time, to reaction channel 11
The structural parameters such as diameter are adjusted, to meet real reaction requirement.
The above is only a preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-mentioned implementation
Example.To those of ordinary skill in the art, obtained improvement and change in the case where not departing from the technology of the present invention concept thereof
It changes and also should be regarded as protection scope of the present invention.
Claims (10)
1. a kind of steam-type high temperature leaching device, it is characterised in that: be connected and drive including reactor (1) and with reactor (1)
The vibration component of reactor (1) vibration, the reactor (1) has the reaction channel (11) for passing through for material, described anti-
Channel (11) are answered to be equipped with feed inlet (111) and discharge port (112), the steam-type high temperature leaching device further includes for reaction
The steam-type heating component that channel (11) interior material is heated.
2. steam-type high temperature leaching device according to claim 1, it is characterised in that: the steam-type heating component includes
It is coated on the external annular steam channel (201) of reaction channel (11), the annular steam channel (201) has steam inlet
(2011) and steam (vapor) outlet (2012).
3. steam-type high temperature leaching device according to claim 2, it is characterised in that: the reaction channel (11) is to curl up
Extension is tilted gradually downward to discharge port (112) reaction channel (11) at the pipeline of multi-turn, and from feed inlet (111).
4. steam-type high temperature leaching device according to claim 3, it is characterised in that: the steam inlet (2011) is located at
At the discharge port (112) of reaction channel (11), the steam (vapor) outlet (2012) is located at the charging close to reaction channel (11)
At mouth (111), the annular steam channel (201) is additionally provided with the condensation for annular steam channel (201) interior condensed water to be discharged
Water outlet (2013).
5. steam-type high temperature leaching device according to claim 1, it is characterised in that: the steam-type heating component includes
Steam heating cavity, the steam heating cavity is with the import entered for steam and for the outlet of steam discharge, the reaction channel
(11) it is set in the steam heating cavity.
6. steam-type high temperature leaching device according to claim 1, it is characterised in that: the reaction channel (11) is equipped with more
A adjustable relief valve (301) for pressure release, multiple adjustable relief valves (301) are along reaction channel (11) successively arranged for interval.
7. steam-type high temperature leaching device according to claim 1, it is characterised in that: the reaction channel (11) is equipped with more
It is a for detecting the thermal detector (302) of reaction channel (11) interior temperature, multiple thermal detectors (302) along reaction channel (11) successively between
Every arrangement.
8. steam-type high temperature leaching device according to claim 1, it is characterised in that: the feed inlet (111) and/or go out
Material mouth (112) is equipped with the valve (113) that can be opened and closed and be adjustable flow；The steam-type high temperature leaching device is additionally provided with based on
Measure the metering pump (303) from discharge port (112) outputting material flow, for weighing from discharge port (112) outputting material weight
Weighing apparatus and at least one of pressure gauge (304) for measuring reaction channel (11) interior pressure, wherein the metering pump
(303) it is set on reaction channel (11) with pressure gauge (304), the weighing apparatus is set to and can accept from discharge port (112) output
At the position of material.
9. steam-type high temperature leaching device according to any one of claim 1 to 8, it is characterised in that: the vibration group
Part includes pedestal (2) and more than one the vibratory drive mechanism being mounted on pedestal (2), and the reactor (1) is floating by elasticity
Dynamic supporting mechanism is mounted on pedestal (2), and the vibratory drive mechanism is connected with the reactor (1).
10. steam-type high temperature leaching device according to claim 9, it is characterised in that: the vibratory drive mechanism includes
Rotary drive (3), transmission shaft (4) and vibrating shaft (5), driving end and the transmission shaft (4) phase of the rotary drive (3)
Even, the transmission shaft (4) is connected by universal joint (6) with vibrating shaft (5), and the vibrating shaft (5) is equipped with several eccentric blocks
(7), the vibrating shaft (5) is connected with reactor (1)；The elastic floating supporting mechanism include it is several be connected to pedestal (2) and
Bearing spring (9) between reactor (1), several bearing springs (9) are evenly arranged in the four of more than one vibratory drive mechanism
Week.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811203446.9A CN109136548A (en) | 2018-10-16 | 2018-10-16 | Steam type high-temperature leaching device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811203446.9A CN109136548A (en) | 2018-10-16 | 2018-10-16 | Steam type high-temperature leaching device |
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| Publication Number | Publication Date |
|---|---|
| CN109136548A true CN109136548A (en) | 2019-01-04 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811203446.9A Pending CN109136548A (en) | 2018-10-16 | 2018-10-16 | Steam type high-temperature leaching device |
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| Country | Link |
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| CN (1) | CN109136548A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1170044A (en) * | 1996-07-05 | 1998-01-14 | 中南工业大学 | Method for recovering zinc from dregs containing zinc ferrite |
| CN104178237A (en) * | 2014-08-13 | 2014-12-03 | 华电电力科学研究院 | Method for leaching and removing sodium element in coal by using water static pressure |
| CN105039731A (en) * | 2015-09-10 | 2015-11-11 | 攀钢集团攀枝花钢铁研究院有限公司 | Method for maintaining system heat balance in titanium slag leaching process |
| CN209039541U (en) * | 2018-10-16 | 2019-06-28 | 湖南行者环保科技有限公司 | A kind of steam-type high temperature leaching device |
-
2018
- 2018-10-16 CN CN201811203446.9A patent/CN109136548A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1170044A (en) * | 1996-07-05 | 1998-01-14 | 中南工业大学 | Method for recovering zinc from dregs containing zinc ferrite |
| CN104178237A (en) * | 2014-08-13 | 2014-12-03 | 华电电力科学研究院 | Method for leaching and removing sodium element in coal by using water static pressure |
| CN105039731A (en) * | 2015-09-10 | 2015-11-11 | 攀钢集团攀枝花钢铁研究院有限公司 | Method for maintaining system heat balance in titanium slag leaching process |
| CN209039541U (en) * | 2018-10-16 | 2019-06-28 | 湖南行者环保科技有限公司 | A kind of steam-type high temperature leaching device |
Non-Patent Citations (2)
| Title |
|---|
| 中国有色金属工业总公司设备情报网: "《国内外采矿选矿冶炼设备 现状与差距 第3册 有色冶炼设备》", 31 December 1989, 中国有色金属工业总公司设备情报网, pages: 140 * |
| 耿玉珍: "《分析化学》", 31 December 2000, 中国林业出版社, pages: 187 * |
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