CN109136304A - A kind of utilization, which is cracked rice, produces the processing technology of fructose syrup - Google Patents
A kind of utilization, which is cracked rice, produces the processing technology of fructose syrup Download PDFInfo
- Publication number
- CN109136304A CN109136304A CN201811086778.3A CN201811086778A CN109136304A CN 109136304 A CN109136304 A CN 109136304A CN 201811086778 A CN201811086778 A CN 201811086778A CN 109136304 A CN109136304 A CN 109136304A
- Authority
- CN
- China
- Prior art keywords
- rice
- added
- fructose syrup
- concentration
- decoloration
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/02—Monosaccharides
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/12—Disaccharides
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/24—Preparation of compounds containing saccharide radicals produced by the action of an isomerase, e.g. fructose
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Jellies, Jams, And Syrups (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention, which provides a kind of utilization and cracks rice, produces the processing technology of fructose syrup, comprising the following steps: impurity elimination-of cracking rice wash rice immersion-defibrination-is sized mixing-liquefy-take off condiment-isomerization-Two-step ion-exchanging-secondary decolourization refined filtration-aseptic filtration-concentration-before albumen-saccharification-decoloration refined filtration-ion exchange-isomery it is secondary be sterile filtered-it is filling stand-by；The present invention, which can will crack rice, to be made full use of, and while producing fructose syrup, can also produce albumen powder of cracking rice, and it selects and cracks rice as raw material, cost is relatively low, and the present invention is more preferable using fructose syrup stability made from corn using fructose syrup ratio obtained of cracking rice, and purity is higher.
Description
Technical field
The present invention relates to a kind of fructose syrup processing technique field, specially a kind of utilization, which is cracked rice, produces adding for fructose syrup
Work technique.
Background technique
Fructose syrup is mainly made of glucose sugar and fructose, and fructose syrup is made of plant amylum hydrolysis and isomerization
Starch sugar is brilliant, is a kind of important sweetener, colourless glutinous thick liquid, and good fluidity under room temperature, odorless, fructose syrup is a kind of
The product of sucrose can be substituted completely, and can be widely used in food and beverage industry as sucrose, especially in beverage row
Application in industry, flavor and mouthfeel are better than sucrose, and with the continuous improvement of fructose syrup application technology in food,
The cost performance of itself and sucrose will be protruded more, and more and more people will understand that fructose syrup, more and more food enterprises
It will be selected, thus, largely substitution sucrose will be at certainty for fructose syrup in food industry.
Containing protein of cracking rice with starch of cracking rice in cracking rice, starch of cracking rice can be made into fructose syrup, and protein of cracking rice can add
Work is at albumen powder of cracking rice, and albumen powder of cracking rice is mainly by four kinds of protein groups such as albumin, globulin, protein,alcohol-soluble and glutelin
At the amino acid composition for albumen of cracking rice is reasonable, and amino acid content is high, is acknowledged as good edible protein, albumen powder of cracking rice
Hypoallergenic, has soft and inirritative taste at non-pigment interference, however existing fructose syrup takes corn for original mostly
Material, is made fructose syrup, fructose syrup obtained by liquefaction, saccharification, isomerization, decolorization filtering, ion exchange, vacuum concentration
Rich in a small amount of impurity and stability it is bad, lack a kind of to the exploitation for producing fructose syrup of cracking rice.
Summary of the invention
In order to solve the problems, such as that above-mentioned background technique proposes, the present invention proposes following technical scheme.
The technical scheme is that a kind of utilization, which is cracked rice, produces the processing technology of fructose syrup, comprising the following steps: broken
Rice impurity elimination-washes rice immersion-defibrination-is sized mixing-and liquefies-take off condiment-isomery before albumen-saccharification-decoloration refined filtration-ion exchange-isomery
Refined filtration-aseptic filtration-concentration-the aseptic filtration-of decolourizing again of change-Two-step ion-exchanging-is filling stand-by.
Specific step is as follows for the processing technology:
A: impurity elimination of cracking rice takes raw material to crack rice, and carries out stone impurity elimination；
B: wash rice immersion, by step A obtain crack rice clean be put into soaking barrel, be added 5 times amount water, impregnate 48-60h；
C: defibrination is cracked rice what step B was obtained to be added in ground rice machine and is ground, is continuously added suitable water extremely during defibrination
Grinding is abundant；
D: sizing mixing, and takes the lotion in step C, and adjusting pH value is 6.0, be added into lotion a- amylase and 19 Baume of calcium chloride into
Row stirring；
E: iodine solution is added into step D for liquefaction, controls temperature at 105-110 DEG C, is kept for a period of time, until Iod R is not shown
Blue obtains DE in 15%-20%；
F: de- albumen, by the obtained Rice & peanut milk sediment of step E by washing protein, filters pressing, drying, packaging, after obtain albumen powder,
Wherein drying uses steam drying；
G: saccharification takes the Rice & peanut milk after step F, and adjusting pH value is 4.2, and carbohydrase is added into Rice & peanut milk and is stirred, stirring temperature
Degree is 60 DEG C, stirs 30h-35h, obtains DE >=95%；
H: decoloration refined filtration takes mixed liquor in step G to be put into decoloration bucket, carries out the stirring of decolourizing with mixing after proper amount of active carbon is added
Time must not be less than 5 minutes, be subsequently placed into filter, be filtered to obtain liquid glucose；
I: the HCL that concentration is 5% is added into the liquid glucose of step H and the NaOH that concentration is 4% carries out ion exchange for ion exchange,
Wherein conductivity is no more than 50ms/cm；
J: condiment before isomery is added magnesium sulfate into step I and sodium pyrosulfite is stirred, and whipping temp is 60 DEG C, stirring
When pH value be 7.5-8.0, stir evenly；
K: isomerization, it is 40-42% isomerase that mass fraction is added into step J, is sufficiently stirred after reaction that obtain 42% fructose different
Structure sugar；
L: the HCL that concentration is 5% is added into step K and the NaOH that concentration is 4% carries out ion exchange, electricity for Two-step ion-exchanging
Conductance is no more than 50ms/cm；
M: secondary decolourization refined filtration takes slurries in step L to be put into decoloration bucket, carries out after proper amount of active carbon is added with mixing, decoloration is stirred
Mixing the time must not be subsequently placed into filter less than 10 minutes, and be filtered；
O: being sterile filtered, step M obtained slurries aseptically, is filtered on the filter membrane that aperture is 0.45 micron；
P: the liquid glucose that step O is obtained is concentrated to get the liquid glucose that mass fraction is 71% through vacuum evaporating pot by concentration；
Q: secondary aseptic filtration, the liquid glucose that step P is obtained are again on 0.45 micron of filter membrane in aperture aseptically
Filtering, obtains finished product fructose syrup；
R: it is filling stand-by, the finished product fructose syrup that step Q is obtained is fitted into finished pot, packed for standby use.
Preferably, the washing protein water that the step F takes off after the filters pressing in albumen can be added directly into step C defibrination, be followed
Ring utilizes.
It preferably, is 7.5~7.8 into column syrup pH value in the step K in isomerization, temperature is 65 DEG C, out column isomery
Sugared pH value is 6.5-7.0.
DE in the present invention refers to that reduced sugar (with glucose meter) accounts for the percentage of syrup dry matter.
Compared with prior art, the beneficial effects of the present invention are: the present invention not only can produce fructose syrup with cracking rice,
Albumen powder of cracking rice can be also produced simultaneously, will crack rice makes full use of and the cost cracked rice is low；When producing fructose syrup, by adjusting
A- amylase and 19 Baume of calcium chloride are added when slurry, ensure that the uniformity of slurries, by the way that magnesium sulfate is added before isomerization
As stabilizer, it is ensured that the stability of the fructose syrup of production refined filtration and is twice sterile filtered by decolourizing twice, be ensure that
The purity of fructose syrup；By the way that the washing protein water after filters pressing in de- albumen can be added directly into defibrination, circulation benefit
With saving certain resource.
Detailed description of the invention
Fig. 1 is processing process figure of the present invention.
Specific embodiment
Technical scheme of the present invention will be further described in the following with reference to the drawings and specific embodiments, but the present invention is not
It is limited to these embodiments.Embodiment 1 is that the traditional handicraft of fructose syrup is prepared using corn.
Embodiment 1, a kind of processing technology using corn starch milk production fructose syrup, comprising the following steps:
A: liquefaction, the starch milk for being 60% by concentration, adjusting pH value is 5.7, adds 10 units/gram dried starch of alpha-amylase, temperature
90 DEG C, kept for certain time, until the not aobvious blue of Iod R.B: saccharification, adjusting pH value is 4.2, adds carbohydrase, controls temperature 60
DEG C, it is stirred to react about 36 hours, makes DE value up to 93%, through decolorization filtering, ion exchange, being concentrated in vacuo to concentration is 45%.C:
Mass fraction is that 40-42% isomerase is added in the liquid glucose that above-mentioned concentration is 45%, while 40 mg/litres are added by isomerization
Magnesium ion is as stabilizer.D: concentration, by liquid glucose made from step C again through decolorization filtering, ion exchange, be concentrated in vacuo to matter
Measuring score is 75% to get embodiment 1.A kind of utilization of embodiment 2, which is cracked rice, produces the processing technology of fructose syrup, including following
Step:
A: cracking rice, and raw material is taken to crack rice, and carries out stone impurity elimination；
B: wash rice immersion, by step A obtain crack rice clean be put into soaking barrel, be added 5 times amount water, impregnate 48h；
C: defibrination is cracked rice what step B was obtained to be added in ground rice machine and is ground, is continuously added suitable water extremely during defibrination
Grinding is abundant；
D: sizing mixing, and takes the lotion in step C, and adjusting pH value is 6.0, be added into lotion a- amylase and 19 Baume of calcium chloride into
Row stirring；
E: iodine solution is added into step D for liquefaction, controls temperature at 105 DEG C, is kept for a period of time, until the not aobvious blue of Iod R,
DE is obtained 15%；
F: de- albumen, by the obtained Rice & peanut milk sediment of step E by washing protein, filters pressing, drying, packaging, after obtain albumen powder,
Wherein drying uses steam drying；
G: saccharification takes the Rice & peanut milk after step F, and adjusting pH value is 4.2, and carbohydrase is added into Rice & peanut milk and is stirred, stirring temperature
Degree is 60 DEG C, stirs 30h, and obtaining DE is 95%；
H: decoloration refined filtration takes mixed liquor in step G to be put into decoloration bucket, carries out the stirring of decolourizing with mixing after proper amount of active carbon is added
Time must not be less than 5 minutes, be subsequently placed into filter, be filtered to obtain liquid glucose；
I: the HCL that concentration is 5% is added into the liquid glucose of step H and the NaOH that concentration is 4% carries out ion exchange for ion exchange,
Wherein conductivity is no more than 50ms/cm；
J: condiment before isomery is added magnesium sulfate into step I and sodium pyrosulfite is stirred, and whipping temp is 60 DEG C, stirring
When pH value be 7.5, stir evenly；
K: isomerization, it is 42% isomerase that mass fraction is added into step J, obtains 42% fructose isomery after reaction is sufficiently stirred
Sugar；
L: the HCL that concentration is 5% is added into step K and the NaOH that concentration is 4% carries out ion exchange, electricity for Two-step ion-exchanging
Conductance is no more than 50ms/cm；
M: secondary decolourization refined filtration takes slurries in step L to be put into decoloration bucket, carries out after proper amount of active carbon is added with mixing, decoloration is stirred
Mixing the time must not be subsequently placed into filter less than 10 minutes, and be filtered；
O: being sterile filtered, step M obtained slurries aseptically, is filtered on the filter membrane that aperture is 0.45 micron；
P: the liquid glucose that step O is obtained is concentrated to get the liquid glucose that mass fraction is 71% through vacuum evaporating pot by concentration；
Q: secondary aseptic filtration, the liquid glucose that step P is obtained are again on 0.45 micron of filter membrane in aperture aseptically
Filtering, obtains finished product fructose syrup；
R: it is filling stand-by, the finished product fructose syrup that step Q is obtained is fitted into finished pot to get embodiment 2.
A kind of utilization of embodiment 3, which is cracked rice, produces the processing technology of fructose syrup, comprising the following steps:
A: impurity elimination of cracking rice takes raw material to crack rice, and carries out stone impurity elimination；
B: wash rice immersion, by step A obtain crack rice clean be put into soaking barrel, be added 5 times amount water, impregnate 60h；
C: defibrination is cracked rice what step B was obtained to be added in ground rice machine and is ground, is continuously added suitable water extremely during defibrination
Grinding is abundant；
D: sizing mixing, and takes the lotion in step C, and adjusting pH value is 6.0, be added into lotion a- amylase and 19 Baume of calcium chloride into
Row stirring；
E: iodine solution is added into step D for liquefaction, controls temperature at 110 DEG C, is kept for a period of time, until the not aobvious blue of Iod R,
DE is obtained 20%；
F: de- albumen, by the obtained Rice & peanut milk sediment of step E by washing protein, filters pressing, drying, packaging, after obtain albumen powder,
Wherein drying uses steam drying；
G: saccharification takes the Rice & peanut milk after step F, and adjusting pH value is 4.2, and carbohydrase is added into Rice & peanut milk and is stirred, stirring temperature
Degree is 60 DEG C, stirs 35h, and obtaining DE is 97%；
H: decoloration refined filtration takes mixed liquor in step G to be put into decoloration bucket, carries out the stirring of decolourizing with mixing after proper amount of active carbon is added
Time must not be less than 5 minutes, be subsequently placed into filter, be filtered to obtain liquid glucose；
I: the HCL that concentration is 5% is added into the liquid glucose of step H and the NaOH that concentration is 4% carries out ion exchange for ion exchange,
Wherein conductivity is no more than 50ms/cm；
J: condiment before isomery is added magnesium sulfate into step I and sodium pyrosulfite is stirred, and whipping temp is 60 DEG C, stirring
When pH value be 8.0, stir evenly；
K: isomerization, it is 40% isomerase that mass fraction is added into step J, obtains 42% fructose isomery after reaction is sufficiently stirred
Sugar；
L: the HCL that concentration is 5% is added into step K and the NaOH that concentration is 4% carries out ion exchange, electricity for Two-step ion-exchanging
Conductance is no more than 50ms/cm；
M: secondary decolourization refined filtration takes slurries in step L to be put into decoloration bucket, carries out after proper amount of active carbon is added with mixing, decoloration is stirred
Mixing the time must not be subsequently placed into filter less than 10 minutes, and be filtered；
O: being sterile filtered, step M obtained slurries aseptically, is filtered on the filter membrane that aperture is 0.45 micron；
P: the liquid glucose that step O is obtained is concentrated to get the liquid glucose that mass fraction is 71% through vacuum evaporating pot by concentration；
Q: secondary aseptic filtration, the liquid glucose that step P is obtained are again on 0.45 micron of filter membrane in aperture aseptically
Filtering, obtains finished product fructose syrup；
R: it is filling stand-by, the finished product fructose syrup that step Q is obtained is fitted into finished pot, is packed up to embodiment 3.
A kind of utilization of embodiment 4, which is cracked rice, produces the processing technology of fructose syrup, comprising the following steps:
A: impurity elimination of cracking rice takes raw material to crack rice, and carries out stone impurity elimination；
B: wash rice immersion, by step A obtain crack rice clean be put into soaking barrel, be added 5 times amount water, impregnate 48-60h；
C: defibrination is cracked rice what step B was obtained to be added in ground rice machine and is ground, is continuously added suitable water extremely during defibrination
Grinding is abundant；
D: sizing mixing, and takes the lotion in step C, and adjusting pH value is 6.0, be added into lotion a- amylase and 19 Baume of calcium chloride into
Row stirring；
E: iodine solution is added into step D for liquefaction, controls temperature at 108 DEG C, is kept for a period of time, until the not aobvious blue of Iod R,
DE is obtained 18%；
F: de- albumen, by the obtained Rice & peanut milk sediment of step E by washing protein, filters pressing, drying, packaging, after obtain albumen powder,
Wherein drying uses steam drying；
G: saccharification takes the Rice & peanut milk after step F, and adjusting pH value is 4.2, and carbohydrase is added into Rice & peanut milk and is stirred, stirring temperature
Degree is 60 DEG C, stirs 32h, and obtaining DE is 96%；
H: decoloration refined filtration takes mixed liquor in step G to be put into decoloration bucket, carries out the stirring of decolourizing with mixing after proper amount of active carbon is added
Time must not be less than 5 minutes, be subsequently placed into filter, be filtered to obtain liquid glucose；
I: the HCL that concentration is 5% is added into the liquid glucose of step H and the NaOH that concentration is 4% carries out ion exchange for ion exchange,
Wherein conductivity is no more than 50ms/cm；
J: condiment before isomery is added magnesium sulfate into step I and sodium pyrosulfite is stirred, and whipping temp is 60 DEG C, stirring
When pH value be 7.7, stir evenly；
K: isomerization, it is 42% isomerase that mass fraction is added into step J, obtains 42% fructose isomery after reaction is sufficiently stirred
Sugar；
L: the HCL that concentration is 5% is added into step K and the NaOH that concentration is 4% carries out ion exchange, electricity for Two-step ion-exchanging
Conductance is no more than 50ms/cm；
M: secondary decolourization refined filtration takes slurries in step L to be put into decoloration bucket, carries out after proper amount of active carbon is added with mixing, decoloration is stirred
Mixing the time must not be subsequently placed into filter less than 10 minutes, and be filtered；
O: being sterile filtered, step M obtained slurries aseptically, is filtered on the filter membrane that aperture is 0.45 micron；
P: the liquid glucose that step O is obtained is concentrated to get the liquid glucose that mass fraction is 71% through vacuum evaporating pot by concentration；
Q: secondary aseptic filtration, the liquid glucose that step P is obtained are again on 0.45 micron of filter membrane in aperture aseptically
Filtering, obtains finished product fructose syrup；
R: it is filling stand-by, the finished product fructose syrup that step Q is obtained is fitted into finished pot to get embodiment 4.
Fructose syrup made from the present embodiment 2-4 meets product quality and executes standard GB/T20882-2007.
The embodiment 1-4 fructose syrup prepared is compared into test, tests the concentration, pH value, coloration of its fructose syrup
And light transmittance.
Since glucose and fructose have a most stable of pH value, glucose is most stable in PH3.0, and fructose is 3.3
When it is most stable, therefore as seen from the above table, the present invention is steady using fructose syrup made from corn using fructose syrup ratio obtained of cracking rice
It is qualitative more preferable, and purity is higher.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (4)
1. a kind of utilization, which is cracked rice, produces the processing technology of fructose syrup, which comprises the following steps: impurity elimination-of cracking rice is washed
Rice immersion-defibrination-is sized mixing-liquefy-take off condiment-isomerization-before albumen-saccharification-decoloration refined filtration-ion exchange-isomery it is secondary from
Secondary aseptic filtration-concentration-the aseptic filtration-of sub- exchange-secondary decolourization refined filtration-is filling stand-by.
2. a kind of utilization according to claim 1, which is cracked rice, produces the processing technology of fructose syrup, it is characterised in that: described to add
Specific step is as follows for work technique:
A: impurity elimination of cracking rice takes raw material to crack rice, and carries out stone impurity elimination；
B: wash rice immersion, by step A obtain crack rice clean be put into soaking barrel, be added 5 times amount water, impregnate 48-60h；
C: defibrination is cracked rice what step B was obtained to be added in ground rice machine and is ground, is continuously added suitable water extremely during defibrination
Grinding is abundant；
D: sizing mixing, and takes the lotion in step C, and adjusting pH value is 6.0, be added into lotion a- amylase and 19 Baume of calcium chloride into
Row stirring；
E: iodine solution is added into step D for liquefaction, controls temperature at 105-110 DEG C, is kept for a period of time, until Iod R is not shown
Blue obtains DE in 15%-20%；
F: de- albumen, by the obtained Rice & peanut milk sediment of step E by washing protein, filters pressing, drying, packaging, after obtain albumen powder,
Wherein drying uses steam drying；
G: saccharification takes the Rice & peanut milk after step F, and adjusting pH value is 4.2, and carbohydrase is added into Rice & peanut milk and is stirred, stirring temperature
Degree is 60 DEG C, stirs 30h-35h, obtains DE >=95%；
H: decoloration refined filtration takes mixed liquor in step G to be put into decoloration bucket, carries out the stirring of decolourizing with mixing after proper amount of active carbon is added
Time must not be less than 5 minutes, be subsequently placed into filter, be filtered to obtain liquid glucose；
I: the HCL that concentration is 5% is added into the liquid glucose of step H and the NaOH that concentration is 4% carries out ion exchange for ion exchange,
Wherein conductivity is no more than 50ms/cm；
J: condiment before isomery is added magnesium sulfate into step I and sodium pyrosulfite is stirred, and whipping temp is 60 DEG C, stirring
When pH value be 7.5-8.0, stir evenly；
K: isomerization, it is 40-42% isomerase that mass fraction is added into step J, is sufficiently stirred after reaction that obtain 42% fructose different
Structure sugar；
L: the HCL that concentration is 5% is added into step K and the NaOH that concentration is 4% carries out ion exchange, electricity for Two-step ion-exchanging
Conductance is no more than 50ms/cm；
M: secondary decolourization refined filtration takes slurries in step L to be put into decoloration bucket, carries out after proper amount of active carbon is added with mixing, decoloration is stirred
Mixing the time must not be subsequently placed into filter less than 10 minutes, and be filtered；
O: being sterile filtered, step M obtained slurries aseptically, is filtered on the filter membrane that aperture is 0.45 micron；
P: the liquid glucose that step O is obtained is concentrated to get the liquid glucose that mass fraction is 71% through vacuum evaporating pot by concentration；
Q: secondary aseptic filtration, the liquid glucose that step P is obtained are again on 0.45 micron of filter membrane in aperture aseptically
Filtering, obtains finished product fructose syrup；
R: it is filling stand-by, the finished product fructose syrup that step Q is obtained is fitted into finished pot, packed for standby use.
3. a kind of utilization according to claim 2, which is cracked rice, produces the production technology of fructose syrup, it is characterised in that: the step
The washing protein water that rapid F takes off after the filters pressing in albumen can be added directly into step C defibrination, be recycled.
4. a kind of utilization according to claim 2, which is cracked rice, produces the production technology of fructose syrup, it is characterised in that: the step
It is 7.5~7.8 into column syrup pH value in rapid K in isomerization, temperature is 65 DEG C, and column isomerized sugar pH value is 6.5-7.0 out.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811086778.3A CN109136304A (en) | 2018-09-18 | 2018-09-18 | A kind of utilization, which is cracked rice, produces the processing technology of fructose syrup |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811086778.3A CN109136304A (en) | 2018-09-18 | 2018-09-18 | A kind of utilization, which is cracked rice, produces the processing technology of fructose syrup |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109136304A true CN109136304A (en) | 2019-01-04 |
Family
ID=64814833
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811086778.3A Pending CN109136304A (en) | 2018-09-18 | 2018-09-18 | A kind of utilization, which is cracked rice, produces the processing technology of fructose syrup |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109136304A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113025672A (en) * | 2021-03-12 | 2021-06-25 | 江西恒顶食品有限公司 | Preparation method of high-purity high fructose corn syrup |
| CN114395591A (en) * | 2022-01-19 | 2022-04-26 | 广西大学 | Preparation method of broken rice crystalline fructose |
| CN116655814A (en) * | 2023-04-17 | 2023-08-29 | 上海交通大学 | Preparation method of rice starch using broken rice as raw material |
| WO2023174315A1 (en) * | 2022-03-18 | 2023-09-21 | 武汉美味源生物工程有限公司 | Method for producing high-purity rice protein powder and rice syrup |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101709336A (en) * | 2009-12-21 | 2010-05-19 | 安徽丰原发酵技术工程研究有限公司 | Method for preparing high-concentration fructose syrup |
| CN101979643A (en) * | 2010-10-01 | 2011-02-23 | 曾爱民 | Preparation process of rice high fructose syrup |
| CN102242167A (en) * | 2011-04-25 | 2011-11-16 | 武汉市金德戈糖业有限公司 | Technology for producing fructose-glucose syrup containing 90% of fructose from rice |
| CN104630312A (en) * | 2015-01-20 | 2015-05-20 | 西王药业有限公司 | Method for producing high fructose corn syrup by employing glucose mother liquor |
| CN105177087A (en) * | 2015-08-10 | 2015-12-23 | 蚌埠丰原涂山制药有限公司 | Method for preparing high fructose corn syrup by using glucose syrup |
| CN106244648A (en) * | 2016-08-30 | 2016-12-21 | 广西慧投互联网金融服务有限公司 | A kind of method of corn starch milk preparation fruit glucose syrup |
| CN107475322A (en) * | 2017-07-25 | 2017-12-15 | 安徽万德生物科技有限公司 | A kind of technique for preparing fructose syrup |
| CN108265091A (en) * | 2018-01-19 | 2018-07-10 | 福建小薇金匙科技孵化有限公司 | A kind of technique for preparing fructose syrup using rice |
-
2018
- 2018-09-18 CN CN201811086778.3A patent/CN109136304A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101709336A (en) * | 2009-12-21 | 2010-05-19 | 安徽丰原发酵技术工程研究有限公司 | Method for preparing high-concentration fructose syrup |
| CN101979643A (en) * | 2010-10-01 | 2011-02-23 | 曾爱民 | Preparation process of rice high fructose syrup |
| CN102242167A (en) * | 2011-04-25 | 2011-11-16 | 武汉市金德戈糖业有限公司 | Technology for producing fructose-glucose syrup containing 90% of fructose from rice |
| CN104630312A (en) * | 2015-01-20 | 2015-05-20 | 西王药业有限公司 | Method for producing high fructose corn syrup by employing glucose mother liquor |
| CN105177087A (en) * | 2015-08-10 | 2015-12-23 | 蚌埠丰原涂山制药有限公司 | Method for preparing high fructose corn syrup by using glucose syrup |
| CN106244648A (en) * | 2016-08-30 | 2016-12-21 | 广西慧投互联网金融服务有限公司 | A kind of method of corn starch milk preparation fruit glucose syrup |
| CN107475322A (en) * | 2017-07-25 | 2017-12-15 | 安徽万德生物科技有限公司 | A kind of technique for preparing fructose syrup |
| CN108265091A (en) * | 2018-01-19 | 2018-07-10 | 福建小薇金匙科技孵化有限公司 | A kind of technique for preparing fructose syrup using rice |
Non-Patent Citations (1)
| Title |
|---|
| 何照范等: "《植物淀粉及其利用》", 31 March 1990 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113025672A (en) * | 2021-03-12 | 2021-06-25 | 江西恒顶食品有限公司 | Preparation method of high-purity high fructose corn syrup |
| CN113025672B (en) * | 2021-03-12 | 2022-10-18 | 江西恒顶食品有限公司 | Preparation method of high-purity fructose syrup |
| CN114395591A (en) * | 2022-01-19 | 2022-04-26 | 广西大学 | Preparation method of broken rice crystalline fructose |
| WO2023174315A1 (en) * | 2022-03-18 | 2023-09-21 | 武汉美味源生物工程有限公司 | Method for producing high-purity rice protein powder and rice syrup |
| CN116655814A (en) * | 2023-04-17 | 2023-08-29 | 上海交通大学 | Preparation method of rice starch using broken rice as raw material |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109136304A (en) | A kind of utilization, which is cracked rice, produces the processing technology of fructose syrup | |
| CN104946448B (en) | A kind of beer-brewing syrup production method based on corn direct method | |
| CN109082347A (en) | A method of improving crystal malt percent crystallization in massecuite | |
| CN107653279A (en) | A kind of glucose syrup production technology | |
| CN101597628A (en) | The method of preparing xylo-oligosaccharide by corn husk enzymatic hydrolysis | |
| CN114410725A (en) | Enzymolysis and decoloration method for protein in potato starch wastewater | |
| CN102747120B (en) | Preparation method of special inverted syrup for moon cakes | |
| CN101613729B (en) | Method for preparing maltodextrin with low DE value by taking rice as raw material | |
| CN1408836A (en) | Enzymatic process for brewing wine through liquid state saccharifying and liquid state fermentation and with millet as raw material | |
| CN105624235A (en) | Method for preparing xylose by utilizing eucalyptus pulp waste liquid | |
| CN1088749C (en) | Malt syrup containing alpha-amino-N and its preparation method | |
| US5833757A (en) | Process for conversion of bananas to sugar syrup | |
| CN111118086A (en) | Method for preparing starch syrup, phytic acid and protein by co-production of bran and starch syrup | |
| CN107287263A (en) | A kind of preparation method of high-purity malt sugar coproduction β limit dextrins | |
| CN113337556A (en) | Preparation process of syrup for snowflake crisp and prepared syrup for snowflake crisp | |
| CN112410387A (en) | Production method of low-iodine value and ultrahigh malt syrup | |
| CN87100414A (en) | With carbohydrate, starch, potato class, Cereals class and soybean is raw material production beer | |
| CN110903938A (en) | Fermented mulberry fruit wine compound clarifying agent and use method thereof | |
| CN109266705A (en) | The production technology of fructose syrup extraction is carried out using rice | |
| JP3875899B2 (en) | Natto and its manufacturing method | |
| JP5938754B1 (en) | Manufacturing method of mirin | |
| KR20180089047A (en) | Manufacturing method of grain syrup using rice | |
| CN116590362A (en) | High fructose syrup production process | |
| CN107022589A (en) | A kind of method of use rice production F42 type fructose syrups | |
| JPS61219374A (en) | Method of brewing refined sake (liquor) |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190104 |