CN109133619A - A kind of glass drill mosaic and preparation method thereof and ornament materials - Google Patents
A kind of glass drill mosaic and preparation method thereof and ornament materials Download PDFInfo
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- CN109133619A CN109133619A CN201811080207.9A CN201811080207A CN109133619A CN 109133619 A CN109133619 A CN 109133619A CN 201811080207 A CN201811080207 A CN 201811080207A CN 109133619 A CN109133619 A CN 109133619A
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- parts
- glass drill
- raw material
- mosaic
- colorant
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/04—Opacifiers, e.g. fluorides or phosphates; Pigments
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a kind of glass drill mosaics, it is characterized in that, including following raw material: quartz sand, soda ash, calcite, scheelite powder, fluorite, prodan, sodium nitrate, colorant, opacifiers, silicon powder and oxide, preparation method are as follows: quartz sand, soda ash, calcite, scheelite powder, fluorite, prodan, sodium nitrate, silicon powder and oxide are mixed, it is smashed and ground；S3: kiln is added in glass drill raw material, so that glass drill melting sources are at melt；S4: colorant and opacifiers are added into melt；S5: colouring melt is taken out from kiln using operated pressing tool compression moulding and obtains glass drill mosaic.Glass drill mosaic surfacing prepared by the present invention is non-microcracked, color bright in luster is good, and fugitive color, thermal stability and wear-resisting property be not good.
Description
Technical field
The present invention relates to ornament preparation technical field, specifically a kind of glass drill mosaic and preparation method thereof and decoration
Material.
Background technique
Mosaic, for being combined into the sheet small tiles of various decorative patterns in building, blank is through semi-dry pressing, kiln
It is inside fired into mosaic, is mainly used for floor file or inner wall decoration, it can also be used to exterior wall finish.
Finishing is all particular about on the exterior wall of modern architecture, interior wall, ground, and then various finishing materials come into being, pottery
Ceramic tile, marble, glass Mosaic etc. are all to be widely used the advantages that its resistance to flushing, bright and clean.And glass
It is again beautiful gorgeous famous with it to bore mosaic, is more liked by people, and general mosaic colorant layer is only attached to glass
The surface layer of glass mosaic ontology, the low in glossiness of color, wearability are poor.
Summary of the invention
It is above-mentioned to solve the purpose of the present invention is to provide a kind of glass drill mosaic and preparation method thereof and ornament materials
The problem of being proposed in background technique.
To achieve the above object, the invention provides the following technical scheme:
A kind of glass drill mosaic, including following raw material in parts by weight: 30-50 parts of quartz sand, 10-30 parts of soda ash, side
Solve stone 2-10 parts, 8-20 parts of scheelite powder, 3-7 parts of fluorite, 5-15 parts of prodan, 1-5 parts of sodium nitrate, 3-9 parts of colorant, milkiness
1-5 parts of agent, 2-10 parts of silicon powder and 4-12 parts of oxide.
As a further solution of the present invention: including following raw material in parts by weight: 35-45 parts of quartz sand, soda ash
15-25 parts, 4-8 parts of calcite, 11-17 parts of scheelite powder, 4-6 parts of fluorite, 8-12 parts of prodan, 2-4 parts of sodium nitrate, colorant
4-8 parts, 2-4 parts of opacifiers, 4-8 parts of silicon powder and 6-10 parts of oxide.
As further scheme of the invention: including following raw material in parts by weight: 40 parts of quartz sand, soda ash 20
Part, 6 parts of calcite, 14 parts of scheelite powder, 5 parts of fluorite, 10 parts of prodan, 3 parts of sodium nitrate, 6 parts of colorant, 3 parts of opacifiers, silicon
6 parts and 8 parts of oxide of powder.
As further scheme of the invention: the oxide is silica, sodium oxide molybdena and calcium oxide therein one
Kind or a variety of mixtures.
As further scheme of the invention: the colorant uses chemical industry colorant.
A kind of preparation method of the glass drill mosaic, comprising the following steps:
S1: each raw material is weighed respectively by weight；
S2: quartz sand, soda ash, calcite, scheelite powder, fluorite, prodan, sodium nitrate, silicon powder and oxide are mixed,
Then it is smashed and ground by pulverizer, obtains glass drill raw material；
S3: kiln is added in glass drill raw material, so that glass drill melting sources are at melt；
S4: colorant and opacifiers being added into melt, and stirring keeps colorant uniform, obtain colouring melt；
S5: taking out colouring melt from kiln, using operated pressing tool compression moulding, then made annealing treatment, obtain glass drill
Mosaic.
As further scheme of the invention: the raw material smashing and grinding granularity of the step S2 is 80-100 mesh.
As further scheme of the invention: the glass melting temperature of the step S3 are as follows: 1200~1600 DEG C, melting time
Are as follows: 60~80min.
A kind of ornament materials, including the glass drill mosaic.
Compared with prior art, the beneficial effects of the present invention are: directly by colorant in glass drill mosaic of the invention
It melted, be blended with raw material, such colorant is located immediately at the inside of glass drill mosaic, and then it is de- to avoid mosaic from being easy
Color, and opacifiers can increase the muddy of mosaic and feel and agglomerate colorant hyperchromic, while silicon powder and sodium nitrate can increase
The wear-resistant strength and hardness of glass drill mosaic and avoid the occurrence of crackle.Glass drill mosaic surfacing prepared by the present invention
Color non-microcracked, bright in luster is good, and fugitive color, thermal stability and wear-resisting property be not good.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment one:
A kind of glass drill mosaic, including following raw material in parts by weight: 30 parts of quartz sand, 10 parts of soda ash, calcite 2
Part, 8 parts of scheelite powder, 3 parts of fluorite, 5 parts of prodan, 1 part of sodium nitrate, 3- parts of colorant, 1 part of opacifiers, 2 parts of silicon powder and oxidation
4 parts of object.
The oxide is silica
The colorant uses chemical industry colorant.
A kind of preparation method of the glass drill mosaic, comprising the following steps:
S1: each raw material is weighed respectively by weight；
S2: quartz sand, soda ash, calcite, scheelite powder, fluorite, prodan, sodium nitrate, silicon powder and oxide are mixed,
Then it is smashed and ground by pulverizer, obtains glass drill raw material；
S3: kiln is added in glass drill raw material, so that glass drill melting sources are at melt；
S4: colorant and opacifiers being added into melt, and stirring keeps colorant uniform, obtain colouring melt；
S5: taking out colouring melt from kiln, using operated pressing tool compression moulding, then made annealing treatment, obtain glass drill
Mosaic.
The raw material smashing and grinding granularity of the step S2 is 80 mesh.
The glass melting temperature of the step S3 are as follows: 1200 DEG C, melting time are as follows: 60min.
A kind of ornament materials, including the glass drill mosaic.
Embodiment two:
A kind of glass drill mosaic, including following raw material in parts by weight: 35 parts of quartz sand, 15 parts of soda ash, calcite 4
Part, 11 parts of scheelite powder, 4 parts of fluorite, 8 parts of prodan, 2 parts of sodium nitrate, 4 parts of colorant, 2 parts of opacifiers, 4 parts of silicon powder and oxidation
6 parts of object.
The oxide is sodium oxide molybdena.
The colorant uses chemical industry colorant.
A kind of preparation method of the glass drill mosaic, comprising the following steps:
S1: each raw material is weighed respectively by weight；
S2: quartz sand, soda ash, calcite, scheelite powder, fluorite, prodan, sodium nitrate, silicon powder and oxide are mixed,
Then it is smashed and ground by pulverizer, obtains glass drill raw material；
S3: kiln is added in glass drill raw material, so that glass drill melting sources are at melt；
S4: colorant and opacifiers being added into melt, and stirring keeps colorant uniform, obtain colouring melt；
S5: taking out colouring melt from kiln, using operated pressing tool compression moulding, then made annealing treatment, obtain glass drill
Mosaic.
The raw material smashing and grinding granularity of the step S2 is 100 mesh.
The glass melting temperature of the step S3 are as follows: 1300 DEG C, melting time are as follows: 65min.
A kind of ornament materials, including the glass drill mosaic.
Embodiment three:
A kind of glass drill mosaic, including following raw material in parts by weight: 40 parts of quartz sand, 20 parts of soda ash, calcite 6
Part, 14 parts of scheelite powder, 5 parts of fluorite, 10 parts of prodan, 3 parts of sodium nitrate, 6 parts of colorant, 3 parts of opacifiers, 6 parts of silicon powder and oxygen
8 parts of compound.
The oxide is calcium oxide.
The colorant uses chemical industry colorant.
A kind of preparation method of the glass drill mosaic, comprising the following steps:
S1: each raw material is weighed respectively by weight；
S2: quartz sand, soda ash, calcite, scheelite powder, fluorite, prodan, sodium nitrate, silicon powder and oxide are mixed,
Then it is smashed and ground by pulverizer, obtains glass drill raw material；
S3: kiln is added in glass drill raw material, so that glass drill melting sources are at melt；
S4: colorant and opacifiers being added into melt, and stirring keeps colorant uniform, obtain colouring melt；
S5: taking out colouring melt from kiln, using operated pressing tool compression moulding, then made annealing treatment, obtain glass drill
Mosaic.
The raw material smashing and grinding granularity of the step S2 is 80 mesh.
The glass melting temperature of the step S3 are as follows: 1400 DEG C, melting time are as follows: 70min.
A kind of ornament materials, including the glass drill mosaic.
Example IV:
A kind of glass drill mosaic, including following raw material in parts by weight: 345 parts of quartz sand, 25 parts of soda ash, calcite 8
Part, 17 parts of scheelite powder, 6 parts of fluorite, 12 parts of prodan, 4 parts of sodium nitrate, 8 parts of colorant, 4 parts of opacifiers, 8 parts of silicon powder and oxygen
10 parts of compound.
The oxide is silica and sodium oxide molybdena, weight ratio 1:2.
The colorant uses chemical industry colorant.
A kind of preparation method of the glass drill mosaic, comprising the following steps:
S1: each raw material is weighed respectively by weight；
S2: quartz sand, soda ash, calcite, scheelite powder, fluorite, prodan, sodium nitrate, silicon powder and oxide are mixed,
Then it is smashed and ground by pulverizer, obtains glass drill raw material；
S3: kiln is added in glass drill raw material, so that glass drill melting sources are at melt；
S4: colorant and opacifiers being added into melt, and stirring keeps colorant uniform, obtain colouring melt；
S5: taking out colouring melt from kiln, using operated pressing tool compression moulding, then made annealing treatment, obtain glass drill
Mosaic.
The raw material smashing and grinding granularity of the step S2 is 100 mesh.
The glass melting temperature of the step S3 are as follows: 1500 DEG C, melting time are as follows: 75min.
A kind of ornament materials, including the glass drill mosaic.
Embodiment five:
A kind of glass drill mosaic, including following raw material in parts by weight: 50 parts of quartz sand, 30 parts of soda ash, calcite 10
Part, 20 parts of scheelite powder, 7 parts of fluorite, 515 parts of prodan, 5 parts of sodium nitrate, 9 parts of colorant, 5 parts of opacifiers, 10 parts of silicon powder and
12 parts of oxide.
The oxide is silica, sodium oxide molybdena and the one such or a variety of mixture of calcium oxide.
The colorant uses chemical industry colorant.
A kind of preparation method of the glass drill mosaic, comprising the following steps:
S1: each raw material is weighed respectively by weight；
S2: quartz sand, soda ash, calcite, scheelite powder, fluorite, prodan, sodium nitrate, silicon powder and oxide are mixed,
Then it is smashed and ground by pulverizer, obtains glass drill raw material；
S3: kiln is added in glass drill raw material, so that glass drill melting sources are at melt；
S4: colorant and opacifiers being added into melt, and stirring keeps colorant uniform, obtain colouring melt；
S5: taking out colouring melt from kiln, using operated pressing tool compression moulding, then made annealing treatment, obtain glass drill
Mosaic.
The raw material smashing and grinding granularity of the step S2 is 100 mesh.
The glass melting temperature of the step S3 are as follows: 1600 DEG C, melting time are as follows: 80min.
A kind of ornament materials, including the glass drill mosaic.
Comparative example 1
Compared with Example 3, not silicon powder-containing, other are same as Example 3.
Comparative example 2
Compared with Example 3, sodium nitrate is free of, other are same as Example 3.
Comparative example 3
Compared with Example 3, not silicon powder-containing and sodium nitrate, other are same as Example 3.
Example 3 and the glass Mosaic of comparative example 1-3 preparation, specification is the square of 20mm × 20mm, right respectively
It carries out wearability and heat stability test.
Heat stability test: 20 blocks of glass without the neat embodiment 1-3 in obvious crack, corner and comparative example 1 are taken respectively
Mosaic, block-by-block are laid in gabion, and basket is put into constant temperature in 90 DEG C of sink, makes water immersion sample.It keeps
It takes out, is immediately placed in 25 DEG C of water after 30min, proposed after keeping 10min, whether there are cracks or damaged for block-by-block range estimation, as a result sees below
Table:
| Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | |
| Thermostabilization situation | It is not cracked | 2 pieces cracked | 1 piece cracked | 6 is cracked, and 1 piece ruptures |
Show that the thermal stability of the glass Mosaic of embodiment 3 is substantially better than comparative example 1-3, therefore thermal stability is more preferable.
Wearability detection: the method according to as defined in GB11950-89 detects the wearability of glass Mosaic, wear-resisting
Property the result is as follows:
| Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 | |
| Revolution under appreciable wear | 1600 | 750 | 900 | 600 |
| Grade | Ⅳ | Ⅲ | Ⅲ | Ⅱ |
As seen from the above table, the wear-resisting grade of the glass Mosaic of embodiment 3 is IV grade, the glass Mosaic of comparative example 1-2
Wear-resisting grade is III grade, and the wear-resisting grade of the glass Mosaic of comparative example 3 is II grade, shows that the glass Mosaic of embodiment 3 is resistance to
Mill property is more preferable.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (9)
1. a kind of glass drill mosaic, which is characterized in that including following raw material in parts by weight: 30-50 parts of quartz sand, pure
10-30 parts of alkali, 2-10 parts of calcite, 8-20 parts of scheelite powder, 3-7 parts of fluorite, 5-15 parts of prodan, 1-5 parts of sodium nitrate, coloring
3-9 parts of agent, 1-5 parts of opacifiers, 2-10 parts of silicon powder and 4-12 parts of oxide.
2. glass drill mosaic according to claim 1, which is characterized in that including following raw material in parts by weight:
35-45 parts of quartz sand, 15-25 parts of soda ash, 4-8 parts of calcite, 11-17 parts of scheelite powder, 4-6 parts of fluorite, 8-12 parts of prodan,
2-4 parts of sodium nitrate, 4-8 parts of colorant, 2-4 parts of opacifiers, 4-8 parts of silicon powder and 6-10 parts of oxide.
3. glass drill mosaic according to claim 1, which is characterized in that including following raw material in parts by weight:
40 parts of quartz sand, 20 parts of soda ash, 6 parts of calcite, 14 parts of scheelite powder, 5 parts of fluorite, 10 parts of prodan, 3 parts of sodium nitrate, coloring
6 parts of agent, 3 parts of opacifiers, 6 parts of silicon powder and 8 parts of oxide.
4. glass drill mosaic according to claim 1, which is characterized in that the oxide is silica, sodium oxide molybdena
One such or a variety of mixture with calcium oxide.
5. glass drill mosaic according to claim 1, which is characterized in that the colorant uses chemical industry colorant.
6. a kind of preparation method of glass drill mosaic a method as claimed in any one of claims 1 to 5, which is characterized in that including following step
It is rapid:
S1: each raw material is weighed respectively by weight；
S2: quartz sand, soda ash, calcite, scheelite powder, fluorite, prodan, sodium nitrate, silicon powder and oxide are mixed,
Then it is smashed and ground by pulverizer, obtains glass drill raw material；
S3: kiln is added in glass drill raw material, so that glass drill melting sources are at melt；
S4: colorant and opacifiers being added into melt, and stirring keeps colorant uniform, obtain colouring melt；
S5: taking out colouring melt from kiln, using operated pressing tool compression moulding, then made annealing treatment, obtain glass drill
Mosaic.
7. the preparation method of glass drill mosaic according to claim 6, which is characterized in that the raw material powder of the step S2
Breakdown mill granularity is 80-100 mesh.
8. the preparation method of glass drill mosaic according to claim 6, which is characterized in that the melted temperature of the step S3
Degree are as follows: 1200~1600 DEG C, melting time are as follows: 60~80min.
9. a kind of ornament materials, which is characterized in that including glass drill mosaic as described in claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811080207.9A CN109133619A (en) | 2018-09-17 | 2018-09-17 | A kind of glass drill mosaic and preparation method thereof and ornament materials |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811080207.9A CN109133619A (en) | 2018-09-17 | 2018-09-17 | A kind of glass drill mosaic and preparation method thereof and ornament materials |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109133619A true CN109133619A (en) | 2019-01-04 |
Family
ID=64814371
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811080207.9A Pending CN109133619A (en) | 2018-09-17 | 2018-09-17 | A kind of glass drill mosaic and preparation method thereof and ornament materials |
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| CN (1) | CN109133619A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106517742A (en) * | 2016-11-28 | 2017-03-22 | 四会市伟祺玻璃建材有限公司 | Glass mosaic and preparation method thereof |
| CN107382059A (en) * | 2017-08-01 | 2017-11-24 | 合肥利裕泰玻璃制品有限公司 | A kind of glass Mosaic and preparation method thereof |
-
2018
- 2018-09-17 CN CN201811080207.9A patent/CN109133619A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106517742A (en) * | 2016-11-28 | 2017-03-22 | 四会市伟祺玻璃建材有限公司 | Glass mosaic and preparation method thereof |
| CN107382059A (en) * | 2017-08-01 | 2017-11-24 | 合肥利裕泰玻璃制品有限公司 | A kind of glass Mosaic and preparation method thereof |
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Application publication date: 20190104 |
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