CN109121963A - A kind of non-yellow twig causes the administering method of citrus yellow - Google Patents

A kind of non-yellow twig causes the administering method of citrus yellow Download PDF

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CN109121963A
CN109121963A CN201810961186.5A CN201810961186A CN109121963A CN 109121963 A CN109121963 A CN 109121963A CN 201810961186 A CN201810961186 A CN 201810961186A CN 109121963 A CN109121963 A CN 109121963A
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yellow
parts
conyza canadensis
renovation agent
extract
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CN109121963B (en
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万立军
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Shaanxi Gurun Crop Science Co Ltd
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Shaanxi Gurun Crop Science Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G17/00Cultivation of hops, vines, fruit trees, or like trees
    • A01G17/005Cultivation methods
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G13/00Protecting plants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
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  • Natural Medicines & Medicinal Plants (AREA)
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  • Inorganic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses the administering methods that a kind of non-yellow twig causes citrus yellow, yellow renovation agent is used to the citrus that yellow occurs, access times are 3~5 times, every minor tick 7~10 days, the yellow renovation agent is divided into two parts when using every time, a portion sprays blade, another part is for pouring root, the yellow renovation agent is that effective component is watered acquisition, the effective component includes Conyza canadensis extract, praseodymium nitrate, 5-ALA, lauroyl glutamate, potassium lactate and potassium cinnamate, the Conyza canadensis extract passes through ethyl acetate, the fresh Conyza canadensis complete stool of the extraction with aqueous solution of ethyl alcohol and hydrogen peroxide obtains.The present invention uses homemade yellow renovation agent, obvious to mandarin tree (caused by the non-yellow twig) repairing effect for having occurred and that yellow, and the green phase that turns of yellow mandarin tree is about 3 months, it is high to turn green rate, hence it is evident that be better than yellow recovery scenario in the prior art.

Description

A kind of non-yellow twig causes the administering method of citrus yellow
Technical field
The present invention relates to fruit-tree breeding and planting technology field, in particular to a kind of non-yellow twig causes the improvement of citrus yellow Method.
Background technique
In the planting process of citrus, the plantation problem that farmer most worries is exactly the yellow problem of citrus, many to plant Family is mistakenly considered yellow twig, to abandon the improvement to citrus.But really causing citrus to generate aetiolation has a lot of reasons, example Such as: 1. cultivation managements: root yellow, physiological drought yellow, orchard product are hurt in the excessive tree vigo(u)r decline yellow of girdling wound tree, fruiting, fertilising Root system yellow, hormone, herbicide excess, soil hardening etc. are infected in rotten yellow of water, soil pests.2. high/low temperature shadow It rings: under high temperature, forming the yellow scab of chlorisis on blade face, burn and aggravate with day, when macula lutea becomes brown, the leaf tissue at the position Death meets rainwater and is easy infection anthracnose, leads to leaf abscission;Under low temperature, citrus is done harm to the cold, will lead to young sprout yellow, it is difficult to It is aging.3. insect pest: after the pests such as longicorn, root-knot nematode, borer, mite class are caused harm, plant can be caused short and small, blade it is small and Thin, it is green slow to turn, and turns to be yellow or in bronze colour, flower, fruit are easy to fall off, and tree vigo(u)r obviously fails.4. disease yellow twig, anthracnose etc..5. Lack nutritional ingredient or element.
It mainly include at present by the improvement of planting technique, the prevention and treatment of pest and disease damage and supplement to the preventing control method of citrus yellow Nutritional ingredient.Planting technique replaces previous single fertilizer using organic-inorganic composite fertilizer, improves to soil;Optimization is poured Technique is filled, ground moistening is kept;Optimize weeding technique, avoids hurting root.The prevention and treatment of pest and disease damage combine yellow twig prevention and control measure and Citrus treelet pest and disease damage General situations carry out integrated control.Nutritional ingredient needed for adding citrus in citrus fertilizer, and it is aided with leaf Face sprays the full nutrition foliage fertilizer of amino acid high calcium.But found in practical plantation, these above-mentioned measures are to controlling after citrus yellow It is poor to manage effect, Citrus Yellowing repairs situation and although makes moderate progress, but yellow repair rate is low, is still difficult to meet the requirements.
Summary of the invention
In order to solve the above technical problems, the present invention provides the administering methods that a kind of non-yellow twig causes citrus yellow, to hair The citrus of raw yellow uses yellow renovation agent, and access times are 3~5 times, and every minor tick 7~10 days will be described when using every time Yellow renovation agent is divided into two parts, and a portion sprays blade, and another part for pouring root, repair by the yellow Multiple agent is that effective component is watered acquisition, and the effective component includes Conyza canadensis extract, praseodymium nitrate, 5-ALA, the moon Osmanthus acyl glutamic acid, potassium lactate and potassium cinnamate, the Conyza canadensis extract pass through ethyl acetate, the aqueous solution of ethyl alcohol and hydrogen peroxide Fresh Conyza canadensis complete stool is extracted to obtain.
Further, the Conyza canadensis extract preparation method the following steps are included:
(1) configuration extraction liquid: the aqueous solution of configuration ethyl acetate, ethyl alcohol and hydrogen peroxide, wherein the quality percentage of ethyl acetate contains Amount is 5%~8%, and the mass percentage of ethyl alcohol is 5%~8%, H2O2Mass percentage be 1.4%~3.6%, remaining is water;
(2) fresh Conyza canadensis complete stool is shredded, the Conyza canadensis after chopping is put into seal pot, then the extracting solution is poured into close Envelope kettle in mix with Conyza canadensis, seal pot is put into vacuum oven and vacuumizes, and under vacuum conditions pressure maintaining standing 10h with On;
(3) seal pot is taken out after the completion of pressure maintaining, seals autoclave body, the mixture in seal pot is then heated to 140~160 DEG C extract, extract after the completion of open seal pot, cooled to room temperature, filtering, after being extracted slag and extraction after liquid;It is described to mention It takes rear liquid to be concentrated under reduced pressure, obtains the Conyza canadensis extract.
Further, in the step (2), the addition weight of the extracting solution is 3~4 times of Conyza canadensis weight, step (3) in, after extraction liquid be concentrated under reduced pressure into extract after liquid product 1/5~1/4.
Further, in the step (2), vacuum degree≤0.2 standard atmospheric pressure that vacuumizes.
Further, in the step (3), the time of 140~160 DEG C of extractions is 30min or more.
Further, each component is calculated by weight as in the effective component: 100 parts of Conyza canadensis extract, praseodymium nitrate 10~15 parts, 10~15 parts of 5-ALA, 2~8 parts of lauroyl glutamate, 22~28 parts of potassium lactate and potassium cinnamate 1 ~5 parts;The effective component and water are according to effective component: water=25~30g:30 jins is converted the synthesis yellow renovation agent.
Further, the part that the yellow renovation agent is used to spray blade is added with adjuvant, the auxiliary Agent includes dodecyldimethylammonium hydroxide inner salt, dodecyl trimethyl ammonium chloride, magnesium gluconate and Dove sugar alcohol calcium.
Further, each component is calculated by weight as in the adjuvant:
10~20 parts of dodecyldimethylammonium hydroxide inner salt;
10~20 parts of dodecyl trimethyl ammonium chloride;
2~5 parts of magnesium gluconate;
1~3 part of Dove sugar alcohol calcium;
Yellow renovation agent for being sprayed to blade is 20~30 times of the adjuvant quality.
Further, the yellow renovation agent is that effective component is watered acquisition, and the amount being watered is the 600 of effective component weight ~1000 times.
The beneficial effects of the present invention are:
1. the present invention uses homemade yellow renovation agent, the mandarin tree (caused by non-yellow twig) for having occurred and that yellow is repaired Effect is obvious, and the green phase that turns of yellow mandarin tree is about 3 months, it is high to turn green rate, hence it is evident that be better than yellow reparation side in the prior art Case;
2. spraying Dove sugar alcohol calcium in blade according to the conventional method, the calcium content of mandarin tree can be supplemented to a certain extent, it is right The yellow reparation of citrus has the effect of certain.But experiment discovery, simple Dove sugar alcohol calcium of spraying is to citrus yellow reparation Act on it is very limited, turn green rate less than 20%.Using adjuvant of the present invention, in conjunction with the homemade yellow renovation agent of the present invention, The repairing effect of yellow renovation agent can be further increased.
Specific embodiment
The present invention will be further explained with reference to the examples below.
Embodiment 1
A kind of yellow renovation agent, the yellow renovation agent are that effective component is watered acquisition, and the effective component includes that Conyza canadensis mentions Object, praseodymium nitrate, 5-ALA, lauroyl glutamate, potassium lactate and potassium cinnamate are taken, each component is according to parts by weight Are as follows: 100 parts of Conyza canadensis extract, 10 parts of praseodymium nitrate, 10 parts of 5-ALA, 2 parts of lauroyl glutamate, 22 parts of potassium lactate With 1 part of potassium cinnamate.The effective component and water are according to effective component: water=25g:30 jins is converted synthesis yellow renovation agent.
The preparation method of Conyza canadensis extract the following steps are included:
(1) configuration extraction liquid: the aqueous solution of configuration ethyl acetate, ethyl alcohol and hydrogen peroxide, wherein the quality percentage of ethyl acetate contains Amount is 5%, and the mass percentage of ethyl alcohol is 5%, H2O2Mass percentage be 1.4%, remaining is water;
(2) fresh Conyza canadensis complete stool is shredded, the Conyza canadensis after chopping is put into seal pot, then the extracting solution is poured into close It is mixed in envelope kettle with Conyza canadensis, the addition weight of extracting solution is 4 times of Conyza canadensis weight;Seal pot is put into vacuum oven and takes out Vacuum degree in vacuum oven is evacuated to 0.1 standard atmospheric pressure by vacuum, and pressure maintaining stands 10h under vacuum conditions;
(3) seal pot is taken out after the completion of pressure maintaining, seals autoclave body, the mixture in seal pot is then heated to 140~160 DEG C extract 30min, extract after the completion of open seal pot, cooled to room temperature, filtering, after being extracted slag and extraction after liquid; After the extraction liquid be concentrated under reduced pressure into extract after liquid product 1/4, obtain the Conyza canadensis extract.
Embodiment 2
A kind of yellow renovation agent, the yellow renovation agent are that effective component is watered acquisition, and the effective component includes that Conyza canadensis mentions Object, praseodymium nitrate, 5-ALA, lauroyl glutamate, potassium lactate and potassium cinnamate are taken, each component is according to parts by weight Are as follows: 100 parts of Conyza canadensis extract, 12 parts of praseodymium nitrate, 12 parts of 5-ALA, 4 parts of lauroyl glutamate, 24 parts of potassium lactate With 2 parts of potassium cinnamate.The effective component and water are according to effective component: water=25g:30 jins is converted synthesis yellow renovation agent.
The preparation method of Conyza canadensis extract the following steps are included:
(1) configuration extraction liquid: the aqueous solution of configuration ethyl acetate, ethyl alcohol and hydrogen peroxide, wherein the quality percentage of ethyl acetate contains Amount is 6%, and the mass percentage of ethyl alcohol is 6%, H2O2Mass percentage be 2.1%, remaining is water;
(2) fresh Conyza canadensis complete stool is shredded, the Conyza canadensis after chopping is put into seal pot, then the extracting solution is poured into close It is mixed in envelope kettle with Conyza canadensis, the addition weight of extracting solution is 4 times of Conyza canadensis weight;Seal pot is put into vacuum oven and takes out Vacuum degree in vacuum oven is evacuated to 0.1 standard atmospheric pressure by vacuum, and pressure maintaining stands 10h under vacuum conditions;
(3) seal pot is taken out after the completion of pressure maintaining, seals autoclave body, the mixture in seal pot is then heated to 140~160 DEG C extract 30min, extract after the completion of open seal pot, cooled to room temperature, filtering, after being extracted slag and extraction after liquid; After the extraction liquid be concentrated under reduced pressure into extract after liquid product 1/4, obtain the Conyza canadensis extract.
Embodiment 3
A kind of yellow renovation agent, the yellow renovation agent are that effective component is watered acquisition, and the effective component includes that Conyza canadensis mentions Object, praseodymium nitrate, 5-ALA, lauroyl glutamate, potassium lactate and potassium cinnamate are taken, each component is according to parts by weight Are as follows: 100 parts of Conyza canadensis extract, 14 parts of praseodymium nitrate, 14 parts of 5-ALA, 6 parts of lauroyl glutamate, 26 parts of potassium lactate With 3 parts of potassium cinnamate.The effective component and water are according to effective component: water=25g:30 jins is converted synthesis yellow renovation agent.
The preparation method of Conyza canadensis extract the following steps are included:
(1) configuration extraction liquid: the aqueous solution of configuration ethyl acetate, ethyl alcohol and hydrogen peroxide, wherein the quality percentage of ethyl acetate contains Amount is 8%, and the mass percentage of ethyl alcohol is 7%, H2O2Mass percentage be 2.6%, remaining is water;
(2) fresh Conyza canadensis complete stool is shredded, the Conyza canadensis after chopping is put into seal pot, then the extracting solution is poured into close It is mixed in envelope kettle with Conyza canadensis, the addition weight of extracting solution is 4 times of Conyza canadensis weight;Seal pot is put into vacuum oven and takes out Vacuum degree in vacuum oven is evacuated to 0.1 standard atmospheric pressure by vacuum, and pressure maintaining stands 10h under vacuum conditions;
(3) seal pot is taken out after the completion of pressure maintaining, seals autoclave body, the mixture in seal pot is then heated to 140~160 DEG C extract 30min, extract after the completion of open seal pot, cooled to room temperature, filtering, after being extracted slag and extraction after liquid; After the extraction liquid be concentrated under reduced pressure into extract after liquid product 1/4, obtain the Conyza canadensis extract.
Embodiment 4
A kind of yellow renovation agent, the yellow renovation agent are that effective component is watered acquisition, and the effective component includes that Conyza canadensis mentions Object, praseodymium nitrate, 5-ALA, lauroyl glutamate, potassium lactate and potassium cinnamate are taken, each component is according to parts by weight Are as follows: 100 parts of Conyza canadensis extract, 14 parts of praseodymium nitrate, 14 parts of 5-ALA, 8 parts of lauroyl glutamate, 26 parts of potassium lactate With 3 parts of potassium cinnamate.The effective component and water are according to effective component: water=25g:30 jins is converted synthesis yellow renovation agent.
The preparation method of Conyza canadensis extract the following steps are included:
(1) configuration extraction liquid: the aqueous solution of configuration ethyl acetate, ethyl alcohol and hydrogen peroxide, wherein the quality percentage of ethyl acetate contains Amount is 8%, and the mass percentage of ethyl alcohol is 5%, H2O2Mass percentage be 3.5%, remaining is water;
(2) fresh Conyza canadensis complete stool is shredded, the Conyza canadensis after chopping is put into seal pot, then the extracting solution is poured into close It is mixed in envelope kettle with Conyza canadensis, the addition weight of extracting solution is 4 times of Conyza canadensis weight;Seal pot is put into vacuum oven and takes out Vacuum degree in vacuum oven is evacuated to 0.1 standard atmospheric pressure by vacuum, and pressure maintaining stands 10h under vacuum conditions;
(3) seal pot is taken out after the completion of pressure maintaining, seals autoclave body, the mixture in seal pot is then heated to 140~160 DEG C extract 30min, extract after the completion of open seal pot, cooled to room temperature, filtering, after being extracted slag and extraction after liquid; After the extraction liquid be concentrated under reduced pressure into extract after liquid product 1/4, obtain the Conyza canadensis extract.
Embodiment 5
A kind of yellow renovation agent, the yellow renovation agent are that effective component is watered acquisition, and the effective component includes that Conyza canadensis mentions Object, praseodymium nitrate, 5-ALA, lauroyl glutamate, potassium lactate and potassium cinnamate are taken, each component is according to parts by weight Are as follows: 100 parts of Conyza canadensis extract, 15 parts of praseodymium nitrate, 15 parts of 5-ALA, 8 parts of lauroyl glutamate, 28 parts of potassium lactate With 5 parts of potassium cinnamate.The effective component and water are according to effective component: water=25g:30 jins is converted synthesis yellow renovation agent.
The preparation method of Conyza canadensis extract the following steps are included:
(1) configuration extraction liquid: the aqueous solution of configuration ethyl acetate, ethyl alcohol and hydrogen peroxide, wherein the quality percentage of ethyl acetate contains Amount is 8%, and the mass percentage of ethyl alcohol is 8%, H2O2Mass percentage be 3.6%, remaining is water;
(2) fresh Conyza canadensis complete stool is shredded, the Conyza canadensis after chopping is put into seal pot, then the extracting solution is poured into close It is mixed in envelope kettle with Conyza canadensis, the addition weight of extracting solution is 4 times of Conyza canadensis weight;Seal pot is put into vacuum oven and takes out Vacuum degree in vacuum oven is evacuated to 0.1 standard atmospheric pressure by vacuum, and pressure maintaining stands 10h under vacuum conditions;
(3) seal pot is taken out after the completion of pressure maintaining, seals autoclave body, the mixture in seal pot is then heated to 140~160 DEG C extract 30min, extract after the completion of open seal pot, cooled to room temperature, filtering, after being extracted slag and extraction after liquid; After the extraction liquid be concentrated under reduced pressure into extract after liquid product 1/4, obtain the Conyza canadensis extract.
Comparative example 1
A kind of yellow renovation agent, the yellow renovation agent are that effective component is watered acquisition, and the effective component includes that Stanley is multiple Hefei, praseodymium nitrate, 5-ALA, lauroyl glutamate, potassium lactate and potassium cinnamate, each component is according to parts by weight Are as follows: 100 parts of Stanley compound fertilizer (Water soluble fertilizer 6-18-36), 14 parts of praseodymium nitrate, 14 parts of 5-ALA, lauroyl paddy ammonia 6 parts of acid, 26 parts of potassium lactate and 3 parts of potassium cinnamate.The effective component and water are according to effective component: water=25g:30 jins is converted synthesis Yellow renovation agent.
Comparative example 2
A kind of yellow renovation agent, the yellow renovation agent are that effective component is watered acquisition, and the effective component is Dove sugar alcohol calcium. Effective component and water are according to effective component: water=25g:30 jins is converted synthesis yellow renovation agent.
Embodiment 6
In same orchard, choose yellow after 4 years or more 30 plants of adult mandarin trees (yellow caused by non-yellow twig), be divided into 6 Group, every group 5 plants.Examples 1 to 5 and the resulting yellow renovation agent of comparative example 1~2 are applied on the mandarin tree after yellow, it is real It applies example 1~5 and comparative example 1 and each mandarin tree group corresponds, the same yellow renovation agent of every group of application.Yellow renovation agent is applied With method are as follows:
Yellow renovation agent is used to the citrus that yellow occurs, access times are 4 times, and every minor tick 10 days is opened in fruit tree for the first time Hua Qian, behind several times in Post flowering.The yellow renovation agent is divided into two parts when using every time, a portion to blade into Row sprinkling, another part is for pouring root.Wherein every plant of mandarin tree fountain height is 4 jin every time, and every plant of citrus usage tree root pours 10 jin.That every group of mandarin tree is observed after 3 months turns green situation, and the results are shown in Table 1.
Embodiment 7
In the same orchard for the mandarin tree chosen with embodiment 6,4 years or more the mandarin trees that grow up after 5 plants of yellows are in addition chosen. The resulting yellow renovation agent of embodiment 3 is applied, application times are 4 times, every minor tick 10 days, for the first time before fruit tree blooms, after In Post flowering, only blade is sprayed when application every time several times in face.Wherein every plant of mandarin tree fountain height is 4 jin every time.3 months That observes every group of mandarin tree afterwards turns green situation, and the results are shown in Table 1.
Embodiment 8
In the same orchard for the mandarin tree chosen with embodiment 6,4 years or more the mandarin trees that grow up after 5 plants of yellows are in addition chosen. The resulting yellow renovation agent of embodiment 3 is applied, application times are 4 times, every minor tick 10 days, for the first time before fruit tree blooms, after Root in Post flowering, is only poured when application every time several times in face.Wherein every plant of citrus usage tree root pours 10 jin.It is observed after 3 months every Group mandarin tree turns green situation, and the results are shown in Table 1.
Embodiment 9
In the same orchard for the mandarin tree chosen with embodiment 6,4 years or more citruses of growing up after 10 plants of yellows are in addition chosen Tree.The resulting yellow renovation agent of embodiment 3 is applied, application times are 4 times, every minor tick 10 days, for the first time before fruit tree blooms, Below several times in Post flowering.The yellow renovation agent is divided into two parts when using every time, a portion sprays blade It spills, another part is for pouring root.Part for being sprayed to blade is added with adjuvant, and the adjuvant includes ten Dialkyl dimethyl glycine betaine, dodecyl trimethyl ammonium chloride, magnesium gluconate and Dove sugar alcohol calcium.
Each component is calculated by weight as in adjuvant:
15 parts of dodecyldimethylammonium hydroxide inner salt;
15 parts of dodecyl trimethyl ammonium chloride;
2 parts of magnesium gluconate;
3 parts of Dove sugar alcohol calcium;
Yellow renovation agent for being sprayed to blade is 26 times of the adjuvant quality.
Wherein every plant of mandarin tree fountain height is 4 jin every time, and every plant of citrus usage tree root pours 10 jin.Every group is observed after 3 months Mandarin tree turns green situation, and the results are shown in Table 1.
Table 1
Experimental group Yellow mandarin tree/strain Turn greenery/strain
Embodiment 1 5 3
Embodiment 2 5 3
Embodiment 3 5 4
Embodiment 4 5 3
Embodiment 5 5 3
Comparative example 1 5 1
Comparative example 2 5 0
Embodiment 7 5 1
Embodiment 8 5 2
Embodiment 9 5 5
All mandarin trees in orchard are all normally applied fertilizer: in late Febuary to early March, every plant is applied 10 kilograms of farmyard manure, Stanley 0.5 kilogram every plant of compound fertilizer (potassium sulfate type) 20-5-20 compound fertilizer.Second is that in late May to early June, every plant of Shi Shidan 2 kilograms of sharp nitro fertile (16-6-20).Third is that every plant is applied uncommon 2 kilograms of star fertilizer industry refined organic fertilizer, and Stanley is compound in July 1 kilogram every plant of fertilizer (potassium sulfate type) 20-5-20 compound fertilizer;In August part, every plant is applied Stanley compound fertilizer (potassium sulfate type) 1 kilogram of 20-5-20 compound fertilizer.Fourth is that every plant is applied 10 kilograms of farmyard manure 15 days before fruit picking.
As shown in table 1, the present invention uses homemade yellow renovation agent, to mandarin tree (the non-yellow twig for having occurred and that yellow It is caused) repairing effect is obvious, it is high to turn green rate, hence it is evident that be better than the yellow recovery scenario of prior art sprinkling Dove sugar alcohol calcium.? The adjuvant mixed in yellow renovation agent carries out sprinkling application to Citrus leaf, can further increase repairing for yellow renovation agent Multiple effect.
Technical solution provided by the present invention is described in detail above, for those of ordinary skill in the art, Thought according to an embodiment of the present invention, there will be changes in the specific implementation manner and application range, in conclusion this theory Bright book content should not be construed as limiting the invention.

Claims (9)

1. the administering method that a kind of non-yellow twig causes citrus yellow, which is characterized in that repaired to the citrus that yellow occurs using yellow Multiple agent, access times are 3~5 times, and the yellow renovation agent is divided into two parts when using every time by every minor tick 7~10 days, Middle a part sprays blade, and another part is that effective component is watered acquisition for pouring root, the yellow renovation agent, The effective component includes Conyza canadensis extract, praseodymium nitrate, 5-ALA, lauroyl glutamate, potassium lactate and cortex cinnamomi Sour potassium, the Conyza canadensis extract are obtained by the fresh Conyza canadensis complete stool of extraction with aqueous solution of ethyl acetate, ethyl alcohol and hydrogen peroxide.
2. the administering method that a kind of non-yellow twig according to claim 1 causes citrus yellow, which is characterized in that described small fluffy The preparation method of careless extract the following steps are included:
(1) configuration extraction liquid: the aqueous solution of configuration ethyl acetate, ethyl alcohol and hydrogen peroxide, wherein the quality percentage of ethyl acetate contains Amount is 5%~8%, and the mass percentage of ethyl alcohol is 5%~8%, H2O2Mass percentage be 1.4%~3.6%, remaining is water;
(2) fresh Conyza canadensis complete stool is shredded, the Conyza canadensis after chopping is put into seal pot, then the extracting solution is poured into close Envelope kettle in mix with Conyza canadensis, seal pot is put into vacuum oven and vacuumizes, and under vacuum conditions pressure maintaining standing 10h with On;
(3) seal pot is taken out after the completion of pressure maintaining, seals autoclave body, the mixture in seal pot is then heated to 140~160 DEG C extract, extract after the completion of open seal pot, cooled to room temperature, filtering, after being extracted slag and extraction after liquid;It is described to mention It takes rear liquid to be concentrated under reduced pressure, obtains the Conyza canadensis extract.
3. the administering method that a kind of non-yellow twig according to claim 2 causes citrus yellow, which is characterized in that the step (2) in, the addition weight of the extracting solution is 3~4 times of Conyza canadensis weight, and in step (3), liquid, which is concentrated under reduced pressure into, after extraction is mentioned Take the 1/5~1/4 of rear liquid product.
4. the administering method that a kind of non-yellow twig according to claim 2 causes citrus yellow, which is characterized in that the step (2) in, vacuum degree≤0.2 standard atmospheric pressure that vacuumizes.
5. the administering method that a kind of non-yellow twig according to claim 2 causes citrus yellow, which is characterized in that the step (3) in, the time of 140~160 DEG C of extractions is 30min or more.
6. a kind of described in any item non-yellow twigs cause the administering method of citrus yellow according to claim 1~5, feature exists In each component is calculated by weight as in the effective component: 100 parts of Conyza canadensis extract, 10~15 parts of praseodymium nitrate, 5- amino 10~15 parts of levulic acid, 2~8 parts of lauroyl glutamate, 22~28 parts of potassium lactate and 1~5 part of potassium cinnamate;It is described effectively at Divide and water is according to effective component: water=25~30g:30 jins is converted the synthesis yellow renovation agent.
7. the administering method that a kind of non-yellow twig according to claim 6 causes citrus yellow, which is characterized in that the yellow Added with adjuvant, the adjuvant includes dodecyl dimethyl beet for the part that renovation agent is used to spray blade Alkali, dodecyl trimethyl ammonium chloride, magnesium gluconate and Dove sugar alcohol calcium.
8. the administering method that a kind of non-yellow twig according to claim 7 causes citrus yellow, which is characterized in that the auxiliary Each component is calculated by weight as in agent:
10~20 parts of dodecyldimethylammonium hydroxide inner salt;
10~20 parts of dodecyl trimethyl ammonium chloride;
2~5 parts of magnesium gluconate;
1~3 part of Dove sugar alcohol calcium;
Yellow renovation agent for being sprayed to blade is 20~30 times of the adjuvant quality.
9. the administering method that a kind of non-yellow twig according to claim 1 causes citrus yellow, which is characterized in that the yellow Renovation agent is that effective component is watered acquisition, and the amount being watered is 600~1000 times of effective component weight.
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