CN109100247A - Class coal petrography stone crustal stress K point test method based on Kaiser effect - Google Patents

Class coal petrography stone crustal stress K point test method based on Kaiser effect Download PDF

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CN109100247A
CN109100247A CN201810788963.0A CN201810788963A CN109100247A CN 109100247 A CN109100247 A CN 109100247A CN 201810788963 A CN201810788963 A CN 201810788963A CN 109100247 A CN109100247 A CN 109100247A
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acoustic emission
point
class coal
load
kaiser effect
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CN109100247B (en
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段东
张百胜
赵凯雷
任惠亮
刘文博
康志勤
陈思顺
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Taiyuan University of Technology
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/32Investigating strength properties of solid materials by application of mechanical stress by applying repeated or pulsating forces
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01LMEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L1/00Measuring force or stress, in general
    • G01L1/25Measuring force or stress, in general using wave or particle radiation, e.g. X-rays, microwaves, neutrons
    • G01L1/255Measuring force or stress, in general using wave or particle radiation, e.g. X-rays, microwaves, neutrons using acoustic waves, or acoustic emission
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/38Concrete; Lime; Mortar; Gypsum; Bricks; Ceramics; Glass
    • G01N33/383Concrete or cement
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0001Type of application of the stress
    • G01N2203/0005Repeated or cyclic
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058Kind of property studied
    • G01N2203/006Crack, flaws, fracture or rupture
    • G01N2203/0067Fracture or rupture
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/06Indicating or recording means; Sensing means
    • G01N2203/0658Indicating or recording means; Sensing means using acoustic or ultrasonic detectors

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Abstract

The class coal petrography stone crustal stress K point test method based on Kaiser effect that the invention discloses a kind of replaces class coal test specimen using undisturbed weak concrete test specimen, to reduce influence caused by primary preservation stress.Acoustic emission signal is acquired simultaneously using two kinds of resonant frequency sensors, Kaiser effect point is primarily determined using 2 representational sound emission time domain parameter synthesis, it tests simultaneously according to the distribution characteristics of its dominant frequency to its accuracy, it is finally verified again in terms of multiband energy-distributing feature, establishes the method that 3 kinds of methods mutually prove, improve test accuracy.

Description

Class coal petrography stone crustal stress K point test method based on Kaiser effect
Technical field
The present invention relates to detecting earth stress field more particularly to a kind of class coal petrography stone based on AE Kaiser effect Stress K point test method.
Background technique
Detecting earth stress method has hydraulic fracturing, stress relief method, strain restoring method, Borehole Breakout Data, sound hair at present Penetrate Kaiser effect method etc., wherein AE Kaiser effect method have it is simple, intuitive, be easy to the advantages of largely testing, can Realize the DCO detailed checkout of crustal stress.The key of Kaiser effect measurement crustal stress is the selection of K point, chooses mode original It constantly brings forth new ideas in parameter selection method, while a large amount of research has been carried out to its validity, and achieve certain achievement.
It is not yet clear whether coal stress suffered during preservation can have an impact AE Kaiser effect, so In application AE Kaiser effect test crustal stress, the accuracy of its test can not be judged.Therefore using it is undisturbed (or Power is computable) concrete sample replace coal carry out detecting earth stress research, the accuracy that it is tested can be judged.
Major part achievement mainly destroy to the rock of preservation in the earth's crust complete using single resonant frequency sensor at present The acquisition of process acoustic emission signal carries out mostly using single parameter to be analyzed when K point determines, due to all kinds of resonant frequency sensors The otherness of signal and the otherness of each feature distribution parameter of sound emission are acquired, causes result of study to show diversity, gives The application of AE Kaiser effect test crustal stress brings difficulty.
Summary of the invention
To solve the deficiencies in the prior art support set forth above, the present invention is to provide a kind of based on AE Kaiser effect The class coal petrography stone crustal stress K point test method answered, the technical solution adopted is as follows:
A kind of class coal petrography stone crustal stress K point test method based on AE Kaiser effect, comprising:
Uniaxial compression test is carried out to class coal rock sample, determines the load peaks of uniaxial compression test, it is right according to load peaks Class coal rock sample carries out uniaxial compression circulation by the way of load load, until being loaded onto destruction, and in experimentation It is monitored by acoustic emission system for monitoring, and the acoustic emission signal generated to acoustic emission system for monitoring is acquired;
It analyzes in different cyclic processes, the absolute energy and Ring-down count of the acoustic emission signal of acoustic emission signal acquisition device acquisition AE Kaiser effect character, while to acoustic emission signal acquisition device acquisition signal carry out Fourier transformation, statistics Basic frequency of signal value in different cyclic processes;
Respectively according in the AE Kaiser effect character and different cyclic processes of sound emission absolute energy and Ring-down count Basic frequency of signal value establishes the preliminary foundation for determining K point;
During different CYCLIC LOADINGs, the waveform near K point primarily determined carries out three layers of wavelet packet decomposition, to each frequency band energy Amount accounting is counted, and the situation of change of each frequency band energy accounting during different CYCLIC LOADINGs is analyzed, to energy accounting High frequency range is counted, and is analyzed the distribution characteristics of energy at K point, is determined K point.
Wherein, in the step of carrying out uniaxial compression test to class coal rock sample, the class coal rock sample is using not The concrete sample disturbed replaces being tested.
Wherein, the manufacturing process steps of concrete sample include:
River sand is dried, is sieved using the sieve of 80 mesh, density is measured;
It will uniformly be smeared around die trial with machine oil, cement, the river sand sieved, water then poured into die trial according to the ratio;
Die trial stands one day under normal temperature environment after completing, and demoulding is then numbered;After demoulding, concrete sample is soaked It ducks in drink, is kept the temperature, control water temperature is 20 DEG C, maintenance to 28d.
Wherein, acoustic emission signal acquisition device is R6 α, NANO30 two kind resonant frequency sensor.
Wherein, during the experiment, sound emission monitoring, the sound are carried out to concrete sample by acoustic emission monitoring system Launch monitor system is PCI-II, Disp acoustic emission monitoring system, and the two is connected to concrete sample;Wherein, R6 α resonance frequency Sensor sensing acquires the acoustic emission signal that Disp acoustic emission monitoring system generates, NANO30 resonant frequency sensor inductive pick-up The acoustic emission signal that PCI-II acoustic emission monitoring system generates.
Wherein, during carrying out uniaxial cycling loading experiment to concrete sample, control mode is loaded using load, Cycle-index is 4 times, and the load value of each CYCLIC LOADING is 20%, 40%, 60%, the 80% of concrete sample peak load, load It is all 0.1kN/s with rate of debarkation, until concrete sample is loaded onto destruction.
It is different from the prior art, the class coal petrography stone crustal stress K point provided by the present invention based on AE Kaiser effect Test method replaces class coal test specimen using undisturbed weak concrete test specimen, to reduce caused by primary preservation stress It influences.Acoustic emission signal is acquired simultaneously using two kinds of resonant frequency sensors, when using 2 representational sound emissions Field parameter synthesis primarily determines Kaiser effect point, while testing according to the distribution characteristics of its dominant frequency to its accuracy, most It is verified again in terms of multiband energy-distributing feature afterwards, establishes the side that test accuracy was mutually proved, improved to 3 kinds of methods Method.
Detailed description of the invention
Fig. 1 is a kind of class coal petrography stone crustal stress K point test method based on AE Kaiser effect provided by the invention Flow diagram.
Fig. 2 is a kind of class coal petrography stone crustal stress K point test method based on AE Kaiser effect provided by the invention Accumulative Ring-down count-absolute energy-time of two kinds of resonance playing card sensors acquisition when middle application load is the 40% of peak load Curve.
Fig. 3 is a kind of class coal petrography stone crustal stress K point test method based on AE Kaiser effect provided by the invention Accumulative Ring-down count-absolute energy-time of two kinds of resonance playing card sensors acquisition when middle application load is the 60% of peak load Curve.
Fig. 4 is a kind of class coal petrography stone crustal stress K point test method based on AE Kaiser effect provided by the invention Accumulative Ring-down count-absolute energy-time of two kinds of resonance playing card sensors acquisition when middle application load is the 80% of peak load Curve.
Fig. 5 is a kind of class coal petrography stone crustal stress K point test method based on AE Kaiser effect provided by the invention When middle apply that load is peak load 100% acquisition of two kinds of resonance playing card sensors it is accumulative Ring-down count-absolute energy-when Half interval contour.
Fig. 6 is a kind of class coal petrography stone crustal stress K point test method based on AE Kaiser effect provided by the invention Flow diagram.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
In the description of the present invention, it is to be understood that, term " on ", "lower", "front", "rear", "left", "right", "top", The orientation or positional relationship of the instructions such as "bottom", "inner", "outside" is to be based on the orientation or positional relationship shown in the drawings, merely to just In description the present invention and simplify description, rather than the device or element of indication or suggestion meaning must have a particular orientation, with Specific orientation construction and operation, therefore be not considered as limiting the invention.
Consult Fig. 1 and Fig. 6, Fig. 1 be a kind of class coal petrography stone based on AE Kaiser effect provided by the invention answer The flow diagram of power K point test method, Fig. 6 are a kind of class coal petrography stone based on AE Kaiser effect provided by the invention The logical schematic of crustal stress K point test method.The step of this method includes:
S110: uniaxial compression test is carried out to class coal rock sample, the load peaks of uniaxial compression test are determined, according to load peak Value, to class coal rock sample using uniaxial compression circulation is carried out by the way of load load, up to being loaded onto destruction, and to testing It is monitored in journey by acoustic emission system for monitoring, and the acoustic emission signal generated to acoustic emission system for monitoring is acquired.
S120: analyzing in different cyclic processes, the absolute energy of the acoustic emission signal of acoustic emission signal acquisition device acquisition With the AE Kaiser effect character of Ring-down count, while to acoustic emission signal acquisition device acquisition signal carry out Fourier Transformation, counts the basic frequency of signal value in different cyclic processes.
S130: the AE Kaiser effect character and different circulations according to sound emission absolute energy and Ring-down count respectively Basic frequency of signal value in the process establishes the preliminary foundation for determining K point.
S140: during different CYCLIC LOADINGs, the waveform near K point primarily determined carries out three layers of wavelet packet decomposition, Each frequency band energy accounting is counted, the situation of change of each frequency band energy accounting during different CYCLIC LOADINGs is analyzed, The frequency range high to energy accounting counts, and analyzes the distribution characteristics of energy at K point, determines K point.
Preferably, in the step of carrying out uniaxial compression test to class coal rock sample, the class coal rock sample is to utilize Undisturbed concrete sample replaces being tested.
Preferably, the manufacturing process steps of concrete sample include:
River sand is dried, is sieved using the sieve of 80 mesh, density is measured;
It will uniformly be smeared around die trial with machine oil, cement, the river sand sieved, water then poured into die trial according to the ratio;
Die trial stands one day under normal temperature environment after completing, and demoulding is then numbered;After demoulding, concrete sample is soaked It ducks in drink, is kept the temperature, control water temperature is 20 DEG C, maintenance to 28d.
Preferably, acoustic emission signal acquisition device is R6 α, NANO30 two kind resonant frequency sensor.
Preferably, during the experiment, sound emission monitoring is carried out to concrete sample by acoustic emission monitoring system, it is described Acoustic emission monitoring system is PCI-II, Disp acoustic emission monitoring system, and the two is connected to concrete sample;Wherein, R6 α resonance frequency Rate sensor sensing acquires the acoustic emission signal that Disp acoustic emission monitoring system generates, and the induction of NANO30 resonant frequency sensor is adopted Collect the acoustic emission signal that PCI-II acoustic emission monitoring system generates.
Preferably, during carrying out uniaxial cycling loading experiment to concrete sample, control mode is added using load It carries, cycle-index is 4 times, and the load value of each CYCLIC LOADING is 20%, 40%, 60%, the 80% of concrete sample peak load, is added It carries and rate of debarkation is all 0.1kN/s, until concrete sample is loaded onto destruction.
It is 1:4, mixed having a size of 50mm × 50mm × 100mm specifically, prepares dust and sand ratio according to preparation step above-mentioned Solidifying soil test specimen.Suggestion according to International Society of Rock Mechanics to laboratory sample size, the injustice in prepared test specimen two ends face Row degree is less than 0.05mm, is polished using SPM-250 double plate wafer lapping machine preparation test specimen two ends, is required with guarantee test.It is logical Excess pressure machine carries out rock mechanics experiment to it, measures its peak load, and test quantity is no less than 5, and peak value takes its average value, Its load peaks is 36kN after carrying out uniaxial compression test to same batch test specimen.
Concrete sample is subjected to uniaxial cycling load, control mode is loaded using load, and cycle-index is 4 times, finally It is loaded onto destruction, the peak load of each CYCLIC LOADING measures 20%, 40%, 60%, the 80% of test specimen peak load before being, adds and unload Carrying rate is all 0.1kN/s.From entire loaded is loaded into for the first time, it is always on PCI-II, Disp acoustic emission monitor(ing) system System destructive process is monitored, and in test specimen destructive process using R6 α, NANO30 two kind sensor to acoustic emission signal into Row acquisition.PCI-II acoustic emission system is connect with NANO30 resonant frequency sensor, Disp acoustic emission system and R6 α resonance frequency The connection of rate sensor.Every kind of resonant frequency sensor each 2, amount to 4.
Under 40% level conditions of peak load (second of CYCLIC LOADING), first increase according to sound emission absolute energy, then Enter again like quiet period, while the phenomenon that Ring-down count is slowly increased can be used as K point distinguishing rule, error is less than 10%, and sound It is Kaiser point that transmitting absolute energy peak point and accumulative Ring-down count curve increase some undecidables suddenly.As shown in Figure 2.NANO30 Have certain interference signal before signal collected K point, R6 α and NANO30 be combined together can effective exclusive PCR, improve quasi- True property.
Under 60% level conditions of peak load (third time CYCLIC LOADING), R6 α and NANO30 resonant frequency sensor is adopted It is significantly different to collect signal distributions feature, then can accurately judge K point in conjunction with the general character of the two.Absolute energy can be substantially increased Add and then reduce again, while Ring-down count curve increases criterion of the phenomenon as K point.As shown in Figure 3.
Under 80% level conditions of peak load (the 4th CYCLIC LOADING), it can choose absolute energy and occur increasing to peak suddenly It is strongly reduced again after value, the feature that Ring-down count increases suddenly is as the foundation for differentiating K point, and error is less than 10%.As shown in Figure 4.R6 The signal collected Ring-down count of α, absolute energy and NANO30 signal collected have different in distribution characteristics, and R6 α is adopted It is more to collect the signal absolute energy high level point frequency of occurrences.Compared with third time recycles, to more one both in the rule of K point differentiation It causes.
Under 100% level conditions of peak load (final load), is rised appreciably with absolute energy and reach first peak value Point, ring curve start to increase phenomenon to be that criterion can determine that as Kaiser point, and error is sentenced less than 10%, but with R6 α acquisition signal There is a certain error for other K point, therefore two class sensors is combined the accuracy and reliability that can be improved the differentiation of K point. As shown in Figure 5.
In entire loading procedure R6 α resonant frequency sensor sound emission dominant frequency collected be mainly distributed on 35-40kHz, The two sections 100kHz or so, NANO30 resonant frequency sensor signal collected are concentrated mainly on the section 225-250kHz It is interior, while caning be found that high frequency sensors have equally collected more low dominant frequency signal at load initial stage and before destroying.It makes a general survey of Entire CYCLIC LOADING process, the main distributed area of acoustic emission signal are included in these three sections.Add in first four times circulations Load stage, acoustic emission signal dominant frequency are gradually developed from low frequency to high frequency, and in final load, basic frequency of signal is all big in high and low frequency Amount occurs.Simultaneously it can be found that the point before sound emission dominant frequency can largely being occurred is determined as K point, error is less than 10%, with reason It coincide substantially by K point.
It is above-mentioned K point is differentiated on the basis of, for analyze each CYCLIC LOADING stage K point signal frequency component difference with Waveform near each CYCLIC LOADING stage K point is carried out WAVELET PACKET DECOMPOSITION, and carried out to each frequency band energy accounting by the connection of K point Statistics analyzes the changing rule of each frequency band energy accounting under different loads level, judges K point according to its rule.
Each CYCLIC LOADING stage is consistent for the determination method of K point, i.e., with successive bands at K point energy accounting one high one Low feature is as the foundation for differentiating K point.For being loaded onto failure stage, for R6 α resonant frequency sensor, energy accounting Uprushing with the frequency range of rapid drawdown is 0 ~ 62.5kHz and 62.5 ~ 125kHz;For NANO30 resonant frequency sensor, energy accounting is prominent Increase the frequency range 187.5 ~ 250kHz and 250 ~ 312.5kHz with rapid drawdown.
It is different from the prior art, the class coal petrography stone crustal stress K point provided by the present invention based on AE Kaiser effect Test method replaces class coal test specimen using undisturbed weak concrete test specimen, to reduce caused by primary preservation stress It influences.Acoustic emission signal is acquired simultaneously using two kinds of resonant frequency sensors, when using 2 representational sound emissions Field parameter synthesis primarily determines Kaiser effect point, while testing according to the distribution characteristics of its dominant frequency to its accuracy, most It is verified again in terms of multiband energy-distributing feature afterwards, establishes the side that test accuracy was mutually proved, improved to 3 kinds of methods Method.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (6)

1. a kind of class coal petrography stone crustal stress K point test method based on Kaiser effect characterized by comprising
Uniaxial compression test is carried out to class coal rock sample, determines the load peaks of uniaxial compression test, it is right according to load peaks Class coal rock sample carries out uniaxial compression circulation by the way of load load, until being loaded onto destruction, and in experimentation It is monitored by acoustic emission system for monitoring, and the acoustic emission signal generated to acoustic emission system for monitoring is acquired;
It analyzes in different cyclic processes, the absolute energy and Ring-down count of the acoustic emission signal of acoustic emission signal acquisition device acquisition AE Kaiser effect character, while to acoustic emission signal acquisition device acquisition signal carry out Fourier transformation, statistics Basic frequency of signal value in different cyclic processes;
Respectively according in the AE Kaiser effect character and different cyclic processes of sound emission absolute energy and Ring-down count Basic frequency of signal value establishes the preliminary foundation for determining K point;
During different CYCLIC LOADINGs, the waveform near K point primarily determined carries out three layers of wavelet packet decomposition, to each frequency band energy Amount accounting is counted, and the situation of change of each frequency band energy accounting during different CYCLIC LOADINGs is analyzed, to energy accounting High frequency range is counted, and is analyzed the distribution characteristics of energy at K point, is determined K point.
2. the class coal petrography stone crustal stress K point test method according to claim 1 based on Kaiser effect, feature exist In in the step of carrying out uniaxial compression test to class coal rock sample, the class coal rock sample is using undisturbed mixed Solidifying soil test specimen replaces being tested.
3. the class coal petrography stone crustal stress K point test method according to claim 2 based on Kaiser effect, feature exist In the manufacturing process steps of concrete sample include:
River sand is dried, is sieved using the sieve of 80 mesh, density is measured;
It will uniformly be smeared around die trial with machine oil, cement, the river sand sieved, water then poured into die trial according to the ratio;
Die trial stands one day under normal temperature environment after completing, and demoulding is then numbered;After demoulding, concrete sample is soaked It ducks in drink, is kept the temperature, control water temperature is 20 DEG C, maintenance to 28d.
4. the class coal petrography stone crustal stress K point test method according to claim 1 based on Kaiser effect, feature exist In acoustic emission signal acquisition device is R6 α, NANO30 two kind resonant frequency sensor.
5. the class coal petrography stone crustal stress K point test method according to claim 4 based on Kaiser effect, feature exist During the experiment, by acoustic emission monitoring system to concrete sample progress sound emission monitoring, the acoustic emission monitor(ing) system System is PCI-II, Disp acoustic emission monitoring system, and the two is connected to concrete sample;Wherein, R6 α resonant frequency sensor incudes Acquire the acoustic emission signal that Disp acoustic emission monitoring system generates, NANO30 resonant frequency sensor inductive pick-up PCI-II sound hair Penetrate the acoustic emission signal of monitoring system generation.
6. the class coal petrography stone crustal stress K point test method according to claim 1 based on Kaiser effect, feature exist During carrying out uniaxial cycling loading experiment to concrete sample, control mode is loaded using load, and cycle-index is 4 times, the load value of each CYCLIC LOADING is 20%, 40%, 60%, the 80% of concrete sample peak load, load and rate of debarkation It is all 0.1kN/s, until concrete sample is loaded onto destruction.
CN201810788963.0A 2018-07-18 2018-07-18 Coal-like rock ground stress K point testing method based on Kaiser effect Active CN109100247B (en)

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