CN109097188A - A kind of preparation method of shortening ziran oil - Google Patents
A kind of preparation method of shortening ziran oil Download PDFInfo
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- CN109097188A CN109097188A CN201811056402.8A CN201811056402A CN109097188A CN 109097188 A CN109097188 A CN 109097188A CN 201811056402 A CN201811056402 A CN 201811056402A CN 109097188 A CN109097188 A CN 109097188A
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- Prior art keywords
- extraction
- shortening
- preparation
- parts
- ziran oil
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a kind of preparation method of shortening ziran oil, comprising the following steps: (1) taking parts by weight is 100 parts of cumin, the water proof boiling 30-50min at 100 DEG C；(2) into the product of step (1), it is added Celery Juice 10-20 parts, 0.5-1.5h is heated at 80-90 DEG C, is then ultrasonically treated, is washed with water 3-5 times, is dried at 100-105 DEG C after filtered filtration residue；(3) by the product of step (2) at 150-160 DEG C frying 8-14min, after natural cooling, crush；(4) it is extracted using supercritical carbon dioxide equipment, carries out 4 extractions respectively.The preparation method of shortening ziran oil provided by the invention, extraction efficiency is high, can reach 38% or so, and the ziran oil prepared is with rich flavor, green non-pollution, and lasting is lasting.
Description
Technical field
The invention belongs to food technology fields, and in particular to a kind of preparation method of shortening ziran oil.
Background technique
Cumin belongs to umbrella shape herbaceous plant also known as cumin, wild fennel and fennel of resting in peace etc..Cumin seed can be used as food
Flavouring use, have the function of the ability of certain anti-lipid peroxidation and protection deoxyribose.
Traditional cumin processing method is that cumin is ground into powder, is prepared into seasoning, still, is processed into powder seasoning
The flavor substance of cumin is easy to scatter and disappear after material, and inferior quality reduces the utilization rate of cumin.So in order to improve product
Class and flavor, it is existing to extract the flavor substance of cumin there are many producer, it is prepared into cumin essential oil, cumin can be made in this way
Flavor save for a long time, utilization rate is high.
Currently, the extracting method of common cumin essential oil has organic solvent extraction, steam distillation, microwave extraction method, surpasses
Critical carbon dioxide extraction.But extraction effect is limited, recovery rate is low, and the utilization rate of cumin receives limitation.
Summary of the invention
In view of the drawbacks of the prior art, the present invention provides a kind of preparation method of shortening ziran oil, and recovery rate is high.
A kind of preparation method of shortening ziran oil, comprising the following steps:
(1) taking parts by weight is 100 parts of cumin, the water proof boiling 30-50min at 100 DEG C；
(2) into the product of step (1), it is added Celery Juice 10-20 parts, 0.5-1.5h is heated at 80-90 DEG C, then at ultrasound
Reason, is washed with water 3-5 times, dries at 100-105 DEG C after filtered filtration residue；
(3) by the product of step (2) at 150-160 DEG C frying 8-14min, after natural cooling, crush；
(4) it is extracted using supercritical carbon dioxide equipment, carries out single extraction, specifically: 28-35 DEG C of extraction temperature, extraction pressure
Power 10-15MPa, carbon dioxide flow 20-30L/h, extraction time 8-15min；
(5) it unloads and is depressed into atmospheric pressure, carry out reextraction, specifically: 35-50 DEG C of extraction temperature, extracting pressure 25-35MPa, dioxy
Change carbon flow is 20-30L/h, extraction time 15-20min；
(6) it unloads and is depressed into atmospheric pressure, extracted three times, specifically: 55-65 DEG C of extraction temperature, extracting pressure 45-55MPa, dioxy
Change carbon flow is 40-50L/h, extraction time 25-35min；
(7) it unloads and is depressed into atmospheric pressure, carry out four extractions, specifically: 70-75 DEG C of extraction temperature, extracting pressure 65MPa, titanium dioxide
Carbon flow is 50L/h, extraction time 5-10min.
Preferably, Celery Juice described in step (2) is prepared by the following method to obtain: celery being cleaned up, is gone
Except leaf, the water mixing of stripping and slicing and 30 times of quality is beaten, and filtering takes filtrate.
Preferably, the condition being ultrasonically treated in step (2) are as follows: supersonic frequency 45KHz, ultrasonic input power are 300W,
Ultrasonic time is 20min-40min.
Preferably, it is 3-5% that moisture content is dried in step (2).
Preferably, it crushes and sieves with 100 mesh sieve in step (3).
The present invention prepares ziran oil, and cumin passes through frying, can directly season use, without heating.
Advantages of the present invention:
The preparation method of shortening ziran oil provided by the invention, extraction efficiency is high, can reach 38% or so, and the cumin prepared
Oily with rich flavor, green non-pollution, lasting are lasting.
Specific embodiment
The Celery Juice used in the embodiment of the present invention is prepared by the following method to obtain: celery being cleaned up, is gone
Except leaf, the water mixing of stripping and slicing and 30 times of quality is beaten, and filtering takes filtrate.
Embodiment 1
A kind of preparation method of shortening ziran oil, comprising the following steps:
(1) taking parts by weight is 100 parts of cumin, the water proof boiling 30min at 100 DEG C；
(2) into the product of step (1), 10 parts of Celery Juice is added, 0.5h is heated at 80 DEG C, is then in supersonic frequency
45KHz, ultrasonic input power are ultrasonically treated 20minmin under conditions of being 300W, are then washed with water 3 times, after filtered filtration residue
It is 3% that moisture content is dried at 100 DEG C；
(3) by the product of step (2) at 150 DEG C frying 14min, after natural cooling, crushing is sieved with 100 mesh sieve；
(4) it is extracted using supercritical carbon dioxide equipment, carries out single extraction, specifically: 28 DEG C of extraction temperature, extracting pressure
10MPa, carbon dioxide flow 20L/h, extraction time 8min；
(5) it unloads and is depressed into atmospheric pressure, carry out reextraction, specifically: 35 DEG C of extraction temperature, extracting pressure 35MPa, carbon dioxide stream
Amount is 30L/h, extraction time 15min；
(6) it unloads and is depressed into atmospheric pressure, extracted three times, specifically: 55 DEG C of extraction temperature, extracting pressure 45MPa, carbon dioxide stream
Amount is 40L/h, extraction time 25min；
(7) it unloads and is depressed into atmospheric pressure, carry out four extractions, specifically: 70 DEG C of extraction temperature, extracting pressure 65MPa, carbon dioxide stream
Amount is 50L/h, extraction time 5min.
Finally obtain the ziran oil of 36.4 parts by weight, recovery rate 36.4%.
Embodiment 2
A kind of preparation method of shortening ziran oil, comprising the following steps:
(1) taking parts by weight is 100 parts of cumin, the water proof boiling 50min at 100 DEG C；
(2) into the product of step (1), 20 parts of Celery Juice is added, 1.5h is heated at 90 DEG C, is then in supersonic frequency
45KHz, ultrasonic input power are ultrasonically treated 40min under conditions of being 300W, are then washed with water 5 times, after filtered filtration residue
It is 5% that moisture content is dried at 105 DEG C；
(3) by the product of step (2) at 160 DEG C frying 8min, after natural cooling, crushing is sieved with 100 mesh sieve；
(4) it is extracted using supercritical carbon dioxide equipment, carries out single extraction, specifically: 35 DEG C of extraction temperature, extracting pressure
15MPa, carbon dioxide flow 30L/h, extraction time 15min；
(5) it unloads and is depressed into atmospheric pressure, carry out reextraction, specifically: 50 DEG C of extraction temperature, extracting pressure 25MPa, carbon dioxide stream
Amount is 20L/h, extraction time 20min；
(6) it unloads and is depressed into atmospheric pressure, extracted three times, specifically: 65 DEG C of extraction temperature, extracting pressure 55MPa, carbon dioxide stream
Amount is 50L/h, extraction time 35min；
(7) it unloads and is depressed into atmospheric pressure, carry out four extractions, specifically: 75 DEG C of extraction temperature, extracting pressure 65MPa, carbon dioxide stream
Amount is 50L/h, extraction time 10min.
Finally obtain the ziran oil of 34.8 parts by weight, recovery rate 34.8%.
Embodiment 3
A kind of preparation method of shortening ziran oil, comprising the following steps:
(1) taking parts by weight is 100 parts of cumin, the water proof boiling 40min at 100 DEG C；
(2) into the product of step (1), be added 15 parts of Celery Juice, 1h is heated at 85 DEG C, then supersonic frequency be 45KHz,
Ultrasonic input power is ultrasonically treated 30min under conditions of being 300W, is then washed with water 5 times, after filtered filtration residue at 105 DEG C
Being dried to moisture content is 4%；
(3) by the product of step (2) at 155 DEG C frying 10min, after natural cooling, crushing is sieved with 100 mesh sieve；
(4) it is extracted using supercritical carbon dioxide equipment, carries out single extraction, specifically: 30 DEG C of extraction temperature, extracting pressure
12MPa, carbon dioxide flow 25L/h, extraction time 10min；
(5) it unloads and is depressed into atmospheric pressure, carry out reextraction, specifically: 40 DEG C of extraction temperature, extracting pressure 30MPa, carbon dioxide stream
Amount is 25L/h, extraction time 20min；
(6) it unloads and is depressed into atmospheric pressure, extracted three times, specifically: 60 DEG C of extraction temperature, extracting pressure 50MPa, carbon dioxide stream
Amount is 45L/h, extraction time 30min；
(7) it unloads and is depressed into atmospheric pressure, carry out four extractions, specifically: 75 DEG C of extraction temperature, extracting pressure 65MPa, carbon dioxide stream
Amount is 50L/h, extraction time 8min.
Finally obtain the ziran oil of 39.1 parts by weight, recovery rate 39.1%.
Comparative example
The cumin for taking parts by weight 100, the frying 14min at 150 DEG C, after natural cooling, crushing is sieved with 100 mesh sieve, and is then implementing
It is extracted under the supercritical carbon dioxide extraction conditions of example 3, finally obtains 9.4 parts by weight of ziran oil, recovery rate 9.4%.
Claims (5)
1. a kind of preparation method of shortening ziran oil, comprising the following steps:
(1) taking parts by weight is 100 parts of cumin, the water proof boiling 30-50min at 100 DEG C；
(2) into the product of step (1), it is added Celery Juice 10-20 parts, 0.5-1.5h is heated at 80-90 DEG C, then at ultrasound
Reason, is washed with water 3-5 times, dries at 100-105 DEG C after filtered filtration residue；
(3) by the product of step (2) at 150-160 DEG C frying 8-14min, after natural cooling, crush；
(4) it is extracted using supercritical carbon dioxide equipment, carries out single extraction, specifically: 28-35 DEG C of extraction temperature, extraction pressure
Power 10-15MPa, carbon dioxide flow 20-30L/h, extraction time 8-15min；
(5) it unloads and is depressed into atmospheric pressure, carry out reextraction, specifically: 35-50 DEG C of extraction temperature, extracting pressure 25-35MPa, dioxy
Change carbon flow is 20-30L/h, extraction time 15-20min；
(6) it unloads and is depressed into atmospheric pressure, extracted three times, specifically: 55-65 DEG C of extraction temperature, extracting pressure 45-55MPa, dioxy
Change carbon flow is 40-50L/h, extraction time 25-35min；
(7) it unloads and is depressed into atmospheric pressure, carry out four extractions, specifically: 70-75 DEG C of extraction temperature, extracting pressure 65MPa, titanium dioxide
Carbon flow is 50L/h, extraction time 5-10min.
2. the preparation method of shortening ziran oil according to claim 1, it is characterised in that: Celery Juice described in step (2) is
It being prepared by the following method: celery is cleaned up, remove leaf, the water mixing of stripping and slicing and 30 times of quality is beaten,
Filtering, takes filtrate.
3. the preparation method of shortening ziran oil according to claim 1, it is characterised in that: the item being ultrasonically treated in step (2)
Part are as follows: supersonic frequency 45KHz, ultrasonic input power are 300W, ultrasonic time 20min-40min.
4. the preparation method of shortening ziran oil according to claim 1, it is characterised in that: be dried to moisture in step (2) and contain
Amount is 3-5%.
5. the preparation method of shortening ziran oil according to claim 1, it is characterised in that: step crushed 100 mesh in (3)
Sieve.
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| CN201811056402.8A CN109097188A (en) | 2018-09-11 | 2018-09-11 | A kind of preparation method of shortening ziran oil |
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| CN201811056402.8A CN109097188A (en) | 2018-09-11 | 2018-09-11 | A kind of preparation method of shortening ziran oil |
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| CN109097188A true CN109097188A (en) | 2018-12-28 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102768252A (en) * | 2012-08-14 | 2012-11-07 | 天津春发生物科技集团有限公司 | Method for analyzing gas chromatograph / mass spectrometer (GC/MS) fingerprint spectrum of cumin essential oil components |
| CN103555426A (en) * | 2013-10-11 | 2014-02-05 | 山东天博食品配料有限公司 | Preparation method for cumin essential oil with cooked flavor |
| CN104982556A (en) * | 2015-06-30 | 2015-10-21 | 南阳汇萃植物制品有限公司 | Oil with cumin flavor, and preparation method for oil |
| CN106072373A (en) * | 2016-06-28 | 2016-11-09 | 吉林福瑞德食品有限公司 | Fructus Cumini Cymini soluble fine and preparation method thereof and its application in soybean processing histone product |
| CN107974351A (en) * | 2017-12-29 | 2018-05-01 | 丽华（广州）香精香料股份有限公司 | A kind of method of ultrasonic wave auxiliary supercritical carbon dioxide extracting vanilla beans essential oil |
-
2018
- 2018-09-11 CN CN201811056402.8A patent/CN109097188A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102768252A (en) * | 2012-08-14 | 2012-11-07 | 天津春发生物科技集团有限公司 | Method for analyzing gas chromatograph / mass spectrometer (GC/MS) fingerprint spectrum of cumin essential oil components |
| CN103555426A (en) * | 2013-10-11 | 2014-02-05 | 山东天博食品配料有限公司 | Preparation method for cumin essential oil with cooked flavor |
| CN104982556A (en) * | 2015-06-30 | 2015-10-21 | 南阳汇萃植物制品有限公司 | Oil with cumin flavor, and preparation method for oil |
| CN106072373A (en) * | 2016-06-28 | 2016-11-09 | 吉林福瑞德食品有限公司 | Fructus Cumini Cymini soluble fine and preparation method thereof and its application in soybean processing histone product |
| CN107974351A (en) * | 2017-12-29 | 2018-05-01 | 丽华（广州）香精香料股份有限公司 | A kind of method of ultrasonic wave auxiliary supercritical carbon dioxide extracting vanilla beans essential oil |
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Application publication date: 20181228 |
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