CN109077949A - A kind of facial mask and preparation method thereof without preservative - Google Patents
A kind of facial mask and preparation method thereof without preservative Download PDFInfo
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- CN109077949A CN109077949A CN201811162832.8A CN201811162832A CN109077949A CN 109077949 A CN109077949 A CN 109077949A CN 201811162832 A CN201811162832 A CN 201811162832A CN 109077949 A CN109077949 A CN 109077949A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The invention belongs to the technical fields of beauty product, disclose a kind of facial mask and preparation method thereof without preservative, wherein, the facial mask without preservative, percentages by weight, include: 10%~30% glycerol, 15%~30% butanediol, 0.2%~0.5% Sodium Hyaluronate, 0.1%~0.6% dipotassium glycyrrhizinate, 0.5%~3% erythrite, 0.1%~1% parahydroxyacet-ophenone, 0.1%~1% 1,2- hexylene glycol, 0.3%~5% oligopeptides -1,1%~5% glycerin polyether -26, remaining is water.The present invention utilizes the parahydroxyacet-ophenone and described 1,2- the hexylene glycol inhibition to fungi and bacterium and inhibitory or killing effect respectively, after being dissolved in the butanediol and the glycerol, can in facial mask fungi and bacterium rise good inhibiting effect, instead of the preservative in traditional facial mask, anti-corrosion effect can be also reached in the case where not adding preservative, can be guaranteed the quality to facial mask, the problem of addition preservative is done harm to huamn body is avoided, is improved the safety of use.
Description
Technical field
The invention belongs to the technical fields of beauty product, and in particular to a kind of without the facial mask of preservative and its preparation side
Method.
Background technique
With the improvement of living standards, people increasingly pay attention to the nursing to oneself face, the face for being intended to oneself is white
Fair-skinned smooth, so the use of facial mask is also more and more, traditional facial mask is due to wherein containing a large amount of moisture and drug, so face
Preservative ingredient must be added in film to guarantee that facial mask undergoes no deterioration, it is well known that preservative be to human body it is harmful, be added to
The facial mask of preservative after people's use, is likely to result in following harm, harm one: may cause cancer, because in facial mask
The preservative being often used is methyl hydroxybenzoate, the molecular biologist discovery of Britain, methyl hydroxybenzoate quilt in the tumour of a large amount of breast cancers
It finds (containing 20 nanograms in average 1 gram of tissue), shows a kind of characteristic of estrogen (hormone for participating in the development of breast cancer method), institute
Thought with Britain applied toxicology magazinist Philips, hydroxyl this formic acid esters in facial mask may result in women and suffer from breast cancer
Probability increases；Harm two: preservative can accelerate skin aging, and Beijing Technology and Business University cosmetics expert Wang Changtao is indicated: " a side
Face, preservative, so can accumulate on the skin of human body, when running up to a certain amount, can not will be accelerated by body metabolism
The aging of skin ", on the other hand, preservative can also accelerate pigementation, keep skin more and more obscure, it is described regardless of businessman how
It flatters, the facial mask containing preservative all can cause skin obscure after being used for a long time.Harm three: skin allergy and skin can be caused
Inflammation, First Hospital of Tsinghua University skin head of the department Wang Xin are indicated: preservative can cause skin abnormality hyperplasia, canceration, in day
It is relevant under the irradiation of light that chemical change occurs at branch, it makes one to generate photaesthesia, rubefaction, blackening and pain, causes people
There is symptom that is red, itching, or causes the burn of skin in allergy.
Summary of the invention
In order to solve the problems, such as that preservative present in existing facial mask can cause various injuries, the purpose of the present invention to human body
It is to provide one kind without preservative, uses the harmless facial mask without preservative.
The technical scheme adopted by the invention is as follows:
A kind of facial mask without preservative, percentages by weight, comprising: 10%~30% glycerol, 15%~
30% butanediol, 0.2%~0.5% Sodium Hyaluronate, 0.1%~0.6% dipotassium glycyrrhizinate, 0.5%~3% it is red
Moss alcohol, 0.1%~1% parahydroxyacet-ophenone, 0.1%~1% 1,2- hexylene glycol, 0.3%~5% oligopeptides -1,1%~
5% glycerin polyether -26, remaining is water.
Optimization, the facial mask without preservative include 10%~25% glycerol, 20%~25% butanediol,
0.25%~0.4% Sodium Hyaluronate, 0.2%~0.5% dipotassium glycyrrhizinate, 1%~3% erythrite, 0.2%~
0.8% parahydroxyacet-ophenone, 0.2%~0.8% 1,2- hexylene glycol, 0.5%~4% oligopeptides -1,2%~4% it is sweet
Oily polyethers -26, remaining is water.
It advanced optimizes, the facial mask without preservative includes 10%~25% glycerol, 20%~25% fourth
Glycol, 0.25%~0.4% Sodium Hyaluronate, 0.2%~0.5% dipotassium glycyrrhizinate, 1%~3% erythrite,
0.5%~0.8% parahydroxyacet-ophenone, 0.5%~0.8% 1,2- hexylene glycol, 0.5%~4% oligopeptides -1,2%~
4% glycerin polyether -26, remaining is water.
Specifically, the facial mask without preservative include 10%~25% glycerol, 20%~25% butanediol,
0.25%~0.4% Sodium Hyaluronate, 0.2%~0.5% dipotassium glycyrrhizinate, 1%~3% erythrite, 0.6%~
0.8% parahydroxyacet-ophenone, 0.6%~0.8% 1,2- hexylene glycol, 0.5%~4% oligopeptides -1,2%~4% it is sweet
Oily polyethers -26, remaining is water.
It is optimal, the facial mask without preservative include 5% glycerol, 17.5% butanediol, 0.3% hyalomitome
Sour sodium, 0.5% dipotassium glycyrrhizinate, 2% erythrite, 0.65% parahydroxyacet-ophenone, 0.6% 1,2- hexylene glycol,
2.3% oligopeptides -1,3% glycerin polyether -26, remaining is water.
The present invention also provides a kind of preparation methods of facial mask without preservative, comprising the following steps:
S101. suitable glycerol, butanediol, Sodium Hyaluronate, erythrite and water are put into emulsion pot, is then stirred
Heating is mixed and stirred, after heating, at least 30 minutes is kept the temperature, obtains mixture A；
S102. cooling is stirred to the mixture A, after cooling, adds the mixture B prepared, stirred
Uniformly, mixture C is obtained, and at least 10 minutes are kept the temperature to the mixture C, the mixture B is by suitable para hydroxybenzene
Ethyl ketone and 1,2 hexylene glycols obtain after being dissolved by heating；
S103. cool down to the mixture C, after cooling, add suitable oligopeptides -1, and stir at least 5
Minute, obtain mixture D；
S104. suitable glycerin polyether -26 is added in the mixture D, and stirred at least 10 minutes, after stirring
Obtain the facial mask for being free of preservative as claimed in any one of claims 1 to 5, wherein.
Optimization, the holding temperature in the step S101 is between 90 DEG C~95 DEG C.
Optimization, in the step S102, the mixture A is cooled between 58 DEG C~62 DEG C.
Optimization, in the step S102, the temperature of the parahydroxyacet-ophenone and 1,2 hexylene glycol heating for dissolving
Between 58 DEG C~62 DEG C.
Optimization, in the step S104, the mixture C is cooled between 43 DEG C~47 DEG C.
The invention has the benefit that
The present invention is a kind of facial mask without preservative, and the present invention makees the inhibition of fungi with the parahydroxyacet-ophenone
With with described 1,2 hexylene glycols make the parahydroxyacet-ophenone and 1, the 2- hexylene glycol cooperate the inhibiting effect of bacterium,
Achieving the effect that inhibit fungi and bacterium in facial mask, the glycerol and the butanediol can play auxiliary fungistatic effect to facial mask,
By above-mentioned design, the preservative in traditional facial mask can be replaced, makes the present invention without preservative, it when in use will not be to human body
It damages, greatly improves the safety used.Specific experiment data are referring to embodiment.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this
Some embodiments of invention for those of ordinary skill in the art without creative efforts, can be with
It obtains other drawings based on these drawings.
Fig. 1 is the specific steps flow diagram of the preparation method of the facial mask provided by the invention without preservative.
Specific embodiment
The present invention is further elaborated combined with specific embodiments below.It should be noted that for these implementations
The explanation of example mode is used to help understand the present invention, but and does not constitute a limitation of the invention.
Term "and/or" in text, only a kind of incidence relation for describing affiliated partner, indicates that there may be three kinds of passes
System, for example, A and/or B, can indicate: individualism A, individualism B exist simultaneously tri- kinds of situations of A and B, the terms
"/and " it is to describe another affiliated partner relationship, indicate may exist two kinds of relationships, for example, A/ and B, can indicate: individually depositing
In A, two kinds of situations of individualism A and B, in addition, character "/" herein, typicallying represent forward-backward correlation object is a kind of "or" pass
System.
Embodiment one
The facial mask of preservative, percentages by weight are free of provided by the present embodiment, comprising: 10%~30% it is sweet
Oil, 15%~30% butanediol, 0.2%~0.5% Sodium Hyaluronate, 0.1%~0.6% dipotassium glycyrrhizinate, 0.5%
~3% erythrite, 0.1%~1% parahydroxyacet-ophenone, 0.1%~1% 1,2- hexylene glycol, 0.3%~5% widow
The glycerin polyether -26 of peptide -1,1%~5%, remaining is water.
In the present embodiment, the glycerol, the butanediol, the Sodium Hyaluronate, the erythrite and the glycerol
Polyethers -26 is used as moisturizer, can play the role of moisturizing water lock, prevention chapped skin to human skin, the glycerol can also
As lytic agent, it can promote to be mutually dissolved between each component, the butanediol, the dipotassium glycyrrhizinate can be neutralized and be reduced
Harmful substance between each composition, reduces the adverse effect to human body, it also has extensive compatibility, can be with others activity
Agent shares, and can accelerate skin to the absorption of each component in facial mask, increase the beneficial effect of facial mask, the parahydroxyacet-ophenone knot
Contain hydroxyl group in structure, there can be good inhibitory effect to fungi, it also has inoxidizability and anti-irritation etc. multiple
Effect, the parahydroxyacet-ophenone have excellent stability, influenced by temperature and pH value it is small, can it is described be free of preservative
Facial mask in be stabilized, described 1,2 hexylene glycols have good inhibitory effect, the parahydroxyacet-ophenone and described to bacterium
1,2 hexylene glycol synergistic effect is able to suppress and presses down the fungi and bacterium that kill in facial mask, and the glycerol and the butanediol can rise
Auxiliary fungistatic effect instead of the effect of the preservative in traditional facial mask, can be avoided in traditional facial mask and contain by above-mentioned design
The problem of some preservatives are done harm to huamn body can allow people safe to use, greatly improve the safety that facial mask uses
Property.The oligopeptides -1 can quickly repair damaged skin, moisturize the skin, and enhance skin elasticity, also have whitening spot-removing, reduce skin
The content of melanin and coloured corpuscle in skin cell accelerates melanocyte and is metabolized the effect to fall off, greatly improves facial mask
Beauty repairing effect.
Embodiment two
Facial mask and embodiment one provided by the present embodiment without preservative the difference is that: it is described to be free of anti-corrosion
The range of the content of each component is reduced relative to embodiment one in the facial mask of agent.
The facial mask that preservative is free of provided by the present embodiment, including 10%~25% glycerol, 20%~25% fourth
Glycol, 0.25%~0.4% Sodium Hyaluronate, 0.2%~0.5% dipotassium glycyrrhizinate, 1%~3% erythrite,
0.2%~0.8% parahydroxyacet-ophenone, 0.2%~0.8% 1,2- hexylene glycol, 0.5%~4% oligopeptides -1,2%~
4% glycerin polyether -26, remaining is water.
In the present embodiment, the range for changing each component content in the facial mask without preservative, makes each component
Content is more accurate, it can be seen that the facial mask without preservative has more obvious fungistatic effect.
Embodiment three
Facial mask and embodiment two provided by the present embodiment without preservative the difference is that: it is described right to increase
The content of hydroxy acetophenone and the 1,2- hexylene glycol.
Child labourer described in the present embodiment without the facial mask in preservative, including 10%~25% glycerol, 20%~25%
Butanediol, 0.25%~0.4% Sodium Hyaluronate, 0.2%~0.5% dipotassium glycyrrhizinate, 1%~3% erythrite,
0.5%~0.8% parahydroxyacet-ophenone, 0.5%~0.8% 1,2- hexylene glycol, 0.5%~4% oligopeptides -1,2%~
4% glycerin polyether -26, remaining is water.
In the present embodiment, the content of the parahydroxyacet-ophenone is increased to 0.5% from 0.2%~0.8%~
0.8%, the content of 1,2- hexylene glycol is mentioned from 0.2%~0.8% and is increased to 0.5%~0.8%, and remaining content is constant, leads to
It crosses in this way, relative to embodiment two, the parahydroxyacet-ophenone and 1, the 2- hexylene glycol are to the bacterium and fungi in facial mask
Inhibitory effect is more obvious, can be improved the shelf effect of the facial mask without preservative.
Example IV
Facial mask and embodiment three provided by the present embodiment without preservative the difference is that: continued growing institute
State the content of parahydroxyacet-ophenone and the 1,2- hexylene glycol.
The facial mask without preservative of offer described in the present embodiment, including 10%~25% glycerol, 20%~25%
Butanediol, 0.25%~0.4% Sodium Hyaluronate, 0.2%~0.5% dipotassium glycyrrhizinate, 1%~3% erythrite,
0.6%~0.8% parahydroxyacet-ophenone, 0.6%~0.8% 1,2- hexylene glycol, 0.5%~4% oligopeptides -1,2%~
4% glycerin polyether -26, remaining is water.
In the present embodiment, the content of the parahydroxyacet-ophenone and 1, the 2- hexylene glycol is increased to 0.6%~
0.8%, and the content of remaining component does not all change, and for embodiment three, only improves the para hydroxybenzene second
The content of ketone and 1, the 2- hexylene glycol, is designed in this way, can make parahydroxyacet-ophenone and 1,2- hexylene glycol opposite
The inhibitory effect of bacterium and fungi in film is more obvious, even up to inhibitory or killing effect, can kill bacterium in facial mask and
Fungi makes the facial mask without preservative not add preservative also and can reach the shelf effect to facial mask.
Embodiment five
The present embodiment relative to example IV the difference is that: by what is respectively formed in the facial mask without preservative
Content is set as determining value.
Be free of the facial mask of preservative provided by the present embodiment, 15% glycerol, 17.5% butanediol, 0.3% it is saturating
Bright matter acid sodium, 0.5% dipotassium glycyrrhizinate, 2% erythrite, 0.65% parahydroxyacet-ophenone, 0.6% 1,2- oneself two
Alcohol, 2.3% oligopeptides -1,3% glycerin polyether -26, remaining is water.
In the present embodiment, by the glycerol, butanediol, the Sodium Hyaluronate, the dipotassium glycyrrhizinate, described
Erythrite, the parahydroxyacet-ophenone, the 1,2- hexylene glycol, the oligopeptides -1 and the glycerin polyether content be set as specific
Value, design, the synergistic effect between each component can be performed to most preferably in this way, so that the face without preservative
Film reaches best skin effect, and reaches best shelf effect, and the facial mask without preservative is made to realize tradition
There is no any injury to human body while facial mask skin-protecting function, eliminate and add preservative in facial mask, greatly improving makes
Safety.
Embodiment six
The present embodiment relative to embodiment one the difference is that: by each component in the facial mask without preservative
Content is minimized.
Be free of the facial mask of preservative provided by the present embodiment, comprising: 10% glycerol, 15% butanediol, 0.2%
Sodium Hyaluronate, 0.1% dipotassium glycyrrhizinate, 0.5% erythrite, 0.1% parahydroxyacet-ophenone, 0.1% 1,2- oneself
Glycol, 0.3% oligopeptides -1,1% glycerin polyether -26, remaining is water.
Embodiment seven
The present embodiment relative to embodiment one the difference is that: by each component in the facial mask without preservative
Content is maximized.
The facial mask without preservative of offer described in the present embodiment, comprising: 30% glycerol, 30% butanediol, 0.5%
Sodium Hyaluronate, 0.6% dipotassium glycyrrhizinate, 3% erythrite, 1% parahydroxyacet-ophenone, 1% 1,2- hexylene glycol,
5% oligopeptides -1,5% glycerin polyether -26, remaining is water.
Embodiment eight
The present embodiment relative to embodiment one the difference is that: by each component in the facial mask without preservative
Median in content Example one.
The facial mask of preservative is free of provided by the present embodiment, comprising: 20% glycerol, 22.5% butanediol,
0.35% Sodium Hyaluronate, 0.35% dipotassium glycyrrhizinate, 1.75% erythrite, 0.55% parahydroxyacet-ophenone,
0.55% 1,2- hexylene glycol, 2.65% oligopeptides -1,3% glycerin polyether -26, remaining is water.
Embodiment nine
The present embodiment relative to embodiment two the difference is that: by each component in the facial mask without preservative
Minimum value in content Example two.
The facial mask without preservative of offer described in the present embodiment, including 10% glycerol, 20% butanediol, 0.25%
Sodium Hyaluronate, 0.2% dipotassium glycyrrhizinate, 1% erythrite, 0.2% parahydroxyacet-ophenone, 0.2% 1,2- oneself
Glycol, 0.5% oligopeptides -1,2% glycerin polyether -26, remaining is water.
Embodiment ten
The present embodiment relative to embodiment two the difference is that: by each component in the facial mask without preservative
Maximum value in content Example two.
The facial mask without preservative of offer described in the present embodiment, including 25% glycerol, 25% butanediol, 0.4%
Sodium Hyaluronate, 0.5% dipotassium glycyrrhizinate, 3% erythrite, 0.8% parahydroxyacet-ophenone, 0.8% 1,2- oneself
Glycol, 4% oligopeptides -1,4% glycerin polyether -26, remaining is water.
Embodiment 11
The present embodiment relative to embodiment two the difference is that: by each component in the facial mask without preservative
Median in content Example two.
The facial mask that preservative is free of provided by the present embodiment, including 17.5% glycerol, 22.5% butanediol,
0.325% Sodium Hyaluronate, 0.35% dipotassium glycyrrhizinate, 0.2% erythrite, 0.5% parahydroxyacet-ophenone,
0.5% 1,2- hexylene glycol, 2.25% oligopeptides -1,3% glycerin polyether -26, remaining is water.
Embodiment 12
The preparation method of facial mask of the preparation without preservative is present embodiments provided, it is unlike the embodiments above to be in
In: the present embodiment is detailed to give the preparation method of the facial mask without preservative.
The preparation method of the facial mask without preservative provided by the present embodiment, comprising the following steps:
S101. suitable glycerol, butanediol, Sodium Hyaluronate, erythrite and water are put into emulsion pot, is then stirred
Heating is mixed and stirred, after heating, at least 30 minutes is kept the temperature, obtains mixture A；
S102. cooling is stirred to the mixture A, after cooling, adds the mixture B prepared, stirred
Uniformly, mixture C is obtained, and at least 10 minutes are kept the temperature to the mixture C, the mixture B is by suitable para hydroxybenzene
Ethyl ketone and 1,2 hexylene glycols obtain after being dissolved by heating；
S103. cool down to the mixture C, after cooling, add suitable oligopeptides -1, and stir at least 5
Minute, obtain mixture D；
S104. suitable glycerin polyether -26 is added in the mixture D, and stirred at least 10 minutes, after stirring
Obtain the facial mask without preservative as described in above-described embodiment any one.
In the present embodiment, " suitable " is the volatilization that those skilled in the art consider chemical substance, so what it was indicated
Amount is greater than the standard volume of institute's additive.
Pass through the specific descriptions of the method to the preparation facial mask without preservative, in the step S101, Bian Jia
The stirring of hot side be in order to which the glycerol, the butanediol, the Sodium Hyaluronate and the erythrite are thoroughly dissolved, it is described sweet
Oil may also help in the better dissolution of the water Yu the butanediol, the Sodium Hyaluronate and the erythrite, heat
Bi Hou, the effect kept the temperature are to the dissolved glycerol, the butanediol, the Sodium Hyaluronate and the erythrite
Solution sterilize, the content of bacterium is controlled in the range of standard.
In the step S102, carrying out cooling to the mixture A is stirred to dissolve the mixture B
Effect be speed in order to accelerate cooling, while also to be stirred during the mixture B is added, the reason is that in order to
It is dissolved into the mixture B more preferably faster in the mixture A, the mixture B is thoroughly dissolved into the mixture A
When, available mixture C, carrying out heat preservation to the mixture C is to keep the temperature duration to sterilize to the mixture C
At least 10 minutes are then to guarantee that the product of production is qualified to guarantee that bacterium can drop in qualified range.
In the step S103, cool down to the mixture C is to dissolve the oligopeptides -1, the purpose of stirring
Be that keep the oligopeptides -1 faster and better is dissolved in the mixture C, stirring duration be at least 5 minutes be then to guarantee
The oligopeptides -1 can completely dissolve, meanwhile, the oligopeptides -1, which not only has, quickly repairs damaged skin, skin care, enhancing
The effect of skin elasticity and whitening spot-removing is also used as each group in the activating agent reduction mixture C and divides it in this step
Between reaction time, while can also make preferably to dissolve between each component, increase beneficial effect.
In the step S104, the glycerin polyether -26 is added in mixture D as moisturizer, it can prevent
The only water loss in the mixture D, while also making the facial mask without preservative prepared that there are moisture-keeping functions.
Optimization, the holding temperature in the step S101 is between 90 DEG C~95 DEG C.In the present embodiment, described sweet
Oily, the described butanediol, the Sodium Hyaluronate, the erythrite and the water heating temperature also between 90 DEG C~95 DEG C it
Between, it designs in this way, can just make the glycerol, the butanediol, the Sodium Hyaluronate and the erythrite thoroughly molten
Solution, and is thoroughly merged with the water, and holding temperature can just make in dissolved solution so also between 90 DEG C~95 DEG C
Inactivation of bacteria, reach qualified standard.
Optimization, in the step S102, the mixture A is cooled between 58 DEG C~62 DEG C.Because only that 58
DEG C~62 DEG C between, the mixture A could completely dissolve the mixture B, obtain the optimal mixing of beneficial effect
Object C, and the mixture B will not lose activity, in this step, holding temperature is also between 58 DEG C~62 DEG C, because
This temperature range, can not only be by the bacteria inactivation in the mixture C, moreover it is possible to guarantee that each component is thin in the mixture C
Born of the same parents will not inactivate.
Optimization, in the step S102, the temperature of the parahydroxyacet-ophenone and 1,2 hexylene glycol heating for dissolving
Between 58 DEG C~62 DEG C.Because only that in this temperature range, the parahydroxyacet-ophenone can with 1, the 2- oneself
Glycol is completely dissolved, and the parahydroxyacet-ophenone will not also inactivate, and obtains effective mixture B, can carry out lower step system
Standby work.
Optimization, in the step S103, the mixture C is cooled between 43 DEG C~47 DEG C.Why described
Mixture C is cooled between 43 DEG C~47 DEG C, is because the oligopeptides -1 to be added in this step, when temperature is higher than this area
Between after, the oligopeptides -1 will inactivate, do not have activating agent and repair damaged skin effect.
Embodiment 13
The preparation method of facial mask provided by the present embodiment without preservative, it and 12 difference of embodiment exist
In: each step gives specific temperature value when producing.
The preparation method of the facial mask without preservative provided by the present embodiment, comprising the following steps:
S101. suitable glycerol, butanediol, Sodium Hyaluronate, erythrite and water are put into emulsion pot, is then stirred
Heating is mixed and stirred, is heated to 90 DEG C, after heating, in this temperature condition down toward few heat preservation 30 minutes, obtains mixture A；
S102. cooling is stirred to the mixture A, is cooled to 60 DEG C, after cooling, add prepare it is mixed
Object B is closed, stirs evenly, obtains mixture C, and at least 10 minutes are kept the temperature to the mixture C under the conditions of temperature, it is described mixed
Closing object B is to be dissolved by heating by suitable parahydroxyacet-ophenone and 1,2 hexylene glycols to obtaining after 60 DEG C；
S103. cool down to the mixture C, be cooled to 45 DEG C, after cooling, add suitable oligopeptides -1,
And stir at least 5 minutes, obtain mixture D；
S104. suitable glycerin polyether -26 is added in the mixture D, and stirred at least 10 minutes, after stirring
Obtain the facial mask without preservative as described in above-described embodiment any one.
In the present embodiment, " suitable " is the volatilization that those skilled in the art consider chemical substance, so what it was indicated
Amount is greater than the standard volume of institute's additive.
It is found through inventor's long-term experiment, when each process parameter setting is such as the present embodiment, the content of bacterium reaches mark
Standard is worth minimum, and the activity of emulsification degree and each component all reaches best, is to prepare facial mask of the present invention without preservative most
Excellent process choice.
Experimental data:
Example five~any one of 11 carry out preservation challenge test
What this experiment was taken is primary plus bacterium 28d antiseptic property test, weighs the film sample without preservative
20g, respectively add 0.2mL mixed cell (staphylococcus aureus, Escherichia coli and pseudomonas aeruginosa combined inoculation, 3 kinds
The inoculation quantity of bacterium is maintained at the same order of magnitude) and mixed fungus (aspergillus niger and saccharomyces albicans combined inoculation, 2 kinds of bacterium
Inoculation quantity be maintained at the same order of magnitude) outstanding bacterium solution, make to be respectively reached 10^ by the bacterium of sample product or the order of magnitude of fungi
5 or 10^6CFU/g is connecing the bacteria containing amount in the after bacterium the 2nd, 7,28 day sampling analysis sample.
Criterion referring to CTFA (cosmetics and flavors and fragrances association) once plus bacterium preservation challenge test evaluation standard,
It is domestic to add bacterium preservation challenge test evaluation standard and " cosmetics health specification " 2015 editions referring to CTFA:
CTFA once adds bacterium preservation challenge test evaluation standard:
It is required that mould reduced by 90% at the 7th day, bacterium reduces by 99.9%, and bacterium number continues to decline in 28 days.
The country adds bacterium preservation challenge test evaluation standard referring to CTFA:
At (1) the 28th day, bacterium or mould > 1000CFU/g (mL) are contained in sample, which cannot be tested by challenge,
Show that the protective system in sample cannot effectively inhibit the effect of hygienic articles, product is easy in production, storage and in
Pollution by microorganism.
At (2) the 28th days, containing bacterium or mould at 100CFU/g~1000CFU/g (mL) in sample, which has ready conditions
It is tested by challenge, i.e., when protein in product or other animals and plants material compositions are not to mention health cup that is not high, while producing
Border burden requirement, when packing material is not susceptible to secondary pollution, which be can be used, and otherwise cannot.
At (3) the 28th days, show the anti-of the sample at 10CFU/g~100CFU/g (mL) containing bacterium or mould in sample
Rotten system to microorganism have it is stronger suppression kill effect, by challenge test, product production, storage and using when be not susceptible to very much
To microbial contamination.
(4) from the 7th day, bacterium or mould < 10CFU/g (mL) in sample illustrate the protective system of the sample to micro-
Biology has the inhibitory or killing effect of extra-heavy, by challenge test, product production, storage and using when be not easy microbial contamination.
" cosmetics health specification " 2015 editions evaluation criterions:
(1) total plate count (CFU/g or CFU/mL)≤1000
(2) yeast and mold is total (CFU/g or CFU/mL)≤100
(3) staphylococcus aureus must not detect, pseudomonas aeruginosa must not detect, heat-resisting coliform must not detect.
Experimental data is as shown below:
Experiment conclusion:
By experimental result as can be seen that being free of preservative provided by embodiment five, embodiment seven and embodiment ten
Facial mask can satisfy CTFA and bacterium preservation challenge test evaluation standard, the country once added to add bacterium preservation challenge to test referring to CTFA
Microorganism Evaluation standard in evaluation criterion and " cosmetics health specification " 2015 editions, demonstrates the parahydroxyacet-ophenone and institute
State 1,2- hexylene glycol in facial mask bacterium and fungi have good inhibitory effect, can in the case where not adding preservative according to
The old anti-corrosion effect reached to facial mask, can be safe to use.
Consider that preferred embodiment five is as of the invention according to anti-corrosion effect, cost of material and to human skin irritation
Optimal case.
The present invention is not limited to above-mentioned optional embodiment, anyone can show that other are various under the inspiration of the present invention
The product of form, however, make any variation in its shape or structure, it is all to fall into the claims in the present invention confining spectrum
Technical solution, be within the scope of the present invention.
Claims (10)
1. a kind of facial mask without preservative, it is characterised in that: percentages by weight, comprising: 10%~30% glycerol,
15%~30% butanediol, 0.2%~0.5% Sodium Hyaluronate, 0.1%~0.6% dipotassium glycyrrhizinate, 0.5%~
3% erythrite, 0.1%~1% parahydroxyacet-ophenone, 0.1%~1% 1,2- hexylene glycol, 0.3%~5% oligopeptides-
1,1%~5% glycerin polyether -26, remaining is water.
2. a kind of facial mask without preservative according to claim 1, it is characterised in that: including 10%~25% it is sweet
Oil, 20%~25% butanediol, 0.25%~0.4% Sodium Hyaluronate, 0.2%~0.5% dipotassium glycyrrhizinate, 1%
~3% erythrite, 0.2%~0.8% parahydroxyacet-ophenone, 0.2%~0.8% 1,2- hexylene glycol, 0.5%~4%
Oligopeptides -1,2%~4% glycerin polyether -26, remaining is water.
3. a kind of facial mask without preservative according to claim 2, it is characterised in that: including 10%~25% it is sweet
Oil, 20%~25% butanediol, 0.25%~0.4% Sodium Hyaluronate, 0.2%~0.5% dipotassium glycyrrhizinate, 1%
~3% erythrite, 0.5%~0.8% parahydroxyacet-ophenone, 0.5%~0.8% 1,2- hexylene glycol, 0.5%~4%
Oligopeptides -1,2%~4% glycerin polyether -26, remaining is water.
4. a kind of facial mask without preservative according to claim 3, it is characterised in that: including 10%~25% it is sweet
Oil, 20%~25% butanediol, 0.25%~0.4% Sodium Hyaluronate, 0.2%~0.5% dipotassium glycyrrhizinate, 1%
~3% erythrite, 0.6%~0.8% parahydroxyacet-ophenone, 0.6%~0.8% 1,2- hexylene glycol, 0.5%~4%
Oligopeptides -1,2%~4% glycerin polyether -26, remaining is water.
5. a kind of facial mask without preservative according to claim 4, it is characterised in that: including 15% glycerol,
17.5% butanediol, 0.3% Sodium Hyaluronate, 0.5% dipotassium glycyrrhizinate, 2% erythrite, 0.65% to hydroxyl
Acetophenone, 0.6% 1,2- hexylene glycol, 2.3% oligopeptides -1,3% glycerin polyether -26, remaining is water.
6. a kind of method for preparing the facial mask without preservative, which comprises the following steps:
S101. will suitable glycerol, butanediol, Sodium Hyaluronate, erythrite and water put into emulsion pot in, be then stirred and
Heating after heating, at least keeps the temperature 30 minutes, obtains mixture A；
S102. cooling is stirred to the mixture A, after cooling, adds the mixture B prepared, stir evenly,
Obtain mixture C, and at least 10 minutes kept the temperature to the mixture C, the mixture B be by suitable parahydroxyacet-ophenone and
The mixture that 1,2 hexylene glycols obtain after being dissolved by heating；
S103. cool down to the mixture C, after cooling, add suitable oligopeptides -1, and stir at least 5 minutes,
Obtain mixture D；
S104. suitable glycerin polyether -26 is added in the mixture D, and stirred at least 10 minutes, obtained after stirring
The facial mask of preservative is free of as claimed in any one of claims 1 to 5, wherein.
7. a kind of preparation method of facial mask without preservative according to claim 6, it is characterised in that: the step
Holding temperature in S101 is between 90 DEG C~95 DEG C.
8. a kind of preparation method of facial mask without preservative according to claim 6, it is characterised in that: in the step
In S102, the mixture A is cooled between 58 DEG C~62 DEG C.
9. a kind of preparation method of facial mask without preservative according to claim 6, it is characterised in that: in the step
In S102, the temperature that the parahydroxyacet-ophenone and 1,2 hexylene glycol dissolve by heating is between 58 DEG C~62 DEG C.
10. a kind of preparation method of facial mask without preservative according to claim 6, it is characterised in that: in the step
In rapid S104, the mixture C is cooled between 43 DEG C~47 DEG C.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811162832.8A CN109077949A (en) | 2018-09-30 | 2018-09-30 | A kind of facial mask and preparation method thereof without preservative |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811162832.8A CN109077949A (en) | 2018-09-30 | 2018-09-30 | A kind of facial mask and preparation method thereof without preservative |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106726743A (en) * | 2016-11-23 | 2017-05-31 | 上海萧雅生物科技股份有限公司 | Facial treatment mask that no added safe pregnant woman can be used and preparation method thereof |
| DE102015224334A1 (en) * | 2015-12-04 | 2017-06-08 | Henkel Ag & Co. Kgaa | Use of additives for the effective preservation / boosting effect of existing preservation of cosmetic emulsions |
| CN107823095A (en) * | 2017-12-07 | 2018-03-23 | 安徽生物肽产业研究院有限公司 | A kind of active peptide facial mask |
| CN108542872A (en) * | 2018-07-16 | 2018-09-18 | 徐杨 | Plant extraction assigns MASQUE APAISANT HYDRATANT living |
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2018
- 2018-09-30 CN CN201811162832.8A patent/CN109077949A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102015224334A1 (en) * | 2015-12-04 | 2017-06-08 | Henkel Ag & Co. Kgaa | Use of additives for the effective preservation / boosting effect of existing preservation of cosmetic emulsions |
| CN106726743A (en) * | 2016-11-23 | 2017-05-31 | 上海萧雅生物科技股份有限公司 | Facial treatment mask that no added safe pregnant woman can be used and preparation method thereof |
| CN107823095A (en) * | 2017-12-07 | 2018-03-23 | 安徽生物肽产业研究院有限公司 | A kind of active peptide facial mask |
| CN108542872A (en) * | 2018-07-16 | 2018-09-18 | 徐杨 | Plant extraction assigns MASQUE APAISANT HYDRATANT living |
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