CN109068709A - instant product and preparation method thereof - Google Patents
instant product and preparation method thereof Download PDFInfo
- Publication number
- CN109068709A CN109068709A CN201880000846.1A CN201880000846A CN109068709A CN 109068709 A CN109068709 A CN 109068709A CN 201880000846 A CN201880000846 A CN 201880000846A CN 109068709 A CN109068709 A CN 109068709A
- Authority
- CN
- China
- Prior art keywords
- instant
- minutes
- thickener
- food
- product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000002360 preparation method Methods 0.000 title abstract description 61
- 238000004519 manufacturing process Methods 0.000 title abstract description 40
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims abstract description 58
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims abstract description 58
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims abstract description 58
- 239000000126 substance Substances 0.000 claims abstract description 36
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Abstract
A kind of instant capacity product and preparation method thereof.The instant product is will to dry to be prepared at 112 DEG C~210 DEG C to molten object and substance A, and the substance A is selected from trehalose or antierythrite.Have the characteristics that good dispersion and quickly dissolution using the product that this technology of preparing is produced and without flake.
Description
Technical field:
The present invention relates to a kind of instant products and preparation method thereof.
Background technique:
Thickener has thickening power because hydration occurs for its molecule, and variety classes thickener is produced because of its own structure
Raw different thickenings and rheological behavior.Thickener is completely dissolved process and needs to undergo two steps, is that hydrone penetrates into thickening first
Agent polymeric inner, so that thickening solvent swell, followed by thickener polymers molecule is uniformly distributed in water, is finally reached completely
Aquation dissolution.However in the practical process for preparation of thickener soln, when the powder of thickener or particle are directly mixed with water, rate
First touch water thickener polymers molecule can rapid water absorption and swelling then dissolve, form highly viscous gelatinous layer and delayed water
Molecule is to thickener internal penetration, to influence the further aquation and dissolution of thickener, should easily form flake in the process, and
And make that cementing formation bulk occurs between particle, its service efficiency is reduced, its further market application extension is also limited.
The preparation method of traditional instant thickener is to be improved by fermenting or extracting purifying technique, or pass through chemistry
Modified method is grafted some hydrophobic groupings, also has plenty of through vacuum drying, the method for being dried under reduced pressure or being freeze-dried.
In field of medicaments, granule is manufactured granular formulations by drug and suitable auxiliary material cooperation, main special
Point is directly to swallow, can also be poured with warm water in water drink into, application and carry it is more convenient, dissolution and infiltration rate compared with
Fastly.
The preparation method of traditional solid beverage, is dried this technique after common mixing and is made and form, some then exist
Increase granulating working procedure on the basis of this.But the solid beverage that this technique is prepared, mostly powdery or loosely organized graininess.
Solid beverage its mobility, dispersibility and the dissolubility being prepared using this technique are poor.
Summary of the invention:
The present inventor develops a kind of instant product and preparation method thereof by further investigation and a large number of experiments.This method
Instant or good dispersion product is needed suitable for thickener, food, raw-food material and drug etc..
In embodiments of the invention, a kind of instant product is provided, which is characterized in that according to the total of the instant product
Weight, the instant product includes: 1-90% (w/w), preferably 1-80% (w/w), 1-70% (w/w), 1-60% (w/w), 1-
50% (w/w's), 1-40% (w/w), 1-30% (w/w), 1-20% (w/w) or 1-10% (w/w) is one or more to molten object,
With
10-99% (w/w), preferably 10-89% (w/w), 10-79% (w/w), 10-69% (w/w), 10-59% (w/w),
10-49% (w/w), 10-39% (w/w), 10-29% (w/w), the substance A of 10-19% (w/w), the substance A are selected from seaweed
Sugar or antierythrite.
In embodiments of the invention, it is preferable that the instant product is will be after molten object be mixed with substance A 112
DEG C~210 DEG C, preferably 112 DEG C -205 DEG C, and 112 DEG C -200 DEG C, 112 DEG C -195 DEG C, 112 DEG C -190 DEG C, 112 DEG C -185 DEG C, 112
DEG C -180 DEG C, 112 DEG C -175 DEG C, 112 DEG C -170 DEG C, 112 DEG C -165 DEG C, 112 DEG C -160 DEG C, 112 DEG C -155 DEG C, 112 DEG C -
150 DEG C, 112 DEG C -145 DEG C, 112 DEG C -140 DEG C, 112 DEG C -135 DEG C, 112 DEG C -130 DEG C, 112 DEG C -125 DEG C, 112 DEG C -120 DEG C
Or it dries and is made at 112 DEG C -115 DEG C.
In embodiments of the invention, according to the total weight of the instant product, the instant product also includes 0-
89% (w/w), more preferable 0-79% (w/w), 0-69% (w/w), 0-59% (w/w), 0-49% (w/w), 0-39% (w/w),
The auxiliary material of 0-29% (w/w) or 0-19% (w/w).
In embodiments of the invention, a kind of method preparing instant product is provided, comprising:
A) will be uniformly mixed to molten object with substance A, wherein the content according to the total weight of the instant product, to molten object
For 1-90% (w/w), preferably 1-80% (w/w), 1-70% (w/w), 1-60% (w/w), 1-50% (w/w), 1-40% (w/
W), 1-30% (w/w), 1-20% (w/w) or 1-10% (w/w);The content of substance A is 10-99% (w/w), preferably 10-89%
(w/w), 10-79% (w/w), 10-69% (w/w), 10-59% (w/w), 10-49% (w/w), 10-39% (w/w), 10-
29% (w/w), 10-19% (w/w),
The substance A is selected from trehalose or antierythrite;
B) by mixed material in 112 DEG C~210 DEG C, preferably 112 DEG C -200 DEG C, 112 DEG C -195 DEG C, 112 DEG C -190 DEG C,
112 DEG C -185 DEG C, 112 DEG C -180 DEG C, 112 DEG C -175 DEG C, 112 DEG C -170 DEG C, 112 DEG C -165 DEG C, 112 DEG C -160 DEG C, 112
DEG C -155 DEG C, 112 DEG C -150 DEG C, 112 DEG C -145 DEG C, 112 DEG C -140 DEG C, 112 DEG C -135 DEG C, 112 DEG C -130 DEG C, 112 DEG C -
It is dried at 125 DEG C, 112 DEG C -120 DEG C or 112 DEG C -115 DEG C.
In embodiments of the invention, further, it will be mixed to molten object and substance A with auxiliary material in step a), it is excellent
Selection of land, the total weight based on instant product, the content of the auxiliary material are 0-89% (w/w), more preferable 0-79% (w/w), 0-
69% (w/w), 0-59% (w/w), 0-49% (w/w), 0-39% (w/w), 0-29% (w/w) or 0-19% (w/w).
In embodiments of the invention, in the step a) before, during or after mixing, will to molten object, substance A and/
Or auxiliary material crushes.
In embodiments of the invention, in the step a) before, during or after mixing, will to molten object, substance A and/
Or auxiliary material dissolution, the solvent are selected from water or organic solvent.
In embodiments of the invention, before carrying out step b), by mixture through stirring evenly, shear treatment,
Homogenization and/or centrifugal treating, then dry finishing.
In embodiments of the invention, it pelletizes before drying.
In embodiments of the invention, whole grain or sub-sieve are carried out in step c).
In embodiments of the invention, the thickener is the fermentation liquid of thickener, thickener semi-finished product, and thickener mentions
Take liquid or thickener refined product.
In embodiments of the invention, the thickener is selected from the group being made of the following: xanthan gum, carboxymethyl are fine
Tie up plain sodium, modified carboxy methyl cellulose sodium, pectin, sodium alginate, gellan gum, locust bean gum, guar gum, konjac glucomannan, konjaku essence
Powder, carragheen, Arabic gum, propylene glycol alginate, hydroxypropyl guar gum, casein sodium, tamarind gum, bassora gum, β-
Glucan, soybean polyoses, pullulan, condensation polysaccharide, zymosan, converted starch or their one or more any groups
It closes.
In embodiments of the invention, the drug is selected from by the group that forms of the following: the drug be selected from by with
The group of lower every composition: antalgesic, α-blockers, antiallergic, antasthmatic treat the drug of allergic rhinitis, and treatment is slow
The drug of property nettle rash, anti-inflammatory agent, antacids, anthelmintic, antiarrhymic, anti-arthritic, antimicrobial, antianxiety
Medicine, anticoagulant, antidepressants, antidiabetic, antidiarrheal agent, antidiuretic, antiepileptic, antifungal, gout suppressant resist
Hypertension agents, anti-incontinence medicine, anti-insomnia medicine, antimalarial, antimigraine, antimuscarinic drug, antineoplastic, immunosuppressor,
Antiprotozoal, antirheumatic drug, anti-rhinitis medicament, antispasmodic, antithyroid drug, antiviral agent, antianxiety agent, sedative,
Somnifacient, stress-reduction agent, beta-Blocking agent resist benign hyperplasia medicine, cardiac inotropic drug, corticosteroid, pectoral, cell toxicant
Property agent, decongestant, diabetes gastric retention, diuretics, enzyme, antiparkinsonian drug, histamine receptor antagonists, sterilizing agent, son
Endometriosis, hormone replacement therapy, lipid regulating agent, local anaesthetics, neuromuscular drug, Nitrates, antianginal drug, treatment
The drug of menstrual disorder, treats the drug of motion sickness, antipain, antinanseant, nutritional agents, opioid analgesic agent, oral vaccine,
Protein drug, reconstituted drug, proton pump inhibitor treat schizoid drug, sex hormone, contraceptive, epilepsy hair
Work/panic disorder, sex dysfunction (male and female), spermatocide, excitant excretory function obstacle treat Animal diseases
Drug or their one or more any combination.
In embodiments of the invention, the drug or pharmaceutical composition include at least one pharmacy activity component, excellent
Selection of land, the pharmacy activity component are selected from compound, peptide, nucleotide, plant extracts, Chinese medical extract or Chinese medical concrete.
In embodiments of the invention, the food or food compositions include raw-food material, the raw-food material choosing
From new resource food, plant extracts, dried fruit juice, Vegetable powder, tea powder, digested tankage or their one or more any combination.
Statement " new resource food " indicate Chinese newly development, new discovery, newly introduce without food custom, meet food
Basic demand food.It is had the following characteristics that according to China's " new resource food management method " regulation new resource food
(1) (1) is in animal, plant and microorganism of the China without food custom;
(2) (2) the microorganism new varieties used in food processing process;
(3) raw-food material that (3) cause original ingredient or structure to change because of production of adopting new technology.
For example, new resource food includes cactus, and Camellia nitidissima, aloe, Bifidobacterium, lactobacillus acidophilus, xylo-oligosaccharide, thoroughly
Bright matter acid sodium, lutein ester, L-arabinose, Sessileflower Acanthopanax Bark, aloe vera gel etc..
Applicant have surprisingly discovered that substance A with above-mentioned after molten object mixes, the non-melt shape within the scope of specific temperature
Fierce contraction is generated under state, molecular conformation changes, this character energy Complete Bind is simultaneously isolated and is easy to cementing to molten
Object makes it not unite and agglomerates and spread out calmly, the method produce resulting Instant instant product substantially increase its
Dispersibility and solution rate in water.
In addition, traditional solid beverage generally needs to form under wet basis environment, solid foaming drink (gassiness can not be solved
Solid beverage or effervescent solid beverage) grain forming problem, this is because organic acid and foaming agent such as sodium bicarbonate or dodium thiosulfate
It is reacted rapidly under wet basis environment.The invention enables of solid foaming drink (gassiness solid beverage or effervescent solid beverage)
Grain formation problems are easily solved.
Detailed description of the invention
Fig. 1: the instant xanthan gum of the method for the present invention preparation figure compared with the dissolution of commercially available xanthan gum;Wherein Fig. 1 a be according to
The instant xanthan gum of the method preparation of embodiment 2 (wherein xanthan gum concentration is 0.7%);Fig. 1 b is commercially available plum blossom biotechnology collection
The prepared solution of xanthan gum of limited liability company of group production, concentration 0.7%.
Fig. 2: instant carboxymethylcellulose sodium prepared by the present invention and other sodium carboxymethylcellulose dissolubility dispersibility ratios
Compared with figure;Wherein Fig. 2 a is the instant carboxymethylcellulose sodium prepared according to the method for embodiment 3;Fig. 2 b is that commercially available carboxymethyl is fine
Tie up the prepared solution of plain sodium.
Fig. 3: the instant kudzu vine powder of the method for the present invention preparation figure compared with the dissolution of other kudzuvine root starch;Wherein Fig. 3 a is according to embodiment
The instant kudzu vine powder solution of 20 method preparation;Fig. 3 b is the kudzuvine root starch of commercially available Jiangxi Yu Ming agricultural product Co., Ltd production.
Fig. 4: the instant milk tea of the method for the present invention preparation figure compared with the dissolution of other milk tea;Wherein 4a figure is according to embodiment
The instant milk tea of 21 method preparation,;4b figure is to substitute milk tea prepared by trehalose completely with white granulated sugar.
Fig. 5: the instant isatis root extract of the method for the present invention preparation figure compared with the dissolution of other isatis root extracts;Wherein
Fig. 5 a is the instant Radix Isatidis prepared according to the method for embodiment 22;Fig. 5 b is that Jiangxi Han Ben Biotechnology Co., Ltd of radically reforming is raw
The banlangen granules, banlangen keli of production.
Fig. 6: the instant eucommia ulmoides extracts of the method for the present invention preparation figure compared with the dissolution of other plate eucommia ulmoides extracts;Fig. 6 a is
Figure is dissolved by instant Duzhong prepared by embodiment 23;Resulting eucommia ulmoides extracts after Fig. 6 b. eucommia ulmoides extract is spray-dried
It is dissolved in water.
Fig. 7: Instant complex thickener prepared by the present invention figure compared with other composite thickening agent dissolubility dispersibilities,
Wherein: Fig. 7 a is the Instant prepared according to the method for embodiment 32;Fig. 2 b is that commercially available sodium carboxymethylcellulose is prepared
Solution.
Fig. 8: the instant kudzu vine powder of the method for the present invention preparation figure compared with control kudzuvine root starch dissolution;Wherein Fig. 1 a is according to embodiment
The instant kudzu vine powder solution of 41 method preparation;Fig. 1 b is the kudzuvine root starch of commercially available Jiangxi Yu Ming agricultural product Co., Ltd production.
Fig. 9: the instant milk tea of the method for the present invention preparation figure compared with control milk tea dissolution;Wherein 2a figure is according to embodiment
The instant milk tea of 40 method preparation;2b figure is control milk tea.
Specific embodiment
Below by specific embodiment, technical scheme of the present invention will be further explained in detail, but following embodiments
It should not be construed as limiting the invention.
In the examples below, trehalose is purchased from Lin Yuan Co., Ltd. of Japan;Antierythrite is purchased from the precious biology of Shandong bowling
Technology Co., Ltd.;Other additives eat Chemical Co., Ltd. purchased from Guangzhou the earth.
In the following examples, the percentage of each substance is hundred of the total weight based on obtained instant product
Divide ratio.
Embodiment 1
47.5% trehalose, 2.5% sodium citrate, (Club Biological Technology Group Co., Ltd is raw for 50% xanthan gum
Produce), it by mixing, crushes, is subsequently placed in drying equipment and is heat-treated 3 minutes for 150 DEG C, then through whole grain, sieving obtains Instant
Xanthan gum.
The Instant xanthan gum 2g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of xanthan gum are
0.5%;Check experiment is to be formulated using the xanthan gum that commercially available Club Biological Technology Group Co., Ltd produces
Solution, concentration 0.5%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved yet within 1 hour | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 4 minutes | All spread out |
Embodiment 2
55% trehalose, 10% maltodextrin, 35% xanthan gum (ibid) are crushed by mixing, are subsequently placed in drying and set
It is heat-treated 4 minutes for 140 DEG C in standby, then through whole grain, sieving obtains Instant xanthan gum.
The Instant xanthan gum 4g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of xanthan gum are
0.7%;Check experiment is to be formulated using the xanthan gum that commercially available Club Biological Technology Group Co., Ltd produces
Solution, concentration 0.7%:
It can be seen from figure 1 that Instant xanthan gum solution (xanthan gum actual concentrations are 0.7%) manufactured in the present embodiment, enters
Water is completely dispersed and comes, and is completely dissolved within 5 minutes, and the Huang of commercially available Club Biological Technology Group Co., Ltd production
Virgin rubber enters water and unites agglomeration, and flake can not mostly be counted.
Embodiment 3
66% trehalose, 4% antierythrite, 30% sodium carboxymethylcellulose (Shanghai Shen optical eclipse Chemical Company
Production), it by mixing, crushes, is subsequently placed in drying equipment and is heat-treated 3 minutes for 150 DEG C, then through whole grain, sieving is obtained instant
Type sodium carboxymethylcellulose.
The Instant sodium carboxymethylcellulose 4g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein carboxymethyl cellulose
The actual concentrations of plain sodium are 0.6%;Check experiment is the carboxylic produced using commercially available Shanghai Shen optical eclipse with Chemical Company
The solution that sodium carboxymethylcellulose pyce is formulated, concentration 0.6%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved yet within 1 hour | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 4 minutes | All spread out |
It is completely dispersed and comes it can be seen in fig. 2 that instant carboxymethylcellulose sodium solution manufactured in the present embodiment enters water, 4
It is completely dissolved in minute;And commercially available Shanghai Shen optical eclipse enters water with the sodium carboxymethylcellulose that Chemical Co., Ltd. produces and unites
Agglomeration, bubble through the water column on, flake mostly can not count, also fail to be completely dissolved after 1 hour.
Embodiment 4
70% trehalose, 5% sodium carboxymethyl starch (ibid), 25% pectin (Yantai Andre Pectic Co., Ltd.
Production), it by mixing, crushes, is subsequently placed in drying equipment and is heat-treated 3 minutes for 160 DEG C, then through whole grain, sieving is obtained instant
Type pectin.
The Instant pectin 6g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of pectin are
0.75%;Check experiment is molten to be formulated using the pectin that commercially available Yantai Andre Pectic Co., Ltd. produces
Liquid, concentration 0.75%:
Embodiment 5
75% trehalose, 10% methylcellulose, 15% sodium alginate (Qingdao bright moon group is sold) pass through mixing, powder
It is broken, it is subsequently placed in drying equipment and is heat-treated 3 minutes for 170 DEG C, then through whole grain, sieving obtains Instant sodium alginate.
The Instant sodium alginate 8g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the reality of sodium alginate is dense
Degree is 0.6%;Check experiment is the solution being formulated using the sodium alginate that commercially available Qingdao bright moon group produces, concentration
It is 0.6%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 40 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 3 minutes | All spread out |
Embodiment 6
99% trehalose, 1% gellan gum (are newly got over maritime business's industry Development Co., Ltd and are sold in Guangzhou), by mixing, crush, so
It is placed in drying equipment and is heat-treated 40 minutes for 112 DEG C, then through whole grain, sieving obtains Instant gellan gum.
The Instant gellan gum 20g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of gellan gum
It is 0.1%;Check experiment newly to get over the solution that the gellan gum sold of maritime business's industry Development Co., Ltd is formulated using Guangzhou,
Concentration is 0.1%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 20 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 3 minutes | All spread out |
Embodiment 7
10% trehalose, 90% sodium carboxymethylcellulose (ibid) are crushed, are subsequently placed in drying equipment by mixing
210 DEG C are heat-treated 3 minutes, then through whole grain, sieving obtains Instant sodium carboxymethylcellulose.
The Instant sodium carboxymethylcellulose 2g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein carboxymethyl cellulose
The actual concentrations of plain sodium are 0.9%;Check experiment is the carboxylic produced using commercially available Shanghai Shen optical eclipse with Chemical Company
The solution that sodium carboxymethylcellulose pyce is formulated, concentration 0.9%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 40 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 4 minutes | All spread out |
Embodiment 8
65% trehalose, 10% inulin, 25% locust bean gum (Guangzhou Jun Long group is sold) are crushed, then by mixing
It is placed in drying equipment and is heat-treated 10 minutes for 130 DEG C, then through whole grain, sieving obtains Instant locust bean gum.
The Instant locust bean gum 4g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the reality of locust bean gum is dense
Degree is 0.5%;The solution that check experiment is formulated for the locust bean gum sold using Guangzhou Jun Long group, concentration are
0.5%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 30 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 4 minutes | All spread out |
Embodiment 9
60% trehalose, 10% potassium chloride, 30% guar gum (Beijing Guar profit Science and Technology Co., Ltd. is sold) pass through
Mixing crushes, and is subsequently placed in drying equipment and is heat-treated 3 minutes for 150 DEG C, then through whole grain, sieving obtains Instant guar gum.
The Instant guar gum 4g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of cluster bean are
0.6%;Check experiment is dense to moisten the solution that the guar gum that Science and Technology Co., Ltd. is sold is formulated using Beijing Guar
Degree is 0.6%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 30 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 4 minutes | All spread out |
Embodiment 10
80% trehalose, 20% Arabic gum (Tai'an your kind effort Jiao Ye Co., Ltd is sold) are crushed, so by mixing
It is placed in drying equipment and is heat-treated 3 minutes for 150 DEG C, then through whole grain, sieving obtains Instant Arabic gum.
The Instant Arabic gum 5g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the reality of Arabic gum is dense
Degree is 0.5%;The solution that check experiment is formulated for the Arabic gum sold using Tai'an your kind effort Jiao Ye Co., Ltd,
Concentration is 0.5%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 40 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 3 minutes | All spread out |
Embodiment 11
20% trehalose, 76% maltodextrin, 3% potassium chloride, the 1% konjac glucomannan (Fujian Lv Xin institute of Food Co., Ltd
Sell), it by mixing, crushes, granulation, is subsequently placed in drying equipment and is heat-treated 60 minutes for 135 DEG C, then through whole grain, sieving is obtained
Instant konjac glucomannan.
The Instant konjac glucomannan 40g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of konjac glucomannan
It is 0.2%;The solution that check experiment is formulated for the konjac glucomannan sold using the Fujian Lv Xin Food Co., Ltd, concentration are
0.2%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 30 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 3 minutes | All spread out |
Embodiment 12
25% trehalose, 25% maltodextrin, 50% carragheen (Fujian Lv Xin Food Co., Ltd is sold), by mixed
It closes, crushes, be subsequently placed in drying equipment and be heat-treated 40 minutes for 145 DEG C, then through whole grain, sieving obtains Instant carragheen.
The Instant carragheen 4g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of carragheen are
1%;The solution that check experiment is formulated for the carragheen sold using the Fujian Lv Xin Food Co., Ltd, concentration 1%:
Embodiment 13
50% trehalose, 50% hydroxypropyl guar gum (Renqiu City is large to be sold up to Chemical Co., Ltd.), passes through mixing, powder
Broken, granulation is subsequently placed in drying equipment and is heat-treated 3 minutes for 186 DEG C, then through whole grain, sieving obtains Instant hydroxypropyl guar
Glue.
The Instant hydroxypropyl guar gum 4g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein hydroxypropyl guar gum
Actual concentrations be 1%;Check experiment to be prepared using the large hydroxypropyl guar gum sold up to Chemical Co., Ltd. of Renqiu City and
At solution, concentration 1%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 30 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 3 minutes | All spread out |
Embodiment 14
50% trehalose, 50% soybean polyoses (Henan table mountain Jin Jing biotech inc is sold), passes through
Mixing crushes, and is subsequently placed in drying equipment and is heat-treated 3 minutes for 150 DEG C, then through whole grain, it is more to obtain Instant soybean for sieving
Sugar.
The Instant soybean polyoses 2g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the reality of soybean polyoses is dense
Degree is 0.5%;Check experiment is prepared for the soybean polyoses sold using Henan table mountain Jin Jing biotech inc
Made of solution, concentration 0.5%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 30 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 3 minutes | All spread out |
Embodiment 15
50% trehalose, 25% sodium carboxymethylcellulose (ibid), 25% xanthan gum (ibid) are crushed, so by mixing
It is placed in drying equipment and is heat-treated 3 minutes for 160 DEG C, then through whole grain, sieving obtains a kind of compound Instant thickener production
Product.
The Instant thickener 4g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of thickener are
1%;The xanthan gum and Shanghai Shen light edible chemical that check experiment is sold by Club Biological Technology Group Co., Ltd have
The solution that the sodium carboxymethylcellulose that limit company is sold each 50% is equipped with, wherein thickener total concentration is 1%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved yet within 1 hour | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 5 minutes | All spread out |
Embodiment 16
50% trehalose, 30% sodium carboxymethylcellulose (ibid), 20% pectin (ibid) are crushed, then by mixing
It is placed in drying equipment and is heat-treated 3 minutes for 160 DEG C, then through whole grain, sieving obtains a kind of compound Instant thickener production
Product.
The Instant thickener 4g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of thickener are
1%;The sodium carboxymethylcellulose and Yantai An Deli pectin that check experiment is sold by Shanghai Shen optical eclipse with Chemical Company
The pectin accounting that limited liability company is sold is 6: 4 solution being equipped with, and wherein thickener total concentration is 1%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved yet within 1 hour | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 5 minutes | All spread out |
Embodiment 17
By cornstarch 5g/100mL, peptone 0.5g/100mL, KH2PO40.4g/100mL, MgSO40.05g/100mL,
FeSO40.025g/100mL, citric acid 0.025g/100mL are inoculated with xanthomonas campestris (Xanthomonas
Campestris), with this condition, 28 DEG C, 180r/min fermented and cultured 72h obtains xanthan gum fermentation broth, then in xanthan gum
Trehalose is added in fermentation liquid, additional amount is the 3% of fermentation liquid total weight, stirs 30 minutes after addition, then adds in 1: 3 ratio
Enter the alcohol of concentration 90%, is mixed 30 minutes, makes xanthan gum and trehalose Precipitation, sediment centrifugal treating is carried out
It is separated by solid-liquid separation, isolated substance is handled with dehydration of alcohol again, is pumped into centrifuge separation of solid and liquid after processing again, is then squeezed
Press-dehydrating, 80 DEG C are dried under reduced pressure processing, and the material after drying carries out crushing shaping, are subsequently placed in drying equipment at 150 DEG C of heat
Reason 3 minutes, then through whole grain, sieving obtains a kind of Instant xanthan gum product.
The Instant xanthan gum 4g of above-mentioned preparation is made an addition in 200ml water, is stirred;Check experiment is plum blossom biotechnology
The solution that the xanthan gum that Group Plc is sold is prepared, concentration 1%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved yet within 1 hour | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 5 minutes | All spread out |
Embodiment 18
70% trehalose, 10% sodium carboxymethylcellulose (ibid), 10% xanthan gum (ibid), 10% pectin (ibid) are logical
Mixing is crossed, is crushed, pelletizes, be subsequently placed in 160 DEG C heat treatment 3 minutes in drying equipment, using sieve, is obtained a kind of compound
Instant thickener products.
The Instant thickener 6g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of thickener are
0.9%;Sodium carboxymethylcellulose that check experiment is sold by Shanghai Shen optical eclipse with Chemical Company, plum blossom biotechnology collection
The pectin each 33.3% that the xanthan gum and Yantai Andre Pectic Co., Ltd. that limited liability company of group is sold are sold is equipped with
Solution, wherein thickener total concentration be 0.9%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved yet within 1 hour | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 5 minutes | All spread out |
Embodiment 19
70% trehalose, 10% sodium carboxymethylcellulose (ibid), 10% locust bean gum (Guangzhou Jun Long group is sold),
5% pectin (ibid), 5% sodium alginate (ibid) are crushed by mixing, are pelletized, are subsequently placed in drying equipment at 160 DEG C of heat
Reason 3 minutes obtains a kind of compound Instant thickener products using sieve.
The Instant thickener 6g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of thickener are
0.9%;Sodium carboxymethylcellulose that check experiment is sold by Shanghai Shen optical eclipse with Chemical Company, Guangzhou institute of Jun Long group
The sodium alginate that the pectin and Qingdao bright moon group that the locust bean gum sold, Yantai Andre Pectic Co., Ltd. are sold are sold
The solution being equipped with respectively in 2: 2: 1: 1 ratio, wherein thickener total concentration is 0.9%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved yet within 1 hour | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 5 minutes | All spread out |
Embodiment 20
20% trehalose, 79% kudzuvine root starch (production of Jiangxi Yu Ming agricultural product Co., Ltd), 1% Aspartame pass through mixing,
It crushes, granulation is subsequently placed in drying equipment and is heat-treated 2 minutes for 186 DEG C, then through whole grain, sieving dispenses and obtains instant kudzu vine powder production
Product.
The Instant kudzuvine root starch 4g of above-mentioned preparation is made an addition in 200ml warm water (60 DEG C), is stirred;Check experiment is that Jiangxi is beautiful
The solution that the kudzuvine root starch of tender tea leaves agricultural product Co., Ltd production is prepared, concentration 1.58%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 20 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 2 minutes | All spread out |
As can be seen from Fig. 3, instant kudzu vine powder manufactured in the present embodiment is completely dissolved after 2 minutes into the water (60 DEG C);And
The kudzuvine root starch of commercially available Jiangxi Yu Ming agricultural product Co., Ltd production, it is not instant (60 DEG C), and flake is more:
Embodiment 21
67% trehalose, 5% black tea extract, 25% skimmed milk power, 2% milk powder essence, 1% xanthan gum pass through mixed
It closes, crushes, granulation is subsequently placed in drying equipment and is heat-treated 8 minutes for 140 DEG C, then through whole grain, is sieved, and packing obtains instant milk tea
Beverage.
The Instant milk tea 40g of above-mentioned preparation is made an addition in 200ml warm water (60 DEG C), is stirred;Check experiment is with white
Granulated sugar substitutes trehalose completely, remaining ingredient is identical, the solution then prepared using identical technique production resulting product, dense
Degree is 20%:
As can be seen from Fig. 4: instant milk tea prepared by the present embodiment 21 enters water (60 DEG C) and is completely dispersed and comes, in 2 minutes
It is completely dissolved: and check experiment, concentration 20%, it is not instant to enter water (60 DEG C), and agglomeration of uniting.
Embodiment 22
70% trehalose, 30% isatis root extract (Jiangxi radically reform Han Ben Biotechnology Co., Ltd production) pass through mixed
It closes, crushes, be subsequently placed in drying equipment and be heat-treated 3 minutes for 210 DEG C, then through whole grain, sieving dispenses and obtains Radix Isatidis granules.
The Radix Isatidis granules can disperse immediately when reconstituting, and quickly dissolve, and occur entirely without flake phenomenon.With traditional Radix Isatidis
Electuary is compared, it can keep good mobility for more time, and will not agglomerate.
The Instant banlangen granules, banlangen keli 4g of above-mentioned preparation is made an addition in 200ml water, is stirred;Check experiment is radically reformed for Jiangxi
The banlangen granules, banlangen keli (2 bags are dissolved in 200ml water) of Han Ben Biotechnology Co., Ltd production:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 20 minutes | Sink to the bottom agglomeration |
The present invention | Without flake | It is completely dissolved within 2 minutes | All spread out |
Embodiment 23
50% trehalose, 50% eucommia ulmoides extracts (Jiangxi radically reform Han Ben Biotechnology Co., Ltd production), by trehalose
Eucommia ulmoides extract is added, is stirred, pelletizes, is subsequently placed in drying equipment and is heat-treated 40 minutes for 112 DEG C, then through whole grain, is sieved,
Packing obtains Duzhong agent.The Duzhong agent can disperse immediately when reconstituting, and quickly dissolve, and occur entirely without flake phenomenon.
And good mobility can be kept for more time, and will not agglomerate.
Embodiment 24
85% trehalose, 15% Bisacody (Hubei Bang Sheng Chemical Co., Ltd. is sold) are crushed, then by mixing
It is placed in drying equipment and is heat-treated 6 minutes for 131 DEG C, then through whole grain, sieving dispenses and obtains Bisacody granule.The product enters
Water can spread out, no adhesion, no flake.
Embodiment 25
98% trehalose, 2% bicyclic alcohols (are sold Beijing XieHe medicine Factory), by mixing, are crushed, whole grain is subsequently placed in baking
It is heat-treated 6 minutes for 138 DEG C in dry equipment, then through whole grain, sieving dispenses and obtains bicyclic alcohols granule.The product, which enters water, to be divided
It scatters and, no adhesion, no flake.
Embodiment 26
80% trehalose, 20% dihydroartemisinine (Kun Yao group is sold) are crushed by mixing, are subsequently placed in drying and set
It is heat-treated 4 minutes for 145 DEG C in standby, then through whole grain, sieving dispenses and obtains dihydroartemisinine granule.The product, which enters water, to be divided
It scatters and, no adhesion, no flake.
Embodiment 27
99% trehalose, 1% benorylate (Hubei Bang Sheng Chemical Co., Ltd. is sold) are crushed, are subsequently placed in by mixing
It is heat-treated 3 minutes for 175 DEG C in drying equipment, then through whole grain, sieving dispenses and obtains benorylate granule.It is i.e. complete that the product enters water
It spreads out entirely, no adhesion, no flake.
Embodiment 28
70% antierythrite, 30% sodium carboxymethylcellulose (Shanghai Shen optical eclipse is produced with Chemical Company), passes through
Mixing is subsequently placed in 150 DEG C drying and processing 5 minutes in drying equipment, then through whole grain, sieving obtains Instant carboxymethyl cellulose
Plain sodium.
The Instant sodium carboxymethylcellulose 2g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein carboxymethyl cellulose
The actual concentrations of plain sodium are 0.3%;Check experiment is the carboxylic produced using commercially available Shanghai Shen optical eclipse with Chemical Company
The solution that sodium carboxymethylcellulose pyce is formulated, concentration 0.3%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved yet within 1 hour | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 4 minutes | All spread out |
Embodiment 29
70% antierythrite, 30% isatis root extract (Jiangxi radically reform Han Ben Biotechnology Co., Ltd production) pass through mixed
It closes, crushes, granulation is subsequently placed in fluid unit, and lumen temperature maintains 126 degree and handles 20 minutes, then through whole grain, mistake
Sieve, packing obtain Radix Isatidis granules.
The Radix Isatidis granules can disperse immediately when reconstituting, and quickly dissolve, and occur entirely without flake phenomenon.With traditional Radix Isatidis
Electuary is compared, it can keep good mobility for more time, and will not agglomerate.
The Instant banlangen granules, banlangen keli 4g of above-mentioned preparation is made an addition in 200ml water, is stirred;Check experiment is radically reformed for Jiangxi
The banlangen granules, banlangen keli (2 bags are dissolved in 200ml water) of Han Ben Biotechnology Co., Ltd production:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 20 minutes | Sink to the bottom agglomeration |
The present invention | Without flake | It is completely dissolved within 2 minutes | All spread out |
Embodiment 30
45% antierythrite, 55% mocha extract (Jiangxi radically reform Han Ben Biotechnology Co., Ltd offer),
It by mixing, crushes, granulation is subsequently placed in 130 DEG C drying and processing 10 minutes in drying equipment, then through whole grain, sieving is dispensed
To instant mocha solid beverage.
The instant mocha solid beverage 20g of above-mentioned preparation is made an addition into 200ml warm water (60 DEG C), concentration is
10%, stirring;Check experiment is to substitute antierythrite completely with white granulated sugar, remaining ingredient is identical, then uses identical technique
The infusion that resulting product is prepared is produced, concentration 10%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 10 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 1 minute | All spread out |
Embodiment 31
75% antierythrite, 5% maltodextrin, (Club Biological Technology Group Co., Ltd is raw for 20% xanthan gum
Produce), 10% sodium carboxymethylcellulose (Shanghai Shen optical eclipse is produced with Chemical Company) is subsequently placed in drying by mixing
170 DEG C drying and processing 2 minutes in equipment, then through whole grain, sieving obtains Instant complex thickener.
The Instant complex thickener 4g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the reality of complex thickener
Border concentration is 0.6%;Check experiment be the xanthan gum that is produced using Club Biological Technology Group Co., Ltd with it is commercially available
Solution made of the sodium carboxymethylcellulose that optical eclipse Chemical Company in Shanghai Shen produces is compounded by 2: 1, concentration are
0.6%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved yet within 1 hour | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 4 minutes | All spread out |
Embodiment 32
10% antierythrite, 90% sodium carboxymethylcellulose (Shanghai Shen optical eclipse is produced with Chemical Company), passes through
Mixing crushes, and is subsequently placed in drying equipment and is heat-treated 2 minutes for 210 DEG C, then through whole grain, it is fine to obtain Instant carboxymethyl for sieving
Tie up plain sodium.
The Instant sodium carboxymethylcellulose 2g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein carboxymethyl cellulose
The actual concentrations of plain sodium are 0.9%;Check experiment is the carboxylic produced using commercially available Shanghai Shen optical eclipse with Chemical Company
The solution that sodium carboxymethylcellulose pyce is formulated, concentration 0.9%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 40 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 4 minutes | All spread out |
Embodiment 33
50% antierythrite, 50% Flos Chrysanthemi extract (Jiangxi radically reform Han Ben Biotechnology Co., Ltd production), will be red
Hang Zhou chrysanthemum flower extract is added in moss sugar alcohol, is stirred, and pelletizes, and is subsequently placed in drying equipment and is heat-treated 40 minutes for 112 DEG C, then through whole
Grain, sieving, packing obtain FLOS CHRYSANTHEMI ALBA from Haizhou of China granule.The FLOS CHRYSANTHEMI ALBA from Haizhou of China granule can disperse immediately when reconstituting, and quickly dissolve, entirely without fish
Eye phenomenon occurs.And good mobility can be kept for more time, and will not agglomerate.
Embodiment 34
99% antierythrite, 1% high acyl gellan gum (newly get over maritime business's industry Development Co., Ltd and sold in Guangzhou), by mixing,
It crushes, is subsequently placed in drying equipment and is heat-treated 40 minutes for 112 DEG C, then through whole grain, sieving obtains the high acyl gellan gum of Instant.
The Instant gellan gum 20g of above-mentioned preparation is made an addition in 200ml water, is stirred, wherein the actual concentrations of gellan gum
It is 0.1%;Check experiment newly to get over the solution that the gellan gum sold of maritime business's industry Development Co., Ltd is formulated using Guangzhou,
Concentration is 0.1%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 20 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 3 minutes | All spread out |
Embodiment 35
58% trehalose, 27% vegetable fat powder, (Jiangxi Han Ben Biotechnology Co., Ltd of radically reforming mentions 15% coffee-extract
For), it by mixing, crushes, granulation is subsequently placed in drying equipment and is heat-treated 4 minutes for 145 DEG C, then through whole grain, sieving is dispensed
To instant coffee solid beverage.
The Instant coffee 20g of above-mentioned preparation is made an addition in 200ml warm water (60 DEG C), concentration 10%, is stirred;Control
To substitute trehalose completely with white granulated sugar, remaining ingredient is identical for test, is then matched using identical technique production resulting product
The infusion of system, concentration 10%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 10 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 1 minute | All spread out |
Embodiment 36
85% trehalose, 15% mocha extract (Jiangxi radically reform Han Ben Biotechnology Co., Ltd offer) lead to
Mixing is crossed, is crushed, granulation is subsequently placed in drying equipment and is heat-treated 20 minutes for 112 DEG C, then through whole grain, sieving dispenses and obtains speed
Molten mocha solid beverage.
The instant mocha solid beverage 20g of above-mentioned preparation is made an addition into 200ml warm water (60 DEG C), concentration is
10%, stirring;Check experiment is to substitute trehalose completely with white granulated sugar, remaining ingredient is identical, then raw using identical technique
The infusion that resulting product is prepared is produced, concentration 10%:
Embodiment 37
83% trehalose, 15% green-tea extract [production of Fujian great Min (ZhangZhou) Food Co., Ltd], 2% jasmine pollen
Last essence is crushed by mixing, is subsequently placed in drying equipment and is heat-treated 4 minutes for 150 DEG C, then through whole grain, sieving is dispensed
To instant jasmine flower green tea solid beverage.
The instant jasmine flower green tea solid beverage 20g of above-mentioned preparation is made an addition in 200ml water, concentration 10%, is stirred;
Check experiment is to substitute trehalose completely with white granulated sugar, remaining ingredient is identical, then produces resulting production using identical technique
The jasmine flower green tea solution that product are prepared, concentration 10%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 10 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 1 minute | All spread out |
Embodiment 38
93% trehalose, 5% Pu'er tea [production of Fujian great Min (ZhangZhou) Food Co., Ltd], 2% tangerine peel powder
Last essence is crushed by mixing, is subsequently placed in drying equipment and is heat-treated 2 minutes for 210 DEG C, then through whole grain, sieving is dispensed
To instant tangerine peel Pu'er tea tea solid beverage.
The instant tangerine peel Pu'er tea tea solid beverage 20g of above-mentioned preparation is made an addition in 200ml water, concentration 10%, is stirred;
Check experiment is to substitute trehalose completely with white granulated sugar, remaining ingredient is identical, then produces resulting production using identical technique
The pericarpium citri reticulatae Pu-erh tea solution that product are prepared, concentration 10%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 10 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 1 minute | All spread out |
Embodiment 39
82% trehalose, 15% black tea extract [production of Fujian great Min (ZhangZhou) Food Co., Ltd], 2% lemon powder
Essence, 0.8% citric acid, 0.2% sodium citrate are crushed by mixing, are subsequently placed in drying equipment and are heat-treated 6 points for 130 DEG C
Clock, then through whole grain, sieving dispenses and obtains instant lemon black tea solid beverage.
The instant lemon black tea solid beverage 20g of above-mentioned preparation is made an addition in 200ml water, concentration 10%, is stirred;It is right
According to test to substitute trehalose completely with white granulated sugar, remaining ingredient is identical, then produces resulting product using identical technique
The lemon black solution of preparation, concentration 10%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 10 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 1 minute | All spread out |
Embodiment 40
67% trehalose, 5% black tea extract [production of Fujian great Min (ZhangZhou) Food Co., Ltd], 25% defatted milk
Powder, 2% milk powder essence, 1% xanthan gum are crushed by mixing, and granulation is subsequently placed in 140 DEG C of heat treatment 8 in drying equipment
Minute, then through whole grain, sieving dispenses and obtains instant milk tea beverage.
The Instant milk tea 40g of above-mentioned preparation is made an addition in 200ml warm water (60 DEG C), concentration 20%, is stirred;Control
To substitute trehalose completely with white granulated sugar, remaining ingredient is identical for test, is then matched using identical technique production resulting product
The milk tea solution of system, concentration 20%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 20 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 2 minutes | All spread out |
It can be seen in fig. 2 that: instant milk tea manufactured in the present embodiment enters water (60 DEG C) and is completely dispersed and comes, complete in 2 minutes
Fully dissolved: and check experiment, concentration 20%, it is not instant to enter water (60 DEG C), and agglomeration of uniting.
Embodiment 41
20% trehalose, 79% kudzuvine root starch (production of Jiangxi Yu Ming agricultural product Co., Ltd), 1% Aspartame pass through mixing,
It crushes, granulation is subsequently placed in drying equipment and is heat-treated 2 minutes for 186 DEG C, then through whole grain, sieving dispenses and obtains instant kudzu vine powder production
Product.
The Instant kudzuvine root starch 4g of above-mentioned preparation is made an addition in 200ml warm water (60 DEG C), is stirred;Check experiment is that Jiangxi is beautiful
The solution that the kudzuvine root starch of tender tea leaves agricultural product Co., Ltd production is prepared, concentration 1.58%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 20 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 2 minutes | All spread out |
It can be seen from figure 1 that instant kudzu vine powder manufactured in the present embodiment is completely dissolved after 2 minutes into the water (60 DEG C);And
The kudzuvine root starch of commercially available Jiangxi Yu Ming agricultural product Co., Ltd production, it is not instant (60 DEG C), and flake is more:
Embodiment 42
67.4% trehalose, 30% branched-chain amino acid, 2% citric acid, 0.6% Sucralose are crushed, so by mixing
It is placed in drying equipment and is heat-treated 8 minutes for 126 DEG C, then through whole grain, sieving dispenses and obtains instant amino acid solid beverage.
The instant amino acid solid beverage 20g of above-mentioned preparation is made an addition in 200ml water, concentration 10%, is stirred;Control
To substitute trehalose completely with white granulated sugar, remaining ingredient is identical for test, is then matched using identical technique production resulting product
The amino acid solution of system, concentration 10%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 10 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 1 minute | All spread out |
Embodiment 43
96% trehalose, 0.5%L- calcium lactate, 0.6% potassium chloride, 0.8% citric acid, 0.4% sodium citrate, 0.5%
Sodium chloride, 0.2% Sucralose, 0.3% vitamin C, 0.075% vitamin B6,0.045% vitamin B2,0.58% grapefruit
Powdered flavor is crushed by mixing, and granulation is subsequently placed in drying equipment and is heat-treated 5 minutes for 150 DEG C, then through whole grain, is sieved,
Packing obtains instant electrolyte solid beverage.
The instant electrolyte solid beverage 20g of above-mentioned preparation is made an addition in 200ml water, concentration 10%, is stirred;Control
To substitute trehalose completely with white granulated sugar, remaining ingredient is identical for test, is then matched using identical technique production resulting product
The electrolyte beverage of system, concentration 10%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 10 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 1 minute | All spread out |
Embodiment 44
10% trehalose, 40% coconut palm starch (offer of Guangzhou Jun Long group), 30% PURE WHEY, 20% milk powder, by mixed
It closes, crushes, granulation is subsequently placed in drying equipment and is heat-treated 6 minutes for 123 DEG C, then through whole grain, is sieved, and packing obtains instant coconut milk
Solid beverage.
The instant coconut milk solid beverage 20g of above-mentioned preparation is made an addition in 200ml water, concentration 10%, is stirred;Control examination
It tests to substitute trehalose completely with white granulated sugar, remaining ingredient is identical, is then prepared using identical technique production resulting product
Coconut milk solution, concentration 10%:
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 10 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 1 minute | All spread out |
Embodiment 45
57% trehalose, 20% Huajuhong extract (Jiangxi radically reform Han Ben Biotechnology Co., Ltd offer), 10%
Citric acid, 10% sodium carbonate, xanthan gum 1%, Aspartame 1%, 1% citrus powdered flavor are crushed by mixing, granulation, so
It is placed in drying equipment and is heat-treated 4 minutes for 150 DEG C, then through whole grain, sieving dispenses and obtains Huajuhong foaming solid beverage.
The Huajuhong foaming solid beverage 20g of above-mentioned preparation is made an addition in 200ml water, concentration 10%, is stirred;It is right
According to test to substitute trehalose completely with white granulated sugar, remaining ingredient is identical, then produces resulting product using identical technique
The Huajuhong solution of preparation, concentration 10%:
It can disperse immediately when the instant Huajuhong foaming solid beverage making, quickly dissolve, go out entirely without flake phenomenon
It is existing.Especially suitable for packed packaging.
Project | 10 minutes fish-eye numbers | Solubility test | Dispersibility |
Check experiment | Flake can not mostly be counted | It is not completely dissolved within 10 minutes | It unites agglomeration |
The present invention | Without flake | It is completely dissolved within 1 minute | All spread out |
Embodiment 46
99%% trehalose, 1% chrysanthemum extract (Jiangxi radically reform Han Ben Biotechnology Co., Ltd offer), by mixed
It closes, crushes, be subsequently placed in drying equipment and be heat-treated 4 minutes for 160 DEG C, then through whole grain, sieving dispenses and obtains instant chrysanthemum solid
Beverage.
The instant chrysanthemum solid beverage can disperse immediately, quickly dissolve, and occur entirely without flake phenomenon, and can the longer time
The features such as keeping good mobility, will not agglomerating.
Embodiment described above is certain preferred embodiments of the invention, is not made in any form to the present invention
Limitation.On the basis of the present invention, some modifications and optimization can be made to formula and technique.Therefore, without departing from spirit of that invention
The formula and technologic modification made and optimization, fall within the scope of the claimed invention.
Claims (17)
1. instant product, which is characterized in that according to the total weight of the instant product, the instant product includes:
1-90% (w/w), preferably 1-80% (w/w), 1-70% (w/w), 1-60% (w/w), 1-50% (w/w), 1-40% (w/
W), 1-30% (w/w), 1-20% (w/w) or 1-10%'s (w/w) is one or more to molten object, and
10-99% (w/w), preferably 10-89% (w/w), 10-79% (w/w), 10-69% (w/w), 10-59% (w/w), 10-
49% (w/w), 10-39% (w/w), 10-29% (w/w), the substance A of 10-19% (w/w), the substance A be selected from trehalose or
Antierythrite.
2. instant product described in claim 1, which is characterized in that the instant product be by substance A with after molten object mixes
In 112 DEG C~210 DEG C, preferably 112 DEG C -205 DEG C, 112 DEG C -200 DEG C, 112 DEG C -195 DEG C, 112 DEG C -190 DEG C, 112 DEG C -185
DEG C, 112 DEG C -180 DEG C, 112 DEG C -175 DEG C, 112 DEG C -170 DEG C, 112 DEG C -165 DEG C, 112 DEG C -160 DEG C, 112 DEG C -155 DEG C,
112 DEG C -150 DEG C, 112 DEG C -145 DEG C, 112 DEG C -140 DEG C, 112 DEG C -135 DEG C, 112 DEG C -130 DEG C, 112 DEG C -125 DEG C, 112
It dries and is made at DEG C -120 DEG C or 112 DEG C -115 DEG C.
3. instant product of any of claims 1 or 2, which is characterized in that described instant according to the total weight of the instant product
Product also includes 0-89% (w/w), preferably 0-79% (w/w), 0-69% (w/w), 0-59% (w/w), 0-49% (w/w), 0-
39% (w/w), the auxiliary material of 0-29% (w/w) or 0-19% (w/w).
4. instant product of any of claims 1 or 2, wherein described be selected from thickener or thickener blend composition, drug to molten object
Or pharmaceutical composition, or, raw-food material or food compositions.
5. the method for preparing instant product, comprising:
A) is mixed one or more to molten object with substance A, and the substance A is selected from trehalose or antierythrite, wherein according to
The total weight of the instant product, to molten object content be 1~90% (w/w), preferably 1-80% (w/w), 1-70% (w/w),
1-60% (w/w), 1-50% (w/w), 1-40% (w/w), 1-30% (w/w), 1-20% (w/w) or 1-10% (w/w);Substance
The content of A is 10~99% (w/w), preferably 10-89% (w/w), 10-79% (w/w), 10-69% (w/w), 10-59% (w/
W), 10-49% (w/w), 10-39% (w/w), 10-29% (w/w) or 10-19% (w/w);
B) by mixed material in 112 DEG C~210 DEG C, preferably 112 DEG C -200 DEG C, 112 DEG C -195 DEG C, 112 DEG C -190 DEG C, 112
DEG C -185 DEG C, 112 DEG C -180 DEG C, 112 DEG C -175 DEG C, 112 DEG C -170 DEG C, 112 DEG C -165 DEG C, 112 DEG C -160 DEG C, 112 DEG C -
155 DEG C, 112 DEG C -150 DEG C, 112 DEG C -145 DEG C, 112 DEG C -140 DEG C, 112 DEG C -135 DEG C, 112 DEG C -130 DEG C, 112 DEG C -125
DEG C, it is dried at 112 DEG C -120 DEG C or 112 DEG C -115 DEG C.
6. method described in claim 5, wherein described be selected from thickener or thickener blend composition, drug or medicine group to molten object
Object is closed, or, raw-food material or food compositions.
7. method described in claim 5 or 6, it is characterised in that by molten object, substance A is mixed with auxiliary material, excellent in step a)
Selection of land, the total weight based on instant product, the content of the auxiliary material are 0-89% (w/w), more preferable 0-79% (w/w), 0-
69% (w/w), 0-59% (w/w), 0-49% (w/w), 0-39% (w/w), 0-29% (w/w) or 0-19% (w/w).
8. method described in claim 5 or 6, it is characterised in that, will be to molten in step a) before, during or after mixing
Object, substance A and/or auxiliary material simultaneously or separately crush.
9. method described in claim 5 or 6, it is characterised in that, will be to molten in step a) before, during or after mixing
Object, substance A and/or auxiliary material separately or concurrently dissolve, and the solvent is selected from water or organic solvent.
10. method described in claim 5 or 6, which is characterized in that before carrying out step b), mixture is equal by stirring
Even, shear treatment, homogenization and/or centrifugal treating, then dry finishing.
11. method described in claim 5 or 6, which is characterized in that pelletize before drying.
12. method described in claim 5 or 6, it is characterised in that the method includes the steps c), carry out whole grain or sub-sieve.
13. instant product as claimed in claim 4 or method of claim 6, which is characterized in that the thickener is
The fermentation liquid of thickener, thickener extracting solution, thickener refined product or thickener semi-finished product.
14. instant product as claimed in claim 4 or method of claim 6, which is characterized in that the thickener choosing
The free group of following composition: xanthan gum, sodium carboxymethylcellulose, modified carboxy methyl cellulose sodium, pectin, sodium alginate,
Gellan gum, locust bean gum, guar gum, konjac glucomannan, konjaku powder, carragheen, Arabic gum, propylene glycol alginate, hydroxypropyl
Guar gum, casein sodium, tamarind gum, bassora gum, beta glucan, soybean polyoses, pullulan, condensation polysaccharide, yeast are more
Sugar, converted starch or their one or more any combination.
15. instant product as claimed in claim 4 or method of claim 6, it is characterised in that the drug or drug
Composition includes at least one pharmacy activity component, it is preferable that the pharmacy activity component is selected from compound, peptide, and nucleotide is planted
Object extract, Chinese medical extract or Chinese medical concrete.
16. instant product as claimed in claim 4 or method of claim 6, it is characterised in that the food or food
Composition include raw-food material, the raw-food material be selected from new resource food, plant extracts, dried fruit juice, Vegetable powder, tea powder,
Digested tankage or their one or more any combination.
17. instant product as claimed in claim 4 or method of claim 6, it is characterised in that the raw-food material choosing
The group of free following composition: food major ingredient, food ingredient, food additives or their one or more any combination.
Applications Claiming Priority (5)
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CN201710554592.5A CN107242425A (en) | 2017-07-07 | 2017-07-07 | A kind of solid beverage and preparation method thereof |
CN2017105542645 | 2017-07-07 | ||
CN2017105545925 | 2017-07-07 | ||
CN201710554264.5A CN107319510B (en) | 2017-07-07 | 2017-07-07 | Instant product and process for its preparation |
PCT/CN2018/084393 WO2019007138A1 (en) | 2017-07-07 | 2018-04-25 | Instant product and preparation method therefor |
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