CN109054973A - A kind of micro-emulsion cutting fluid, Preparation method and use - Google Patents
A kind of micro-emulsion cutting fluid, Preparation method and use Download PDFInfo
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- CN109054973A CN109054973A CN201811175449.6A CN201811175449A CN109054973A CN 109054973 A CN109054973 A CN 109054973A CN 201811175449 A CN201811175449 A CN 201811175449A CN 109054973 A CN109054973 A CN 109054973A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M173/00—Lubricating compositions containing more than 10% water
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/16—Antiseptic; (micro) biocidal or bactericidal
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/244—Metal working of specific metals
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/244—Metal working of specific metals
- C10N2040/245—Soft metals, e.g. aluminum
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/244—Metal working of specific metals
- C10N2040/246—Iron or steel
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
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Abstract
The present invention provides a kind of micro-emulsion cutting fluid, Preparation method and use.Micro-emulsion cutting fluid of the present invention, including the following each component of weight proportion: 6-8 parts of alkaline matter；6-9 parts of antirust agent；Hard water resistance dose 0.5-3 parts；4-6 parts of nonionic surfactant；10-15 parts of emulsifier；2-6 parts of extreme-pressure lubricant；10-50 parts of base oil；1-3 parts of fungicide；0.5-2 parts of metal inhibitor；20-60 parts of water.The invention also discloses the preparation methods of micro-emulsion cutting fluid simultaneously.Invention, which provides a kind of micro-emulsion cutting fluid, has good extreme boundary lubrication, cooling, antiseptic and rustproof, cleaning and other effects；It is nontoxic, free from extraneous odour, non-stimulated to skin, it is easy to use；Economical rationality can be used with the dilution of water high magnification numbe；It can prevent equipment from getting rusty and corroding, can effectively extend the service life of cutter and lathe；Anti-foaming property is good, and service life is long, and use cost is low.
Description
Technical field
The present invention relates to grinding technique more particularly to a kind of micro-emulsion cutting fluids, Preparation method and use.
Background technique
Micro-emulsion cutting fluid belongs to universal cutting fluid, is compounded by various ingredients, can be used for various material machining
Lubrication, cooling, cleaning and antirust.But currently, micro-emulsion cutting fluid it is different degrees of there are poor lubricity, cooling effects not
It is good, cleaning effect is poor, rustless property cannot be met the requirements, easily it is smelly the disadvantages of.
Summary of the invention
It is an object of the present invention to which for the poor lubricity of current micro-emulsion cutting fluid, cooling effect is bad, cleaning effect
Difference, rustless property cannot meet the requirements, easily smelly problems, propose a kind of micro-emulsion cutting fluid, the micro-emulsion cutting fluid
Grinding, machining or severe suitable for aluminium and the materials such as aluminium alloy, copper and its alloy, cast iron, carbon steel, steel alloy add
Work.
To achieve the above object, the technical solution adopted by the present invention is that: a kind of micro-emulsion cutting fluid, including weight proportion is such as
Under each component:
Further, the micro-emulsion cutting fluid, including the following each component of weight proportion:
Further, the alkaline matter is one of ethanol amine, sodium hydroxide, potassium hydroxide and sodium carbonate or a variety of
Mixing.
Further, the antirust agent is one of organic carboxylate, molybdate, borate, borate and phosphate
Or a variety of mixing.
Further, described hard water resistance dose is ethylenediamine tetra-acetic acid (EDTA) sodium salt, nitrilotriacetic acid (NTA) sodium salt and ammonia
One of three methylenephosphonic acid of base (ATMP) or a variety of mixing.
Further, the nonionic surfactant be fatty alcohol polyethenoxy ether class, induced by alkyl hydroxybenzene polyoxyethylene ether,
One of polypropylene glycol ethylene oxide adduct and fatty acid soaps or a variety of mixing.
Further, the emulsifier is one of polyol ester, petroleum sulfonate, alkylolamides and oleic acid or more
The mixing of kind.
Further, the extreme-pressure lubricant is phosphate, aliphatic ester, chlorinated paraffin, vulcanization grease and molybdenum compound
One of or a variety of mixing.
Further, the metal inhibitor is in organophosphorus ester, organosiloxane, benzotriazole and imidazoline
One or more mixing.
Further, the base oil is one of mineral oil, transformer oil and machinery oil or a variety of mixing.
Further, the fungicide is triazines, morpholine derivative, isothiazolinone, pyridines and iodo propinyl
One of butyl carbamate (IPBC) or a variety of mixing.
Further, the metal inhibitor is aluminium corrosion inhibiter.
Another object of the present invention also discloses a kind of preparation method of micro-emulsion cutting fluid, comprising the following steps:
Water is first added in reaction vessel step 1, and starting stirring successively puts into alkaline matter, hard water resistance according to the proportion
Agent, stir 5-30 minutes to being completely dissolved, preferably 10 minutes；
Step 2, under stiring successively puts into antirust agent, surfactant according to the proportion, is sufficiently stirred 10-30 minutes, excellent
It is selected as 20 minutes；
Step 3, under stiring successively puts into base oil, extreme-pressure lubricant, metal inhibitor, fungicide again according to the proportion,
10-30 minutes, preferably 20 minutes are sufficiently stirred；
Step 4, it is last emulsifier is slowly put into reaction vessel under stiring, stir 1 hour with complete up to solution
It is transparent, micro-emulsion cutting fluid is prepared.
Another object of the present invention also discloses a kind of micro-emulsion cutting fluid in aluminium and aluminium alloy, copper and its alloy, casting
Iron, carbon steel, the grinding of steel alloy, machining, severe manufacture field (the unmanageable mode such as tapping, drilling) are answered
With.
Further, the grinding micro-emulsion cutting fluid concentration is 2-4%wt.
Further, the machining micro-emulsion cutting fluid concentration is 3-5%wt.
Further, the machining micro-emulsion cutting fluid concentration is 5-10%wt.
Further, be suitable for various general-purpose grinders, the various grindings of numerical control special purpose grinder and turning, milling etc. it is light plus
Work and the processing of middle load.
1. selecting cleaning agent appropriate thoroughly to wash original gold in hopper and equipment using before micro-emulsion cutting fluid
Belong to working fluid, chip and dirt.If hopper by biological pollution, can be selected suitable fungicide and carry out sterilization processing.
Solution recycles 30 minutes, then discharges.It can be used after being finally incorporated the working solution cycle balance of this product.
2. preparation method: diluting this product according to a certain percentage using clean tap water, stir evenly, after emulsifying completely i.e.
It can be used.
3. being recommended to use concentration:
Grinding: 2%~4%.Moderate processing: 3%~5%.
Sawing: 3%~5%.Severe processing: 5%~10%.
Concentration can be used according to adjustment such as material, the processing requests of workpieces processing.
4. the daily maintenance of case liquid: when case liquid requires supplementation with, the microemulsified that corresponding proportion is added while water should be added to cut
Liquid is cut, the oil slick for answering chip in timely removing case liquid and lathe to leak out during use, the pH value of periodic monitoring case liquid and dense
Degree, and suitably supplement or more renew liquid.
Points for attention when use:
Working solution should keep cleaning, good ventilation, and lathe should have complete filtering, slag removing system, remove iron filings in time, float
The impurity such as oil periodically should carry out idle loop and oxygenation to case liquid if lathe more days do not start；Prevent from freezing, if this product compared with
It is cold or store at a temperature of can freezing, it may be layered or retrogradation.But properties of product will not change.Before use, being warmed to
Room temperature simultaneously can thoroughly use after stirring；Child getting in contact is avoided even to wrongly take.
Micro-emulsion cutting fluid of the present invention, has the advantage that compared with prior art
1) micro-emulsion cutting fluid of the present invention has good extreme boundary lubrication, cooling, antiseptic and rustproof, cleaning and other effects；This hair
Contain special surfactant component in bright micro-emulsion cutting fluid, there is good cleaning performance, so that the workpiece after processing
Surface keeps clean.
Micro-emulsion cutting fluid of the present invention extreme-pressure lubricant containing there are many, can provide excellent lubricity, it might even be possible to full
The highly difficult processing method of foot, the processing to drill such as tapping
2) micro-emulsion cutting fluid of the present invention is nontoxic, free from extraneous odour, non-stimulated to skin, easy to use；
3) micro-emulsion cutting fluid economical rationality of the present invention can be used with the dilution of water high magnification numbe；
4) micro-emulsion cutting fluid of the present invention can prevent equipment from getting rusty and corroding, and can effectively extend the use longevity of cutter and lathe
Life；The antirust component that emulsion cutting fluid of the present invention contains has excellent rustless property, can effectively prevent invading for harmful substance
Erosion is played the role of protecting workpiece.
5) anti-foaming property is good, and service life is long, and use cost is low；
In short, micro-emulsion cutting fluid of the present invention has several big advantages: excellent lubrication compared with existing similar-type products
Property, improve drilling tool, the service life of lathe and the machining accuracy of workpiece；Good cooling results do not generate oil smoke, operate visibility
By force；Cleaning effect is good, and the effective greasy dirt removed on workpiece and lathe improves workpiece surface finish, mitigate machine maintenance at
This.Excellent rustless property meets the antirust requirement in machining process between the antirust and process of workpiece；Unique sterilization body
It is smelly to can effectively prevent working fluid corruption under hot environment so that the anti-microbial property of product is prominent for system.It is cut as microemulsified
Liquid overcomes synthetic cutting fluid greasy property difference and the perishable smelly disadvantage of oil emulsion, is answered extensively in many industries
With.
Specific embodiment
The present invention is further described with reference to embodiments:
Embodiment 1
Present embodiment discloses a kind of micro-emulsion cutting fluids, including the following each component of weight proportion:
The alkaline matter is the mixing of potassium hydroxide and ethanol amine that mass ratio is 1:1, and the antirust agent is mass ratio
Organic carboxylate and phosphatic mixing for 1:2, described hard water resistance dose is nitrilotriacetic acid (NTA) sodium salt, the nonionic
Surfactant is fatty acid soaps, and the emulsifier is the mixing of polyol ester and oleic acid that mass ratio is 1:1, the extreme pressure profit
Lubrication prescription is phosphate, and the metal inhibitor is organophosphorus ester, and the base oil is machinery oil, and the fungicide is mass ratio
For the mixing of the isothiazolinone of 1:1:3, pyridines and iodopropynyl butyl formate.
The preparation method of the micro-emulsion cutting fluid, which comprises the following steps:
Water is first added in reaction vessel step 1, and starting stirring successively puts into alkaline matter, hard water resistance dose, stirring 10
Minute to being completely dissolved；
Step 2, under stiring successively puts into antirust agent, surfactant, is sufficiently stirred 20 minutes；
Step 3, under stiring, then base oil, extreme-pressure lubricant, metal inhibitor, fungicide are successively put into, it is sufficiently stirred
20 minutes；
Step 4, it is last emulsifier is slowly put into reaction vessel under stiring, stirring at least 1 hour is complete to solution
It is transparent.
Being detected micro-emulsion cutting fluid of the present invention is amber thick liquid, density 1.000g/cm3.Following detection
Mesh presses 3%wt dilution:
Transparency: transparent
PH value: 9.6
Surface tension: 31.12mN/m
Spumescence :≤2ml/10min
Corrosivity (55 ± 2 DEG C, cast iron, red copper, aluminium are complete to soak): qualified
Rust-preventing characteristic (35 ± 2 DEG C, RH > 95%, cast iron, monolithic, lamination): qualified
Embodiment 2
Present embodiment discloses a kind of micro-emulsion cutting fluids, including the following each component of weight proportion:
Wherein, the alkaline matter is the mixing of ethanol amine and sodium hydroxide that mass ratio is 2:1, and the antirust agent is matter
For amount than the mixing of the organic carboxylate and molybdate that are 1:2, described hard water resistance dose is ethylenediamine tetra-acetic acid that mass ratio is 1:1
(EDTA) sodium salt and nitrilotriacetic acid (NTA) sodium salt, the nonionic surfactant are the fatty alcohol polyoxy that mass ratio is 1:3
The mixing of ethylene ethers and induced by alkyl hydroxybenzene polyoxyethylene ether, the emulsifier are the alkylolamides and oil that mass ratio is 1:1.5
The mixing of acid, the extreme-pressure lubricant is the mixing of chlorinated paraffin and phosphate that mass ratio is 2:1, and the metal inhibitor is
Mass ratio is the mixing of the organophosphorus ester and imidazoline of 2:3, and the base oil is mineral oil, and the fungicide is that mass ratio is
The triazines of 1:3 and the mixing of iodopropynyl butyl formate.
The preparation method of the micro-emulsion cutting fluid, which comprises the following steps:
Water is first added in reaction vessel step 1, and starting stirring successively puts into alkaline matter, hard water resistance dose, stirring 10
Minute to being completely dissolved；
Step 2, under stiring successively puts into antirust agent, surfactant, is sufficiently stirred 20 minutes；
Step 3, under stiring, then base oil, extreme-pressure lubricant, metal inhibitor, fungicide are successively put into, it is sufficiently stirred
20 minutes；
Step 4, it is last emulsifier is slowly put into reaction vessel under stiring, stirring 2 hours are completely saturating to solution
It is bright.
Being detected micro-emulsion cutting fluid of the present invention is amber thick liquid, density 1.000g/cm3.Following detection
Mesh presses 3%wt dilution:
Transparency: transparent
PH value: 9.6
Surface tension: 33.11mN/m
Spumescence :≤2ml/10min
Corrosivity (55 ± 2 DEG C, cast iron, red copper, aluminium are complete to soak): qualified
Rust-preventing characteristic (35 ± 2 DEG C, RH > 95%, cast iron, monolithic, lamination): qualified
Finally, it should be noted that the above embodiments are only used to illustrate the technical solution of the present invention., rather than its limitations；To the greatest extent
Pipe present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that: its according to
So be possible to modify the technical solutions described in the foregoing embodiments, or to some or all of the technical features into
Row equivalent replacement；And these are modified or replaceed, various embodiments of the present invention technology that it does not separate the essence of the corresponding technical solution
The range of scheme.
Claims (10)
1. a kind of micro-emulsion cutting fluid, which is characterized in that including the following each component of weight proportion:
2. micro-emulsion cutting fluid according to claim 1, which is characterized in that the alkaline matter be ethanol amine, sodium hydroxide,
One of potassium hydroxide and sodium carbonate or a variety of mixtures.
3. micro-emulsion cutting fluid according to claim 1, which is characterized in that the antirust agent be organic carboxylate, molybdate,
One of borate, borate and phosphate or a variety of mixing.
4. micro-emulsion cutting fluid according to claim 1, which is characterized in that described hard water resistance dose is sodium ethylene diamine tetracetate
One of salt, nitrilotriacetic acid sodium salt and aminotrimethylenephosphonic acid or a variety of mixtures.
5. micro-emulsion cutting fluid according to claim 1, which is characterized in that the nonionic surfactant is poly alkyl alcohol
One of ethylene oxide ethers, alkyl phenol polyoxyethylene ether class, polypropylene glycol ethylene oxide adduct and fatty acid soaps are a variety of
Mixing.
6. micro-emulsion cutting fluid according to claim 1, which is characterized in that the emulsifier is polyol ester, mahogany acid
One of salt, alkylolamides and oleic acid or a variety of mixing.
7. micro-emulsion cutting fluid according to claim 1, which is characterized in that the metal inhibitor is organophosphorus ester, has
One of organic siloxane, benzotriazole and imidazoline or a variety of mixing.
8. micro-emulsion cutting fluid according to claim 1, which is characterized in that the fungicide be triazines, morpholine derivative,
One of isothiazolinone, pyridines and iodopropynyl butyl formate or a variety of mixing.
9. a kind of preparation method of micro-emulsion cutting fluid described in claim 1-8 any one, which is characterized in that including following step
It is rapid:
Water is first added in reaction vessel step 1, and starting stirring successively puts into alkaline matter, hard water resistance dose according to the proportion, stirs
5-30 minutes are mixed to being completely dissolved；
Step 2, under stiring successively puts into antirust agent, surfactant according to the proportion, is sufficiently stirred 10-30 minutes；
Step 3, under stiring successively puts into base oil, extreme-pressure lubricant, metal inhibitor, fungicide according still further to proportion, sufficiently
Stirring 10-30 minutes；
Step 4, it is last emulsifier is slowly put into reaction vessel under stiring, stir 1 hour with completely saturating up to solution
It is bright, micro-emulsion cutting fluid is prepared.
10. micro-emulsion cutting fluid described in a kind of claim 1-8 any one is in aluminium and aluminium alloy, copper and its alloy, cast iron, carbon
The grinding of steel or steel alloy, the application of machining, severe manufacture field.
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Cited By (7)
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| CN110257144A (en) * | 2019-07-10 | 2019-09-20 | 东莞市晶索润滑科技有限公司 | It is a kind of for copper and its cutting fluid of alloy and preparation method thereof |
| CN111484891A (en) * | 2020-04-26 | 2020-08-04 | 北美防锈技术（上海）有限公司 | Emulsified anti-rust oil |
| CN111732994A (en) * | 2020-07-21 | 2020-10-02 | 南京正明观新材料有限公司 | Water-based metal machining cutting fluid for steel and aluminum and preparation method thereof |
| CN112852521A (en) * | 2021-01-11 | 2021-05-28 | 陈雪莲 | Method for preventing metal working fluid from smelling by adopting biological balance technology |
| CN113736551A (en) * | 2021-09-08 | 2021-12-03 | 长沙艾森设备维护技术有限公司 | Metal extrusion tapping liquid |
| CN115058283A (en) * | 2022-06-27 | 2022-09-16 | 重庆信人科技发展有限公司 | High-performance cutting fluid for aviation mixed processing |
| CN115820331A (en) * | 2022-11-23 | 2023-03-21 | 俄美达（武汉）有限公司 | Cutting fluid for gem processing and preparation method thereof |
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| CN110257144A (en) * | 2019-07-10 | 2019-09-20 | 东莞市晶索润滑科技有限公司 | It is a kind of for copper and its cutting fluid of alloy and preparation method thereof |
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| CN112852521A (en) * | 2021-01-11 | 2021-05-28 | 陈雪莲 | Method for preventing metal working fluid from smelling by adopting biological balance technology |
| CN113736551A (en) * | 2021-09-08 | 2021-12-03 | 长沙艾森设备维护技术有限公司 | Metal extrusion tapping liquid |
| CN115058283A (en) * | 2022-06-27 | 2022-09-16 | 重庆信人科技发展有限公司 | High-performance cutting fluid for aviation mixed processing |
| CN115820331A (en) * | 2022-11-23 | 2023-03-21 | 俄美达（武汉）有限公司 | Cutting fluid for gem processing and preparation method thereof |
| CN115820331B (en) * | 2022-11-23 | 2023-07-28 | 俄美达（武汉）有限公司 | Cutting fluid for precious stone processing and preparation method thereof |
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