CN109054969A - A kind of water solubility micro-emulsion cutting fluid and preparation method thereof - Google Patents

A kind of water solubility micro-emulsion cutting fluid and preparation method thereof Download PDF

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Publication number
CN109054969A
CN109054969A CN201810693177.2A CN201810693177A CN109054969A CN 109054969 A CN109054969 A CN 109054969A CN 201810693177 A CN201810693177 A CN 201810693177A CN 109054969 A CN109054969 A CN 109054969A
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water
cutting fluid
emulsion cutting
micro
oil
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杨伟帅
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Suzhou Rui Qili New Material Co Ltd
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Suzhou Rui Qili New Material Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
    • C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/108—Polyethers, i.e. containing di- or higher polyoxyalkylene groups etherified
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/08—Halogenated waxes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/08—Amides
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/223—Five-membered rings containing nitrogen and carbon only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/225—Heterocyclic nitrogen compounds the rings containing both nitrogen and oxygen
    • C10M2215/226—Morpholines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/10—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring
    • C10M2219/104—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring containing sulfur and carbon with nitrogen or oxygen in the ring
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/04—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions having a silicon-to-carbon bond, e.g. organo-silanes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/16—Antiseptic; (micro) biocidal or bactericidal
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/20—Metal working
    • C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of water-soluble micro-emulsion cutting fluids, including following component by weight: base oil 20~50%, oiliness improver 3~10%, anionic surfactant 3~10%, nonionic surfactant 3~10%, triethanolamine 3~5%, oleamide 1~5%, chlorinated paraffin 0~15%, anticorrosion and bactericidal agent 1~3%, benzotriazole corrosion inhibiter 0.1~0.2%, organic silicon defoamer 0~0.2%, water softener 0.1~0.5%, cosolvent 3~10%, deionized water 10~50%.The present invention is free of sodium nitrite, and stability is good, and antibiotic property is strong, harmless to skin without pessimal stimulation, applicable various high load capacities processing and steel, cast iron, aluminium vehicle, cut, grind, drilling, processing, the comprehensive performance such as tapping it is strong.

Description

A kind of water solubility micro-emulsion cutting fluid and preparation method thereof
Technical field
The present invention relates to cutting fluid technical field, especially a kind of water-soluble micro-emulsion cutting fluid and preparation method thereof.
Background technique
In process of metal working, in order to reduce cutting force when cutting, take away in time in cutting region generate heat with Cutting temperature is reduced, tool life is improved, to improve production efficiency, improves workpiece surface roughness, guarantees work pieces process Precision reaches optimal economic effect, usually using metal working fluid.Metal and its alloy are in cutting, forming, processing and protection Etc. industrial type fluid used in processes, be referred to as cutting fluid.
Micro-emulsion cutting fluid is also known as semi-synthetic cutting fluid, and between emulsion cutting fluid and fully synthetic cutting fluid, it is had concurrently The lubricity of emulsion cutting fluid, and have the cleaning of fully synthetic cutting fluid concurrently.The row access cycle of micro-emulsion cutting fluid is obvious It is longer than emulsion cutting fluid." the deposit alkali number " of one side micro-emulsion cutting fluid may be significantly raising, up to emulsification cutting The several times of liquid.On the other hand, the pH value of micro-emulsion cutting fluid opposite can also improve.This " alkaline reserve amount " makes micro-emulsion cutting fluid exist In continuous use, it is not easy to which rancid rotten, service life extends.The micro-emulsion cutting fluid of general single machine slot, can make in summer With 3~April, and multimachine large trough, under the premise of non-adding of germicide, service life is up to more than half a year.In addition, microemulsified is cut Liquid is due to " alkaline reserve amount " height, so the rust-preventing characteristic of its aqueous solution is also substantially better than emulsion cutting fluid.
In the machining flexible manufacturing system introduced at home, available is nearly all emulsion cutting fluid and microemulsified Cutting fluid, and micro-emulsion cutting fluid is more dominant compared to emulsion cutting fluid, it not only has, and to be not easy smelly, longer life expectancy etc. excellent Point also has better cleaning performance and to the better protective value of lathe.Currently, the product of domestic micro-emulsion cutting fluid is ground Hair and production have also reached certain level, and occupation rate of market is also constantly rising.
Summary of the invention
The purpose of the present invention is to provide a kind of water-soluble micro-emulsion cutting fluids and preparation method thereof.The cutting fluid is without Asia Sodium nitrate, stability is good, and antibiotic property is strong, and to skin without pessimal stimulation, harmless, comprehensive performance is strong.
Technical scheme is as follows:
Base oil 20~50%
Oiliness improver 3~10%
Anionic surfactant 3~10%
Nonionic surfactant 0~10%
Triethanolamine 3~5%
Oleamide 1~5%
Chlorinated paraffin 0~15%
Anticorrosion and bactericidal agent 1~3%
Benzotriazole corrosion inhibiter 0.1~0.2%
Organic silicon defoamer 0~0.2%
Water softener 0.1~0.5%
Cosolvent 3~10%
Deionized water 10~50%
The preparation method of the water solubility micro-emulsion cutting fluid, comprising the following steps:
(1) base oil, oiliness improver and anionic surfactant, nonionic surfactant are first subjected to microemulsified, stirring is extremely Homogeneous transparent, it is spare；
(2) suitable deionized water will first be added in blender, under low speed state, is successively slowly added to oleamide, benzene Triazole corrosion inhibiter, water softener, triethanolamine, chlorinated paraffin, anticorrosion and bactericidal agent and cosolvent are heated to 40 ~ 60 DEG C, and stirring makes It is completely dissolved；
(3) mixed liquor of step (1) is poured slowly into step (2), then stirring at normal temperature to homogeneous transparent is added organic Silicon defoaming agent stirs 10 ~ 20 minutes.
Above-mentioned cutting fluid, used base oil be 5-32# base oil, 22# bobbin oil, 5# white oil it is one such, two Kind or two or more compositions.
Above-mentioned cutting fluid, used oiliness improver be oleic acid, tall oil, ricinoleic acid it is one such, two kinds or two kinds Composition.
Above-mentioned cutting fluid, used anionic surfactant are petroleum sodium sulfonate, barium mahogany sulfonate, sulfonic acid castor oil Equal sulfonate series is one such, two or more composition.
Above-mentioned cutting fluid, used nonionic surfactant are fatty alcohol polyoxyethylene ether.
Above-mentioned cutting fluid, used anticorrosion and bactericidal agent are morpholine derivative (MBM) and 1,2- phenylpropyl alcohol isothiazoline -3- ketone (BIT) mass ratio of the anticorrosion and bactericidal agent compounded, MBM and BIT are 10:1 ~ 4:1.
Above-mentioned cutting fluid, used water softener are disodium edta.
Beneficial effects of the present invention:
The cutting fluid can play a protective role to copper using benzotriazole；Using compounding MBM and BIT anticorrosion and bactericidal agent, greatly improve The service life of product, central fluid supply can be recycled for a long time；Applicable various high load capacity processing and steel, cast iron, aluminium The vehicle of material is cut, grinds, drilling, the processing such as tapping, and comprehensive performance is strong.
Specific embodiment
The technical solution in present example will be clearly and completely described below, it is clear that described embodiment It is only a part of the embodiments of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field All other embodiment that art personnel are obtained without making creative work, shall fall within the protection scope of the present invention.
Embodiment 1
A kind of water solubility micro-emulsion cutting fluid, it is characterised in that: including following components by weight:
22# bobbin oil 31%
Oleic acid 4%
Petroleum sodium sulfonate 10%
Fatty alcohol polyoxyethylene ether 3%
Triethanolamine 2%
Oleamide 4%
Chlorinated paraffin 10%
MBM 2%
BIT 0.2%
Benzotriazole corrosion inhibiter 0.2%
Organic silicon defoamer 0.2%
Water softener 0.4%
Cosolvent 3%
Deionized water 30%
The preparation method of the water solubility micro-emulsion cutting fluid, comprising the following steps:
(1) base oil, oiliness improver and anionic surfactant, nonionic surfactant are first subjected to microemulsified, stirring is extremely Homogeneous transparent, it is spare；
(2) suitable deionized water will first be added in blender, under low speed state, is successively slowly added to oleamide, benzene Triazole corrosion inhibiter, water softener, triethanolamine, 7 wax of chlorination stone, anticorrosion and bactericidal agent and cosolvent are heated to 40 ~ 60 DEG C, stirring It makes it completely dissolved；
(3) mixed liquor of step (1) is poured slowly into step (2), then organosilicon is added in stirring at normal temperature to homogeneous transparent Defoaming agent stirs 10 ~ 20 minutes.
Embodiment 2
A kind of water solubility micro-emulsion cutting fluid, it is characterised in that: including following components by weight:
22# bobbin oil 26%
Appropriate youngster's oil 8%
Petroleum sodium sulfonate 12%
Fatty alcohol polyoxyethylene ether 2%
Triethanolamine 2%
Oleamide 4%
Chlorinated paraffin 10%
MBM 2%
BIT 0.2%
Benzotriazole corrosion inhibiter 0.2%
Organic silicon defoamer 0.2%
Water softener 0.4%
Cosolvent 3%
Deionized water 30%
The preparation method is the same as that of Example 1 for the water solubility micro-emulsion cutting fluid.
Embodiment 3
A kind of water solubility micro-emulsion cutting fluid, it is characterised in that: including following components by weight:
5# white oil 25%
Oleic acid 5%
Petroleum sodium sulfonate 10%
Fatty alcohol polyoxyethylene ether 7%
Triethanolamine 2%
Oleamide 5%
Chlorinated paraffin 10%
MBM 2%
BIT 0.2%
Benzotriazole corrosion inhibiter 0.2%
Organic silicon defoamer 0.2%
Water softener 0.4%
Cosolvent 3%
Deionized water 30%
The preparation method is the same as that of Example 1 for the water solubility micro-emulsion cutting fluid.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks Domain is included within the scope of the present invention.

Claims (8)

1. a kind of water solubility micro-emulsion cutting fluid, it is characterised in that: including following components by weight:
Base oil 20~50%
Oiliness improver 3~10%
Anionic surfactant 3~10%
Nonionic surfactant 3~10%
Triethanolamine 3~5%
Oleamide 1~5%
Chlorinated paraffin 0~15%
Anticorrosion and bactericidal agent 1~3%
Benzotriazole corrosion inhibiter 0.1~0.2%
Organic silicon defoamer 0~0.2%
Water softener 0.1~0.5%
Cosolvent 3~10%
Deionized water 10~50%.
2. a kind of water-soluble micro-emulsion cutting fluid according to claim 1, which is characterized in that used base oil is 5- 32# base oil, 22# bobbin oil, 5# white oil be one such, two or more composition.
3. a kind of water-soluble micro-emulsion cutting fluid according to claim 1, which is characterized in that used oiliness improver is oil Acid, tall oil, ricinoleic acid be one such, two or more composition.
4. a kind of water-soluble micro-emulsion cutting fluid according to claim 1, which is characterized in that used anionic surface Activating agent be the sulfonate series such as petroleum sodium sulfonate, barium mahogany sulfonate, sulfonic acid castor oil it is one such, two or more Composition.
5. a kind of water-soluble micro-emulsion cutting fluid according to claim 1, which is characterized in that used non-ionic surface Activating agent is fatty alcohol polyoxyethylene ether.
6. a kind of water-soluble micro-emulsion cutting fluid according to claim 1, which is characterized in that used anticorrosion and bactericidal agent For morpholine derivative (MBM) and 1, the anticorrosion and bactericidal agent of 2- phenylpropyl alcohol isothiazoline -3- ketone (BIT) compounding, the quality of MBM and BIT Than for 10:1 ~ 4:1.
7. a kind of water-soluble micro-emulsion cutting fluid according to claim 1, which is characterized in that used water softener is Disodium edta.
8. a kind of preparation method of water-soluble micro-emulsion cutting fluid according to claim 1, which is characterized in that including following Step:
(1) base oil, oiliness improver and anionic surfactant, nonionic surfactant are first subjected to microemulsified, stirring is extremely Homogeneous transparent, it is spare；
(2) suitable deionized water will first be added in blender, under low speed state, is successively slowly added to oleamide, benzene Triazole corrosion inhibiter, water softener, triethanolamine, chlorinated paraffin, anticorrosion and bactericidal agent and cosolvent are heated to 40 ~ 60 DEG C, and stirring makes It is completely dissolved；
(3) mixed liquor of step (1) is poured slowly into step (2), then organosilicon is added in stirring at normal temperature to homogeneous transparent Defoaming agent stirs 10 ~ 20 minutes.
CN201810693177.2A 2018-06-29 2018-06-29 A kind of water solubility micro-emulsion cutting fluid and preparation method thereof Pending CN109054969A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115651744A (en) * 2022-08-22 2023-01-31 安徽启明表面技术有限公司 Environment-friendly microemulsion cutting fluid
CN115873654A (en) * 2022-12-01 2023-03-31 滁州默尔新材料科技有限公司 Preparation method of photovoltaic glass cutting fluid with good lubricating effect

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CN101240218A (en) * 2008-02-29 2008-08-13 益田润石（北京）化工有限公司 Emulsification type metal cutting liquor composition
CN103031195A (en) * 2011-10-10 2013-04-10 洛科斯润滑油（上海）有限公司 Microemulsion cutting fluid
CN103897791A (en) * 2013-11-11 2014-07-02 东南大学 Preparation raw materials and method of chloride-free extreme-pressure microemulsion cutting fluid
CN104312707A (en) * 2014-10-17 2015-01-28 江苏鑫露新材料股份有限公司 Micro-emulsified water-soluble cutting fluid and preparation method thereof
CN107011962A (en) * 2017-06-08 2017-08-04 苏州瑞奇丽新材料有限公司 A kind of aqueous lubricating oil

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101240218A (en) * 2008-02-29 2008-08-13 益田润石（北京）化工有限公司 Emulsification type metal cutting liquor composition
CN103031195A (en) * 2011-10-10 2013-04-10 洛科斯润滑油（上海）有限公司 Microemulsion cutting fluid
CN103897791A (en) * 2013-11-11 2014-07-02 东南大学 Preparation raw materials and method of chloride-free extreme-pressure microemulsion cutting fluid
CN104312707A (en) * 2014-10-17 2015-01-28 江苏鑫露新材料股份有限公司 Micro-emulsified water-soluble cutting fluid and preparation method thereof
CN107011962A (en) * 2017-06-08 2017-08-04 苏州瑞奇丽新材料有限公司 A kind of aqueous lubricating oil

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115651744A (en) * 2022-08-22 2023-01-31 安徽启明表面技术有限公司 Environment-friendly microemulsion cutting fluid
CN115651744B (en) * 2022-08-22 2023-06-30 安徽启明表面技术有限公司 Environment-friendly microemulsion cutting fluid
CN115873654A (en) * 2022-12-01 2023-03-31 滁州默尔新材料科技有限公司 Preparation method of photovoltaic glass cutting fluid with good lubricating effect
CN115873654B (en) * 2022-12-01 2023-12-15 滁州默尔新材料科技有限公司 Preparation method of photovoltaic glass cutting fluid with good lubricating effect

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Application publication date: 20181221