CN109047750A - The preparation method of 310 powder of stainless steel feeding of environment-friendly type and 310 powder of stainless steel components - Google Patents

The preparation method of 310 powder of stainless steel feeding of environment-friendly type and 310 powder of stainless steel components Download PDF

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Publication number
CN109047750A
CN109047750A CN201810792375.4A CN201810792375A CN109047750A CN 109047750 A CN109047750 A CN 109047750A CN 201810792375 A CN201810792375 A CN 201810792375A CN 109047750 A CN109047750 A CN 109047750A
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China
Prior art keywords
stainless steel
powder
feeding
parts
preparation
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CN201810792375.4A
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Chinese (zh)
Inventor
张伟明
张柯
庞前列
Original Assignee
Dongguan Jinsheng Precision Electronic Components Ltd
Guangdong Janus Intelligent Group Corp Ltd
Dongguan Huajing Powder Metallurgy Co Ltd
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Application filed by Dongguan Jinsheng Precision Electronic Components Ltd, Guangdong Janus Intelligent Group Corp Ltd, Dongguan Huajing Powder Metallurgy Co Ltd filed Critical Dongguan Jinsheng Precision Electronic Components Ltd
Priority to CN201810792375.4A priority Critical patent/CN109047750A/en
Publication of CN109047750A publication Critical patent/CN109047750A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/10Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
    • B22F1/102Metallic powder coated with organic material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/10Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
    • B22F1/108Mixtures obtained by warm mixing

Abstract

The present invention relates to a kind of 310 powder of stainless steel feedings of environment-friendly type and preparation method thereof, including 310 powder of stainless steel and forming agent, the two to prepare by weight the ratio of 100:2~100:5;The granularity of 310 powder of stainless steel is 500 mesh, tap density 4.5-4.8g/cm3, used auxiliary material when sintered carbide ball is planetary ball mill machine mixing accounts for the 30%-50% of all material total weight.The diameter 5mm-10mm of the sintered carbide ball.The invention has the advantages that passing through 310 stainless steel metal powder pressing forming feedings of invention and preparation method, change traditional 310 stainless steels, processing difficulties, process-cycle is long, the high disadvantage of processing cost, the production and processing cost for greatly reducing by 310 stainless steel parts of complexity responds country and calls, and improves domestic manufacturing industry technological innovation production level.

Description

The preparation of 310 powder of stainless steel feeding of environment-friendly type and 310 powder of stainless steel components Method
Technical field
The present invention relates to the preparation methods of a kind of 310 powder of stainless steel feedings and 310 powder of stainless steel feeding components.
Background technique
With being constantly progressive for social science and technology and flourishing for global industry, powder metallurgical production technique is all due to its More advantages, industry development is rapid, and technology has been widely used in the fields such as military affairs, traffic, machinery, electronics, space flight, aviation.
Feeding be metal powder metallurgy product preparation core head section technique, the preparation method of feeding be by metal powder with The two according to a certain percentage, under certain condition, is homogenously mixed together by forming agent using equipment.
310 stainless steel materials, because of manufactured fabricated part, corrosion-resistant and high-temperature resistant, processing performance is good, therefore is widely used in Fiber optic communication industry, furniture decoration industry and food medical treatment etc. industry.
Because of traditional 310 stainless steel parts manufacturing methods (vehicle mill, is milled, cut, sparking etc. machining), production efficiency Low, processing difficulties processing cost is high, and certain complicated products, which can't process, to be come, and is unable to satisfy modern society's system completely Make the high speed development demand of industry.
Summary of the invention
To overcome the shortcomings of existing technologies, the present invention provides 10 powder of stainless steel feedings of one kind and 310 powder of stainless steel are fed Expect the preparation method of components, the technical scheme is that
A kind of 310 powder of stainless steel feeding of environment-friendly type, including 310 powder of stainless steel and forming agent, the two by weight 100:2~ The ratio of 100:5 is prepared;The granularity of 310 powder of stainless steel is 500 mesh, tap density 4.5-4.8g/cm3
The forming agent includes each component of following parts by weight, and half concise paraffin wax 39-41 parts, white bee is 39-41 parts cured, gathers 19-21 parts of ethylene glycol.
40 parts of the concise paraffin wax of described half, cured 40 parts, 20 parts of polyethylene glycol of white bee.
A method of preparing 310 powder of stainless steel feeding of environment-friendly type, comprising the following steps:
(1) 310 powder of stainless steel are poured into planet kneading machine to be kneaded in tank, adds each component of forming agent;
(2) the analysis alcohol that sintered carbide ball, 85 DEG C of pure water, concentration are greater than 90% is then sequentially added, covers and is kneaded cover After lock;Wherein, the total weight of the sintered carbide ball of addition is the 30%-50% of powder and forming agent total weight;The hard The diameter 5mm-10mm of alloying pellet;Wherein, sintered carbide ball, pure water and analytically pure plastid ratio are 1: 1: 1;
(3) open machine operation machine, revolving speed 400 turns/min, runing time 30min, after take out be kneaded tank in feeding mixture;
(4) feeding mixture is put into electric oven, 55 DEG C of temperature, toasts 30min, it is rear to take out, it grinds.
(5) it grinds after feeding powder crosses 30 mesh stainless steel mesh, completes feeding preparation.
A kind of preparation method of 310 stainless steel metal part, comprising the following steps:
S4, selection take the mold of required product specification, are installed on pressure forming machine, and the feeding of preparation is packed into pressure forming machine Interior, processing forms manufactured part blank, and manufactured part blank pressure is 9-12 tons every square centimeter, dwell time 0.5-1 second, close Scale standard is 5.8 ± 0.03g/cm3
S5, manufactured part blank is packed into closed pressure sintering furnace, carries out vacuum-sintering, be sintered vacuum degree 10Pa- 500Pa, obtains 310 stainless steel metal parts products, density >=7.8g/cm by 1220 DEG C~1240 DEG C of temperature after coming out of the stove3
The invention has the advantages that being changed by 310 stainless steel metal powder pressing forming feedings of invention and preparation method Traditional 310 stainless steels, processing difficulties, the process-cycle is long, the high disadvantage of processing cost, greatly reduces by 310 stainless steel zero of complexity The production and processing cost of part responds country and calls, and improves domestic manufacturing industry technological innovation production level.
Specific embodiment
The invention will now be further described with reference to specific embodiments, the advantages and features of the present invention will be with description and It is apparent.But examples are merely exemplary for these, and it is not intended to limit the scope of the present invention in any way.Those skilled in the art Member it should be understood that without departing from the spirit and scope of the invention can details to technical solution of the present invention and form into Row modifications or substitutions, but these modifications and replacement are fallen within the protection scope of the present invention.
Embodiment 1: a kind of 310 powder of stainless steel feeding of environment-friendly type, including 310 powder of stainless steel and forming agent, the two are pressed Weight ratio 100:2 ratio is prepared;The granularity of 310 powder of stainless steel is 500 mesh, tap density 4.5g/cm3
The forming agent includes each component of following parts by weight, half 39 parts of concise paraffin wax, cured 39 parts of white bee, polyethylene glycol 19 parts.Semi-refined paraffin wax fusing point is low >=and 60 DEG C, tensile strength, caking property is good, and cleanliness is high, and chemical stability is good, is not easily decomposed. Cera alba improves feeding chemical stability, is not easily decomposed, and enhances mobility;The AR grade molecular weight 2000-6000 of polyethylene glycol.
The features such as this programme forming agent has forming stability good, and degreasing speed is fast, product size stabilization and asepsis environment-protecting, It can be applied to 310 stainless steel metal products of the labyrinth that various compacting tool sets can work it out.
A method of preparing 310 powder of stainless steel feeding of environment-friendly type, comprising the following steps:
(1) 310 powder of stainless steel are poured into planet kneading machine to be kneaded in tank, adds each component of forming agent;
(2) the analysis alcohol (alcohol) that sintered carbide ball, 85 DEG C of pure water, concentration are greater than 90% is then sequentially added, mixing is covered It is locked after cover;Wherein, the total weight of the sintered carbide ball of addition is the 30% of powder and forming agent total weight;Described is hard The diameter 5mm of matter alloying pellet.
Wherein, sintered carbide ball, the sintered carbide ball that pure water and analytically pure plastid ratio are 1: 1: 1(, that is, 1g, The pure water of 1ml and the analysis alcohol of 1ml);Sintered carbide ball does not participate in reaction in ball milling mixing process, and ball milling calendering process is complete It all takes out, plays the role of as auxiliary stirring material at rear;
(3) open machine operation machine, revolving speed 400 turns/min, runing time 30min, after take out be kneaded tank in feeding mixture;
(4) feeding mixture is put into electric oven, 55 DEG C of temperature, toasts 30min, it is rear to take out, it grinds.
(5) it grinds after feeding powder crosses 30 mesh stainless steel mesh, completes feeding preparation.
A kind of preparation method of 310 stainless steel metal part, comprising the following steps:
S4, selection take the mold of required product specification, are installed on pressure forming machine, and the feeding of preparation is packed into pressure forming machine It is interior, it processes and forms manufactured part blank, 9 tons every square centimeter of manufactured part blank pressure, the dwell time 0.5 second, density criterion For 5.97g/cm3
S5, manufactured part blank is packed into closed pressure sintering furnace, carries out vacuum-sintering, be sintered vacuum degree 10Pa, temperature 1220 DEG C, 310 stainless steel metal parts products, density 7.8g/cm are obtained after coming out of the stove3
Embodiment 2: a kind of 310 powder of stainless steel feeding of environment-friendly type, including 310 powder of stainless steel and forming agent, the two are pressed The ratio of weight ratio 100:3 is prepared;The granularity of 310 powder of stainless steel is 500 mesh, tap density 4.6g/cm3;It is described Sintered carbide ball diameter 8mm.
40 parts of the concise paraffin wax of described half, cured 40 parts of white bee, 20 parts of polyethylene glycol,.
A method of preparing 310 powder of stainless steel feeding of environment-friendly type, comprising the following steps:
(1) 310 powder of stainless steel are poured into planet kneading machine to be kneaded in tank, adds each component of forming agent;
(2) the analysis alcohol that sintered carbide ball, 85 DEG C of pure water, concentration are greater than 90% is then sequentially added, covers and is kneaded cover After lock;Wherein, the total weight of the sintered carbide ball of addition is the 40% of powder and forming agent total weight;It is sintered carbide ball, pure Sintered carbide ball, the pure water of 1ml and the analysis alcohol of 1ml that water and analytically pure plastid ratio are 1: 1: 1(, that is, 1g), it is described Sintered carbide ball diameter 8mm.
(3) open machine operation machine, revolving speed 400 turns/min, runing time 30min, after take out that be kneaded feeding in tank mixed Close object;
(4) feeding mixture is put into electric oven, 55 DEG C of temperature, toasts 30min, it is rear to take out, it grinds.
(5) it grinds after feeding powder crosses 30 mesh stainless steel mesh, completes feeding preparation.
A kind of preparation method of 310 stainless steel metal part, comprising the following steps:
S4, selection take the mold of required product specification, are installed on pressure forming machine, and the feeding of preparation is packed into pressure forming machine It is interior, it processes and forms manufactured part blank, 10 tons every square centimeter of manufactured part blank pressure, the dwell time 0.8 second, density criterion For 5.8g/cm3
S5, manufactured part blank is packed into closed pressure sintering furnace, carries out vacuum-sintering, be sintered vacuum degree 300Pa, temperature 1230 DEG C, 310 stainless steel metal parts products, density 8.2g/cm are obtained after coming out of the stove3
Embodiment 3: a kind of 310 powder of stainless steel feeding of environment-friendly type, including 310 powder of stainless steel and forming agent, the two are pressed The ratio of weight ratio 100:5 is prepared;The granularity of 310 powder of stainless steel is 500 mesh, tap density 4.8g/cm3;It is described Sintered carbide ball diameter 10mm.
The forming agent includes each component of following parts by weight, half 41 parts of concise paraffin wax, cured 41 parts of white bee, polyethylene glycol 21 parts.
A method of preparing 310 powder of stainless steel feeding of environment-friendly type, comprising the following steps:
(1) 310 powder of stainless steel are poured into planet kneading machine to be kneaded in tank, adds each component of forming agent;
(2) the analysis alcohol that sintered carbide ball, 85 DEG C of pure water, concentration are greater than 90% is then sequentially added, covers and is kneaded cover After lock;Wherein, the total weight of the sintered carbide ball of addition is the 50% of powder and forming agent total weight;It is sintered carbide ball, pure Sintered carbide ball, the pure water of 1ml and the analysis alcohol of 1ml that water and analytically pure plastid ratio are 1: 1: 1(, that is, 1g), it is described Sintered carbide ball diameter 10mm.
(3) open machine operation machine, revolving speed 400 turns/min, runing time 30min, after take out that be kneaded feeding in tank mixed Close object;
(4) feeding mixture is put into electric oven, 55 DEG C of temperature, toasts 30min, it is rear to take out, it grinds.
(5) it grinds after feeding powder crosses 30 mesh stainless steel mesh, completes feeding preparation.
A kind of preparation method of 310 stainless steel metal part, comprising the following steps:
S4, selection take the mold of required product specification, are installed on pressure forming machine, and the feeding of preparation is packed into pressure forming machine It is interior, it processes and forms manufactured part blank, 12 tons every square centimeter of manufactured part blank pressure, the dwell time 1 second, density criterion For 5.83g/cm3
S5, manufactured part blank is packed into closed pressure sintering furnace, carries out vacuum-sintering, be sintered vacuum degree 500Pa, temperature 1240 DEG C, 310 stainless steel metal parts products, density 8.6g/cm are obtained after coming out of the stove3
It can also be required according to different products, carry out different grinding and polishings and the processing such as sandblast, to reach customer drawings Technical requirements meet and use.

Claims (5)

1. a kind of 310 powder of stainless steel feeding of environment-friendly type, which is characterized in that including 310 powder of stainless steel and forming agent, the two is pressed The ratio of weight ratio 100:2~100:5 is prepared;The granularity of 310 powder of stainless steel is 500 mesh, tap density 4.5- 4.8g/cm3
2. 310 powder of stainless steel feeding of environment-friendly type according to claim 1, which is characterized in that the forming agent includes The each component of following parts by weight, half concise paraffin wax 39-41 parts, white bee is 39-41 parts cured, and 19-21 parts of polyethylene glycol.
3. 310 powder of stainless steel feeding of environment-friendly type according to claim 2, which is characterized in that half 40 parts of concise paraffin wax is white Cured 40 parts of bee, 20 parts of polyethylene glycol.
4. a kind of method for preparing 310 powder of stainless steel feeding of environment-friendly type described in claims 1 to 3 any one, feature It is, comprising the following steps:
(1) 310 powder of stainless steel are poured into planet kneading machine to be kneaded in tank, adds each component of forming agent;
(2) the analysis alcohol that sintered carbide ball, 85 DEG C of pure water, concentration are greater than 90% is then sequentially added, covers and is kneaded cover After lock;Wherein, the total weight of the sintered carbide ball of addition is the 30%-50% of powder and forming agent total weight;The hard The diameter 5mm-10mm of alloying pellet;
Wherein, sintered carbide ball, pure water and analytically pure plastid ratio are 1: 1: 1;
(3) open machine operation machine, revolving speed 400 turns/min, runing time 30min, after take out be kneaded tank in feeding mixture;
(4) feeding mixture is put into electric oven, 55 DEG C of temperature, toasts 30min, it is rear to take out, it grinds;
(5) it grinds after feeding powder crosses 30 mesh stainless steel mesh, completes feeding preparation.
5. a kind of preparation method of 310 stainless steel metal parts, which comprises the following steps:
S4, selection take the mold of required product specification, are installed on pressure forming machine, and feeding prepared by claim 4 is packed into In pressure forming machine, processing forms manufactured part blank, and manufactured part blank pressure is 9-12 tons every square centimeter, the dwell time 0.5-1 seconds, density criterion be 5.8 ±
0.03g/cm3
S5, manufactured part blank is packed into closed pressure sintering furnace, carries out vacuum-sintering, be sintered vacuum degree 10Pa- 500Pa, obtains 310 stainless steel metal parts products, density >=7.8g/cm by 1220 DEG C~1240 DEG C of temperature after coming out of the stove3
CN201810792375.4A 2018-07-18 2018-07-18 The preparation method of 310 powder of stainless steel feeding of environment-friendly type and 310 powder of stainless steel components Pending CN109047750A (en)

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