CN109045092A - The preparation method of atractylodes slice - Google Patents
The preparation method of atractylodes slice Download PDFInfo
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- CN109045092A CN109045092A CN201810912246.4A CN201810912246A CN109045092A CN 109045092 A CN109045092 A CN 109045092A CN 201810912246 A CN201810912246 A CN 201810912246A CN 109045092 A CN109045092 A CN 109045092A
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- rhizoma atractylodis
- atractylodis macrocephalae
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Abstract
The invention discloses a kind of preparation methods of atractylodes slice, are related to prepared slices of Chinese crude drugs technical field, its key points of the technical solution are that the following steps are included: (1) arranges；(2) it cleans；(3) it impregnates；(4) wrappage is smeared；(5) cutting；(6) dry；(7) it is sieved；(8) vacuum freeze drying；(9) it packs.The present invention solves atractylodes slice, and active principle is easy to run off in process of production, and slow problem was precipitated in active principle during the cooking process.Wrappage is smeared on Rhizoma Atractylodis Macrocephalae, and utilizes vacuum freeze drying, active principle can be made to not easily run off in process, and active principle is easily precipitated during the cooking process.
Description
Technical field
The present invention relates to prepared slices of Chinese crude drugs technical fields, more specifically, it is related to a kind of preparation method of atractylodes slice.
Background technique
Medicine materical crude slice refers to that Chinese medicine is as needed, handles and the Chinese medicine for formula of formation by processing, or can directly use
In the Chinese medicine of tcm clinical practice.The prepared slices of Chinese crude drugs are the essence places of traditional Chinese medicine, and medicinal material passes through different concocting methods, pharmacological property and function
The characteristics of effect can change, be middle medical drugs and advantage.
Rhizoma Atractylodis Macrocephalae is the dry rhizome of compositae plant Rhizoma Atractylodis Macrocephalae, and the chemical component for clinical conventional Chinese medicine, Rhizoma Atractylodis Macrocephalae is predominantly volatilized
Oil, polysaccharide, amino acid etc. wherein contain atractylone, atractylol, γ-elemene, β -3,4- dimethyl-benzenebutanoic acid in volatile oil
The effective components such as isopropyl ester and furanodiene, Rhizoma Atractylodis Macrocephalae I ester, Rhizoma Atractylodis Macrocephalae II ester, polysaccharide include two kinds of single sugar of PSAM-1 and PSAM-2,
Rhizoma Atractylodis Macrocephalae have strengthening the spleen and replenishing qi, eliminate dampness and have diuretic effect, the function of hidroschesis miscarriage prevention, be used for spleen eating less, abdominal distention diarrhea, phlegm retention anti-dazzle nervous, oedema, from
Sweat, threatened abortion.
Currently, the concocting method of Rhizoma Atractylodis Macrocephalae there are tens kinds, there is Rhizoma Atractylodis Macrocephalae preparata, rhizoma atractylodis macrocephalae, stir-baked RHIZOMA ATRACTYLODIS MACROCEPHALAE with soil, steams Rhizoma Atractylodis Macrocephalae, stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran
Deng being processed obtained atractylodes slice has the effect of invigorating the spleen and benefiting qi well.
In the prior art, it can refer to the Chinese invention patent application file that application publication number is CN107375391A, it is public
The atractylodes slice having opened a kind of processing method of atractylodes slice and having been obtained by this method comprising following steps: it infiltration: takes white
Art raw material is added water and did not had raw material surface to be impregnated；It steams profit: material being erected on the water surface, in a manner of the bored profit of steam
Soften Rhizoma Atractylodis Macrocephalae raw material, the temperature for steaming profit is controlled by temperature control system；Slice: the Rhizoma Atractylodis Macrocephalae raw material through steaming profit processing is sliced；
It is dry: slice being dried, atractylodes slice is obtained.
The processing method of existing this atractylodes slice is directly sliced after steaming profit, is easy to make in the process of slice white
Effective component is lost in art medicine materical crude slice, and usual drying method is easy to make atractylodes slice that active principle is difficult to analyse in use
Out.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide a kind of preparation method of atractylodes slice,
The effective component in Rhizoma Atractylodis Macrocephalae can largely be retained, and active principle is easy to be precipitated atractylodes slice in use.
To achieve the above object, the present invention provides the following technical scheme that a kind of preparation method of atractylodes slice, including with
Lower step:
(1) it arranges: taking the Rhizoma Atractylodis Macrocephalae root of fresh excavation, trim fibrous root, stem foot picks black oil only, and go rotten rotten Rhizoma Atractylodis Macrocephalae, and picks
Remove the impurity such as stone；(2) it cleans: rinsing Rhizoma Atractylodis Macrocephalae with giant, wash away silt, dried in the air naturally to surface moisture content in 30-
Between 45%；(3) it impregnates: Rhizoma Atractylodis Macrocephalae being placed in the fermentation vat equipped with hydrogen peroxide and salt water mixed solution and is impregnated 5-8 hours, dioxygen
The weight ratio of water and salt water is 1:1, and the weight of hydrogen peroxide and salt water mixed liquid is 1.5-2.5 times of Rhizoma Atractylodis Macrocephalae weight, hydrogen peroxide
Concentration is 3-10%, and the concentration of salt water is 3-6%, and control soaking temperature is maintained at 25-40 DEG C, is rushed repeatedly after taking-up with clear water
It washes, dries；(4) smear wrappage: will uniformly be sprayed on the Rhizoma Atractylodis Macrocephalae dried one layer dilution after and sugar content between 15-19%
Honey, then one layer of mandarin oil is uniformly smeared, it is 15-20 times of agar by 30-45 parts of agar additions by taking 500-600 parts of Rhizoma Atractylodis Macrocephalaes as an example
Water in, keep the temperature between 50-60 DEG C, after being uniformly mixed, rice bran be added thereto, after being uniformly mixed,
And be uniformly applied to it on Rhizoma Atractylodis Macrocephalae, standing is dried；(5) cutting: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained is sliced, and at thickness
For the slice of 2-4mm；(6) dry: Rhizoma Atractylodis Macrocephalae slice is spread out in baking pan, shakeouts, with a thickness of 2-3cm, baking pan is put into drying chamber,
The temperature for controlling drying chamber is 60-80 DEG C, until Rhizoma Atractylodis Macrocephalae water content is less than 12%；(7) it is sieved: will be on the Rhizoma Atractylodis Macrocephalae slice after drying
Wrappage knocks out, and is put on vibrating screen, weeds out fines.(8) Rhizoma Atractylodis Macrocephalae after sieving vacuum freeze drying: is subjected to vacuum refrigeration
Dry, the moisture after drying is no more than 12%；(9) it packs: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps obtain being packed as requested, is placed in
It is stored at aeration-drying.
By using above-mentioned technical proposal, the processing such as smearing wrappage, cutting and drying is carried out with the Rhizoma Atractylodis Macrocephalae of fresh excavation,
Rhizoma Atractylodis Macrocephalae is fabricated to atractylodes slice, not only effective component can be caused to be lost to avoid convection drying after immersion, Rhizoma Atractylodis Macrocephalae can also be made
Prepared slice quality is relatively stable, and production method is simple, compared with traditional handicraft, can greatly shorten the production cycle；First use hydrogen peroxide
Mixing with salt water is easy to impregnate Rhizoma Atractylodis Macrocephalae, can achieve the effect that sterilizing, and clear water repeated flushing is used after taking-up, can avoid double
Oxygen water and residue of saline are on Rhizoma Atractylodis Macrocephalae surface；Honey be sticky transparent or semitransparent colloidal liquid, honey can clearing heat and moistening dryness,
Mandarin oil have refresh oneself, stomach invigorating, resolving sputum and other effects, mandarin oil has certain oiliness, the honey and orange being sprayed on Rhizoma Atractylodis Macrocephalae
Oil can reduce effective component and flow out with moisture, and agar has the characteristic of colloid, and rice bran can be adhered to the surface of Rhizoma Atractylodis Macrocephalae,
Rice bran can increase the gas permeability of Rhizoma Atractylodis Macrocephalae, guide hot-air is incremental to enter in wrappage when heated, keep Rhizoma Atractylodis Macrocephalae maximum
The reservation effective component of degree simultaneously achievees the effect that dry；Using Rhizoma Atractylodis Macrocephalae of the vacuum drying by after sieving and surface without wrappage into
Row be vacuum-treated, vacuum freeze drying processing when, the moisture in Rhizoma Atractylodis Macrocephalae is directly detached, in Rhizoma Atractylodis Macrocephalae the position of script hydrone because
For moisture evaporation and form porous structure, when Rhizoma Atractylodis Macrocephalae is during edible, hydrone enters in porous structure, Rhizoma Atractylodis Macrocephalae water suction it is swollen
Swollen, hydrone makes the effective component in meat be easier to be precipitated in the porous middle meat for squeezing Rhizoma Atractylodis Macrocephalae.
The present invention is further arranged to: being dipped to and is moisturized in the step (3), and is pinched with hand without hard sense.
By using above-mentioned technical proposal, Rhizoma Atractylodis Macrocephalae is completely soaked and is moisturized, until being pinched with hand without hard sense, Rhizoma Atractylodis Macrocephalae can be made rear
It is heated more evenly in continuous drying course, prevents Rhizoma Atractylodis Macrocephalae from impregnating uneven, lead to uneven drying, cause atractylodes slice quality not
It is good.
The present invention is further arranged to: the method for dilution honey in the step (4) are as follows: take the honey of 1Kg, 4- is added
5Kg temperature is stirred in 30-45 DEG C of warm water, and mixing speed is 600-700 revs/min.
By using above-mentioned technical proposal, warm water is added in honey, can be made in honey dilution, it is diluted more equal
It is even, make the control of honey sugar content in 15-19%, prevents honey sugar content higher, influence the medical value of atractylodes slice.
The present invention is further arranged to: the mixing speed of stirring agar is 300-400 revs/min in the step (4), is stirred
Mixing the time is 3-5 hours.
By using above-mentioned technical proposal, mixing speed, which is 300-400 revs/min, can make agar have faster dissolution speed
Degree improves rate of dissolution, and stirs 3-5 hours, and agar dissolution can be made complete.
The present invention is further arranged to: the stirring rate of stirring rice bran is 350-450 revs/min in above-mentioned steps (4), is stirred
Mixing the time is 2-3 hours.
By using above-mentioned technical proposal, rice bran is placed in dissolved agar, stirring rate is 350-450 revs/min
Clock, mixing time are 2-3 hours, rice bran can be made to be evenly distributed in agar, be applied on Rhizoma Atractylodis Macrocephalae convenient for subsequent, make rice bran white
It is evenly distributed in art.
The present invention is further arranged to: needing to carry out disinfection by ultraviolet light processing to Rhizoma Atractylodis Macrocephalae before the step (9).
By using above-mentioned technical proposal, disinfection by ultraviolet light is carried out to Rhizoma Atractylodis Macrocephalae, the practical safety of Rhizoma Atractylodis Macrocephalae can be improved.
The present invention is further arranged to: it is primary to stir Rhizoma Atractylodis Macrocephalae slice in the step (6) every about 1 hour.
Rhizoma Atractylodis Macrocephalae slice can be made dried per Rhizoma Atractylodis Macrocephalae slice is stirred up and down every other hour by using above-mentioned technical proposal
Cheng Zhong is heated more evenly, improves the rate of drying of Rhizoma Atractylodis Macrocephalae slice.
The present invention is further arranged to: it is small that the Rhizoma Atractylodis Macrocephalae slice time to be dried cut in the step (5) must not exceed 8
When.
By using above-mentioned technical proposal, keeps Rhizoma Atractylodis Macrocephalae slice dry in time, prevent Rhizoma Atractylodis Macrocephalae chip drying not in time, glue
Even with mouldy situation, the quality of production of atractylodes slice is influenced.
In conclusion the present invention has the advantages that compared with the prior art
(1) present invention on Rhizoma Atractylodis Macrocephalae by wrapping up one layer of wrappage, using the honey with stickiness and with the mandarin oil of oiliness,
The loss that Rhizoma Atractylodis Macrocephalae active principle in process can be reduced, keeps Rhizoma Atractylodis Macrocephalae property relatively stable；
(2) present invention can be made in Rhizoma Atractylodis Macrocephalae by the way that Rhizoma Atractylodis Macrocephalae is dried using vacuum freeze drying without containing extra water
Point, and so that moisture is rapidly entered Rhizoma Atractylodis Macrocephalae slice during the cooking process, and make Rhizoma Atractylodis Macrocephalae slice expansion, convenient for active principle analysis in Rhizoma Atractylodis Macrocephalae
Out；
(3) present invention first is easy to impregnate Rhizoma Atractylodis Macrocephalae, can reach sterilizing in soaking process with the mixing of hydrogen peroxide and salt water
Effect, clear water repeated flushing is used after taking-up, hydrogen peroxide and residue of saline is can avoid on Rhizoma Atractylodis Macrocephalae surface, influences the medicine of atractylodes slice
With value.
Specific embodiment
A kind of embodiment 1: preparation method of atractylodes slice, comprising the following steps:
(1) it arranges: taking the Rhizoma Atractylodis Macrocephalae root of fresh excavation, trim fibrous root, stem foot picks black oil only, and go rotten rotten Rhizoma Atractylodis Macrocephalae, and picks
Remove the impurity such as stone；
(2) it cleans: rinsing Rhizoma Atractylodis Macrocephalae with giant, wash away silt, dried in the air naturally to surface moisture content between 30%；
(3) it impregnates: Rhizoma Atractylodis Macrocephalae being placed in the fermentation vat equipped with hydrogen peroxide and salt water mixed solution and is impregnated 5 hours, hydrogen peroxide and salt
The weight ratio of water is 1:1, and the weight of hydrogen peroxide and salt water mixed liquid is 1.5 times of Rhizoma Atractylodis Macrocephalae weight, and the concentration of hydrogen peroxide is 3%,
The concentration of salt water is 3%, and control soaking temperature is maintained at 25 DEG C, is dipped to and moisturizes, and is pinched with hand without hard sense, uses clear water after taking-up
Repeated flushing is dried；
(4) smear wrappage: will uniformly be sprayed on the Rhizoma Atractylodis Macrocephalae dried one layer dilution after and honey of the sugar content between 15%, then
One layer of mandarin oil is uniformly smeared, by taking 500 parts of Rhizoma Atractylodis Macrocephalaes as an example, it is in 15 times of agar of water, to keep temperature that 30 parts of agar, which are added,
Between 50 DEG C, mixing speed is 300 revs/min, and mixing time is 5 hours, and after being uniformly mixed, rice is added thereto
Chaff, stirring rate are 350 revs/min, and mixing time is 3 hours, after being uniformly mixed, and it are uniformly applied to Rhizoma Atractylodis Macrocephalae
On, standing is dried；Wherein dilute the method for honey are as follows: the honey of 1Kg is taken, 4Kg temperature is added and is stirred in 30 DEG C of warm water,
Mixing speed is 600 revs/min；
(5) cutting: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained is sliced, and at the slice with a thickness of 2mm, the Rhizoma Atractylodis Macrocephalae that cuts slice to
Drying time must not exceed 8 hours；
(6) dry: Rhizoma Atractylodis Macrocephalae slice being spread out in baking pan, shakeouts, with a thickness of 2cm, baking pan is put into drying chamber, control the temperature of drying chamber
Degree is 60 DEG C, and it is primary that Rhizoma Atractylodis Macrocephalae slice was stirred every about 1 hour, until Rhizoma Atractylodis Macrocephalae water content is less than 12%；
(7) it is sieved: the wrappage on the Rhizoma Atractylodis Macrocephalae slice after drying being knocked out, and is put on vibrating screen, fines is weeded out；
(8) vacuum freeze drying: the Rhizoma Atractylodis Macrocephalae after sieving is subjected to vacuum freeze drying, the moisture after drying is no more than 12%；
(9) pack: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained carries out disinfection by ultraviolet light processing, and is packed as requested, is placed in logical
Air-dry dry place's storage.
A kind of embodiment 2: preparation method of atractylodes slice, comprising the following steps:
(1) it arranges: taking the Rhizoma Atractylodis Macrocephalae root of fresh excavation, trim fibrous root, stem foot picks black oil only, and go rotten rotten Rhizoma Atractylodis Macrocephalae, and picks
Remove the impurity such as stone；
(2) it cleans: rinsing Rhizoma Atractylodis Macrocephalae with giant, wash away silt, dried in the air naturally to surface moisture content between 35%；
(3) it impregnates: Rhizoma Atractylodis Macrocephalae being placed in the fermentation vat equipped with hydrogen peroxide and salt water mixed solution and is impregnated 6 hours, hydrogen peroxide and salt
The weight ratio of water is 1:1, and the weight of hydrogen peroxide and salt water mixed liquid is 1.8 times of Rhizoma Atractylodis Macrocephalae weight, and the concentration of hydrogen peroxide is 5%,
The concentration of salt water is 4%, and control soaking temperature is maintained at 30 DEG C, is dipped to and moisturizes, and is pinched with hand without hard sense, uses clear water after taking-up
Repeated flushing is dried；
(4) smear wrappage: will uniformly be sprayed on the Rhizoma Atractylodis Macrocephalae dried one layer dilution after and honey of the sugar content between 16%, then
One layer of mandarin oil is uniformly smeared, by taking 530 parts of Rhizoma Atractylodis Macrocephalaes as an example, it is in 16 times of agar of water, to keep temperature that 35 parts of agar, which are added,
Between 52 DEG C, mixing speed is 330 revs/min, and mixing time is 4.5 hours, and after being uniformly mixed, rice is added thereto
Chaff, stirring rate are 380 revs/min, and mixing time is 2.8 hours, after being uniformly mixed, and it are uniformly applied to Rhizoma Atractylodis Macrocephalae
On, standing is dried, wherein the method for dilution honey are as follows: takes the honey of 1Kg, 4.2Kg temperature is added and is stirred in 35 DEG C of warm water
It mixes, mixing speed is 620 revs/min；
(5) cutting: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained is sliced, and at the slice with a thickness of 2.8mm, the Rhizoma Atractylodis Macrocephalae slice cut
Time to be dried must not exceed 8 hours；
(6) dry: Rhizoma Atractylodis Macrocephalae slice being spread out in baking pan, shakeouts, with a thickness of 2.5cm, baking pan is put into drying chamber, controls drying chamber
Temperature is 68 DEG C, and it is primary that Rhizoma Atractylodis Macrocephalae slice was stirred every about 1 hour, until Rhizoma Atractylodis Macrocephalae water content is less than 12%；
(7) it is sieved: the wrappage on the Rhizoma Atractylodis Macrocephalae slice after drying being knocked out, and is put on vibrating screen, fines is weeded out；
(8) vacuum freeze drying: the Rhizoma Atractylodis Macrocephalae after sieving is subjected to vacuum freeze drying, the moisture after drying is no more than 12%；
(9) pack: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained carries out disinfection by ultraviolet light processing, and is packed as requested, is placed in logical
Air-dry dry place's storage.
A kind of embodiment 3: preparation method of atractylodes slice, comprising the following steps:
(1) it arranges: taking the Rhizoma Atractylodis Macrocephalae root of fresh excavation, trim fibrous root, stem foot picks black oil only, and go rotten rotten Rhizoma Atractylodis Macrocephalae, and picks
Remove the impurity such as stone；
(2) it cleans: rinsing Rhizoma Atractylodis Macrocephalae with giant, wash away silt, dried in the air naturally to surface moisture content between 40%；
(3) it impregnates: Rhizoma Atractylodis Macrocephalae being placed in the fermentation vat equipped with hydrogen peroxide and salt water mixed solution and is impregnated 7 hours, hydrogen peroxide and salt
The weight ratio of water is 1:1, and the weight of hydrogen peroxide and salt water mixed liquid is 2.2 times of Rhizoma Atractylodis Macrocephalae weight, and the concentration of hydrogen peroxide is 8%,
The concentration of salt water is 5%, and control soaking temperature is maintained at 35 DEG C, is dipped to and moisturizes, and is pinched with hand without hard sense, uses clear water after taking-up
Repeated flushing is dried；
(4) smear wrappage: will uniformly be sprayed on the Rhizoma Atractylodis Macrocephalae dried one layer dilution after and honey of the sugar content between 17%, then
One layer of mandarin oil is uniformly smeared, by taking 560 parts of Rhizoma Atractylodis Macrocephalaes as an example, it is in 18 times of agar of water, to keep temperature that 40 parts of agar, which are added,
Between 56 DEG C, mixing speed is 360 revs/min, and mixing time is 3.5 hours, and after being uniformly mixed, rice is added thereto
Chaff, stirring rate are 400 revs/min, and mixing time is 2.5 hours, after being uniformly mixed, and it are uniformly applied to Rhizoma Atractylodis Macrocephalae
On, standing is dried, wherein the method for dilution honey are as follows: takes the honey of 1Kg, 4.4Kg temperature is added and is stirred in 40 DEG C of warm water
It mixes, mixing speed is 640 revs/min；
(5) cutting: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained is sliced, and at the slice with a thickness of 3.5mm, the Rhizoma Atractylodis Macrocephalae slice cut
Time to be dried must not exceed 8 hours；
(6) dry: Rhizoma Atractylodis Macrocephalae slice being spread out in baking pan, shakeouts, with a thickness of 2.5cm, baking pan is put into drying chamber, controls drying chamber
Temperature is 72 DEG C, and it is primary that Rhizoma Atractylodis Macrocephalae slice was stirred every about 1 hour, until Rhizoma Atractylodis Macrocephalae water content is less than 12%；
(7) it is sieved: the wrappage on the Rhizoma Atractylodis Macrocephalae slice after drying being knocked out, and is put on vibrating screen, fines is weeded out；
(8) vacuum freeze drying: the Rhizoma Atractylodis Macrocephalae after sieving is subjected to vacuum freeze drying, the moisture after drying is no more than 12%；
(9) pack: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained carries out disinfection by ultraviolet light processing, and is packed as requested, is placed in logical
Air-dry dry place's storage.
A kind of embodiment 4: preparation method of atractylodes slice, comprising the following steps:
(1) it arranges: taking the Rhizoma Atractylodis Macrocephalae root of fresh excavation, trim fibrous root, stem foot picks black oil only, and go rotten rotten Rhizoma Atractylodis Macrocephalae, and picks
Remove the impurity such as stone；
(2) it cleans: rinsing Rhizoma Atractylodis Macrocephalae with giant, wash away silt, dried in the air naturally to surface moisture content between 45%；
(3) it impregnates: Rhizoma Atractylodis Macrocephalae being placed in the fermentation vat equipped with hydrogen peroxide and salt water mixed solution and is impregnated 8 hours, hydrogen peroxide and salt
The weight ratio of water is 1:1, and the weight of hydrogen peroxide and salt water mixed liquid is 2.5 times of Rhizoma Atractylodis Macrocephalae weight, and the concentration of hydrogen peroxide is 10%,
The concentration of salt water is 6%, and control soaking temperature is maintained at 40 DEG C, is dipped to and moisturizes, and is pinched with hand without hard sense, uses clear water after taking-up
Repeated flushing is dried；
(4) smear wrappage: will uniformly be sprayed on the Rhizoma Atractylodis Macrocephalae dried one layer dilution after and honey of the sugar content between 19%, then
One layer of mandarin oil is uniformly smeared, by taking 600 parts of Rhizoma Atractylodis Macrocephalaes as an example, it is in 20 times of agar of water, to keep temperature that 45 parts of agar, which are added,
Between 60 DEG C, mixing speed is 400 revs/min, and mixing time is 3 hours, and after being uniformly mixed, rice is added thereto
Chaff, stirring rate are 450 revs/min, after mixing time was uniformly mixed for 2 hours, and it are uniformly applied on Rhizoma Atractylodis Macrocephalae,
Standing is dried, wherein the method for dilution honey are as follows: takes the honey of 1Kg, 5Kg temperature is added and is stirred in 45 DEG C of warm water, stirs
Mixing speed is 700 revs/min；
(5) cutting: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained is sliced, and at the slice with a thickness of 4mm, the Rhizoma Atractylodis Macrocephalae that cuts slice to
Drying time must not exceed 8 hours；
(6) dry: Rhizoma Atractylodis Macrocephalae slice being spread out in baking pan, shakeouts, with a thickness of 3cm, baking pan is put into drying chamber, control the temperature of drying chamber
Degree is 68 DEG C, and it is primary that Rhizoma Atractylodis Macrocephalae slice was stirred every about 1 hour, until Rhizoma Atractylodis Macrocephalae water content is less than 12%；
(7) it is sieved: the wrappage on the Rhizoma Atractylodis Macrocephalae slice after drying being knocked out, and is put on vibrating screen, fines is weeded out；
(8) vacuum freeze drying: the Rhizoma Atractylodis Macrocephalae after sieving is subjected to vacuum freeze drying, the moisture after drying is no more than 12%；
(9) pack: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained carries out disinfection by ultraviolet light processing, and is packed as requested, is placed in logical
Air-dry dry place's storage.
A kind of comparative example 1: preparation method of atractylodes slice, comprising the following steps:
(1) it arranges: taking the Rhizoma Atractylodis Macrocephalae root of fresh excavation, trim fibrous root, stem foot picks black oil only, and go rotten rotten Rhizoma Atractylodis Macrocephalae, and picks
Remove the impurity such as stone；
(2) it cleans: rinsing Rhizoma Atractylodis Macrocephalae with giant, wash away silt, dried in the air naturally to surface moisture content between 40%；
(3) it impregnates: Rhizoma Atractylodis Macrocephalae being placed in the fermentation vat equipped with hydrogen peroxide and salt water mixed solution and is impregnated 7 hours, hydrogen peroxide and salt
The weight ratio of water is 1:1, and the weight of hydrogen peroxide and salt water mixed liquid is 2.2 times of Rhizoma Atractylodis Macrocephalae weight, and the concentration of hydrogen peroxide is 8%,
The concentration of salt water is 5%, and control soaking temperature is maintained at 35 DEG C, is dipped to and moisturizes, and is pinched with hand without hard sense, uses clear water after taking-up
Repeated flushing is dried；
(4) cutting: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained is sliced, and at the slice with a thickness of 3.5mm, the Rhizoma Atractylodis Macrocephalae slice cut
Time to be dried must not exceed 8 hours；
(5) dry: Rhizoma Atractylodis Macrocephalae slice being spread out in baking pan, shakeouts, with a thickness of 2.5cm, baking pan is put into drying chamber, controls drying chamber
Temperature is 72 DEG C, and it is primary that Rhizoma Atractylodis Macrocephalae slice was stirred every about 1 hour, until Rhizoma Atractylodis Macrocephalae water content is less than 12%；
(6) it is sieved: the wrappage on the Rhizoma Atractylodis Macrocephalae slice after drying being knocked out, and is put on vibrating screen, fines is weeded out；
(7) vacuum freeze drying: the Rhizoma Atractylodis Macrocephalae after sieving is subjected to vacuum freeze drying, the moisture after drying is no more than 12%；
(8) pack: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained carries out disinfection by ultraviolet light processing, and is packed as requested, is placed in logical
Air-dry dry place's storage.
A kind of comparative example 2: preparation method of atractylodes slice, comprising the following steps:
(1) it arranges: taking the Rhizoma Atractylodis Macrocephalae root of fresh excavation, trim fibrous root, stem foot picks black oil only, and go rotten rotten Rhizoma Atractylodis Macrocephalae, and picks
Remove the impurity such as stone；
(2) it cleans: rinsing Rhizoma Atractylodis Macrocephalae with giant, wash away silt, dried in the air naturally to surface moisture content between 40%；
(3) it impregnates: Rhizoma Atractylodis Macrocephalae being placed in the fermentation vat equipped with hydrogen peroxide and salt water mixed solution and is impregnated 7 hours, hydrogen peroxide and salt
The weight ratio of water is 1:1, and the weight of hydrogen peroxide and salt water mixed liquid is 2.2 times of Rhizoma Atractylodis Macrocephalae weight, and the concentration of hydrogen peroxide is 8%,
The concentration of salt water is 5%, and control soaking temperature is maintained at 35 DEG C, is dipped to and moisturizes, and is pinched with hand without hard sense, uses clear water after taking-up
Repeated flushing is dried；
(4) smear wrappage: will uniformly be sprayed on the Rhizoma Atractylodis Macrocephalae dried one layer dilution after and honey of the sugar content between 17%, then
One layer of mandarin oil is uniformly smeared, by taking 560 parts of Rhizoma Atractylodis Macrocephalaes as an example, it is in 18 times of agar of water, to keep temperature that 40 parts of agar, which are added,
Between 56 DEG C, mixing speed is 360 revs/min, and mixing time is 3.5 hours, and after being uniformly mixed, rice is added thereto
Chaff, stirring rate are 400 revs/min, and mixing time is 2.5 hours, after being uniformly mixed, and it are uniformly applied to Rhizoma Atractylodis Macrocephalae
On, standing is dried, wherein the method for dilution honey are as follows: takes the honey of 1Kg, 4.4Kg temperature is added and is stirred in 40 DEG C of warm water
It mixes, mixing speed is 640 revs/min；
(5) cutting: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained is sliced, and at the slice with a thickness of 3.5mm, the Rhizoma Atractylodis Macrocephalae slice cut
Time to be dried must not exceed 8 hours；
(6) dry: Rhizoma Atractylodis Macrocephalae slice being spread out in baking pan, shakeouts, with a thickness of 2.5cm, baking pan is put into drying chamber, controls drying chamber
Temperature is 72 DEG C, and it is primary that Rhizoma Atractylodis Macrocephalae slice was stirred every about 1 hour, until Rhizoma Atractylodis Macrocephalae water content is less than 12%；
(7) it is sieved: the wrappage on the Rhizoma Atractylodis Macrocephalae slice after drying being knocked out, and is put on vibrating screen, fines is weeded out；
(8) pack: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained carries out disinfection by ultraviolet light processing, and is packed as requested, is placed in logical
Air-dry dry place's storage.
A kind of comparative example 3: preparation method of atractylodes slice, comprising the following steps:
(1) it arranges: taking the Rhizoma Atractylodis Macrocephalae root of fresh excavation, trim fibrous root, stem foot picks black oil only, and go rotten rotten Rhizoma Atractylodis Macrocephalae, and picks
Remove the impurity such as stone；
(2) it cleans: rinsing Rhizoma Atractylodis Macrocephalae with giant, wash away silt, dried in the air naturally to surface moisture content between 40%；
(3) it impregnates: Rhizoma Atractylodis Macrocephalae being placed in the fermentation vat equipped with hydrogen peroxide and salt water mixed solution and is impregnated 7 hours, hydrogen peroxide and salt
The weight ratio of water is 1:1, and the weight of hydrogen peroxide and salt water mixed liquid is 2.2 times of Rhizoma Atractylodis Macrocephalae weight, and the concentration of hydrogen peroxide is 8%,
The concentration of salt water is 5%, and control soaking temperature is maintained at 35 DEG C, is dipped to and moisturizes, and is pinched with hand without hard sense, uses clear water after taking-up
Repeated flushing is dried；
(4) cutting: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained is sliced, and at the slice with a thickness of 3.5mm, the Rhizoma Atractylodis Macrocephalae slice cut
Time to be dried must not exceed 8 hours；
(5) dry: Rhizoma Atractylodis Macrocephalae slice being spread out in baking pan, shakeouts, with a thickness of 2.5cm, baking pan is put into drying chamber, controls drying chamber
Temperature is 72 DEG C, and it is primary that Rhizoma Atractylodis Macrocephalae slice was stirred every about 1 hour, until Rhizoma Atractylodis Macrocephalae water content is less than 12%；
(6) it is sieved: the wrappage on the Rhizoma Atractylodis Macrocephalae slice after drying being knocked out, and is put on vibrating screen, fines is weeded out；
(7) pack: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained carries out disinfection by ultraviolet light processing, and is packed as requested, is placed in logical
Air-dry dry place's storage.
Comparative example 4: application reference publication No. is the Chinese invention patent application file of CN107375391A, and it discloses one
The processing method of kind atractylodes slice and the atractylodes slice obtained by this method comprising immersion step: taking Rhizoma Atractylodis Macrocephalae raw material, is added
Water did not had raw material surface to be impregnated, and it is 30~50 DEG C that when immersion, which is heated to water temperature,；Steam profit step: by material be erected at the water surface it
On, soften Rhizoma Atractylodis Macrocephalae raw material in a manner of the bored profit of steam, it is 40~60 DEG C that the temperature steamed and moistened is controlled by temperature control system；Slice step
It is rapid: the Rhizoma Atractylodis Macrocephalae raw material through steaming profit processing being sliced, bighead atractylodes rhizome piece is obtained；Drying steps: being dried bighead atractylodes rhizome piece, obtains white
Art medicine materical crude slice.
Sample of the atractylodes slice made from Example 1-4 and comparative example 1-4 as test, each embodiment and comparative example
The sample mass of middle acquirement is identical, and each sample is put into the casserole equipped with same volume, and it is sample that weight is added into casserole
The water that 24 times of weight heats each sample 1 hour with same heating rate, chooses different time points and contains to sample cooking water
The relative amount of some main components is detected, and testing result is shown in table 1.
Atractylodes slice Contents of Main Components testing result made from table 1 embodiment 1-4 and comparative example 1-4
As shown in Table 1, under same conditions of cooking, the boiling of same time is carried out to the atractylodes slice of phase homogenous quantities, is being steamed
When boiling completion, the volatile oil content in the cooking liquor of atractylodes slice made from embodiment 1-4 is greater than Rhizoma Atractylodis Macrocephalae made from comparative example 1-4
Volatile oil content in the cooking liquor of medicine materical crude slice, and in same time point, the volatile oil of atractylodes slice made from embodiment 1-4
Amount of precipitation is greater than the amount of precipitation of the volatile oil of atractylodes slice made from comparative example 1-4, illustrates atractylodes slice made from embodiment 1-4
Middle effective component is easier to be precipitated, and in process of production, and there is no be lost for effective component；Equally, when boiling is completed, implement
The content of polysaccharide is greater than polysaccharide in atractylodes slice cooking liquor made from comparative example 1-4 in atractylodes slice cooking liquor made from example 1-4
Content, and during the cooking process, the speed of separating out of polysaccharide is greater than the speed of separating out of polysaccharide in comparative example 1-4 in embodiment 1-4,
Amino acid is also also such.
With the volatile oil in the cooking liquor that supercritical extraction extracts each embodiment and each comparative example boiling is completed, will extract
Object n-hexane dissolution carries out GC-MS measurement analysis, measures the main component and content in volatile oil, measurement result is shown in table
2。
The main component and content table of volatile oil in table 2 embodiment 1-4 and comparative example 1-4
Main component content is more in volatile oil in embodiment 1-4 as can be seen from Table 2, illustrates that embodiment 1-4 atractylodes slice exists
In digestion process, active principle is easier to be precipitated, and is lost in process less.
Amino acid is extracted and is detected in the cooking liquor completed to boiling in embodiment 1-4 and comparative example 1-4, and according to
In " food sanitary testing method (physical and chemical part) " at Contents of Amino Acids standard GB/T18246-2000 routine acid-hydrolysis method
Reason, instrument are Hitachi 835-50 type amino-acid analyzer, and type and content, testing result are shown in amino acid in detection cooking liquor
Table 3.
The type and mass fraction of amino acid in table 3 embodiment 1-4 and comparative example 1-4
Data in contrast table 3 can be seen that essential amino acid in embodiment 1-4 and non-essential amino acid content is higher than comparison
The content of essential amino acid and nonessential amino acid, illustrates that atractylodes slice is effective during the cooking process in embodiment 1-4 in example 1-4
It is fast at analyzing, and in boiling, active principle is lost less.
The above is only a preferred embodiment of the present invention, protection scope of the present invention is not limited merely to above-mentioned implementation
Example, all technical solutions belonged under thinking of the present invention all belong to the scope of protection of the present invention.It should be pointed out that for the art
Those of ordinary skill for, several improvements and modifications without departing from the principles of the present invention, these improvements and modifications
It should be regarded as protection scope of the present invention.
Claims (8)
1. a kind of preparation method of atractylodes slice, it is characterised in that: the following steps are included:
(1) it arranges: taking the Rhizoma Atractylodis Macrocephalae root of fresh excavation, trim fibrous root, stem foot picks black oil only, and go rotten rotten Rhizoma Atractylodis Macrocephalae, and picks
Remove the impurity such as stone；
(2) it cleans: rinsing Rhizoma Atractylodis Macrocephalae with giant, wash away silt, dried in the air naturally to surface moisture content between 30-45%；
(3) impregnate: Rhizoma Atractylodis Macrocephalae is placed in the fermentation vat equipped with hydrogen peroxide and salt water mixed solution and is impregnated 5-8 hours, hydrogen peroxide with
The weight ratio of salt water is 1:1, and the weight of hydrogen peroxide and salt water mixed liquid is 1.5-2.5 times of Rhizoma Atractylodis Macrocephalae weight, the concentration of hydrogen peroxide
For 3-10%, the concentration of salt water is 3-6%, and control soaking temperature is maintained at 25-40 DEG C, clear water repeated flushing is used after taking-up, is dried；
(4) smear wrappage: will uniformly be sprayed on the Rhizoma Atractylodis Macrocephalae dried one layer dilution after and honey of the sugar content between 15-19%,
One layer of mandarin oil is uniformly smeared again, is 15-20 times of agar of water by 30-45 parts of agar additions by taking 500-600 parts of Rhizoma Atractylodis Macrocephalaes as an example
In, it keeps the temperature between 50-60 DEG C, after being uniformly mixed, rice bran is added thereto, after being uniformly mixed, and will
It is uniformly applied on Rhizoma Atractylodis Macrocephalae, and standing is dried；
(5) cutting: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps are obtained is sliced, and at the slice with a thickness of 2-4mm；
(6) dry: Rhizoma Atractylodis Macrocephalae slice being spread out in baking pan, shakeouts, with a thickness of 2-3cm, baking pan is put into drying chamber, controls drying chamber
Temperature is 60-80 DEG C, until Rhizoma Atractylodis Macrocephalae water content is less than 12%；
(7) it is sieved: the wrappage on the Rhizoma Atractylodis Macrocephalae slice after drying being knocked out, and is put on vibrating screen, fines is weeded out；
(8) vacuum freeze drying: the Rhizoma Atractylodis Macrocephalae after sieving is subjected to vacuum freeze drying, the moisture after drying is no more than 12%；
(9) it packs: the Rhizoma Atractylodis Macrocephalae that above-mentioned steps obtain is packed as requested, be placed at aeration-drying and store.
2. the preparation method of atractylodes slice according to claim 1, it is characterised in that: be dipped to profit in the step (3)
Thoroughly, and with hand it pinches without hard sense.
3. the preparation method of atractylodes slice according to claim 1, it is characterised in that: dilute honey in the step (4)
Method are as follows: take the honey of 1Kg, 4-5Kg temperature be added and is stirred in 30-45 DEG C of warm water, mixing speed 600-700
Rev/min.
4. the preparation method of atractylodes slice according to claim 1, it is characterised in that: stir agar in the step (4)
Mixing speed be 300-400 revs/min, mixing time be 3-5 hours.
5. the preparation method of atractylodes slice according to claim 1, it is characterised in that: stir rice bran in above-mentioned steps (4)
Stirring rate be 350-450 revs/min, mixing time be 2-3 hours.
6. the preparation method of atractylodes slice according to claim 1, it is characterised in that: need before the step (9) pair
Rhizoma Atractylodis Macrocephalae carries out disinfection by ultraviolet light processing.
7. the preparation method of atractylodes slice according to claim 1, it is characterised in that: every 1 hour in the step (6)
It is primary that Rhizoma Atractylodis Macrocephalae slice is stirred up and down.
8. the preparation method of atractylodes slice according to claim 1, it is characterised in that: cut in the step (5) white
The art slice time to be dried must not exceed 8 hours.
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| CN109846917A (en) * | 2018-12-26 | 2019-06-07 | 北京康美制药有限公司 | A kind of processing method of atractylodes slice |
| CN114376214A (en) * | 2021-12-15 | 2022-04-22 | 江苏省原子医学研究所 | Processing method for vacuum freeze-drying dry slices of radix momordicae |
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| CN114376214A (en) * | 2021-12-15 | 2022-04-22 | 江苏省原子医学研究所 | Processing method for vacuum freeze-drying dry slices of radix momordicae |
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