CN109044872A - Skin cleans concentrate and preparation method thereof - Google Patents
Skin cleans concentrate and preparation method thereof Download PDFInfo
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- CN109044872A CN109044872A CN201811001393.2A CN201811001393A CN109044872A CN 109044872 A CN109044872 A CN 109044872A CN 201811001393 A CN201811001393 A CN 201811001393A CN 109044872 A CN109044872 A CN 109044872A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/43—Guanidines
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/02—Drugs for dermatological disorders for treating wounds, ulcers, burns, scars, keloids, or the like
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Organic Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of skin cleaning concentrates and preparation method thereof, by 10 parts of polypeptide amide, 8 parts of lauryl sodium sulfate, 7 parts of peregal, 5 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, 1 part of chlorohexidene, 1 part of nipalgin, 2 parts of essence, 66 parts of distilled water be prepared, and preparation method includes water-bath dissolution, ethanol solution, mixing and adjusts pH value；The present invention has the advantages that it is antibacterial, disinfection, it is antipruritic.It is suitble to children, bed patient, the elderly to use, releases skin and disturb and itch, prevent bedsore.There is refrigerant sense, nonirritant to skin.It is particularly suitable for the water shortages environment such as tourism field work, convenient, healthy safety.
Description
Technical field
The present invention relates to a kind of detergent, specifically a kind of skin cleaning concentrate and preparation method thereof belongs to clear
Clean dose of field.
Background technique
China has a vast territory, and numerous bed patients, people in the countryside and field operator are numerous.Summer and autumn, they endured to the fullest extent
Can not have a bath the hardship that can not be had a bath with water shortage, and skin of not having a bath for a long time is extremely itching, or even causes skin disease.It severely impacts
With interference people's work and rest, the health of the mankind is endangered.Often cleaning skin, it is tired for eliminating, prevent disease,
Enhancing health but plays an important role.And soap meets hard water and generates insoluble calcium soap, magnesium soap in alkalinity, adheres to skin
On, it can just be washed away with a large amount of water, therefore skin cleaner cannot be done.
Summary of the invention
To solve the above-mentioned problems, the present invention devises a kind of skin cleaning concentrate, sterilizes antibacterial, easy to use, section
Water is about used, is worked well, it is without any side effects.
The technical solution of the present invention is as follows:
Concentrate is cleaned as skin, not only there are enough dirt-removing powers, but also require the pH to no skin irritation, with skin
Close, remaining will not injure skin on the skin, and performance can only be selected mild, can be in the surface-active that alkalescence condition uses
Agent.
Skin cleans concentrate, is mainly prepared by following raw material:
10 parts of polypeptide amide, 8 parts of lauryl sodium sulfate, 7 parts of peregal, 5 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, chlorohexidene
1 part, 1 part of nipalgin, 2 parts of essence, 66 parts of distilled water.
Polypeptide amide is nonionic surfactant (including 4 parts by weight of edible gelatin, the dodecane prepared with collagen
Sour 2 parts by weight, 4 parts by weight of dimethyl hydramine), there are good dirt-removing functions, have good maintenance to act on skin；
Lauryl sodium sulfate has good washing effect and foaming effect；
Peregal (fatty alcohol polyoxyethylene ether) has good wetting emulsification, dispersion, cleaning and decontamination；
The compatibility of sodium sulfate of polyethenoxy ether of fatty alcohol is good, resistance to hard water, and foam is stablized, and soil release performance is good；
Chlorohexidene (chlorhexidine) has disinfection bacteriostasis；
Nipalgin (ethyl-para-hydroxybenzoate) is preservative；
Essence is conditioning products fragrance；
20% phosphoric acid is for adjusting solution ph to 6.5-7.0.
Above-mentioned skin cleaning concentrate the preparation method is as follows:
(1) each raw material is weighed, polypeptide amide, peregal are added into equivalent amount of water, water-bath dissolution；
(2) lauryl sodium sulfate, polyethenoxy ether sodium sulfate are added into equivalent amount of water, water-bath dissolution；
(3) 70% ethyl alcohol of mass fraction is used to dissolve respectively chlorohexidene, nipalgin；
(4) essence 70% ethyl alcohol of mass fraction is diluted；
(4) successively the solution that step (2), (3), (4) obtain is added in the solution that step (1) obtains, is stirred evenly；
(5) mass fraction 20%H is used3PO4The pH value 6.5-7.0 for the solution that pacing rapid (5) obtains, finally plus distilled water, stirring
Uniformly.
The present invention has the advantages that it is antibacterial, disinfection, it is antipruritic.It is suitble to children, bed patient, the elderly to use, releases skin
It disturbs and itches, prevents bedsore.There is refrigerant sense, nonirritant to skin.It is particularly suitable for the water shortages environment such as tourism field work, conveniently, defends
Raw safety.
The present invention is further explained in the light of specific embodiments.
Specific embodiment
Hereinafter, preferred embodiments of the present invention will be described, it should be understood that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
The percentage sign " % " being related in the present invention refers to mass percent if not specified；But the percentage of solution,
Unless otherwise specified, refer to and contain several grams of solute in solution 100ml；Percentage between liquid, capacity when referring to 20 DEG C
Ratio.
Embodiment 1
Skin cleans concentrate, is mainly prepared by following raw material:
10 parts of polypeptide amide, 8 parts of lauryl sodium sulfate, 7 parts of peregal, 5 parts of sodium sulfate of polyethenoxy ether of fatty alcohol, chlorohexidene
1 part, 1 part of nipalgin, 2 parts of essence, 66 parts of distilled water.
Polypeptide amide is nonionic surfactant (including 4 parts by weight of edible gelatin, dodecane prepared with collagen
Sour 2 parts by weight, 4 parts by weight of dimethyl hydramine mix), there are good dirt-removing functions, have good maintenance to make skin
With；
Lauryl sodium sulfate has good washing effect and foaming effect；
Peregal (fatty alcohol polyoxyethylene ether) has good wetting emulsification, dispersion, cleaning and decontamination；
The compatibility of sodium sulfate of polyethenoxy ether of fatty alcohol is good, resistance to hard water, and foam is stablized, and soil release performance is good；
Chlorohexidene (chlorhexidine) has disinfection bacteriostasis；
Nipalgin (ethyl-para-hydroxybenzoate) is preservative；
Essence is conditioning products fragrance；
20% phosphoric acid is for adjusting solution ph to 6.5-7.0.
Above-mentioned skin cleaning concentrate the preparation method is as follows:
(1) each raw material is weighed, polypeptide amide, peregal are added into equivalent amount of water, water-bath dissolution；
(2) lauryl sodium sulfate, polyethenoxy ether sodium sulfate are added into equivalent amount of water, water-bath dissolution；
(3) 70% ethyl alcohol of mass fraction is used to dissolve respectively chlorohexidene, nipalgin；
(4) essence 70% ethyl alcohol of mass fraction is diluted；
(4) successively the solution that step (2), (3), (4) obtain is added in the solution that step (1) obtains, is stirred evenly；
(5) 20% H of mass fraction is used3PO4The pH value 6.5-7.0 for the solution that pacing rapid (5) obtains, finally plus distilled water, stirring
Uniformly.
Product of the present invention has the effect of antibacterial, antipruritic, suitable children, bed patient, the elderly's use, cleaning, releasing
Skin, which is disturbed, itches, prevents bedsore, prevents prickly heat, dermopathic generation.There is refrigerant sense, nonirritant to skin.It is particularly suitable for tourism
The water shortages environment such as field work, convenient, healthy safety.
In use, taking this product 2.5ml (one) plus water 500ml (about one mug water) adhesional wetting towel, i.e., for people wiping
Wipe whole body.It need not be rinsed with water after wiping.
Skin cleans the clean effect test of concentrate
(1) key instrument equipment: ZBD whiteness instrument, 1 ultrasonic cleaner of CX-.
(2) principle: the circular filter paper of artificial contamination cleans concentrate and ultrasonic cleaning with skin under conditions selected
Device washing, can partially remove the dirt on filter paper.With variation of the whiteness instrument measurement filter paper before and after washing, sample is calculated as follows
Decontamination value (R).
The rear whiteness value-of R (%)=wash washes whiteness value * 100 before preceding whiteness value/filter paper whiteness value-is washed
This number can objectively evaluate clean effect obtained by leucometer survey calculation.But it is not the decontamination number of detergent
Value, it is only indicated in a certain dirt-removing power under the conditions of selecting, for this purpose, using distilled water decontamination value as the white control in bottom, with laundry
As standard sample, skin cleans concentrate decontamination value should be suitable with the washing powder of same concentration, soap for powder, soap decontamination value.
(3) result:
1. skin cleans clean effect of the concentrate under different quality, it is shown in Table 1.
1 skin of table cleans the decontamination value under concentrate different quality
1. the 100ppm hard water that we prepare is approximately equivalent to 16 DEG C of (Cao) hard water, between medium hard water.150ppm hard water is about
25 DEG C of (Cao) hard water are equivalent to, hard water range is belonged to, as it can be seen from table 1 the hardness with dampening increases, decontamination value has decline
Trend, but still have certain clean effect, skin cleaning concentrate can use in hard water, make in medium-hard water certainly
It is preferable with effect.
2. the clean effect after skin cleaning concentrate storage: No. 10 samples, 3 parts of a formula will be tested；It (1) number is -20 DEG C
Store half a year, (2) number for after being placed 1 month in 40 DEG C of incubators when being stored at room temperature to 1 year；(3) number it is stored 1 year for normal temperature,
It the results are shown in Table 2.Various different temperatures
The decontamination value of storage is still suitable with washing powder decontamination value.
Table 2
One, safety
(1) it small white mouse median lethal dose: is tested by karber's method, obtains LD50=2.096mg/Kg (intraperitoneal injection).According to domestic work
Industry toxicological regulations, this numerical value belong to the micro- malicious range of toxicity lowermost level.
(2) lagophthalmos irritant experiment: bent grey rabbit 19 is instilled in rabbit left eye with 1:100 skin cleaning concentrate,
Right eye makees own control, drop medicine 1 hour, 6 hours, the variations of 24 hours observations conjunctivas and cornea.1 hour after drop, there are 3 rabbit knots
Film has mild hyperaemia, and there are also 1 rabbit conjunctivals to seem congested within 6 hours, and conjunctival congestion all disappears after 24 hours, does not generate knot
Film secretion and opacity of the cornea phenomenon.
The above experiment shows: skin cleans that concentrate is substantially nontoxic and irritation, is safe applied to human body.
Two, bacteriostatic experiment
(1) material
1. strain: Escherichia coli, staphylococcus aureus, S. cervisiae, black-koji mould.
2. culture medium: broth medium, Sa Shi agar medium.
(2) test method and result:
1,1:10,1:50,1:100,1:200,1:400,1:800,1 fungistatic effect: are made into skin cleaning concentrate stoste:
The culture medium of 1600 equal various concentrations is cultivated 96 hours under certain temperature after being inoculated with strain, is observed as a result, with asepsis growth
Highest dilution is the minimum inhibitory concentration of the sample, the results are shown in Table 3.
The fungistatic effect of table 3, skin cleaning concentrate
2, sterilizing time: being inoculated with strain with the skin cleaning concentrate of 3 kinds of concentration, act on 5,10,30,60,120 minutes respectively and
24, the different times such as 48,96 hours, then turn to be inoculated in 5ml culture medium by upper liquid with oese, 48 are cultivated at a certain temperature
Hour observation the results are shown in Table 4 as a result, using the shortest time without elder is given birth to as sterilizing time.
4 skin of table cleans concentrate sterilizing time
3, from the above antibacterial kind of sterilization result as it can be seen that skin cleans concentrate to Escherichia coli, staphylococcus aureus and wine brewing
Saccharomycete has preferable antibacterial and bactericidal effect, also there is certain antibacterial and killing effect to the black-koji mould in environment.Cause
This, wound contamination caused by concentrate will not be cleaned when use because of skin, and be enough to ensure that skin cleaning concentrate in storage, no
It can mildew putrid and deteriorated.
Three, human experimentation
(1) application method: skin cleaning concentrate is diluted with water to 1:200 concentration, everyone about 500ml soaks towel complete
Body is wiped repeatedly, and is then dried off the towel, and whole body is dried.
(2) scene is on probation: by certain hospital doctor, interrogation doctor collectively constitutes group with us, and doctor is instructed to try
It tests, observes clean effect, and registered by table by nurse, result on trial is shown in Table 5.
5 skin of table cleans concentrate scene normal individual trial result
Live probationary certificate: skin cleaning concentrate is easy to use, saves water, the deep welcome by the water shortage all circles people.
Four, quality examination
(1) transparency: detecting by an unaided eye is brownish red clear liquid.
(2) it resists cold: being in frozen state after placing 48 hours in -20 DEG C of refrigerators.It restores to the original state after being heated in hot water.
(3) heat-resisting: in 40 DEG C of baking ovens, 48 hours unchanged.
(4) measurement of pH value: being made into 1:200 concentration for stoste with distilled water, is measured in terms of PH, should be 6.5-7.0.
(5) decontamination value: suitable with washing powder.
Skin cleans concentrate and passes through raw material, and the screening of formula, quality examination and zoopery, human experimentation prove
It has the advantages that
(1) skin dirt can be removed, and has certain restraining and sterilizing bacteria to act on；
(2) securely and reliably, nontoxic, nonirritant；
(3) easy to use, it saves water；
(4) rear relaxation and happiness are washed, fatigue can be eliminated.
Raw materials used in the present invention is to commonly use raw material in the production of this field, can be obtained from market, and for production
As a result it will not have an impact；Various equipment employed in the present invention are conventional equipment used in the production technology of this field,
And operation, the parameter etc. of each equipment are carried out according to routine operation, have no special feature.
Claims (3)
1. skin cleans concentrate, it is characterised in that: 10 parts of polypeptide amide, 8 parts of lauryl sodium sulfate, 7 parts of peregal, fat
5 parts of alcohol polyethenoxy ether sodium sulfate, 1 part of chlorohexidene, 1 part of nipalgin, 2 parts of essence, 66 parts of distilled water.
2. skin according to claim 1 cleans concentrate, it is characterised in that: the polypeptide amide is with collagen system
Standby nonionic surfactant.
3. a kind of preparation of skin cleaning concentrate as claimed in claim 1 or 2, characterized by the following steps:
(1) each raw material is weighed, polypeptide amide, peregal are added into equivalent amount of water, water-bath dissolution；
(2) lauryl sodium sulfate, polyethenoxy ether sodium sulfate are added into equivalent amount of water, water-bath dissolution；
(3) 70% ethyl alcohol of mass fraction is used to dissolve respectively chlorohexidene, nipalgin；
(4) essence 70% ethyl alcohol of mass fraction is diluted；
(4) successively the solution that step (2), (3), (4) obtain is added in the solution that step (1) obtains, is stirred evenly；
(5) 20% H of mass fraction is used3PO4The pH value 6.5-7.0 for the solution that pacing rapid (5) obtains, finally plus distilled water, stirring
Uniformly.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811001393.2A CN109044872A (en) | 2018-08-30 | 2018-08-30 | Skin cleans concentrate and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811001393.2A CN109044872A (en) | 2018-08-30 | 2018-08-30 | Skin cleans concentrate and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109044872A true CN109044872A (en) | 2018-12-21 |
Family
ID=64757843
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811001393.2A Pending CN109044872A (en) | 2018-08-30 | 2018-08-30 | Skin cleans concentrate and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114621881A (en) * | 2021-12-30 | 2022-06-14 | 广州君研生物科技有限公司 | Saccharomyces cerevisiae fermentation liquor and skin care product comprising saccharomyces cerevisiae fermentation liquor |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1687345A (en) * | 2005-05-10 | 2005-10-26 | 刘桂堂 | Concentrated solution for washing and preparation method thereof |
| CN1995308A (en) * | 2005-12-31 | 2007-07-11 | 天津威欧斯生物科技发展有限公司 | Sterilizing paper soap |
| CN102746951A (en) * | 2011-04-19 | 2012-10-24 | 南通宏利达针织有限公司 | Paper soap and preparation method thereof |
| CN102746959A (en) * | 2011-04-19 | 2012-10-24 | 南通宏利达针织有限公司 | Liquid perfumed soap |
| CN103142422A (en) * | 2013-03-24 | 2013-06-12 | 成都携恩科技有限公司 | Lotion for cleaning and nourishing skin surface |
| CN104055703A (en) * | 2014-06-18 | 2014-09-24 | 中山职业技术学院 | Dandruff-removing itching-relieving liquid shampoo and preparation method thereof |
-
2018
- 2018-08-30 CN CN201811001393.2A patent/CN109044872A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1687345A (en) * | 2005-05-10 | 2005-10-26 | 刘桂堂 | Concentrated solution for washing and preparation method thereof |
| CN1995308A (en) * | 2005-12-31 | 2007-07-11 | 天津威欧斯生物科技发展有限公司 | Sterilizing paper soap |
| CN102746951A (en) * | 2011-04-19 | 2012-10-24 | 南通宏利达针织有限公司 | Paper soap and preparation method thereof |
| CN102746959A (en) * | 2011-04-19 | 2012-10-24 | 南通宏利达针织有限公司 | Liquid perfumed soap |
| CN103142422A (en) * | 2013-03-24 | 2013-06-12 | 成都携恩科技有限公司 | Lotion for cleaning and nourishing skin surface |
| CN104055703A (en) * | 2014-06-18 | 2014-09-24 | 中山职业技术学院 | Dandruff-removing itching-relieving liquid shampoo and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114621881A (en) * | 2021-12-30 | 2022-06-14 | 广州君研生物科技有限公司 | Saccharomyces cerevisiae fermentation liquor and skin care product comprising saccharomyces cerevisiae fermentation liquor |
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Application publication date: 20181221 |