CN109014225A - Globular metallic powder preparation facilities reactor and globular metallic powder preparation facilities - Google Patents

Globular metallic powder preparation facilities reactor and globular metallic powder preparation facilities Download PDF

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Publication number
CN109014225A
CN109014225A CN201811207588.2A CN201811207588A CN109014225A CN 109014225 A CN109014225 A CN 109014225A CN 201811207588 A CN201811207588 A CN 201811207588A CN 109014225 A CN109014225 A CN 109014225A
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CN
China
Prior art keywords
preparation facilities
reaction chamber
chamber
metallic powder
powder preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811207588.2A
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Chinese (zh)
Inventor
邢雪青
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Institute of High Energy Physics of CAS
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Institute of High Energy Physics of CAS
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Priority to CN201811207588.2A priority Critical patent/CN109014225A/en
Publication of CN109014225A publication Critical patent/CN109014225A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/0832Handling of atomising fluid, e.g. heating, cooling, cleaning, recirculating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/088Fluid nozzles, e.g. angle, distance
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/0888Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid casting construction of the melt process, apparatus, intermediate reservoir, e.g. tundish, devices for temperature control

Abstract

The invention discloses globular metallic powder preparation facilities reactors, including reaction chamber, gas nozzle is provided on the reaction chamber, the outer wall of the reaction chamber is equipped with heat transfer mechanism, the heat transfer mechanism includes gas heating chamber and cooling chamber, the gas heating chamber is contacted with reacting outdoor wall, and is connected to the gas nozzle, and the cooling chamber is contacted with gas heating chamber.The invention also discloses a kind of globular metallic powder preparation facilities using above-mentioned reactor.It is an advantage of the current invention that the heat using reaction chamber heats inert gas, it is ensured that air-flow, with certain temperature, avoids that blocking package phenomenon occurs, improve material property when impacting molten metal;The temperature of powder high-pressure inert gas usually processed is -69 DEG C or so, and cooling medium is generally room temperature, utilizes the reactor, gas two-way absorption heat out of reaction chamber wall body and cooling chamber is heated, also cooled down simultaneously to cooling medium, energy consumption, save the cost is effectively reduced.

Description

Globular metallic powder preparation facilities reactor and globular metallic powder preparation facilities
Technical field
The invention belongs to the preparation facilities technical fields of increasing material manufacturing globular metallic powder, and in particular to a kind of spherical gold Belong to powder preparing unit reactor and globular metallic powder preparation facilities.
Background technique
Increases material manufacturing technology, also known as 3D printing technique are that the whole world is first in the past 30 years as a kind of non-traditional processing technology A kind of advanced manufacturing technology for collecting light, mechanical, electrical, computer, numerically-controlled machine tool, new material etc. with one risen into manufacturing field.
Currently, dusty material used in metal material increasing field is globular metallic powder, main preparation methods packet Include vacuum induction gas atomization (VIGA), electrode induction gas atomization (EIGA), plasma atomization process (PA), radio frequency etc. Ion spheroidizing process (PS), ultrasonic atomization technique etc..The common feature of above-mentioned various methods be all formed in reaction chamber it is small Granular metal liquid, then through rapidly cooling to form spherical powder.In aerosolization technology, high-speed flow impact fusion molten metal it Before, after air-flow is heated, atomization process can be significantly improved, so that atomization success rate, material properties are promoted.Conventional at present Powder manufacturing apparatus is heated such as electric heater unit to gas by being equipped with independent gas-heating apparatus.In addition, in powder processed The molten metal bath of process high temperature meeting knock-on reaction chamber interior walls under the impact of air-flow, cause reaction chamber temperature to increase, to protect Normal powder processed is demonstrate,proved, needs to be equipped with cooling equipment and cools down to reaction chamber, common cooling equipment is water cooling plant, cooling water one As be room temperature, when use, also needs to cool down to it.
Summary of the invention
Technical problem to be solved by the present invention lies in: existing fuel pulverizing plant needs to be equipped with gas-heating apparatus and reaction chamber Cooling device, leading to it, energy consumption is high, at high cost.
The present invention solves above-mentioned technical problem using following technical scheme:
Globular metallic powder preparation facilities reactor, including reaction chamber are provided with gas nozzle on the reaction chamber, institute The outer wall for stating reaction chamber is equipped with heat transfer mechanism, and the heat transfer mechanism includes gas heating chamber and cooling chamber, the gas Heating chamber is contacted with reacting outdoor wall, and is connected to the gas nozzle, and the cooling chamber is contacted with gas heating chamber.
Preferably, globular metallic powder preparation facilities reactor of the present invention is set on the outer wall of the reaction chamber There is the intraformational bed being connected with gas nozzle, the intraformational bed is equipped with outside sandwich, the intraformational bed structure away from the side of reaction chamber At the gas heating chamber, the outside sandwich constitutes the cooling chamber.
Preferably, globular metallic powder preparation facilities reactor of the present invention, the outer wall of the reaction chamber are submitted It is alternately disposed with first runner and second flow channel, the first runner is connected to constitute the gas heating with the gas nozzle Chamber, the second flow channel constitute the cooling chamber.
Preferably, globular metallic powder preparation facilities reactor of the present invention, the first runner and second Road in the shape of a spiral, and surround reaction chamber.
Preferably, globular metallic powder preparation facilities reactor of the present invention, the reacting outdoor wall are equipped with One interlayer, the interlayer is interior to be divided into multiple first runners and multiple second flow channels by partition.
Preferably, globular metallic powder preparation facilities reactor of the present invention, the outer wall of the reaction chamber are submitted The first slot and the second slot are alternately offered, cover board is also covered on reacting outdoor wall, between first slot and cover board described in formation First runner forms the second flow channel between second slot and cover board.
The present invention also provides a kind of globular metallic powder preparation facilities comprising reactor, the reactor are above-mentioned Spherical metal put preparation facilities reactor.
The technology of the present invention the utility model has the advantages that
Technical solution of the present invention introduces gas heating chamber on reacting outdoor wall, using reaction chamber wall body heat to lazy Property gas heated, with certain temperature, avoid that blocking package phenomenon occurs to ensure air-flow when impacting molten metal, improve material Expect performance;The temperature of powder high-pressure inert gas usually processed is -69 DEG C or so, and cooling medium is generally room temperature, utilizes the reaction Device, gas two-way absorption heat out of reaction chamber wall body and cooling chamber is heated, while also being cooled down to cooling medium, is had Effect reduces energy consumption, save the cost.
Detailed description of the invention
Fig. 1 is the cross-sectional view of globular metallic powder preparation facilities reactor described in the embodiment of the present invention one;
Fig. 2 is the cross-sectional view of globular metallic powder preparation facilities reactor described in the embodiment of the present invention two;
Fig. 3 is the cross-sectional view of globular metallic powder preparation facilities reactor described in the embodiment of the present invention three.
Specific embodiment
For convenient for those skilled in the art understand that technical solution of the present invention, now in conjunction with Figure of description to the technology of the present invention side Case is described further.
It is as shown in Figure 1 globular metallic powder preparation facilities reactor of the present invention comprising reaction chamber 1, instead It answers the upper end of room 1 to be provided with gas nozzle 2, heat transfer mechanism 3, the hot transmitting machine is provided on the outer wall of reaction chamber 1 Structure 3 include gas heating chamber 31 and waterway 32, wherein the gas heating chamber 31 is contacted with the outer wall of reaction chamber 1, and with institute State the connection of gas nozzle 2;The waterway 32 is contacted with gas heating chamber 31.In powder processed, high pressure inert gas gas coming through adds Hot 31 inflow gas nozzle of chamber, during this, high pressure inert air-flow can be absorbed from the wall body and waterway 32 of reaction chamber 1 heat into Row preheating, prepares globular metallic powder to impact fusion molten metal.
It is illustrated below by way of structure of the specific embodiment to the globular metallic powder preparation facilities reactor.
Embodiment one
Refering to fig. 1, it is provided with intraformational bed on the outer wall of the reaction chamber 1, which is connected with the gas nozzle 2 To constitute the gas heating chamber 31;The side away from reaction chamber 1 of intraformational bed is provided with outside sandwich, which is constituted The waterway 32.
It is passed through room temperature cooling water when powder processed, in outside sandwich, high pressure inert air-flow is passed through in intraformational bed, high pressure inert air-flow exists During intraformational bed inflow gas nozzle 2, heat exchange, two-way absorption can be carried out with the wall body and outside sandwich of reaction chamber 1 Heat is reached and sprays powder processed by gas nozzle 2 after certain temperature effectively to be heated to high pressure inert air-flow.
Embodiment two
It is the diagrammatic cross-section of globular metallic powder preparation facilities reactor described in the present embodiment, at this shown in Fig. 2 In embodiment, first runner and second flow channel, the first runner and institute are alternately disposed on the outer wall of the reaction chamber 1 The connection of gas nozzle 2 is stated to constitute the gas heating chamber 31, the second flow channel constitutes the cooling chamber 32.
Specifically, the outer wall of the reaction chamber 1 is equipped with an interlayer, passes through partition 33 in the interlayer and is divided into several The first runner and several described second flow channels.
Preferably, the first runner and second flow channel are helical form and surround reaction chamber 1, it is able to extend gas in this way The length of body heating chamber 31 enables the wall of air-flow, reaction chamber 1 substantially more to realize heat exchange, further improves high pressure The heating effect of inert gas.
Embodiment three
It is the cross-sectional view of globular metallic powder preparation facilities reactor described in the present embodiment, the present embodiment described in Fig. 3 It is that first runner, the generation type of second flow channel are different from the difference of embodiment two, is by being realized with flowering structure: The first slot and the second slot are alternately offered on the outer wall of the reaction chamber 1, and cover board 34, institute are also covered on 1 outer wall of reaction chamber It states and forms the first runner between the first slot and cover board 34, form the second flow channel between second slot and cover board 34.
Example IV
Present embodiments provide a kind of globular metallic powder preparation facilities comprising reactor, the reactor are real Apply any reactor of the example one into embodiment three.Here globular metallic powder preparation facilities includes vacuum induction aerosolization Powder manufacturing apparatus, plasma powder by atomization equipment, radio frequency plasma nodularization powder manufacturing apparatus, surpasses electrode induction gas-atomized powder equipment Sound wave powder by atomization equipment etc..
Technical solution of the present invention is exemplarily described invention above in conjunction with attached drawing, it is clear that present invention specific implementation It is not subject to the restrictions described above, changes as long as using the various unsubstantialities that the inventive concept and technical scheme of the present invention carry out Into, or it is not improved the conception and technical scheme of invention are directly applied into other occasions, in protection scope of the present invention Within.

Claims (7)

1. globular metallic powder preparation facilities reactor, including reaction chamber, it is provided with gas nozzle on the reaction chamber, it is special Sign is, the outer wall of the reaction chamber is equipped with heat transfer mechanism, and the heat transfer mechanism includes gas heating chamber and cooling chamber, The gas heating chamber is contacted with reacting outdoor wall, and is connected to the gas nozzle, and the cooling chamber connects with gas heating chamber Touching.
2. globular metallic powder preparation facilities reactor according to claim 1, which is characterized in that the reaction chamber Outer wall is equipped with the intraformational bed being connected with gas nozzle, and the intraformational bed is equipped with outside sandwich away from the side of reaction chamber, described Intraformational bed constitutes the gas heating chamber, and the outside sandwich constitutes the cooling chamber.
3. globular metallic powder preparation facilities reactor according to claim 1, which is characterized in that the reaction chamber First runner and second flow channel are alternately disposed on outer wall, the first runner is connected to described to constitute with the gas nozzle Gas heating chamber, the second flow channel constitute the cooling chamber.
4. globular metallic powder preparation facilities reactor according to claim 3, which is characterized in that the first runner In the shape of a spiral with second flow channel, and around reaction chamber.
5. globular metallic powder preparation facilities reactor according to claim 3 or 4, which is characterized in that the reaction Chamber outer wall is equipped with an interlayer, and the interlayer is interior to be divided into the first runner and the second flow channel by partition.
6. globular metallic powder preparation facilities reactor according to claim 3 or 4, which is characterized in that the reaction The first slot and the second slot are alternately offered on the outer wall of room, and cover board, first slot and lid are also covered on reacting outdoor wall The first runner is formed between plate, forms the second flow channel between second slot and cover board.
7. globular metallic powder preparation facilities comprising reactor, which is characterized in that the reactor is appointed for claim 1-6 Spherical metal described in one puts preparation facilities reactor.
CN201811207588.2A 2018-10-17 2018-10-17 Globular metallic powder preparation facilities reactor and globular metallic powder preparation facilities Pending CN109014225A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811207588.2A CN109014225A (en) 2018-10-17 2018-10-17 Globular metallic powder preparation facilities reactor and globular metallic powder preparation facilities

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811207588.2A CN109014225A (en) 2018-10-17 2018-10-17 Globular metallic powder preparation facilities reactor and globular metallic powder preparation facilities

Publications (1)

Publication Number Publication Date
CN109014225A true CN109014225A (en) 2018-12-18

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Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3297411A (en) * 1963-06-10 1967-01-10 Laporte Titanium Ltd Burner reactor apparatus
KR800000526B1 (en) * 1975-10-07 1980-06-14 죠지후랭크린 타가드쥬니어 High temperature chemical reaction processes utilizing fluic-wall reactors
JP2002226903A (en) * 2001-02-01 2002-08-14 Hitachi Metals Ltd Equipment for manufacturing fine metal ball
CN101125369A (en) * 2007-09-29 2008-02-20 清华大学 Device for preparing welding tin ball
CN102027208A (en) * 2007-12-27 2011-04-20 英什沃克斯公司 High-efficiency catalytic converters for treating exhaust gases
KR20110049487A (en) * 2009-11-05 2011-05-12 덕산하이메탈(주) Apparatus for manufacturing the metal powder
CN103736435A (en) * 2013-12-27 2014-04-23 中国神华能源股份有限公司 Device and system for spheroidizing powder by using alternating-current plasmas
CN103846447A (en) * 2012-12-06 2014-06-11 北京有色金属研究总院 Gas atomization preparation method of fine spherical titanium or titanium alloy powder
CN105458277A (en) * 2015-12-19 2016-04-06 江永斌 Device and method for producing high-purity metal powder through multi-head non-transferred arc plasma polymerization
KR20160084530A (en) * 2015-01-05 2016-07-14 공주대학교 산학협력단 Multi Cooling System for Producing Metal and Alloy Spherical Powders
CN105855560A (en) * 2016-05-27 2016-08-17 广州纳联材料科技有限公司 Spherical metal powder and preparation method thereof
CN106914626A (en) * 2017-04-10 2017-07-04 西安铂力特激光成形技术有限公司 The preparation facilities and preparation method of a kind of submicron metal
CN107175337A (en) * 2017-05-22 2017-09-19 加拿大艾浦莱斯有限公司 A kind of metal powder preparation method and its device based on plasma atomization technique
CN108188408A (en) * 2018-01-04 2018-06-22 北京理工大学 A kind of spherical atomization magnesium zinc non-crystaline amorphous metal powder and preparation method thereof
CN108465822A (en) * 2018-05-02 2018-08-31 朱秀峰 A kind of preparation method and preparation facilities of globular metallic powder
CN208913140U (en) * 2018-10-17 2019-05-31 中国科学院高能物理研究所 Globular metallic powder preparation facilities reactor and globular metallic powder preparation facilities

Patent Citations (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3297411A (en) * 1963-06-10 1967-01-10 Laporte Titanium Ltd Burner reactor apparatus
GB1092883A (en) * 1963-06-10 1967-11-29 Laporte Titanium Ltd Improvements in and relating to the manufacture of oxides
KR800000526B1 (en) * 1975-10-07 1980-06-14 죠지후랭크린 타가드쥬니어 High temperature chemical reaction processes utilizing fluic-wall reactors
JP2002226903A (en) * 2001-02-01 2002-08-14 Hitachi Metals Ltd Equipment for manufacturing fine metal ball
CN101125369A (en) * 2007-09-29 2008-02-20 清华大学 Device for preparing welding tin ball
CN102027208A (en) * 2007-12-27 2011-04-20 英什沃克斯公司 High-efficiency catalytic converters for treating exhaust gases
KR20110049487A (en) * 2009-11-05 2011-05-12 덕산하이메탈(주) Apparatus for manufacturing the metal powder
CN103846447A (en) * 2012-12-06 2014-06-11 北京有色金属研究总院 Gas atomization preparation method of fine spherical titanium or titanium alloy powder
CN103736435A (en) * 2013-12-27 2014-04-23 中国神华能源股份有限公司 Device and system for spheroidizing powder by using alternating-current plasmas
KR20160084530A (en) * 2015-01-05 2016-07-14 공주대학교 산학협력단 Multi Cooling System for Producing Metal and Alloy Spherical Powders
CN105458277A (en) * 2015-12-19 2016-04-06 江永斌 Device and method for producing high-purity metal powder through multi-head non-transferred arc plasma polymerization
CN105855560A (en) * 2016-05-27 2016-08-17 广州纳联材料科技有限公司 Spherical metal powder and preparation method thereof
CN106914626A (en) * 2017-04-10 2017-07-04 西安铂力特激光成形技术有限公司 The preparation facilities and preparation method of a kind of submicron metal
CN107175337A (en) * 2017-05-22 2017-09-19 加拿大艾浦莱斯有限公司 A kind of metal powder preparation method and its device based on plasma atomization technique
CN108188408A (en) * 2018-01-04 2018-06-22 北京理工大学 A kind of spherical atomization magnesium zinc non-crystaline amorphous metal powder and preparation method thereof
CN108465822A (en) * 2018-05-02 2018-08-31 朱秀峰 A kind of preparation method and preparation facilities of globular metallic powder
CN208913140U (en) * 2018-10-17 2019-05-31 中国科学院高能物理研究所 Globular metallic powder preparation facilities reactor and globular metallic powder preparation facilities

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