CN109010225A - A kind of coral reef peel off pack and preparation method thereof - Google Patents

A kind of coral reef peel off pack and preparation method thereof Download PDF

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Publication number
CN109010225A
CN109010225A CN201810961160.0A CN201810961160A CN109010225A CN 109010225 A CN109010225 A CN 109010225A CN 201810961160 A CN201810961160 A CN 201810961160A CN 109010225 A CN109010225 A CN 109010225A
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parts
coral reef
peel
pack
alcohol
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王子玉
汪稔
徐功娣
徐秋阳
沈悦
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Hainan Tropical Ocean University
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Hainan Tropical Ocean University
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Priority to CN201810961160.0A priority Critical patent/CN109010225A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/731Cellulose; Quaternized cellulose derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/736Chitin; Chitosan; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8129Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Zoology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of coral reef peels off pack and preparation method thereof, in parts by weight, including following component: 4~6 parts of hydroxy propyl cellulose, 5~9 parts of polyvinyl alcohol, 5~9 parts of chitosan quaternary ammonium salt, 2~4 parts of propylene glycol, 4~8 parts of coral reef alcohol extraction liquid, 3~5 parts of ethyl alcohol, 0.1~0.14 part of Bergamot, 0.06~0.1 part of eucalyptus quintessence oil, 64~70 parts of deionized water;Through extraction, weighs, is mixed with to obtain.Coral reef peel off pack provided by the invention, for appearance luster naturally, the gel that is creamy white, skin sense is salubrious, mild nonirritant, easy to apply uniform, does not expand pore, film forming is strong, is easy to tear;It is coral reef peel off pack energy cleaning skin of the invention, oil-control, moisturizing, anti-oxidant, and physical stability is high, bacteriostasis property is excellent, moreover it is possible to make full use of the coral reef resource in ocean.

Description

A kind of coral reef peel off pack and preparation method thereof
Technical field
The present invention relates to cosmetic field, it is specifically related to a kind of coral reef peel off pack and preparation method thereof.
Background technique
Coral reef is a kind of reef rock mass made of reef-building coral and other reef-building organism remains long time sedimentations, and coral reef is total Area conservative estimation is 28.43 ten thousand square kilometres, accounts for about the 2.5% of global ocean area, about accumulates 6.4 hundred million tons of carbonic acid every year Salt.Global coral is more common in the Perenniporia martius shallow sea area between 30 degree of north and south latitude, especially with peaceful midocean, western residence More, coral reef gross area conservative estimation is 28.43 ten thousand square kilometres, and coral reef sea area accounts for about the 2.5% of global ocean area.It removes Part Gem Grade coral, common coral is widely distributed in Hainan Region, rich reserves, and reasonable development can form a kind of renewable money Source.
Coral reef mineralogical composition is mainly aragonite and high-magnesian calcite, and chemical component is mainly calcium carbonate, coral sand, due to Its depositional environment is special, and remains the Small Holes in protist skeleton mostly without long-distance carrying during the deposition process Therefore gap forms and is also easy to produce the features such as cementing between particle porous gap, in irregular shape, easily broken, particle, wherein removing mineral A large amount of organic matters are also retained outside ingredient.
Coral reef has the effect of skin maintenance and cosmetic benefits, blood circulation-activating eyesight-improving, is a kind of rare medicinal herbs.But at present with coral reef be mainly at Point facial mask it is less, therefore need a kind of coral reef facial mask, can beautifying face and moistering lotion, moreover it is possible to make full use of marine resources.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of energy cleaning skins, oil-control, moisturizing, oxidation resistant coral reef Facial mask.
To achieve the above object, the invention adopts the following technical scheme:
A kind of coral reef peel off pack, in parts by weight, including following component: 4~6 parts of hydroxy propyl cellulose, gather 5~9 parts of vinyl alcohol, 5~9 parts of chitosan quaternary ammonium salt, 2~4 parts of propylene glycol, 4~8 parts of coral reef alcohol extraction liquid, ethyl alcohol 3~5 Part, 0.1~0.14 part of Bergamot, 0.06~0.1 part of eucalyptus quintessence oil, 64~70 parts of deionized water.
Hydroxy propyl cellulose is used as thickener, and coral reef peel off pack is made to have certain consistency, easily shapes.
Polyvinyl alcohol is pharmaceutical grade, is a kind of extremely safe macromolecule organic, nontoxic to the human body, without side-effects, is had Good biocompatibility, uses as film forming agent, after coral reef peel off pack is smeared uniformly, becomes the film that can be torn Shape.
Chitosan quaternary ammonium salt has good antibiotic property, film forming, Cation adsorption, moisture absorbability and moisture retentivity, flocculability, resists The performances such as static behaviour.
Coral reef alcohol extraction liquid is adjustable skin pH, controls skin water and oil balance, moreover it is possible to anti-oxidant.
Bergamot is extracted from finger citron tree, and Rutaceae Citrus is belonged to, and taste is pure and fresh, can be created one kind and be put Loose and pleasant feeling;And antibacterial action is obvious, to eczema, chronic eczema, acne, scabies, varication, wound, bubble rash, skin and The seborrheic dermatitis of scalp is effective in cure;It is especially beneficial to Oily, the smegma of oily skin can be balanced, and outstanding Add sharp essential oil and used time, it is excellent to skin ulcer curative effect.
Eucalyptus quintessence oil can prevent bacteria breed, promote neoblastic construction.
Preferably, a kind of coral reef peel off pack, in parts by weight, including following component: hydroxy propyl cellulose 5 Part, 7 parts of polyvinyl alcohol, 7 parts of chitosan quaternary ammonium salt, 3 parts of propylene glycol, 6 parts of coral reef alcohol extraction liquid, 4 parts of ethyl alcohol, bergamot essence 0.12 part, 0.08 part of eucalyptus quintessence oil, 67 parts of deionized water of oil.
Further, a kind of preparation method of coral reef peel off pack, the specific steps are as follows:
(1) it produces coral reef alcohol extraction liquid: coral reef is crushed to 250~300 mesh, coral reef powder is pressed with ethyl alcohol The ratio of 1:1 (parts by weight) mixes, 16~20 DEG C, 700~1000rpm/min, shakes 1~3 day, 4000~6000rpm/ Min is centrifuged 15~20min, takes supernatant, obtains coral reef alcohol extraction liquid;
(2) it weighs: the coral reef alcohol extraction liquid that step (1) is prepared, hydroxy propyl cellulose, polyvinyl alcohol, Chitosan quaternary ammonium salt, propylene glycol, ethyl alcohol, Bergamot, eucalyptus quintessence oil and deionized water, weigh in parts by weight respectively, It is spare;
(3) propylene glycol that step (2) weigh is added into deionized water dissolving;
(4) by hydroxy propyl cellulose, polyvinyl alcohol, step (3) plus deionized water dissolving is added with ethanol wet Propylene glycol, dissolve by heating at 65~75 DEG C, obtain mixture A;
(5) chitosan quaternary ammonium salt, coral reef alcohol extraction liquid are mixed, then with Bergamot, eucalyptus quintessence oil and cold But the mixture A mixing after, obtains mixture B;
(6) mixture B 800~1200rpm/min of refiner is stirred into 20~40min, obtains mixture C;
(7) mixture C is dispensed, is vacuum-packed, obtains coral reef peel off pack finished product.It is protected from light low temperature or is stored at room temperature.
Preferably, step (1) produces coral reef alcohol extraction liquid: coral reef is crushed to 300 mesh, by coral reef powder with Ethyl alcohol is mixed in the ratio of 1:1, and 18 DEG C, 800rpm/min shake 2 days, and 4000rpm/min is centrifuged 20min, is taken supernatant, is obtained Coral reef alcohol extraction liquid.
Preferably, hydroxy propyl cellulose, polyvinyl alcohol are added step (3) with ethanol wet plus gone by step (4) The propylene glycol of ionized water dissolution, dissolves by heating at 70 DEG C, obtains mixture A.
Preferably, mixture B refiner 1000rpm/min is stirred 30min by step (6), obtains mixture C.
The beneficial effects of the present invention are: coral reef peel off pack of the invention, appearance luster is naturally, the gel that is creamy white Shape, skin sense is salubrious, mild nonirritant, easy to apply uniform, does not expand pore, film forming is strong, is easy to tear;Coral of the invention It is reef peel off pack energy cleaning skin, oil-control, moisturizing, anti-oxidant, and physical stability is high, bacteriostasis property is excellent, moreover it is possible to sufficiently Utilize the coral reef resource in ocean.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this The embodiment of invention for those of ordinary skill in the art without creative efforts, can also basis The attached drawing of offer obtains other attached drawings.
Fig. 1 attached drawing is the test result of skin surface water content after applying coral reef peel off pack prepared by embodiment 1 Figure;
Fig. 2 attached drawing is the skin picture applied before coral reef peel off pack prepared by embodiment 1;
Fig. 3 attached drawing is the coral reef peel off pack 20min for applying embodiment 1 and preparing, and tears the skin after removal facial mask Skin picture;
Fig. 4 attached drawing is to smear olive oil, the fuel-displaced picture of simulated skin;
Fig. 5 attached drawing is the picture applied after coral reef peel off pack prepared by embodiment 1;
Fig. 6 attached drawing is the coral reef peel off pack 20min for applying embodiment 1 and preparing, and tears the skin after removal facial mask Skin picture.
Specific embodiment
The given examples are served only to explain the present invention below, is not intended to limit the scope of the present invention.
Embodiment 1
A kind of coral reef peel off pack, in parts by weight, including following component: 5 parts of hydroxy propyl cellulose, polyethylene 7 parts of alcohol, 7 parts of chitosan quaternary ammonium salt, 3 parts of propylene glycol, 6 parts of coral reef alcohol extraction liquid, 4 parts of ethyl alcohol, 0.12 part of Bergamot, 0.08 part of eucalyptus quintessence oil, 67 parts of deionized water.
The preparation method of coral reef peel off pack, the specific steps are as follows:
(1) it produces coral reef alcohol extraction liquid: coral reef is crushed to 300 mesh, by coral reef powder and ethyl alcohol by 1:1's Ratio mixing, 18 DEG C, 800rpm/min shake 2 days, and 4000rpm/min is centrifuged 20min, takes supernatant, obtain coral reef ethyl alcohol extraction Take liquid;
(2) it weighs: the coral reef alcohol extraction liquid that step (1) is prepared, hydroxy propyl cellulose, polyvinyl alcohol, Chitosan quaternary ammonium salt, propylene glycol, ethyl alcohol, Bergamot, eucalyptus quintessence oil and deionized water, weigh in parts by weight respectively, It is spare;
(3) propylene glycol that step (2) weigh is dissolved in water;
(4) by hydroxy propyl cellulose, polyvinyl alcohol, step (3) plus deionized water dissolving is added with ethanol wet Propylene glycol, dissolve by heating at 70 DEG C, obtain mixture A;
(5) chitosan quaternary ammonium salt, coral reef alcohol extraction liquid are mixed, then with Bergamot, eucalyptus quintessence oil and cold But the mixture A mixing after, obtains mixture B;
(6) mixture B refiner 1000rpm/min is stirred into 30min, obtains mixture C;
(7) mixture C is dispensed to bag, is vacuum-packed, obtains coral reef peel off pack finished product.
Embodiment 2
A kind of coral reef peel off pack, in parts by weight, including following component: 4 parts of hydroxy propyl cellulose, polyethylene 5 parts of alcohol, 5 parts of chitosan quaternary ammonium salt, 2 parts of propylene glycol, 4 parts of coral reef alcohol extraction liquid, 3 parts of ethyl alcohol, 0.1 part of Bergamot, 0.06 part of eucalyptus quintessence oil, 64 parts of deionized water.
The preparation method of coral reef peel off pack, the specific steps are as follows:
(1) it produces coral reef alcohol extraction liquid: coral reef is crushed to 250 mesh, by coral reef powder and ethyl alcohol by 1:1's Ratio mixing, 16 DEG C, 700rpm/min shake 3 days, and 6000rpm/min is centrifuged 15min, takes supernatant, obtain coral reef ethyl alcohol extraction Take liquid;
(2) it weighs: the coral reef alcohol extraction liquid that step (1) is prepared, hydroxy propyl cellulose, polyvinyl alcohol, Chitosan quaternary ammonium salt, propylene glycol, ethyl alcohol, Bergamot, eucalyptus quintessence oil and deionized water, weigh in parts by weight respectively, It is spare;
(3) propylene glycol that step (2) weigh is dissolved in water;
(4) by hydroxy propyl cellulose, polyvinyl alcohol, step (3) plus deionized water dissolving is added with ethanol wet Propylene glycol, dissolve by heating at 65 DEG C, obtain mixture A;
(5) chitosan quaternary ammonium salt, coral reef alcohol extraction liquid are mixed, then with Bergamot, eucalyptus quintessence oil and cold But the mixture A mixing after, obtains mixture B;
(6) mixture B refiner 800rpm/min is stirred into 40min, obtains mixture C;
(7) mixture C is dispensed to plastic tank, is vacuum-packed, obtains coral reef peel off pack finished product.
Embodiment 3
A kind of coral reef peel off pack, in parts by weight, including following component: 6 parts of hydroxy propyl cellulose, polyethylene 9 parts of alcohol, 9 parts of chitosan quaternary ammonium salt, 4 parts of propylene glycol, 8 parts of coral reef alcohol extraction liquid, 5 parts of ethyl alcohol, 0.14 part of Bergamot, 0.1 part of eucalyptus quintessence oil, 70 parts of deionized water.
The preparation method of coral reef peel off pack, the specific steps are as follows:
(1) it produces coral reef alcohol extraction liquid: coral reef is crushed to 280 mesh, by coral reef powder and ethyl alcohol by 1:1's Ratio mixing, 20 DEG C, 1000rpm/min shake 1 day, and 5000rpm/min is centrifuged 18min, take supernatant, obtain coral reef ethyl alcohol Extract liquor;
(2) it weighs: the coral reef alcohol extraction liquid that step (1) is prepared, hydroxy propyl cellulose, polyvinyl alcohol, Chitosan quaternary ammonium salt, propylene glycol, ethyl alcohol, Bergamot, eucalyptus quintessence oil and deionized water, weigh in parts by weight respectively, It is spare;
(3) propylene glycol that step (2) weigh is dissolved in water;
(4) by hydroxy propyl cellulose, polyvinyl alcohol, step (3) plus deionized water dissolving is added with ethanol wet Propylene glycol, dissolve by heating at 75 DEG C, obtain mixture A;
(5) chitosan quaternary ammonium salt, coral reef alcohol extraction liquid are mixed, then with Bergamot, eucalyptus quintessence oil and cold But the mixture A mixing after, obtains mixture B;
(6) mixture B refiner 1200rpm/min is stirred into 20min, obtains mixture C;
(7) mixture C is dispensed, is vacuum-packed, obtains coral reef peel off pack finished product.
Embodiment 4
Embodiment 1-3 coral reef peel off pack produced is carried out according to 2015 " cosmetics safety technical specification " Detection, testing result are as shown in Table 1.
Table one:
By above-mentioned testing result it is found that coral reef peel off pack prepared by the present invention meets " cosmetics safety skill Art specification ", securely and reliably.
5 skin hypersensitivity of embodiment test (volunteer of the present invention meets subject and volunteers inclusion criteria)
(1) coral reef peel off pack prepared by embodiment 1-3 more rabbits are applied to respectively to scrape on the skin of hair, As a result, it has been found that more rabbits do not occur any cutaneous anaphylaxis phenomenon, more rabbits are acted normally after coating.
(2) 15 volunteers are collected, are divided into 3 groups, coral reef peel off pack prepared by 1-3 of the embodiment of the present invention is smeared In experimenter's skin of dorsum of hand, volunteer indicates that coating part has clearly moist feeling.In 7d, 15 volunteers do not occur Any cutaneous anaphylaxis phenomenon, does not feel any stimulation yet after coating.
The test of 6 film-formation result of embodiment
6 volunteers are collected, are named as No. 1-6, are divided into 3 groups, after cleaning volunteer's hand and drying, smears implement respectively The coral reef peel off pack of example 1-3 preparation, film formation time are as shown in Table 2.
Table two:
The result shows that after 20min, facial mask go completely into can tear it is membranaceous;Film-formation result is good, and film quality is softer, tears Without obvious pain, without red and swollen phenomenon after tearing;Film is more easily separated, tears clean noresidue.
7 moisturizing of embodiment test
Volunteer is collected, volunteer's hand skin is cleaned, then applies coral reef peel off pack prepared by embodiment 1. Afterwards respectively at before use, after use (coating 20min, after removal tears facial mask), using rear 1h, skin surface water content is tested, As a result as shown in Figure 1 (skin moisture content is as a percentage).The result shows that facial mask of the invention after use has skin Obvious moisturizing effect, is also able to maintain certain moisture after using 1 hour.And picture is compared before and after the use of microscope photographing See, after use (Fig. 3) than (Fig. 2) before use, the obvious fine and smooth many of skin.
The test of 8 cleaning force of embodiment
Olive oil is smeared into volunteer's skin, simulated skin is fuel-displaced.Coral reef prepared by the embodiment of the present invention 1 is smeared later Peel off pack tears after 20min, records the process with microscope.It, can such as Fig. 4-6 as can be seen that the facial mask cleaning force is good Skin surface excess oil is removed, and is not felt after use tight.Image when by forming a film as it can be seen that the facial mask film forming is good, point Cloth is uniform, has good surface tension.
Other tests of embodiment 9
Test content Test method Test result
Physical stability Repeatedly centrifugation Physical stability is high
Inoxidizability It is tested in exposure air Stablize 7 days or more
Biocidal property Inhibition zone Biocidal property is excellent
Embodiment 10
By coral reef peel off pack prepared by the present invention compared with dew orchid Ji Na bamboo charcoal available on the market tears facial mask, Facial mask of the invention is easier to push open, is not dried with rear skin, does not expand pore, and is easier to tear.
The foregoing is merely presently preferred embodiments of the present invention, is not intended to limit the invention, it is all in spirit of the invention and Within principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims (6)

1. a kind of coral reef peel off pack, which is characterized in that in parts by weight, including following component: hydroxy propyl cellulose 4 ~6 parts, 5~9 parts of polyvinyl alcohol, 5~9 parts of chitosan quaternary ammonium salt, 2~4 parts of propylene glycol, 4~8 parts of coral reef alcohol extraction liquid, 3~5 parts of ethyl alcohol, 0.1~0.14 part of Bergamot, 0.06~0.1 part of eucalyptus quintessence oil, 64~70 parts of deionized water.
2. a kind of coral reef peel off pack according to claim 1, which is characterized in that in parts by weight, including it is as follows Component: 5 parts of hydroxy propyl cellulose, 7 parts of polyvinyl alcohol, 7 parts of chitosan quaternary ammonium salt, 3 parts of propylene glycol, coral reef alcohol extraction liquid 6 parts, 4 parts of ethyl alcohol, 0.12 part of Bergamot, 0.08 part of eucalyptus quintessence oil, 67 parts of deionized water.
3. a kind of preparation method of coral reef peel off pack, which is characterized in that specific step is as follows:
(1) it produces coral reef alcohol extraction liquid: coral reef is crushed to 250~300 mesh, coral reef powder and ethyl alcohol are pressed into 1:1 Ratio mixing, 16~20 DEG C, 700~1000rpm/min, shake 1~3 day, 4000~6000rpm/min centrifugation 15~ 20min takes supernatant, obtains coral reef alcohol extraction liquid;
(2) weigh: the coral reef alcohol extraction liquid that step (1) is prepared, hydroxy propyl cellulose, polyvinyl alcohol, shell are poly- Sugared quaternary ammonium salt, propylene glycol, ethyl alcohol, Bergamot, eucalyptus quintessence oil and deionized water, weigh in parts by weight respectively, spare;
(3) propylene glycol that step (2) weigh is added into deionized water dissolving;
(4) by hydroxy propyl cellulose, polyvinyl alcohol, the third of step (3) plus deionized water dissolving is added with ethanol wet Glycol dissolves by heating at 65~75 DEG C, obtains mixture A;
(5) chitosan quaternary ammonium salt, coral reef alcohol extraction liquid are mixed, then with Bergamot, eucalyptus quintessence oil and it is cooling after Mixture A mixing, obtain mixture B;
(6) mixture B 800~1200rpm/min of refiner is stirred into 20~40min, obtains mixture C;
(7) mixture C is dispensed, is vacuum-packed, obtains coral reef peel off pack finished product.
4. a kind of preparation method of coral reef peel off pack according to claim 3, which is characterized in that step (1) system It takes coral reef alcohol extraction liquid: coral reef is crushed to 300 mesh, coral reef powder and ethyl alcohol are mixed in the ratio of 1:1,18 DEG C, 800rpm/min, shake 2 days, 4000rpm/min be centrifuged 20min, take supernatant, obtain coral reef alcohol extraction liquid.
5. a kind of preparation method of coral reef peel off pack according to claim 3, which is characterized in that step (4) will Hydroxy propyl cellulose, polyvinyl alcohol, are added the propylene glycol of step (3) plus deionized water dissolving with ethanol wet, and 70 DEG C Lower heating for dissolving, obtains mixture A.
6. a kind of preparation method of coral reef peel off pack according to claim 3, which is characterized in that step (6) will Mixture B stirs 30min with refiner 1000rpm/min, obtains mixture C.
CN201810961160.0A 2018-08-22 2018-08-22 A kind of coral reef peel off pack and preparation method thereof Pending CN109010225A (en)

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CN107456433A (en) * 2017-08-30 2017-12-12 广东芭薇生物科技股份有限公司 A kind of deep water supplement preparation
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104095883A (en) * 2013-04-01 2014-10-15 统欣生物科技股份有限公司 Coral extract, its extraction method and use, and coral extract health product
CN104224645A (en) * 2013-06-18 2014-12-24 谭汉卿 Freckle-removing and whitening mask
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Application publication date: 20181218