CN108951114A - Color fourth imitates the low solid content of nylon feel and applies silver process - Google Patents

Color fourth imitates the low solid content of nylon feel and applies silver process Download PDF

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Publication number
CN108951114A
CN108951114A CN201810481402.6A CN201810481402A CN108951114A CN 108951114 A CN108951114 A CN 108951114A CN 201810481402 A CN201810481402 A CN 201810481402A CN 108951114 A CN108951114 A CN 108951114A
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China
Prior art keywords
fabric
desizing
feel
color
agent
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Chinese (zh)
Inventor
许尔明
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Zhejiang Shengshan Textile Co Ltd
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Zhejiang Shengshan Textile Co Ltd
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Priority to CN201810481402.6A priority Critical patent/CN108951114A/en
Publication of CN108951114A publication Critical patent/CN108951114A/en
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/50Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with hydrogen peroxide or peroxides of metals; with persulfuric, permanganic, pernitric, percarbonic acids or their salts
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144Alcohols; Metal alcoholates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/263Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50Modified hand or grip properties; Softening compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

A kind of color fourth provided by the invention imitates the low solid content of nylon feel and applies silver process, comprising the following steps: color fourth embryo cloth is entered desizing machine and carries out boiling-off pre-treatment by a.;B. the fabric after desizing is subjected to overflow dyeing processing;C. the fabric of dyeing is subjected to washing process, pre-setting processing then is carried out to the fabric in an oven, and control temperature at 200-210 DEG C;D. finishing agent is added in the fabric after pre-setting, setting treatment in progress, wherein setting temperature control is at 186-192 DEG C;By weight percentage, the finishing agent includes waterproofing agent 2-4%, fabric moisture leavening agent 1-2% and feel leavening agent 1.3-1.7%;E. configured gluing is coated on press polish treated fabric;It obtains applying gel coating cloth.Shaping process in increasing after the presetting technology that color fourth imitates the low solid content painting silver process of nylon feel in the present invention, so that Se Dingbu yarn sufficiently opens the node of fiber interweaving under the action of feel leavening agent and hygroscopic agent, come flexibility and fluffy sense to webbing.

Description

Color fourth imitates the low solid content of nylon feel and applies silver process
Technical field
The present invention relates to textile production fields, and in particular to a kind of color fourth imitates the low solid content of nylon feel and applies silver process.
Background technique
With the development of the stamp umbrella cloth market demand, demand of the client to product additional function is higher and higher, especially Color fourth applies silver products and requires the service performance for strictly increasing umbrella cloth by nylon feel, applies silver using low solid content and reduces cloth cover auxiliary agent The standards such as residual.240TH washs its fabric of Se Dingyin in weaving using the woven satin face class fabric of twill intertexture method, fabric fibre More slightly cause cloth cover entirety feel relatively stiffening, it is difficult to reach the soft feeling of customer demand.From the angle analysis of production umbrella, fabric Preferable feel flexility promotes umbrella folding effect, improves umbrella service life.
The existing patent document application No. is CN201010600939.3 discloses a kind of " imitative digital printer of color fourth Skill ", include: in the printing technology production plain net halftone, modulation sizing liquor, 4) stamp, evaporate, wash and setting process;The work The obtained product feel of skill is harder, and fold resistant, does not cause service life lower.
Summary of the invention
(1) technical problems to be solved
The low solid content of nylon feel is imitated the object of the present invention is to provide a kind of color fourth and applies silver process, solves existing Se Dingbuyin The harder defect of product feel is made in flower process.
(2) technical solution
In order to solve the above technical problem, the present invention provides a kind of color fourth imitate the low solid content of nylon feel and apply silver process, including Following steps:
A. color fourth embryo cloth is entered into desizing machine and carries out boiling-off pre-treatment;
B. the fabric after desizing is subjected to overflow dyeing processing;
C. the fabric of dyeing is subjected to washing process, pre-setting processing then is carried out to the fabric in an oven, and control temperature At 200-210 DEG C;
D. finishing agent is added in the fabric after pre-setting, setting treatment in progress, wherein setting temperature control is in 186-192 ℃;By weight percentage, the finishing agent includes waterproofing agent 2-4%, fabric moisture leavening agent 1-2% and feel leavening agent 1.3- 1.7%;
E. configured gluing is coated on press polish treated fabric;It obtains applying gel coating cloth.It is imitative in color fourth in the present invention The low solid content of nylon feel applies shaping process in the presetting technology increase later of silver process, and is added in middle sizing by waterproofing agent The finishing agent of 2-4%, fabric moisture leavening agent 1-2% and feel leavening agent 1.3-1.7% composition, so that Se Dingbu yarn is in feel The node that fiber interweaving is sufficiently opened under the action of leavening agent and hygroscopic agent comes flexibility and fluffy sense to webbing.More preferably, The ethyl alcohol of 1-2% antioxidant and 5-10% is added in the finishing agent.Antioxidant, which is added, can increase fabric in subsequent coating The performance of fire-resistant oxidation resistant in technique.The ethyl alcohol that 5-10% is added makes antioxidant, waterproofing agent, fabric moisture leavening agent It is more easily dispersed in water phase with feel leavening agent, so that above-mentioned auxiliary agent is evenly dispersed in fabric, improves finishing effect, into One step improves the flexibility and fluffy sense of fabric, while the azeotropic effect of water and ethyl alcohol, so that moisture is fast in type-approval process The evaporation of speed, improves the efficiency of arrangement;Remaining ethyl alcohol is retained in coating process in middle setting process, further takes away portion The toluene solvant divided, improves the recovery efficiency of toluene solvant, reduces the residual of toluene solvant in finished product.By by new product 100 comparisons are folded after making umbrella with conventional products, new product folding line is slight and nothing falls silver-colored light leakage phenomenon, conventional products folding line Seriously and there is degumming phenomenon (glue film fastness is bad).New product advantage is prominent.Product feel flexibility close to nylon product feel, Far superior to conventional color fourth applies silver-colored feel.Color fastness Indexs measure: being compared by detection new product and conventional products, and new product is dry Wet friction color fastness wants 1-2 grades high.
Preferably, the predetermined process controls setting temperature at 200-210 DEG C;The upper and lower of the cloth feeding area of forming machine surpasses Feeding is 1.1-1.2%.Pre-setting temperature is adjusted to 200-210 DEG C by conventional 220 DEG C by the present invention, is reduced high temperature and is hardened to fabric Facilitation.Meanwhile overfeeding is adjusted to 1.2% up and down in cloth feeding area, mitigating over-stressed stretching leads to fabric distortion phenomenon.
Preferably, calendering operation, the calendering operation are additionally provided with after the coating procedure are as follows: gel coating cloth will be applied and carried out Calendering processing, wherein calendering is 95-125 DEG C of temperature, pressure 80-120kg/cm2, calendering speed control is in 10-25m/ min.
Preferably, the calendering operation is divided into two stages, and first stage wherein calendering is to slowly warm up to by 95 DEG C of temperature 120 DEG C, pressure 80-110kg/cm2, calendering speed control is in 16-25m/ min;Second stage, control calendering temperature be 120 ± 1 DEG C, 115 ± 2kg/cm of pressure2, calendering speed is 15-17m/ min.Calendering operation part two stages of the invention carry out, wherein The medium temperature calendering of second stage is handled, thick and solid degree unavoidably is rolled it is thin so that the flexibility of feel increases.
Preferably, the slurry groove temperature that moves back is 98-100 DEG C;The speed of desizing vehicle is 50-70m/min, and padding machine pressure is 1.5-2.0kg/cm2
Preferably, desizing mixed liquor is added in the desizing process, by weight, the desizing mixed liquor includes 45-50 Part desizing agent, 40-60 parts of liquid alkaline, 1-2 parts of refining agents and 1-2 parts of hydrogen peroxide.
Preferably, the desizing agent is added at one time 15-20 parts in charging, and subsequent every myriametre is continuous to add 10 parts.
Preferably, the gluing being added in the coating procedure, by weight, comprising: 90-110 parts of cyanoacrylates are viscous Mixture, 25-35 parts of SS-2050 epithelium glue, 2-4 parts of smooth, soft agent, 8-10 parts of feel leavening agents, 4-6 parts of bridging agents and 20-25 Part toluene solvant.Coating of the invention using cyanoacrylate adhesive configuration enable its feel reach optimal pliability and Epithelium sense, coating product feel are similar to the sense of touch of nylon facing material.More preferably, gluing further includes 5-10 parts of ethyl alcohol.The present invention The middle toluene solvant that part is taken away using ethyl alcohol, improves the recovery efficiency of toluene solvant, reduces toluene solvant in finished product Residual.
(3) beneficial effect
A kind of color fourth provided by the invention imitates the low solid content of nylon feel and applies silver process, has the advantage that
1, shaping process in increasing after the presetting technology that color fourth imitates the low solid content painting silver process of nylon feel in the present invention, And the arrangement being made of waterproofing agent 2-4%, fabric moisture leavening agent 1-2% and feel leavening agent 1.3-1.7% is added in middle sizing Agent gives webbing so that Se Dingbu yarn sufficiently opens the node of fiber interweaving under the action of feel leavening agent and hygroscopic agent Come flexibility and fluffy sense.By folding 100 comparisons after new product and conventional products are made umbrella, new product folding line is slight And without silver-colored light leakage phenomenon is fallen, conventional products folding line is serious and has degumming phenomenon (glue film fastness is bad).New product advantage is prominent.It produces Product feel flexibility applies silver-colored feel close to nylon product feel, far superior to conventional color fourth.Color fastness Indexs measure: pass through detection New product and conventional products comparison, new product dry and wet colorfastness to rubbing want 1-2 grades high.
2, antioxidant is added in the present invention can increase the property of fire-resistant oxidation resistant of the fabric in subsequent coating process Energy.The ethyl alcohol that 5-10% is added is more easily dispersed in antioxidant, waterproofing agent, fabric moisture leavening agent and feel leavening agent Water phase improves finishing effect so that above-mentioned auxiliary agent is evenly dispersed in fabric, further improve fabric flexibility and Fluffy sense, while the azeotropic effect of water and ethyl alcohol improves the effect of arrangement so that moisture quickly evaporates in type-approval process Rate;Remaining ethyl alcohol is retained in coating process in middle setting process, is further taken away the toluene solvant of part, is improved toluene The recovery efficiency of solvent reduces the residual of toluene solvant in finished product.
3, calendering operation part two stages of the invention carry out, wherein the medium temperature calendering processing of second stage, by thickness unavoidably Solidity roll it is thin so that the flexibility of feel increases.
4, pre-setting temperature is adjusted to 200-210 DEG C by conventional 220 DEG C by the present invention, reduces the rush that high temperature hardens fabric Into effect.Meanwhile overfeeding is adjusted to 1.2% up and down in cloth feeding area, mitigating over-stressed stretching leads to fabric distortion phenomenon.
5, coating of the invention using cyanoacrylate adhesive configuration enable its feel reach optimal pliability and Epithelium sense, coating product feel are similar to the sense of touch of nylon facing material.More preferably, gluing further includes 5-10 parts of ethyl alcohol.The present invention The middle toluene solvant that part is taken away using ethyl alcohol, improves the recovery efficiency of toluene solvant, reduces toluene solvant in finished product Residual.
Detailed description of the invention
Fig. 1 is the process flow diagram that color fourth of the invention imitates that the low solid content of nylon feel applies silver process.
Specific embodiment
With reference to the accompanying drawings and examples, specific embodiments of the present invention will be described in further detail.Following instance For illustrating the present invention, but it is not intended to limit the scope of the invention.
Antioxidant in the present invention uses the antioxygen of Guangzhou Jin Yue textile auxiliary Co., Ltd JINCOLOR T01 Change auxiliary agent.Cyanoacrylate adhesive uses the Ailete3388 glue of Ai Lete company in the present invention.Waterproof in the present invention Agent uses methyl type silicone oil.Fabric moisture leavening agent takes the multi-functional leavening agent of Nanjing Chinese olive Chemical Co., Ltd..Feel is fluffy Loose agent uses the TF-432 leavening agent of Haicheng City Ze Hang trade Co., Ltd sale.It is desizing agent, refining agent, bridging agent, smooth soft The soft dose of product being all made of on the market.
Embodiment 1: a kind of color fourth provided by the invention imitates the low solid content of nylon feel and applies silver process, comprising the following steps:
A. color fourth embryo cloth is entered into desizing machine and carries out boiling-off pre-treatment;
B. the fabric after desizing is subjected to overflow dyeing processing;The slurry groove temperature that moves back is 98-100 DEG C;The speed of desizing vehicle is 50m/min, padding machine pressure are 1. kg/cm2.Desizing mixed liquor is added in the desizing process, by weight, the desizing is mixed Closing liquid includes 45 parts of desizing agents, 40 parts of liquid alkaline, 1 part of refining agent and 1 part of hydrogen peroxide;The desizing agent disposably adds in charging Enter 15 parts, subsequent every myriametre is continuous to add 10 parts.
C. the fabric of dyeing is subjected to washing process, pre-setting processing then is carried out to the fabric in an oven;Wherein, it controls Setting temperature processed is at 200 DEG C;The overfeeding up and down in the cloth feeding area of forming machine is 1.1%.
D. finishing agent is added in the fabric after pre-setting, setting treatment in progress, wherein setting temperature control is 186 ℃;By weight percentage, the finishing agent includes waterproofing agent 2%, fabric moisture leavening agent 1% and feel leavening agent 1.3%;
E. configured gluing is coated on press polish treated fabric;It obtains applying gel coating cloth.
F. gel coating cloth will be applied and carry out calendering processing, wherein calendering is 95 DEG C of temperature, pressure 80kg/cm2, calendering speed control System is in 10m/ min.Wherein, calendering operation is divided into two stages, and first stage wherein calendering is to slowly warm up to by 95 DEG C of temperature 120 DEG C, pressure 80kg/cm2, calendering speed control is in 16m/ min;Second stage, control calendering temperature are 120 ± 1 DEG C, pressure 115 ± 2kg/cm of power2, calendering speed is 15m/ min.
Embodiment 2: a kind of color fourth provided by the invention imitates the low solid content of nylon feel and applies silver process, comprising the following steps:
A kind of color fourth provided by the invention imitates the low solid content of nylon feel and applies silver process, comprising the following steps:
A. color fourth embryo cloth is entered into desizing machine and carries out boiling-off pre-treatment;
B. the fabric after desizing is subjected to overflow dyeing processing;The slurry groove temperature that moves back is 100 DEG C;The speed of desizing vehicle is 70m/ Min, padding machine pressure are 2.0kg/cm2.Desizing mixed liquor, by weight, the desizing mixed liquor are added in the desizing process Including 50 parts of desizing agents, 60 parts of liquid alkaline, 2 parts of refining agents and 2 parts of hydrogen peroxide;The desizing agent is added at one time 20 in charging Part, subsequent every myriametre is continuous to add 10 parts.
C. the fabric of dyeing is subjected to washing process, pre-setting processing then is carried out to the fabric in an oven;Wherein, it controls Setting temperature processed is at 210 DEG C;The overfeeding up and down in the cloth feeding area of forming machine is 1.2%.
D. finishing agent is added in the fabric after pre-setting, setting treatment in progress, wherein setting temperature control is 192 ℃;By weight percentage, the finishing agent includes waterproofing agent 4%, fabric moisture leavening agent 2% and feel leavening agent 1.7%;
E. configured gluing is coated on press polish treated fabric;It obtains applying gel coating cloth.
F. gel coating cloth will be applied and carry out calendering processing, wherein calendering is 125 DEG C of temperature, pressure 120kg/cm2, calendering speed Control is in 25m/ min.Wherein, calendering operation is divided into two stages, first stage wherein calendering, by 95 DEG C of slowly heatings of temperature To 120 DEG C, pressure 110kg/cm2, calendering speed control is in 25m/ min;Second stage, control calendering temperature are 120 ± 1 DEG C, 115 ± 2kg/cm of pressure2, calendering speed is 17m/ min.
Embodiment 3: a kind of color fourth provided by the invention imitates the low solid content of nylon feel and applies silver process, comprising the following steps:
A. color fourth embryo cloth is entered into desizing machine and carries out boiling-off pre-treatment;
B. the fabric after desizing is subjected to overflow dyeing processing;The slurry groove temperature that moves back is 99 DEG C;The speed of desizing vehicle is 60m/ Min, padding machine pressure are 1.75kg/cm2.Desizing mixed liquor, by weight, the desizing mixed liquor are added in the desizing process Including 47.5 parts of desizing agents, 50 parts of liquid alkaline, 1.5 parts of refining agents and 1.5 parts of hydrogen peroxide.The desizing agent is disposable in charging 17.5 parts are added, subsequent every myriametre is continuous to add 10 parts.
C. the fabric of dyeing is subjected to washing process, pre-setting processing then is carried out to the fabric in an oven, it is described pre- Shaping process controls setting temperature at 205 DEG C;The overfeeding up and down in the cloth feeding area of forming machine is 1.15%.
D. finishing agent is added in the fabric after pre-setting, setting treatment in progress, wherein setting temperature control is 189 ℃;By weight percentage, the finishing agent include waterproofing agent 2-4%, fabric moisture leavening agent 1.5%, feel leavening agent 1.5%, 1.5% antioxidant and 7.5% ethyl alcohol;
E. configured gluing is coated on press polish treated fabric;It obtains applying gel coating cloth.Add in the coating procedure The gluing entered, by weight, comprising: 90 parts of cyanoacrylate adhesives, 25 parts of SS-2050 epithelium glue, 2 parts of smooth, softs Agent, 8 parts of feel leavening agents, 4 parts of bridging agents, 20 parts of toluene solvants and 5 parts of ethyl alcohol.
F. gel coating cloth will be applied and carry out calendering processing, wherein calendering is 110 DEG C of temperature, pressure 100kg/cm2, calendering speed Control is in 17.5m/ min.The calendering operation is divided into two stages, first stage wherein calendering, by 95 DEG C of slowly heatings of temperature To 120 DEG C, pressure 95kg/cm2, calendering speed control is in 20m/ min;Second stage, control calendering temperature are 119 DEG C, pressure 113kg/cm2, calendering speed is 16m/ min.
Embodiment 4: a kind of color fourth provided by the invention imitates the low solid content of nylon feel and applies silver process, comprising the following steps:
A. color fourth embryo cloth is entered into desizing machine and carries out boiling-off pre-treatment;
B. the fabric after desizing is subjected to overflow dyeing processing;The slurry groove temperature that moves back is 99 DEG C;The speed of desizing vehicle is 60m/ Min, padding machine pressure are 1.75kg/cm2.Desizing mixed liquor, by weight, the desizing mixed liquor are added in the desizing process Including 47.5 parts of desizing agents, 50 parts of liquid alkaline, 1.5 parts of refining agents and 1.5 parts of hydrogen peroxide.The desizing agent is disposable in charging 17.5 parts are added, subsequent every myriametre is continuous to add 10 parts.
C. the fabric of dyeing is subjected to washing process, pre-setting processing then is carried out to the fabric in an oven, it is described pre- Shaping process controls setting temperature at 205 DEG C;The overfeeding up and down in the cloth feeding area of forming machine is 1.15%.
D. finishing agent is added in the fabric after pre-setting, setting treatment in progress, wherein setting temperature control is 189 ℃;By weight percentage, the finishing agent include waterproofing agent 2-4%, fabric moisture leavening agent 1.5%, feel leavening agent 1.5%, 1.5% antioxidant and 7.5% ethyl alcohol;
E. configured gluing is coated on press polish treated fabric;It obtains applying gel coating cloth.Add in the coating procedure The gluing entered, by weight, comprising: 110 parts of cyanoacrylate adhesives, 35 parts of SS-2050 epithelium glue, 4 parts of smooth, softs Agent, 10 parts of feel leavening agents, 6 parts of bridging agents, 25 parts of toluene solvants and 10 parts of ethyl alcohol.
F. gel coating cloth will be applied and carry out calendering processing, wherein calendering is 110 DEG C of temperature, pressure 100kg/cm2, calendering speed Control is in 17.5m/ min.The calendering operation is divided into two stages, first stage wherein calendering, by 95 DEG C of slowly heatings of temperature To 120 DEG C, pressure 95kg/cm2, calendering speed control is in 20m/ min;Second stage, control calendering temperature are 121 DEG C, pressure 117kg/cm2, calendering speed is 16m/ min.
Comparative example 1: a kind of color fourth provided by the invention imitates the low solid content of nylon feel and applies silver process, comprising the following steps:
A. color fourth embryo cloth is entered into desizing machine and carries out boiling-off pre-treatment;
B. the fabric after desizing is subjected to overflow dyeing processing;The slurry groove temperature that moves back is 98-100 DEG C;The speed of desizing vehicle is 40m/min, padding machine pressure are 1.4kg/cm2.Desizing mixed liquor is added in the desizing process, by weight, the desizing is mixed Closing liquid includes 44 parts of desizing agents, 61 parts of liquid alkaline, 0.9 part of refining agent and 0.9 part of hydrogen peroxide.The desizing agent is primary in charging Property be added 14 parts, subsequent every myriametre is continuous plus 9 parts.
C. the fabric of dyeing is subjected to washing process, pre-setting processing then is carried out to the fabric in an oven, it is described pre- Shaping process controls setting temperature at 198 DEG C;The overfeeding up and down in the cloth feeding area of forming machine is 1.0%.
D. finishing agent is added in the fabric after pre-setting, setting treatment in progress, wherein setting temperature control is 185 ℃;By weight percentage, the finishing agent includes waterproofing agent 1%, fabric moisture leavening agent 0.9%, feel leavening agent 1.2%, 0.9% Antioxidant and 4% ethyl alcohol;
E. configured gluing is coated on press polish treated fabric;It obtains applying gel coating cloth.Add in the coating procedure The gluing entered, by weight, comprising: 88 parts of cyanoacrylate adhesives, 24 parts of SS-2050 epithelium glue, 1 part of smooth, soft Agent, 7 parts of feel leavening agents, 3 parts of bridging agents, 18 parts of toluene solvants and 4 parts of ethyl alcohol.
F. gel coating cloth will be applied and carry out calendering processing, wherein calendering is 94 DEG C of temperature, pressure 78kg/cm2, calendering speed control System is in 9m/ min.The calendering operation is divided into two stages, and first stage wherein calendering is to slowly warm up to 120 by 95 DEG C of temperature DEG C, pressure 78kg/cm2, calendering speed control is in 15m/ min;Second stage, control calendering temperature are 118 DEG C, pressure 112kg/cm2, calendering speed is 14m/ min.
Comparative example 2: a kind of color fourth provided by the invention imitates the low solid content of nylon feel and applies silver process, comprising the following steps:
A. color fourth embryo cloth is entered into desizing machine and carries out boiling-off pre-treatment;
B. the fabric after desizing is subjected to overflow dyeing processing;The slurry groove temperature that moves back is 102 DEG C;The speed of desizing vehicle is 71m/ Min, padding machine pressure are 2.1kg/cm2.Desizing mixed liquor, by weight, the desizing mixed liquor are added in the desizing process Including 51 parts of desizing agents, 38 parts of liquid alkaline, 3 parts of refining agents and 3 parts of hydrogen peroxide.The desizing agent is added at one time 21 in charging Part, subsequent every myriametre is continuous to add 11 parts.
C. the fabric of dyeing is subjected to washing process, pre-setting processing then is carried out to the fabric in an oven, it is described pre- Shaping process controls setting temperature at 211 DEG C;The overfeeding up and down in the cloth feeding area of forming machine is 1.13%.
D. finishing agent is added in the fabric after pre-setting, setting treatment in progress, wherein setting temperature control is 193 ℃;By weight percentage, the finishing agent includes that waterproofing agent 5%, fabric moisture leavening agent 3%, feel leavening agent 2%, 3% are anti-oxidant Agent and 11% ethyl alcohol;
E. configured gluing is coated on press polish treated fabric;It obtains applying gel coating cloth.Add in the coating procedure The gluing entered, by weight, comprising: 112 parts of cyanoacrylate adhesives, 37 parts of SS-2050 epithelium glue, 5 parts of smooth, softs Agent, 11 parts of feel leavening agents, 7 parts of bridging agents, 26 parts of toluene solvants and 11 parts of ethyl alcohol.
F. gel coating cloth will be applied and carry out calendering processing, wherein calendering is 126 DEG C of temperature, pressure 121kg/cm2, calendering speed Control is in 26m/ min.The calendering operation is divided into two stages, and first stage wherein calendering is to slowly warm up to by 95 DEG C of temperature 120 DEG C, pressure 112kg/cm2, calendering speed control is in 26m/ min;Second stage, control calendering temperature are 122 DEG C, pressure 120kg/cm2, calendering speed is 18m/ min.
Textile (umbrella cover made from above-described embodiment 1, embodiment 2, embodiment 3, embodiment 4 and comparative example 1, comparative example 2 Cloth) performance parameter be compared as follows: wherein color fastness using GB/T 5713-2013 (textile color stability tests resistance to water colour Fastness) it is detected.Glue film fastness uses company standard, which is the experimental data after folding 100 times.Weaving The complete performance of product takes GB/T18318.4-2009 " measurement of textile bending property " to be detected;Wherein, bending stiffness (B) it is detected with bending lag square (HB) using bending property tester.Solvent detection limit takes paper, and " textile is harmful The study on determination method of volatile matter residual quantity and the amount of migration " solvent detection method in (weaving 46-50 pages of university's flow separation Zhen) It is operated.
Product index project Dry and wet colorfastness to rubbing Flexility (soft grade) Glue film fastness after folding 100 times Crease-flex test Bending stiffness (B) Bending lag square (HB) Dissolvent residual detection
Embodiment 1 5.0 grade 1 510gf Folding line is slight and nothing falls silver-colored light leakage phenomenon 0.156 0.268 1 sample exceeds detection limit
Embodiment 2 5.0 grade 1 520gf Folding line is slight and nothing falls silver-colored light leakage phenomenon 0.176 0.288 Without departing from detection limit
Embodiment 3 5.5 grade 1 630gf Folding line is slight and nothing falls silver-colored light leakage phenomenon 0.146 0.251 Without departing from detection limit
Embodiment 4 5.5 grade 1 620gf Folding line is slight and nothing falls silver-colored light leakage phenomenon 0.136 0.247 Without departing from detection limit
Comparative example 1 3.5 grade 4 320gf Folding line is serious and has degumming phenomenon 0.536 0.624 10 samples exceed detection limit
Comparative example 2 3.5 grade 3 330gf Folding line is serious and has degumming phenomenon 0.533 0.610 10 samples exceed detection limit
Market colouring fourth cloth 3.5 grade 4 380gf Folding line is serious and has degumming phenomenon 0.455 0.526 8 samples exceed detection limit
In conclusion using the dry of the embodiment 1 of present invention process, embodiment 2, embodiment 3, embodiment 4 product made from it Wet friction color fastness, soft grade, fold 100 times after glue film fastness, crease-flex test, bending stiffness (B) and bending lag square (HB) it is better than comparative example 1, comparative example 2 and market colouring fourth cloth beyond processing range.Especially take optimization technique Embodiment 3, embodiment 4, dry and wet colorfastness to rubbing is than 2 high 2 grades of embodiment 1, embodiment, soft grade, after folding 100 times Glue film fastness, crease-flex test, bending stiffness (B) and bending lag square (HB) are also superior to embodiment 1 and implement 2 experiment number According to;Existing Se Dingbu folding resistance can be worse, and bending stiffness (B) and bending lag square (HB) are worse than product of the invention. Present invention process be added ethyl alcohol after toluene solvant residue detection statistics indicate that, improve toluene volatility, reduce toluene Detection limit.
The various embodiments described above are merely to illustrate the present invention, wherein the structure of each component, connection type etc. are all can be Variation, all equivalents and improvement carried out based on the technical solution of the present invention should not be excluded of the invention Except protection scope.

Claims (7)

1. a kind of color fourth imitates the low solid content of nylon feel and applies silver process, which comprises the following steps:
A. color fourth embryo cloth is entered into desizing machine and carries out boiling-off pre-treatment;
B. the fabric after desizing is subjected to overflow dyeing processing;
C. the fabric of dyeing is subjected to washing process, pre-setting processing then is carried out to the fabric in an oven;
D. finishing agent is added in the fabric after pre-setting, setting treatment in progress, wherein setting temperature control is in 186-192 ℃;By weight percentage, the finishing agent includes waterproofing agent 2-4%, fabric moisture leavening agent 1-2% and feel leavening agent 1.3- 1.7%;
E. configured gluing is coated on press polish treated fabric;It obtains applying gel coating cloth.
2. color fourth as described in claim 1 imitates the low solid content of nylon feel and applies silver process, which is characterized in that the pre-setting work Sequence controls setting temperature at 200-210 DEG C;The overfeeding up and down in the cloth feeding area of forming machine is 1.1-1.2%.
3. color fourth as described in claim 1 imitates the low solid content of nylon feel and applies silver process, which is characterized in that the coating procedure It is additionally provided with calendering operation, the calendering operation later are as follows: gel coating cloth will be applied and carry out calendering processing, wherein calendering is temperature 95- 125 DEG C, pressure 80-120kg/cm2, calendering speed control is in 10-25m/ min.
4. color fourth as claimed in claim 3 imitates the low solid content of nylon feel and applies silver process, which is characterized in that the calendering operation It is divided into two stages, first stage wherein calendering is to slowly warm up to 120 DEG C by 95 DEG C of temperature, pressure 80-110kg/cm2, calendering Speed control is in 16-25m/ min;Second stage, control calendering temperature are 120 ± 1 DEG C, 115 ± 2kg/cm of pressure2, calendering speed Degree is 15-17m/ min.
5. color fourth as claimed in claim 1 or 2 or 3 or 4 imitates the low solid content of nylon feel and applies silver process, which is characterized in that institute Stating and moving back slurry groove temperature is 98-100 DEG C;The speed of desizing vehicle is 50-70m/min, and padding machine pressure is 1.5-2.0kg/cm2
6. color fourth as claimed in claim 5 imitates the low solid content of nylon feel and applies silver process, which is characterized in that the desizing process Middle addition desizing mixed liquor, by weight, the desizing mixed liquor include 45-50 parts of desizing agents, 40-60 parts of liquid alkaline, 1-2 parts of essences Refine agent and 1-2 parts of hydrogen peroxide.
7. color fourth as claimed in claim 6 imitates the low solid content of nylon feel and applies silver process, which is characterized in that the desizing agent exists 15-20 parts are added at one time when charging, subsequent every myriametre is continuous to add 10 parts.
CN201810481402.6A 2018-05-18 2018-05-18 Color fourth imitates the low solid content of nylon feel and applies silver process Pending CN108951114A (en)

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CN115852678A (en) * 2021-09-24 2023-03-28 浙江圣山科纺有限公司 Antibacterial and mildewproof waterproof agent and production method of antibacterial and mildewproof waterproof polyester fabric using same

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Application publication date: 20181207