CN108939588A - The process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility - Google Patents

The process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility Download PDF

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Publication number
CN108939588A
CN108939588A CN201811029245.1A CN201811029245A CN108939588A CN 108939588 A CN108939588 A CN 108939588A CN 201811029245 A CN201811029245 A CN 201811029245A CN 108939588 A CN108939588 A CN 108939588A
Authority
CN
China
Prior art keywords
pipeline
valve
communicated
filter
pump
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201811029245.1A
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Chinese (zh)
Inventor
郑小华
徐振祥
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JIANGMEN HYDROGEN PEROXIDE SOLUTION CO Ltd
Original Assignee
JIANGMEN HYDROGEN PEROXIDE SOLUTION CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JIANGMEN HYDROGEN PEROXIDE SOLUTION CO Ltd filed Critical JIANGMEN HYDROGEN PEROXIDE SOLUTION CO Ltd
Priority to CN201811029245.1A priority Critical patent/CN108939588A/en
Publication of CN108939588A publication Critical patent/CN108939588A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/22Evaporating by bringing a thin layer of the liquid into contact with a heated surface
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/30Accessories for evaporators ; Constructional details thereof
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/11Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with bag, cage, hose, tube, sleeve or like filtering elements
    • B01D29/13Supported filter elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/11Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with bag, cage, hose, tube, sleeve or like filtering elements
    • B01D29/13Supported filter elements
    • B01D29/23Supported filter elements arranged for outward flow filtration
    • B01D29/27Filter bags
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D35/00Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
    • B01D35/02Filters adapted for location in special places, e.g. pipe-lines, pumps, stop-cocks
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01Hydrogen peroxide
    • C01B15/013Separation; Purification; Concentration
    • C01B15/017Anhydrous hydrogen peroxide; Anhydrous solutions or gaseous mixtures containing hydrogen peroxide

Abstract

The present invention relates to the process unit technical fields of filter, the process system of flush distillation circulation fluid filtration device in especially a kind of hydrogen peroxide enrichment facility, falling film evaporator lower end is communicated with circulating and evaporating liquid pump by pipeline, circulating and evaporating liquid pump is communicated with pump outlet check valve by pipeline, pump discharge pressure table is additionally provided on pipeline between pump outlet check valve and circulating and evaporating liquid pump, pump outlet check valve is communicated with ball valve by pipeline, ball valve is communicated with filter by pipeline, filter upper end also passes through pipeline and is provided with blow valve, filter lower end is communicated with filter bottom reduced pipe, filter bottom reduced pipe also passes through pipeline and is communicated with visor valve, visor valve is communicated with solenoid valve by pipeline, it has also been respectively communicated with filter on pipeline between solenoid valve and visor valve and has drained valve and delivery gauge, solenoid valve also passes through pipeline Connection is in falling film evaporator upper end.The present invention can be improved the safety of device and the quality of chemical grade product.

Description

The process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility
Technical field
The present invention relates to once steam in the process unit technical field of filter more particularly to a kind of hydrogen peroxide enrichment facility Send out the process system of circulation fluid filtration device.
Background technique
Hydrogen peroxide enrichment facility purifies and is concentrated dioxygen aquatic products with rectification process process generally by evaporation, essence The charging for evaporating tower is the saturated vapor containing hydrogen peroxide to come from falling film evaporator, according to the technological requirements falling film evaporator bottom Hydrogen peroxide feed liquid must beat circulation, under vacuum conditions, form closed cycle, and have a bypass to remove part circulation fluid and go technology Grade product storage tank.When we require chemical grade product yield higher, removal quantity will be reduced, and then make falling film evaporator bottom Raffinate in nonvolatile matter and organic carbon concentration correspondingly increase, viscosity is also high, the impurity of these high viscosities is once enter Rectifying column can be attached on the surface of filler.The resistance of filler will be made to increase as the production time extends, give production operation band Carry out very big difficulty.For this purpose, our devices are often furnished with flush distillation circulation fluid filtration device, to remove partial particulate at 10 microns Above sticky contaminant improves security of system and product quality.However, containing high concentration dioxygen in vaporization cycle liquid filter The organic impurities of water (65 ~ 70%), high concentration, once there is situations such as abnormal conditions such as power failure, vacuum degree decline in system, easily Decomposing hydrogen dioxide solution explosion accident occurs, the oxygen released again can combustion-supporting organic substance.Therefore flush distillation how is made good use of to follow Ring liquid filter prevents the generation of accident, and it is very important.
Summary of the invention
The purpose of the present invention is to solve disadvantages existing in the prior art, and a kind of hydrogen peroxide enrichment facility proposed The process system of middle flush distillation circulation fluid filtration device.
To achieve the goals above, present invention employs following technical solutions:
A kind of process system of flush distillation circulation fluid filtration device in hydrogen peroxide enrichment facility, including falling film evaporator are designed, and Falling film evaporator lower end is communicated with circulating and evaporating liquid pump by pipeline, and the circulating and evaporating liquid pump is communicated with pump discharge by pipeline Check-valves, and pump discharge pressure table is additionally provided on the pipeline between pump outlet check valve and circulating and evaporating liquid pump, it is described to pump out Mouth check-valves is communicated with ball valve by pipeline, and the ball valve is communicated with filter by pipeline, and the filter upper end also passes through Pipeline is provided with blow valve, and filter lower end is communicated with filter bottom reduced pipe, and the filter bottom reduced pipe is also logical Piping is communicated with visor valve, and visor valve is communicated with solenoid valve by pipeline, the pipeline between the solenoid valve and visor valve On be also respectively communicated with filter and drain valve and delivery gauge, the solenoid valve is also connected to by pipeline in falling film evaporator Upper end.
Preferably, bypass valve is also communicated on the pipeline between the solenoid valve and falling film evaporator, and bypass valve is also logical Piping connection is on the pipeline between ball valve and pump outlet check valve.
Preferably, electromagnetic flowmeter, the electromagnetism are also communicated on the pipeline between the ball valve and pump outlet check valve Flowmeter is communicated with flow control valve by pipeline, and flow control valve is communicated with technical grade product slot by pipeline.
Preferably, inlet pressure gauge is additionally provided on the pipeline between the filter and ball valve.
The process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility proposed by the present invention, beneficial to effect Fruit is: in the hydrogen peroxide enrichment facility process system of flush distillation circulation fluid filtration device can be improved device safety and The quality of chemical grade product has positive effect, and using side into lower follow-on filter out, material disengaging is more reasonable, makes just Material and impurity time of contact are shorter when often production or abnormal conditions, without buildup in filter, will not make the dioxygen of high concentration Even if water decomposition also all can all flow into evaporator, i.e., in filter occur to have a power failure suddenly without buildup according to potential difference While improving product quality, also inherently solve the hidden danger of accident, it is suitable for large-scale promotion.
Detailed description of the invention
Fig. 1 is the process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility proposed by the present invention Structural schematic diagram.
In figure: falling film evaporator 1, filter drain valve 2, visor valve 3, filter bottom reduced pipe 4, filter 5, emptying Valve 6, delivery gauge 8, ball valve 9, bypass valve 10, circulating and evaporating liquid pump 11, pump discharge pressure table 12, pumps out inlet pressure gauge 7 Mouth check-valves 13, electromagnetic flowmeter 14, flow control valve 15, technical grade product slot 16, solenoid valve 17.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
Referring to Fig.1, in a kind of hydrogen peroxide enrichment facility flush distillation circulation fluid filtration device process system, including falling liquid film steam Device 1 is sent out, the liquid level of 1 bottom of falling film evaporator is interlocked with the dioxygen water flow for entering battery limit (BL), and 1 lower end of falling film evaporator is logical Piping is communicated with circulating and evaporating liquid pump 11, and circulating and evaporating liquid pump 11 is communicated with pump outlet check valve 13 by pipeline, and pumps out Pump discharge pressure table 12 is additionally provided on pipeline between mouth check-valves 13 and circulating and evaporating liquid pump 11, pump outlet check valve 13 is logical Piping is communicated with ball valve 9, and the setting of ball valve 9, pump discharge pressure table 12 and pump outlet check valve 13 can prevent from stopping suddenly It is flow backwards when electric.
Electromagnetic flowmeter 14 is also communicated on pipeline between ball valve 9 and pump outlet check valve 13, electromagnetic flowmeter 14 is logical Piping is communicated with flow control valve 15, and flow control valve 15 is communicated with technical grade product slot 16 by pipeline, and ball valve 9 passes through Pipeline is communicated with filter 5, and filter 5 is specially flush distillation circulation fluid filtration device, the pipe between filter 5 and ball valve 9 It is additionally provided with inlet pressure gauge 7 on road, flush distillation circulation fluid filtration device is located at falling film evaporator top floor, and circulation fluid is from mistake 5 side of filter enters, and bottom comes out, and inlet/outlet pipe is equipped with pressure gauge, and bottom, which comes out, reduced pipe, pipeline is amplified, to reduce out Expect resistance, flush distillation circulation fluid filtration equipment matter must use 316, filter core filter bag have to it is anti-oxidant, it is convenient normally to give birth to Also filter sock can be replaced when production, from 5 bottom of filter to 1 top entry pipeline of falling film evaporator, it is necessary to it is unimpeded, it has prevented Generate hydrops position.
5 upper end of filter also passes through pipeline and is provided with blow valve 6, and 5 lower end of filter is communicated with filter bottom reducing Pipe 4, filter bottom reduced pipe 4 is also communicated with visor valve 3 by pipeline, and visor valve 3 is communicated with solenoid valve 17 by pipeline, It has also been respectively communicated with filter on pipeline between solenoid valve 17 and visor valve 3 and has drained valve 2 and delivery gauge 8, solenoid valve 17 are also connected to by pipeline in 1 upper end of falling film evaporator.
Bypass valve 10 is also communicated on pipeline between solenoid valve 17 and falling film evaporator 1, and bypass valve 10 also passes through pipe Road connection is on the pipeline between ball valve 9 and pump outlet check valve 13.
Falling film evaporator 1, circulating and evaporating liquid pump 11, pump discharge pressure table 12, pump discharge non-return are sequentially connected by pipeline Valve ball valve 13, branch remove electromagnetic flowmeter 14, flow control valve 15, technical grade product slot 16;Main road removes flush distillation circulation fluid Filter inlet pipeline and ball valve 9, filter 5, filter bottom reduced pipe 4, visor valve 3, filter drain valve 2, then arrive drop 1 top of film evaporator.
Filter 5 is provided with inlet pressure gauge 7, and delivery gauge 8 drains valve 2, and sets bypass valve 10, blow valve 6, During normal production, bypass valve 10 and blow valve 6 are closed, ball valve 9 and solenoid valve 17 are opened, material enters from ball valve 9, electromagnetism Valve 17, which comes out, to be entered in 1 top of falling film evaporator.
Filter sock can be being replaced during normal production, at this point, closing ball valve 9 and solenoid valve 17, open bypass valve 10, Material, by directly going to 1 top of falling film evaporator, is opened the hydrogen peroxide drained in 2 emissions filter 5 of valve, is opened from bypass valve 10 Blow valve 6 is vented, and filter bag can be then replaced.
Filter 5 and falling film evaporator 1 is kept to have a poor location, filter 5 uses side into bottom principle, either normally Production or whens abnormal conditions, can keep filter to be in empty state, avoid high concentration hydrogen peroxide and impurity screening it is long when Between contact.
Working principle of the present invention is as follows: the electromagnetic flowmeter 14 of starting circulating and evaporating liquid pump 11, branch controls a constant current Technical grade product slot 16 is entered after amount, enters back into subsequent processing;Main road is through ball valve 9, filter 5, reduced pipe 4, visor valve 3 And solenoid valve 17 is flowed into falling film evaporator 1, when stopping production, is closed circulating and evaporating liquid pump 11, is closed pump discharge non-return Valve 13 and flow control valve 15, and keep 5 blank state of filter.
More than, it is merely preferred embodiments of the present invention, but scope of protection of the present invention is not limited thereto, it is any Those familiar with the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its invents Design is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (4)

1. the process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility, which is characterized in that including falling liquid film Evaporator (1), and falling film evaporator (1) lower end is communicated with circulating and evaporating liquid pump (11) by pipeline, the circulating and evaporating liquid pump (11) it is communicated with pump outlet check valve (13) by pipeline, and between pump outlet check valve (13) and circulating and evaporating liquid pump (11) It is additionally provided on pipeline pump discharge pressure table (12), the pump outlet check valve (13) is communicated with ball valve (9) by pipeline, described Ball valve (9) is communicated with filter (5) by pipeline, and filter (5) upper end also passes through pipeline and is provided with blow valve (6), and Filter (5) lower end is communicated with filter bottom reduced pipe (4), and the filter bottom reduced pipe (4) is also connected to by pipeline Have visor valve (3), and visor valve (3) is communicated with solenoid valve (17) by pipeline, between the solenoid valve (17) and visor valve (3) Pipeline on be also respectively communicated with filter and drain valve (2) and delivery gauge (8), the solenoid valve (17) also passes through pipeline Connection is in falling film evaporator (1) upper end.
2. the process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility according to claim 1, It is characterized in that, being also communicated with bypass valve (10) on pipeline between the solenoid valve (17) and falling film evaporator (1), and bypass On pipeline of the valve (10) also by pipeline connection between ball valve (9) and pump outlet check valve (13).
3. the process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility according to claim 1, It is characterized in that, being also communicated with electromagnetic flowmeter (14), institute on pipeline between the ball valve (9) and pump outlet check valve (13) It states electromagnetic flowmeter (14) to be communicated with flow control valve (15) by pipeline, and flow control valve (15) is communicated with skill by pipeline Art grade product slot (16).
4. the process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility according to claim 1, It is characterized in that, being additionally provided with inlet pressure gauge (7) on pipeline between the filter (5) and ball valve (9).
CN201811029245.1A 2018-09-05 2018-09-05 The process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility Pending CN108939588A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811029245.1A CN108939588A (en) 2018-09-05 2018-09-05 The process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811029245.1A CN108939588A (en) 2018-09-05 2018-09-05 The process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility

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Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB590439A (en) * 1945-04-17 1947-07-17 Laporte Ltd B Improvements in and relating to the concentration and purification of hydrogen peroxide by distillation
CH258840A (en) * 1945-07-11 1948-12-31 Buffalo Electro Chem Co A method for concentrating and purifying aqueous solutions of hydrogen peroxide.
GB872925A (en) * 1956-08-27 1961-07-12 Columbia Southern Chem Corp Method of concentrating aqueous hydrogen peroxide solutions
GB1155886A (en) * 1966-08-09 1969-06-25 Mojonnier Bros Co Flow Control For A Multiple-Effect Evaporator
CN1104995A (en) * 1993-09-13 1995-07-12 三菱瓦斯化学株式会社 Method for enrichment and purification of aqueous hydrogen peroxide solution
JPH0840708A (en) * 1993-09-13 1996-02-13 Mitsubishi Gas Chem Co Inc Concentrating purification of aqueous hydrogen peroxide solution
US20040107597A1 (en) * 2000-11-22 2004-06-10 Ismo Hirvonen Process and device for evaporating liquids, for example black liquor from cellulose cooking, which contain solid and dissolved substances
JP2008127231A (en) * 2006-11-17 2008-06-05 Santoku Kagaku Kogyo Kk Method and apparatus for purifying hydrogen peroxide solution
CN102086028A (en) * 2009-12-07 2011-06-08 郑国玉 Concentration method for producing highly-concentrated chemical-grade hydrogen peroxide solution
CN102161475A (en) * 2009-11-02 2011-08-24 郑国玉 Concentration method in production of hydrogen peroxide by anthraquinone method
CN204237558U (en) * 2014-11-27 2015-04-01 山东晋煤明水化工集团有限公司 The after-treatment device of hydrogen peroxide obtained by anthraquinone process production technique
CN206063809U (en) * 2016-08-30 2017-04-05 江山市双氧水有限公司 Alkali system control device is steamed in a kind of hydrogen peroxide serialization
CN107619024A (en) * 2017-10-20 2018-01-23 山东明化新材料有限公司 Hydrogen peroxide manufacture anthraquinone degradation products Dual alkali regenerating unit
CN208852441U (en) * 2018-09-05 2019-05-14 江山市双氧水有限公司 The process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility

Patent Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB590439A (en) * 1945-04-17 1947-07-17 Laporte Ltd B Improvements in and relating to the concentration and purification of hydrogen peroxide by distillation
CH258840A (en) * 1945-07-11 1948-12-31 Buffalo Electro Chem Co A method for concentrating and purifying aqueous solutions of hydrogen peroxide.
GB872925A (en) * 1956-08-27 1961-07-12 Columbia Southern Chem Corp Method of concentrating aqueous hydrogen peroxide solutions
GB1155886A (en) * 1966-08-09 1969-06-25 Mojonnier Bros Co Flow Control For A Multiple-Effect Evaporator
CN1104995A (en) * 1993-09-13 1995-07-12 三菱瓦斯化学株式会社 Method for enrichment and purification of aqueous hydrogen peroxide solution
JPH0840708A (en) * 1993-09-13 1996-02-13 Mitsubishi Gas Chem Co Inc Concentrating purification of aqueous hydrogen peroxide solution
US20040107597A1 (en) * 2000-11-22 2004-06-10 Ismo Hirvonen Process and device for evaporating liquids, for example black liquor from cellulose cooking, which contain solid and dissolved substances
JP2008127231A (en) * 2006-11-17 2008-06-05 Santoku Kagaku Kogyo Kk Method and apparatus for purifying hydrogen peroxide solution
CN102161475A (en) * 2009-11-02 2011-08-24 郑国玉 Concentration method in production of hydrogen peroxide by anthraquinone method
CN102086028A (en) * 2009-12-07 2011-06-08 郑国玉 Concentration method for producing highly-concentrated chemical-grade hydrogen peroxide solution
CN204237558U (en) * 2014-11-27 2015-04-01 山东晋煤明水化工集团有限公司 The after-treatment device of hydrogen peroxide obtained by anthraquinone process production technique
CN206063809U (en) * 2016-08-30 2017-04-05 江山市双氧水有限公司 Alkali system control device is steamed in a kind of hydrogen peroxide serialization
CN107619024A (en) * 2017-10-20 2018-01-23 山东明化新材料有限公司 Hydrogen peroxide manufacture anthraquinone degradation products Dual alkali regenerating unit
CN208852441U (en) * 2018-09-05 2019-05-14 江山市双氧水有限公司 The process system of flush distillation circulation fluid filtration device in a kind of hydrogen peroxide enrichment facility

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Application publication date: 20181207

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