CN108938532A - Method for preparing series cosmetics from donkey milk - Google Patents

Method for preparing series cosmetics from donkey milk Download PDF

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Publication number
CN108938532A
CN108938532A CN201810762848.6A CN201810762848A CN108938532A CN 108938532 A CN108938532 A CN 108938532A CN 201810762848 A CN201810762848 A CN 201810762848A CN 108938532 A CN108938532 A CN 108938532A
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donkey milk
skin
extract
added
heating
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CN108938532B (en
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董金豹
潘玉柱
何涛
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Hello Donkey Tianjin International Trade Co ltd
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Hello Donkey Tianjin International Trade Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
    • A61K8/986Milk; Derivatives thereof, e.g. butter
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/23Sulfur; Selenium; Tellurium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/26Organic compounds, e.g. vitamins containing oxygen
    • C11D9/262Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Veterinary Medicine (AREA)
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  • Molecular Biology (AREA)
  • Inorganic Chemistry (AREA)
  • Emergency Medicine (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Zoology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a method for preparing series cosmetics by donkey milk, belonging to the technical field of cosmetic preparation. A method for preparing series of cosmetics from donkey milk comprises mixing donkey milk with adjuvant ingredients, wherein the series of cosmetics comprises bath lotion, shampoo and milk soap; according to the donkey milk, the donkey milk is matched with the auxiliary ingredients, the donkey milk is rich in functional whey protein and unsaturated fatty acid, has unique functional effects of prolonging life, enhancing resistance and immunity, protecting liver and stomach, whitening skin and the like, is natural in all effects, is matched with various auxiliary ingredients, can play a good cleaning role on skin, can play roles in whitening skin, protecting skin, shrinking pores, replenishing water and beautifying, also has the advantages of removing skin melanin, increasing skin elasticity and reducing skin wrinkles, is suitable for any skin, does not have any side effect, and is convenient to popularize and apply.

Description

A method of serial cosmetics are prepared using donkey milk
Technical field
The present invention relates to technical field of cosmetic preparation more particularly to a kind of sides that serial cosmetics are prepared using donkey milk Method.
Background technique
Donkey milk is a kind of natural health milk, her trophism with it is both effectiveness be inherent, donkey milk category lactalbumin Newborn class, biological value are high, and taro alkali acid contained in donkey milk can beauty treatment skin whitening, skin care item, which are made, using donkey milk has Very big advantage function, donkey milk skin care item have made first appearance on the market, but donkey milk skin care item in the market are also situation list One, it acts on limited.
The skin of health is water and oil balance, and acid-base scale of skin is moderate, and smooth pliable elasticity, ruddy and glossy, pore is thin It is small, lines marshalling, what sulci of skin moved towards in length and breadth, in recent years, with the improvement of people's life quality, the requirement to cosmetics It is higher and higher;Most of the cosmetics that people use at present have that effect is indefinite and certain adverse reaction, institute occur With people be highly desirable to definite effect, action pathway multiplicity, safely, have no adverse reaction have moisturizing, whitening and antioxygen The product of change effect;Since social competition is increasingly fierce, life and work tempo increase, currently used maintenance product effect is not Enough ideals.
Summary of the invention
The purpose of the present invention is to solve the moisturizing of donkey milk cosmetic, whitening and antioxidation are low, and it is unfavorable for people The problem of body absorbs, and a kind of method for preparing serial cosmetics using donkey milk proposed.
To achieve the goals above, present invention employs following technical solutions:
A method of serial cosmetics are prepared using donkey milk, comprising the following steps:
S1, new fresh donkey milk, Flos Rosae Rugosae extract, emblic extract, gelatin, triethanolamine, galam butter, deionization are chosen Water, sodium carboxymethylcellulose, radix-polygoni multiflori extract, aloe gel, sodium citrate, Cocoamidopropyl betaine, tea oil, chrysanthemum Flower extract smears the raw materials such as tea oil, rose hip oil, sulphur, soap base;
S2, new fresh donkey milk 500g, emblic extract 5-15g and sulphur 15-25g is taken to stir evenly obtained mixed raw material;
S3, Flos Rosae Rugosae extract 3-5g, emblic extract 2-3g, gelatin 5-8g, triethanolamine 1-3g, galam butter 5-7g are taken It is mixed evenly with deionized water 90-110g, sodium carboxymethylcellulose 2-4g is then added into mixed liquor, be mixed equal It is even, it adds mixed raw material 46-108g in S2 and donkey milk shower cream is made;
S4, radix-polygoni multiflori extract 3-4g, emblic extract 2-3g, aloe gel 8-10g, sodium citrate 6-8g, cocounut oil acyl are taken In amine propyl betaine 2-4g, tea oil 5-7g and deionized water 90-110g investment mixing machine, 0.5h, temperature is mixed in heating Auxiliary material 2-4g is added at 75 DEG C -85 DEG C in degree control after being stirred, continue emulsification heating 1-2h, and emulsification heating temperature is 90 DEG C -95 DEG C, mixed raw material 50-116g in S2 is added, after sterilizing after stirring and evenly mixing, donkey milk shampoo is made in vacuum outgas;
S5, mixed raw material 50-55g in S2 is slowly poured into after taking soap base 35-40g heating and melting, chrysanthemum is then added thereto again Flower extract 2-4g, emblic extract 0.8-1.2g, tea oil 10-15g, sodium carboxymethylcellulose 2-4g and rose hip oil 2- are smeared 4g Hybrid Heating, heating temperature are 30 DEG C -40 DEG C, heating time 25-30min, are poured into after mixing evenly cooling solidifying in mold Donkey milk soap is made Gu demoulding.
Preferably, donkey milk soap is produced in the S5 using cold preparation method, the cold preparation method overall process is lower than 40 DEG C.
Preferably, auxiliary material is prepared by following procedure in the S4: being taken 9.5ml glacial acetic acid to be put into beaker, will be burnt Cup is put into cryostat in ice water, then 3.5ml chlorosulfonic acid is added into beaker, and after continuing cryostat for a period of time, 10g dodecanol is existed It is slowly added in beaker in five minutes, after stirring 30min, dodecanol is made to be completely dissolved it, 30g n-butanol is added thereto, And uniform stirring 3min, it is slowly added to 3.0ml saturated sodium carbonate solution during uniform stirring, waits until reaction solution PH > When 7,10g solid solid anhydrous sodium carbonate is added, later pours into upper solution in 250ml separatory funnel, then plus the positive fourth of 20ml Alcohol pours into the beaker originally reacted, and stirring stands and then pours into upper solution in above-mentioned 250ml separatory funnel, then will After 250ml separatory funnel stands 5min, upper solution is poured into another beaker, if heating evaporation obtains auxiliary material It is dry.
Preferably, sterilization uses pasteurization in the S4, the material stirred evenly is heated to 68~70, and keep Rapid cooling is to 4-5 DEG C after this temperature 30min.
Preferably, cooled and solidified in the S5, mixed solution is placed in the zubzero temperature of inert gas shielding, freezing It is demoulded after dry 1h.
Preferably, the mold in the S5, using composite material mould.
Preferably, vacuum outgas in the S4, vacuum cavitations are in 3-4Mpa.
Compared with prior art, the present invention provides a kind of method for preparing serial cosmetics using donkey milk, have following The utility model has the advantages that
(1) present invention is matched by donkey milk and auxiliary ingredients, and donkey milk is rich in functional whey protein and unsaturated fatty acid, tool Have and lengthen the life, strength and immunity, liver-protecting and stomach-protecting, the effect of the unique functions such as skin whitening are supported in enhancing, and donkey milk institute is powerful all Be it is natural, arrange in pairs or groups multiple auxiliary materials, good cleaning action can be played to skin, can not only play whitening and skin-protecting, shrink Pore, moisturizing beauty treatment effect, while also have except dermal melanin, increase skin elasticity, reduce wrinkle of skin the advantages of, fit It is easy to promote and utilize for any skin quality and without any side effects;
(2) donkey milk soap is produced in the present invention and uses cold preparation method, is saponified in the environment of room temperature in manufacturing process, whole Make temperature no more than 40 DEG C, such production method can become to avoid the nutrient for being lost part because of high temperature and certain greases The case where matter, occurs, and during only making, requires a great deal of time, and plus natural new fresh donkey milk, does not surpass in temperature In the case where crossing 40 DEG C, the nutritional ingredient that can be very good to save in donkey milk is not destroyed, and using can allow people to feel especially It is salubrious moisten, be preferably minimized soap soap to skin irritatin degree, use composite die, can make demoulding it is lighter, no It will cause unnecessary waste
(3) sterilization of donkey milk shampoo uses pasteurization in the present invention, and temperature is no more than 70 DEG C, has effectively locked donkey Nutrient in milk is not lost in the event of high temperatures, and in the case where rapid cooling, can also preferably save it In moisture;Vacuum outgas is additionally used, effectively avoids the pollution of external environment, and shampoo can be made to use More silk is sliding.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation Example is only a part of the embodiment of the present invention, instead of all the embodiments.
In the description of the present invention, it is to be understood that, term " on ", "lower", "front", "rear", "left", "right", "top", The orientation or positional relationship of the instructions such as "bottom", "inner", "outside", is merely for convenience of description of the present invention and simplification of the description, rather than The device or element of indication or suggestion meaning must have a particular orientation, be constructed and operated in a specific orientation, therefore cannot It is interpreted as limitation of the present invention.
Embodiment 1:
A method of serial cosmetics are prepared using donkey milk, comprising the following steps:
S1, new fresh donkey milk, Flos Rosae Rugosae extract, emblic extract, gelatin, triethanolamine, galam butter, deionization are chosen Water, sodium carboxymethylcellulose, radix-polygoni multiflori extract, aloe gel, sodium citrate, Cocoamidopropyl betaine, tea oil, chrysanthemum Flower extract smears the raw materials such as tea oil, rose hip oil, sulphur, soap base;
S2, new fresh donkey milk 500g, emblic extract 5-15g and sulphur 15-25g is taken to stir evenly obtained mixed raw material;
S3, Flos Rosae Rugosae extract 3-5g, emblic extract 2-3g, gelatin 5-8g, triethanolamine 1-3g, galam butter 5-7g are taken It is mixed evenly with deionized water 90-110g, sodium carboxymethylcellulose 2-4g is then added into mixed liquor, be mixed equal It is even, it adds mixed raw material 46-108g in S2 and donkey milk shower cream is made;
S4, radix-polygoni multiflori extract 3-4g, emblic extract 2-3g, aloe gel 8-10g, sodium citrate 6-8g, cocounut oil acyl are taken In amine propyl betaine 2-4g, tea oil 5-7g and deionized water 90-110g investment mixing machine, 0.5h, temperature is mixed in heating Auxiliary material 2-4g is added at 75 DEG C -85 DEG C in degree control after being stirred, continue emulsification heating 1-2h, and emulsification heating temperature is 90 DEG C -95 DEG C, mixed raw material 50-116g in S2 is added, after sterilizing after stirring and evenly mixing, donkey milk shampoo is made in vacuum outgas;
S5, mixed raw material 50-55g in S2 is slowly poured into after taking soap base 35-40g heating and melting, chrysanthemum is then added thereto again Flower extract 2-4g, emblic extract 0.8-1.2g, tea oil 10-15g, sodium carboxymethylcellulose 2-4g and rose hip oil 2- are smeared 4g Hybrid Heating, heating temperature are 30 DEG C -40 DEG C, heating time 25-30min, are poured into after mixing evenly cooling solidifying in mold Donkey milk soap is made Gu demoulding.
Donkey milk soap is produced in S5 using cold preparation method, cold preparation method overall process is lower than 40 DEG C.
Auxiliary material is prepared by following procedure in S4: taking 9.5ml glacial acetic acid to be put into beaker, beaker is put into ice water Cryostat, then 3.5ml chlorosulfonic acid is added into beaker, after continuing cryostat for a period of time, in five minutes slowly by 10g dodecanol It is added in beaker, after stirring 30min, dodecanol is made to be completely dissolved it, 30g n-butanol, and uniform stirring are added thereto 3min is slowly added to 3.0ml saturated sodium carbonate solution during uniform stirring, until reaction solution PH > 7, is added 10g solid solid anhydrous sodium carbonate, later pours into upper solution in 250ml separatory funnel, then plus 20ml n-butanol pour into original In the beaker first reacted, stirring stands and then pours into upper solution in above-mentioned 250ml separatory funnel, then by 250ml liquid separation After funnel stands 5min, upper solution is poured into another beaker, it is several that heating evaporation obtains auxiliary material.
Sterilization uses pasteurization in S4, the material stirred evenly is heated to 68~70, and keep this temperature 30min Rapid cooling is to 4-5 DEG C afterwards.
Cooled and solidified in S5, mixed solution is placed in the zubzero temperature of inert gas shielding, is taken off after being freeze-dried 1h Mould.
Mold in S5, using composite material mould.
Vacuum outgas in S4, vacuum cavitations are in 3-4Mpa.
Embodiment 2:
Take Flos Rosae Rugosae extract 4g, emblic extract 2.5g, gelatin 6.5g, triethanolamine 2g, galam butter 6g and deionization Water 100g is mixed evenly, and sodium carboxymethylcellulose 3g and sulphur 7g is then added into mixed liquor, is mixed evenly, most Donkey milk 100g is added afterwards to mix;
The shower cream can be moisturized the skin effectively, and due to joined donkey milk, donkey milk itself has more collagen, Moisturizing and other effects effectively can be carried out to skin, and since donkey milk is closest to a kind of liquid of human body lotion, so having The generation for avoiding anaphylaxis problem of effect, and when preparation, effectively avoid disappearing for donkey milk nutrient itself Consumption more preferably can carry out moisturizing and other effects to human body.
Embodiment 3:
Take radix-polygoni multiflori extract 3.5g, emblic extract 2.5g, aloe gel 9g, sodium citrate 7g, cocamidopropyl propyl amide sweet tea Dish alkali 3g, tea oil 6g, deionized water 100g are put into mixing machine, and half an hour is mixed in heating, and temperature is controlled at 80 DEG C, Dodecyl ether sulfate 3g and sulphur 10g is added after being stirred, continues emulsification heating 1.5 hours, controlled at 92 DEG C, finally by donkey milk 115g is added, rear pasteurize is stirred and evenly mixed, is packed after vacuum outgas and donkey milk shampoo is made;
The sterilization of donkey milk shampoo uses pasteurization, and temperature is no more than 70 DEG C, has effectively locked the nutrition in donkey milk Element is not lost in the event of high temperatures, and in the case where rapid cooling, can also preferably save moisture therein;Also Using vacuum outgas, the pollution of external environment is effectively avoided, and it is sliding that shampoo can be made to use more silk.
Embodiment 4:
The method for preparing milk soap using donkey milk will slowly pour into donkey milk 52g after soap base 38g heating and melting according to parts by weight, so Chrysanthemum extract 3g, emblic extract 1.0g is added thereto again afterwards, smears tea oil 12g, sodium carboxymethylcellulose 3g, fructus rosae Oily 3g and sulphur 4.5g Hybrid Heating;Temperature 45 C is controlled, incorporation time is 30 minutes;It pours into after mixing evenly cooling in mold Solidification demoulds and donkey milk soap is made;
Donkey milk soap uses cold preparation method, is saponified in the environment of room temperature in manufacturing process, and whole process only makees temperature no more than 40 DEG C, such production method can to avoid generation the case where the nutrient and certain grease deteriorations for being lost part because of high temperature, It during only making, requires a great deal of time, is adding natural new fresh donkey milk, the case where temperature is no more than 40 DEG C Under, the nutritional ingredient that can be very good to save in donkey milk is not destroyed, and using can allow people to feel especially salubrious moist, is made Soap soap is preferably minimized skin irritatin degree, uses composite die, and demoulding can be made lighter, do not will cause unnecessary Waste.
Embodiment 5:
The present invention is matched by donkey milk and auxiliary ingredients, and donkey milk is rich in functional whey protein and unsaturated fatty acid, is had Lengthen the life, strength and immunity, liver-protecting and stomach-protecting, the effect of the unique functions such as skin whitening are supported in enhancing, and donkey milk institute powerful is all Natural, multiple auxiliary materials of arranging in pairs or groups can play good cleaning action to skin, can not only play whitening and skin-protecting, shrink hair Hole, moisturizing beauty treatment effect, while also have except dermal melanin, increase skin elasticity, reduce wrinkle of skin the advantages of, be applicable in It is easy to promote and utilize in any skin quality and without any side effects;
And donkey milk can be very good a series of problems, such as avoiding allergy as a kind of liquid closest to human milk, can have In the case where the protection human body of effect, the operation such as moisturizing is carried out to human body, and when making cosmetics, it is conscious to evade It is most of to make the operation that nutrient consumes in donkey milk, can the significantly more efficient nutrition saved in donkey milk, more preferably Human body is protected and is repaired.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (7)

1. a kind of method for preparing serial cosmetics using donkey milk, which comprises the following steps:
S1, new fresh donkey milk, Flos Rosae Rugosae extract, emblic extract, gelatin, triethanolamine, galam butter, deionization are chosen Water, sodium carboxymethylcellulose, radix-polygoni multiflori extract, aloe gel, sodium citrate, Cocoamidopropyl betaine, tea oil, chrysanthemum Flower extract smears the raw materials such as tea oil, rose hip oil, sulphur, soap base;
S2, new fresh donkey milk 500g, emblic extract 5-15g and sulphur 15-25g is taken to stir evenly obtained mixed raw material;
S3, Flos Rosae Rugosae extract 3-5g, emblic extract 2-3g, gelatin 5-8g, triethanolamine 1-3g, galam butter 5-7g are taken It is mixed evenly with deionized water 90-110g, sodium carboxymethylcellulose 2-4g is then added into mixed liquor, be mixed equal It is even, it adds mixed raw material 46-108g in S2 and donkey milk shower cream is made;
S4, radix-polygoni multiflori extract 3-4g, emblic extract 2-3g, aloe gel 8-10g, sodium citrate 6-8g, cocounut oil acyl are taken In amine propyl betaine 2-4g, tea oil 5-7g and deionized water 90-110g investment mixing machine, 0.5h, temperature is mixed in heating Auxiliary material 2-4g is added at 75 DEG C -85 DEG C in degree control after being stirred, continue emulsification heating 1-2h, and emulsification heating temperature is 90 DEG C -95 DEG C, mixed raw material 50-116g in S2 is added, after sterilizing after stirring and evenly mixing, donkey milk shampoo is made in vacuum outgas;
S5, mixed raw material 50-55g in S2 is slowly poured into after taking soap base 35-40g heating and melting, chrysanthemum is then added thereto again Flower extract 2-4g, emblic extract 0.8-1.2g, tea oil 10-15g, sodium carboxymethylcellulose 2-4g and rose hip oil 2- are smeared 4g Hybrid Heating, heating temperature are 30 DEG C -40 DEG C, heating time 25-30min, are poured into after mixing evenly cooling solidifying in mold Donkey milk soap is made Gu demoulding.
2. a kind of method for preparing serial cosmetics using donkey milk according to claim 1, it is characterised in that: in the S5 Donkey milk soap is produced using cold preparation method, the cold preparation method overall process is lower than 40 DEG C.
3. a kind of method for preparing serial cosmetics using donkey milk according to claim 1, it is characterised in that: in the S4 Auxiliary material passes through following procedure and prepares: taking 9.5ml glacial acetic acid to be put into beaker, beaker is put into cryostat in ice water, then to burning 3.5ml chlorosulfonic acid is added in cup, after continuing cryostat for a period of time, 10g dodecanol is slowly added in beaker in five minutes, After stirring 30min, dodecanol is made to be completely dissolved it, 30g n-butanol, and uniform stirring 3min are added thereto, is uniformly stirring It is slowly added to 3.0ml saturated sodium carbonate solution during mixing, until reaction solution PH > 7,10g solid solid water-free is added Sodium carbonate later pours into upper solution in 250ml separatory funnel, then plus 20ml n-butanol pour into the beaker originally reacted, Stirring stand and then upper solution is poured into above-mentioned 250ml separatory funnel, then by 250ml separatory funnel stand 5min it Afterwards, upper solution is poured into another beaker, it is several that heating evaporation obtains auxiliary material.
4. a kind of method for preparing serial cosmetics using donkey milk according to claim 1, it is characterised in that: in the S4 Sterilization uses pasteurization, the material stirred evenly is heated to 68~70, and rapid cooling after this temperature 30min is kept to arrive 4-5℃。
5. a kind of method for preparing serial cosmetics using donkey milk according to claim 1, it is characterised in that: in the S5 Mixed solution is placed in the zubzero temperature of inert gas shielding by cooled and solidified, is demoulded after being freeze-dried 1h.
6. a kind of method for preparing serial cosmetics using donkey milk according to claim 1, it is characterised in that: in the S5 Mold, using composite material mould.
7. a kind of method for preparing serial cosmetics using donkey milk according to claim 1, it is characterised in that: in the S4 Vacuum outgas, vacuum cavitations are in 3-4Mpa.
CN201810762848.6A 2018-07-12 2018-07-12 Method for preparing series cosmetics from donkey milk Active CN108938532B (en)

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