CN108926863B - Quick heating distillation device in refining process of high-purity titanium tetrachloride - Google Patents
Quick heating distillation device in refining process of high-purity titanium tetrachloride Download PDFInfo
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- CN108926863B CN108926863B CN201811227176.5A CN201811227176A CN108926863B CN 108926863 B CN108926863 B CN 108926863B CN 201811227176 A CN201811227176 A CN 201811227176A CN 108926863 B CN108926863 B CN 108926863B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/022—Titanium tetrachloride
- C01G23/024—Purification of tetrachloride
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Abstract
The invention discloses a rapid heating distillation device in a refining process of high-purity titanium tetrachloride, which comprises a feeding pipeline, a sealing cover, a distillation device main body, a deslagging pipeline, a sealing cover and a supporting mechanism arranged on the lower surface of the distillation device main body, wherein the top end of the distillation device main body is provided with a fixing mechanism, and the fixing mechanism comprises a first L-shaped fixing block, a nut, a threaded rod, a second L-shaped fixing block, a second arc-shaped groove, a fixing hole, a limiting groove, a limiting block, a sliding groove and a first arc-shaped groove; the limiting block slides in the limiting groove, so that the second L-shaped fixed block is prevented from falling off and being lost from the inside of the sliding groove, the use cost of a user is reduced, the nut is rotated on the surface of the threaded rod clockwise, the second L-shaped fixed block conveniently slides upwards in the sliding groove to enable the joint of the sealing cover and the distillation device main body to be tightly attached, the sealing cover is conveniently installed and placed at the top end of the distillation device main body, and the sealing cover is conveniently detached and maintained from the surface of the distillation device main body.
Description
Technical Field
The invention belongs to the technical field of rapid heating distillation devices, and particularly relates to a rapid heating distillation device in a refining process of high-purity titanium tetrachloride.
Background
In the refining process of titanium tetrachloride, impurities are separated by a distillation method or a rectification method according to the characteristic that the difference between the boiling points or the relative volatilities of high-boiling-point impurities and low-boiling-point impurities in crude titanium tetrachloride is large. The high boiling point impurities which are easy to separate are separated by a distillation method, and the low boiling point impurities which are difficult to separate are separated by a rectification method.
In the use process of the existing distillation device, the sealing cover is complicated in steps during sealing, the tightness is required to be checked repeatedly, an installer is easy to make mistakes during sealing, the normal use of the distillation device is affected, and the working efficiency of the distillation device is reduced, so that the quick heating distillation device in the refining process of the high-purity titanium tetrachloride is provided.
Disclosure of Invention
The invention aims to provide a rapid heating distillation device in the refining process of high-purity titanium tetrachloride, so as to solve the problems that in the prior art, the sealing cover has complex steps in the sealing process, the tightness needs to be repeatedly checked, the installer is easy to make mistakes in the sealing process, the normal use of the distillation device is influenced, and the working efficiency of the distillation device is reduced.
In order to achieve the above purpose, the present invention provides the following technical solutions: the utility model provides a high-purity titanium tetrachloride refining in-process rapid heating distillation plant, includes feed pipe, sealed lid, distillation plant main part, slag discharge pipeline, closing cap and distillation plant main part lower surface setting's supporting mechanism, the top of distillation plant main part is provided with fixed establishment, fixed establishment includes first L type fixed block, nut, threaded rod, second L type fixed block, second arc recess, fixed orifices, spacing groove, stopper, sliding tray and first arc recess, feed pipe installs and fixes at the upper surface of sealed lid, sealed lid installation is placed on the top of distillation plant main part, slag discharge pipeline installation is fixed in the bottom of distillation plant main part, the upper surface at feed pipe is fixed in the surface junction of distillation plant main part and sealed lid in the installation of first L type fixed block symmetry, the nut cover is established at the upper surface of threaded rod and is located the upper surface of first L type fixed block, the threaded rod is installed and is fixed at the upper surface of second L type fixed block and place at the inside of fixed orifices, the fixed orifices is seted up at the upper surface of first L type fixed block and is fixed at the upper surface of second L type fixed block and the inside the fixed slot, the second L type fixed block and the side of second L type fixed block and the inside the fixed block and the side of fixed groove is seted up at the inside the two side of the fixed groove, the side of the second L type fixed block and the inside the fixed groove is seted up at the side of the fixed groove, the second L type fixed block and the inside the side of L type fixed block is fixed at the side of the fixed groove, the first arc-shaped groove is formed in the inner surface of the first L-shaped fixing block and is clamped with the edge of the bottom end of the sealing cover, the first L-shaped fixing block and the second L-shaped fixing block are combined and clamped at the edges of the sealing cover and the distillation device main body, and a control mechanism is arranged on the upper surface of the feeding pipeline.
Preferably, the control mechanism comprises a U-shaped fixing plate, a rotating disc, rotating rods, threaded holes, clamping grooves, fixing protrusions and rotating grooves, wherein the U-shaped fixing plate is symmetrically installed and fixed at the top end of a feeding pipeline, fixing blocks are symmetrically arranged on the side surfaces of the feeding pipeline, the rotating grooves are formed in the surfaces of the fixing blocks, the fixing protrusions are symmetrically fixed on the two sides of the U-shaped fixing plate and placed in the rotating grooves, the threaded holes are formed in the upper surfaces of the U-shaped fixing plate and penetrate through the lower surfaces of the U-shaped fixing plate, the rotating rods are installed and placed on the lower surfaces of the rotating discs and placed in the threaded holes, the rotating discs are installed and fixed at the top ends of the rotating rods, the bottom ends of the rotating rods penetrate through the threaded holes and are placed in the clamping grooves, threads are arranged on the surfaces of the rotating rods, the clamping grooves are symmetrically formed in the edge positions of the upper surfaces of the sealing covers, and the bottom ends of the rotating rods are placed in the clamping grooves.
Preferably, the support mechanism comprises support legs, the support legs are symmetrically fixed on the lower surface of the distillation device main body, and the lower surface of the support legs is provided with a antiskid plate.
Preferably, fixing pull rings are symmetrically arranged at the edge positions of the upper surface of the sealing cover, and the upper surface of the sealing cover is provided with a steam pipeline and is communicated with the inside of the distillation device main body.
Preferably, the surface of distillation plant main part is provided with the return conduit, the connecting hole has been seted up to the surface symmetry of return conduit, the side of distillation plant main part is provided with overflow pipeline, the surface symmetry of distillation plant main part is provided with the connecting block and is located the upside of return conduit.
Compared with the prior art, the invention has the beneficial effects that:
(1) The limiting block slides in the limiting groove, so that the second L-shaped fixing block is prevented from falling off and being lost from the inside of the sliding groove, the use cost of a user is reduced, the nut is rotated on the surface of the threaded rod clockwise, the second L-shaped fixing block conveniently slides upwards in the sliding groove to enable the joint of the sealing cover and the distillation device main body to be tightly attached, the sealing cover is conveniently installed and placed at the top end of the distillation device main body, the sealing cover is conveniently detached and maintained from the surface of the distillation device main body at the later stage, the first L-shaped fixing block can slide at the edge of the bottom end of the sealing cover through the first arc-shaped groove, and the position of the first L-shaped fixing block is conveniently adjusted on the surface of the sealing cover.
(2) The bottom end of the rotating rod is placed in the clamping groove, the rotating rod is prevented from sliding and falling off from the upper surface of the sealing cover, the firmness of the U-shaped fixing plate on the upper surface of the sealing cover is increased, meanwhile, the firmness of the sealing cover on the upper surface of the feeding pipeline is increased, air leakage at the joint of the sealing cover and the feeding pipeline is prevented, the rotating plate is rotated anticlockwise and drives the rotating rod to rotate in the threaded hole, the U-shaped fixing plate is conveniently separated from the upper surface of the sealing cover, the sealing cover is conveniently taken down from the top end of the feeding pipeline, and the sealing cover is conveniently installed and fixed on the upper surface of the feeding pipeline again.
Drawings
FIG. 1 is a schematic diagram of the structure of the present invention;
FIG. 2 is a schematic side view of a first L-shaped fixing block according to the present invention;
FIG. 3 is a schematic cross-sectional elevation view of a first L-shaped fixing block according to the present invention;
FIG. 4 is an enlarged cross-sectional view of the structure of FIG. 1A according to the present invention;
FIG. 5 is a schematic side view of the distillation apparatus main body of the present invention;
in the figure: 1. a feed conduit; 2. sealing cover; 3. a first L-shaped fixed block; 4. a distillation apparatus main body; 5. a return line; 6. support legs; 7. a slag discharge pipeline; 8. an overflow pipe; 9. fixing the pull ring; 10. a U-shaped fixing plate; 11. a closing cap; 12. a nut; 13. a threaded rod; 14. a second L-shaped fixed block; 15. a second arcuate recess; 16. a fixing hole; 17. a limit groove; 18. a limiting block; 19. a sliding groove; 20. a rotating disc; 21. a rotating rod; 22. a threaded hole; 23. a clamping groove; 24. a fixing protrusion; 25. a rotating groove; 26. a first arcuate recess.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1: referring to fig. 1, fig. 2, fig. 3 and fig. 4, a rapid heating distillation apparatus in the refining process of high purity titanium tetrachloride comprises a feed pipe 1, a sealing cover 2, a distillation apparatus main body 4, a slag discharge pipe 7, a sealing cover 11 and a supporting mechanism arranged on the lower surface of the distillation apparatus main body 4, wherein the top end of the distillation apparatus main body 4 is provided with a fixing mechanism, the fixing mechanism comprises a first L-shaped fixing block 3, a nut 12, a threaded rod 13, a second L-shaped fixing block 14, a second arc-shaped groove 15, a fixing hole 16, a limiting groove 17, a limiting block 18, a sliding groove 19 and a first arc-shaped groove 26, the feed pipe 1 is fixedly arranged on the upper surface of the sealing cover 2, the sealing cover 2 is fixedly arranged on the top end of the distillation apparatus main body 4, the slag discharge pipe 7 is fixedly arranged at the bottom end of the distillation apparatus main body 4, the sealing cover 11 is fixedly arranged on the upper surface of the feed pipe 1, the first L-shaped fixing block 3 is symmetrically arranged and fixed at the surface connection part of the distillation device main body 4 and the sealing cover 2, the nut 12 is sleeved on the surface of the threaded rod 13 and positioned on the upper surface of the first L-shaped fixing block 3, the threaded rod 13 is arranged and fixed on the upper surface of the second L-shaped fixing block 14 and placed in the fixing hole 16, the fixing hole 16 is arranged on the upper surface of the first L-shaped fixing block 3 and communicated with the sliding groove 19, the second L-shaped fixing block 14 is arranged and placed in the first L-shaped fixing block 3 and positioned in the sliding groove 19, the sliding groove 19 is arranged on the side surface of the first L-shaped fixing block 3 and penetrates through the lower surface of the first L-shaped fixing block 3, the limiting block 18 is symmetrically arranged and fixed on two sides of the second L-shaped fixing block 14 and placed in the limiting groove 17, the limiting block 17 is symmetrically arranged on the inner surface of the sliding groove 19, the limiting block 18 slides in the limiting groove 17, prevent that second L type fixed block 14 from droing from the inside of sliding tray 19 and losing, increase the whole corollary nature of first L type fixed block 3 and second L type fixed block 14, and reduce user's use cost, second arc recess 15 is offered at the internal surface of second L type fixed block 14 and is with distillation plant main part 4 top edge block, first arc recess 26 is offered at the internal surface of first L type fixed block 3 and is with sealed lid 2 bottom edge block, first L type fixed block 3 and second L type fixed block 14 combination and block are at sealed lid 2 and distillation plant main part 4's edge, through clockwise at threaded rod 13 surface rotation nut 12, make things convenient for second L type fixed block 14 to make sealing lid 2 and distillation plant main part 4 junction closely laminate in the inside of sliding tray 19, make things convenient for sealed lid 2 installation to place on distillation plant main part 4's top, and increase sealed lid 2 and distillation plant main part 4 junction, and 2 follow distillation plant main part 4 surface dismantlement maintenance in the sealed lid 2 later stage, first L type fixed block 3 can be through first L type fixed block 26 at the sealed lid 2 of the sealed lid of the sealed 4 junction of first L type 4, the sealed lid of the installation of the sealed lid 2 is convenient for the installation mechanism is provided with the sealed lid 1 on the sealed lid position of the first L type 1 on the fixed surface of the pipeline 1 is fixed surface of the arc-shaped 1.
In order to facilitate the installation and fixation of the closing cap 11 on the upper surface of the feeding pipe 1, in this embodiment, preferably, the control mechanism comprises a U-shaped fixing plate 10, a rotating disc 20, a rotating rod 21, a threaded hole 22, a clamping groove 23, a fixing protrusion 24 and a rotating groove 25, wherein the U-shaped fixing plate 10 is symmetrically installed and fixed on the top end of the feeding pipe 1, the side surface of the feeding pipe 1 is symmetrically provided with a fixing block, the surface of the fixing block is provided with the rotating groove 25, the fixing protrusion 24 is symmetrically fixed on both sides of the U-shaped fixing plate 10 and placed in the rotating groove 25, one end of the U-shaped fixing plate 10 is conveniently turned over on the side surface of the feeding pipe 1, the threaded hole 22 is formed on the upper surface of the U-shaped fixing plate 10 and penetrates through the lower surface of the U-shaped fixing plate 10, the rotating rod 21 is installed and placed on the lower surface of the rotating disc 20 and placed in the threaded hole 22, the rotating disc 20 is installed and fixed on the top end of the rotating rod 21, the bottom of rotary rod 21 runs through screw hole 22's inside and places in draw-in groove 23's inside, the surface of rotary rod 21 is provided with the screw thread, draw-in groove 23 symmetry is seted up in the upper surface border position department of closing cap 11, the bottom of rotary rod 21 is placed in the inside of draw-in groove 23, prevent rotary rod 21 at closing cap 11 upper surface slip and drop, increase the fastness of U type fixed plate 10 at closing cap 11 upper surface, increase the fastness of closing cap 11 at feeding pipeline 1 upper surface simultaneously, prevent closing cap 11 and feeding pipeline 1 junction gas leakage, through anticlockwise rotation rolling disc 20 and drive rotary rod 21 in screw hole 22's inside rotation, make things convenient for U type fixed plate 10 to break away from closing cap 11's upper surface, and make things convenient for closing cap 11 to take off from feeding pipeline 1's top, make things convenient for closing cap 11 to install again simultaneously and fix at feeding pipeline 1's upper surface.
In order to increase the stability of the support legs 6 on the ground, in this embodiment, it is preferable that the support mechanism includes the support legs 6, the support legs 6 are symmetrically fixed to the lower surface of the distillation apparatus main body 4, and the lower surface of the support legs 6 is provided with a cleat.
In order to facilitate lifting of the sealing cover 2 from the upper surface of the distillation apparatus main body 4, in this embodiment, it is preferable that fixing tabs 9 are symmetrically provided at the edge position of the upper surface of the sealing cover 2, and the upper surface of the sealing cover 2 is provided with a steam pipe and communicates with the inside of the distillation apparatus main body 4.
In order to facilitate connection of the reflux pipeline 5 with other pipelines, in this embodiment, preferably, the surface of the distillation apparatus main body 4 is provided with the reflux pipeline 5, the surface of the reflux pipeline 5 is symmetrically provided with connecting holes, the side surface of the distillation apparatus main body 4 is provided with the overflow pipeline 8, and the surface of the distillation apparatus main body 4 is symmetrically provided with connecting blocks and is located at the upper side of the reflux pipeline 5.
Example 2: referring to fig. 2, 3, 4 and 5, a rapid heating distillation apparatus in a refining process of high purity titanium tetrachloride comprises a feed pipe 1, a sealing cover 2, a distillation apparatus main body 4, a slag discharge pipe 7, a sealing cover 11 and a supporting mechanism arranged on the lower surface of the distillation apparatus main body 4, wherein the top end of the distillation apparatus main body 4 is provided with a fixing mechanism, the fixing mechanism comprises a first L-shaped fixing block 3, a nut 12, a threaded rod 13, a second L-shaped fixing block 14, a second arc-shaped groove 15, a fixing hole 16, a limiting groove 17, a limiting block 18, a sliding groove 19 and a first arc-shaped groove 26, the feed pipe 1 is fixedly arranged on the upper surface of the sealing cover 2, the sealing cover 2 is fixedly arranged on the top end of the distillation apparatus main body 4, the slag discharge pipe 7 is fixedly arranged at the bottom end of the distillation apparatus main body 4, the sealing cover 11 is fixedly arranged on the upper surface of the feed pipe 1, the first L-shaped fixing block 3 is symmetrically arranged and fixed at the surface connection part of the distillation device main body 4 and the sealing cover 2, the nut 12 is sleeved on the surface of the threaded rod 13 and positioned on the upper surface of the first L-shaped fixing block 3, the threaded rod 13 is arranged and fixed on the upper surface of the second L-shaped fixing block 14 and placed in the fixing hole 16, the fixing hole 16 is arranged on the upper surface of the first L-shaped fixing block 3 and communicated with the sliding groove 19, the second L-shaped fixing block 14 is arranged and placed in the first L-shaped fixing block 3 and positioned in the sliding groove 19, the sliding groove 19 is arranged on the side surface of the first L-shaped fixing block 3 and penetrates through the lower surface of the first L-shaped fixing block 3, the limiting block 18 is symmetrically arranged and fixed on two sides of the second L-shaped fixing block 14 and placed in the limiting groove 17, the limiting block 17 is symmetrically arranged on the inner surface of the sliding groove 19, the limiting block 18 slides in the limiting groove 17, prevent that second L type fixed block 14 from droing from the inside of sliding tray 19 and losing, increase the whole corollary nature of first L type fixed block 3 and second L type fixed block 14, and reduce user's use cost, second arc recess 15 is offered at the internal surface of second L type fixed block 14 and is with distillation plant main part 4 top edge block, first arc recess 26 is offered at the internal surface of first L type fixed block 3 and is with sealed lid 2 bottom edge block, first L type fixed block 3 and second L type fixed block 14 combination and block are at sealed lid 2 and distillation plant main part 4's edge, through clockwise at threaded rod 13 surface rotation nut 12, make things convenient for second L type fixed block 14 to make sealing lid 2 and distillation plant main part 4 junction closely laminate in the inside of sliding tray 19, make things convenient for sealed lid 2 installation to place on distillation plant main part 4's top, and increase sealed lid 2 and distillation plant main part 4 junction, and 2 follow distillation plant main part 4 surface dismantlement maintenance in the sealed lid 2 later stage, first L type fixed block 3 can be through first L type fixed block 26 at the sealed lid 2 of the sealed lid of the sealed 4 junction of first L type 4, the sealed lid of the installation of the sealed lid 2 is convenient for the installation mechanism is provided with the sealed lid 1 on the sealed lid position of the first L type 1 on the fixed surface of the pipeline 1 is fixed surface of the arc-shaped 1.
In order to facilitate the installation and fixation of the closing cap 11 on the upper surface of the feeding pipe 1, in this embodiment, preferably, the control mechanism comprises a U-shaped fixing plate 10, a rotating disc 20, a rotating rod 21, a threaded hole 22, a clamping groove 23, a fixing protrusion 24 and a rotating groove 25, wherein the U-shaped fixing plate 10 is symmetrically installed and fixed on the top end of the feeding pipe 1, the side surface of the feeding pipe 1 is symmetrically provided with a fixing block, the surface of the fixing block is provided with the rotating groove 25, the fixing protrusion 24 is symmetrically fixed on both sides of the U-shaped fixing plate 10 and placed in the rotating groove 25, one end of the U-shaped fixing plate 10 is conveniently turned over on the side surface of the feeding pipe 1, the threaded hole 22 is formed on the upper surface of the U-shaped fixing plate 10 and penetrates through the lower surface of the U-shaped fixing plate 10, the rotating rod 21 is installed and placed on the lower surface of the rotating disc 20 and placed in the threaded hole 22, the rotating disc 20 is installed and fixed on the top end of the rotating rod 21, the bottom of rotary rod 21 runs through screw hole 22's inside and places in draw-in groove 23's inside, the surface of rotary rod 21 is provided with the screw thread, draw-in groove 23 symmetry is seted up in the upper surface border position department of closing cap 11, the bottom of rotary rod 21 is placed in the inside of draw-in groove 23, prevent rotary rod 21 at closing cap 11 upper surface slip and drop, increase the fastness of U type fixed plate 10 at closing cap 11 upper surface, increase the fastness of closing cap 11 at feeding pipeline 1 upper surface simultaneously, prevent closing cap 11 and feeding pipeline 1 junction gas leakage, through anticlockwise rotation rolling disc 20 and drive rotary rod 21 in screw hole 22's inside rotation, make things convenient for U type fixed plate 10 to break away from closing cap 11's upper surface, and make things convenient for closing cap 11 to take off from feeding pipeline 1's top, make things convenient for closing cap 11 to install again simultaneously and fix at feeding pipeline 1's upper surface.
In order to facilitate the movement of the support legs 6 on the ground, in this embodiment, it is preferable that the support mechanism includes the support legs 6, the support legs 6 are symmetrically fixed to the lower surface of the distillation apparatus body 4, and the lower surfaces of the support legs 6 are provided with rollers.
In order to facilitate lifting of the sealing cover 2 from the upper surface of the distillation apparatus main body 4, in this embodiment, it is preferable that fixing tabs 9 are symmetrically provided at the edge position of the upper surface of the sealing cover 2, and the upper surface of the sealing cover 2 is provided with a steam pipe and communicates with the inside of the distillation apparatus main body 4.
In order to facilitate connection of the reflux pipeline 5 with other pipelines, in this embodiment, preferably, the surface of the distillation apparatus main body 4 is provided with the reflux pipeline 5, the surface of the reflux pipeline 5 is symmetrically provided with connecting holes, the side surface of the distillation apparatus main body 4 is provided with the overflow pipeline 8, and the surface of the distillation apparatus main body 4 is symmetrically provided with connecting blocks and is located at the upper side of the reflux pipeline 5.
The working principle and the using flow of the invention are as follows: when the invention is used, the sealing cover 2 is firstly arranged on the upper surface of the distillation device main body 4, then the first L-shaped fixed block 3 and the second L-shaped fixed block 14 are respectively arranged on the edges of the sealing cover 2 and the distillation device main body 4, then the first L-shaped fixed block 3 slides and adjusts the position at the bottom end edge of the sealing cover 2 through the first arc-shaped groove 26, then the nut 12 is rotated clockwise on the surface of the threaded rod 13 to enable the second L-shaped fixed block 14 to slide upwards in the sliding groove 19, meanwhile, the limiting block 18 slides in the limiting groove 17, the nut 12 is continuously rotated to enable the second arc-shaped groove 15 on the inner surface of the second L-shaped fixed block 14 to be clamped with the edge of the distillation device main body 4, the lower surface of the sealing cover 2 is tightly adhered to the upper surface of the distillation device main body 4, then the sealing cover 11 is arranged on the upper surface of the feeding pipeline 1, then the U-shaped fixed plate 10 is turned over to enable the fixing boss 24 to rotate in the rotating groove 25, the U-shaped fixed plate 10 is turned over to the upper surface of the sealing cover 11, then the rotating disc 20 is rotated clockwise and the rotating rod 21 is driven to rotate in the threaded hole 22, and then the bottom end of the rotating rod 21 is fixed in the clamping groove 23, and the invention can be used after the invention is finished.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (3)
1. The utility model provides a quick heating distillation plant in high-purity titanium tetrachloride refining process, includes feed line (1), sealed lid (2), distillation plant main part (4), arranges sediment pipeline (7), closing cap (11) and distillation plant main part (4) lower surface setting's supporting mechanism, its characterized in that: the top of the distillation device main body (4) is provided with a fixing mechanism, the fixing mechanism comprises a first L-shaped fixing block (3), a nut (12), a threaded rod (13), a second L-shaped fixing block (14), a second arc-shaped groove (15), a fixing hole (16), a limiting groove (17), a limiting block (18), a sliding groove (19) and a first arc-shaped groove (26), the feeding pipeline (1) is fixedly arranged on the upper surface of the sealing cover (2), the sealing cover (2) is fixedly arranged at the top of the distillation device main body (4), the slag discharging pipeline (7) is fixedly arranged at the bottom of the distillation device main body (4), the sealing cover (11) is fixedly arranged on the upper surface of the feeding pipeline (1), the first L-shaped fixing block (3) is fixedly arranged at the surface joint of the distillation device main body (4) and the sealing cover (2), the nut (12) is sleeved on the surface of the threaded rod (13) and is positioned on the upper surface of the first L-shaped fixing block (3), the threaded rod (13) is fixedly arranged on the second L-shaped fixing block (14) and is fixedly arranged on the surface of the second L-shaped fixing block (16) and is communicated with the surface of the first L-shaped fixing block (16), the second L-shaped fixing block (14) is arranged in the first L-shaped fixing block (3) and is positioned in the sliding groove (19), the sliding groove (19) is formed in the side surface of the first L-shaped fixing block (3) and penetrates through the lower surface of the first L-shaped fixing block (3), the limiting blocks (18) are symmetrically arranged and fixed on two sides of the second L-shaped fixing block (14) and are placed in the limiting grooves (17), the limiting grooves (17) are symmetrically formed in the inner surface of the sliding groove (19), the second arc-shaped grooves (15) are formed in the inner surface of the second L-shaped fixing block (14) and are clamped with the top end edge of the distillation device main body (4), the first arc-shaped grooves (26) are formed in the inner surface of the first L-shaped fixing block (3) and are clamped with the bottom end edge of the sealing cover (2), the first L-shaped fixing block (3) and the second L-shaped fixing block (14) are combined and clamped with the sealing cover (2) and the edge of the distillation device main body (4), and the upper surface of the pipeline (1) is provided with a control mechanism;
the control mechanism comprises a U-shaped fixing plate (10), a rotating disc (20), a rotating rod (21), threaded holes (22), clamping grooves (23), fixing protrusions (24) and rotating grooves (25), wherein the U-shaped fixing plate (10) is symmetrically installed and fixed at the top end of a feeding pipeline (1), fixing blocks are symmetrically arranged on the side surfaces of the feeding pipeline (1), the rotating grooves (25) are formed in the surfaces of the fixing blocks, the fixing protrusions (24) are symmetrically fixed on two sides of the U-shaped fixing plate (10) and placed in the rotating grooves (25), the threaded holes (22) are formed in the upper surface of the U-shaped fixing plate (10) and penetrate through the lower surface of the U-shaped fixing plate (10), the rotating rod (21) is installed and placed on the lower surface of the rotating disc (20) and placed in the threaded holes (22), the rotating disc (20) is installed and fixed at the top end of the rotating rod (21), the bottom end of the rotating rod (21) penetrates through the inner portion of the threaded holes (22) and is placed in the clamping grooves (23), the surface of the rotating rod (21) is provided with the clamping grooves (23), and the clamping grooves (23) are symmetrically formed in the bottom end of the rotating rod (21) and placed on the edge of the rotating disc (11).
The support mechanism comprises support legs (6), wherein the support legs (6) are symmetrically fixed on the lower surface of the distillation device main body (4), and anti-skid plates are arranged on the lower surfaces of the support legs (6).
2. The rapid heating distillation apparatus for refining high purity titanium tetrachloride according to claim 1, wherein: the upper surface edge position department symmetry of sealed lid (2) is provided with fixed pull ring (9), the upper surface of sealed lid (2) is provided with steam conduit and communicates with the inside of distillation plant main part (4).
3. The rapid heating distillation apparatus for refining high purity titanium tetrachloride according to claim 1, wherein: the surface of distillation plant main part (4) is provided with backflow pipeline (5), the connecting hole has been seted up to backflow pipeline (5) surface symmetry, the side of distillation plant main part (4) is provided with overflow pipeline (8), distillation plant main part (4) surface symmetry is provided with the connecting block, the connecting block is located backflow pipeline (5) upside.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811227176.5A CN108926863B (en) | 2018-10-22 | 2018-10-22 | Quick heating distillation device in refining process of high-purity titanium tetrachloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811227176.5A CN108926863B (en) | 2018-10-22 | 2018-10-22 | Quick heating distillation device in refining process of high-purity titanium tetrachloride |
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| Publication Number | Publication Date |
|---|---|
| CN108926863A CN108926863A (en) | 2018-12-04 |
| CN108926863B true CN108926863B (en) | 2023-10-03 |
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| CN201811227176.5A Active CN108926863B (en) | 2018-10-22 | 2018-10-22 | Quick heating distillation device in refining process of high-purity titanium tetrachloride |
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