CN108913065A - A kind of conductive fabric glue and preparation method thereof - Google Patents
A kind of conductive fabric glue and preparation method thereof Download PDFInfo
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- CN108913065A CN108913065A CN201810415930.1A CN201810415930A CN108913065A CN 108913065 A CN108913065 A CN 108913065A CN 201810415930 A CN201810415930 A CN 201810415930A CN 108913065 A CN108913065 A CN 108913065A
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- conductive fabric
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/04—Homopolymers or copolymers of esters
- C09J133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
- C09J133/08—Homopolymers or copolymers of acrylic acid esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/21—Paper; Textile fabrics
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/30—Adhesives in the form of films or foils characterised by the adhesive composition
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J9/00—Adhesives characterised by their physical nature or the effects produced, e.g. glue sticks
- C09J9/02—Electrically-conducting adhesives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Conductive Materials (AREA)
Abstract
The invention discloses conductive fabric glue of a kind of suitable transfer coated and preparation method thereof, glue component includes 20-40 parts of acrylic acid isooctyl polymer in parts by weight, 30-60 parts of butyl acrylate object, 10-15 parts of terpene resin, 5-10 parts of alkyl phenolic resin, 1-3 parts of add-on type epoxy hardener, 2-5 parts of isocyanate curing agent, 4-6 parts of sheet nickel coated graphite powder, 6-8 parts of carbon black, preparation method of the present invention is simple, glue curing speed obtained is fast, it is not easy to penetrate into the conductive fabric back side, it is suitble to transfer coated, it cuts and good with conductive fabric binding force, it conducts electricity very well, adhesive strength is high, it is not easily to fall off, improve the coating convenience and service performance of conductive fabric.
Description
Technical field
The present invention relates to conductive fabric glue manufacture technology field, the conductive fabric glue of specially a kind of suitable transfer coated and
Preparation method.
Background technique
Conductive fabric is to impose plating metal after preposition processing for substrate with fiber cloth (generally common polyester fiber cloth)
Coating makes it have metallic character and becoming conductive fibre fabric can be divided into:Nickel plating conductive fabric, gold-plated conductive fabric plate charcoal conductive fabric,
Aluminium foil fiber composite cloth.There are plain weave and grid to distinguish in appearance
Currently, the glue used in conductive fabric is dissolved in and penetrates into the conductive fabric back side and conductive fabric binding force is poor, it is easy to fall off, shadow
The service performance of conductive fabric is rung.
Summary of the invention
The purpose of the present invention is to provide a kind of conductive fabric glue and preparation method thereof, to solve to mention in above-mentioned background technique
Out the problem of.
To achieve the above object, the present invention provides the following technical solutions：A kind of conductive fabric glue, glue component is by weight
Number includes 20-40 parts of acrylic acid isooctyl polymer, 30-60 parts of butyl acrylate object, 10-15 parts of terpene resin, alkyl
5-10 parts of phenolic resin, 1-3 parts of add-on type epoxy hardener, 2-5 parts of isocyanate curing agent, 4-6 parts of sheet nickel coated graphite powder,
6-8 parts of carbon black.
Preferably, the preferred composition proportion of glue component includes that 25 parts of acrylic acid isooctyl polymer, butyl acrylate are poly-
Close 40 parts of object, 12 parts of terpene resin, 6 parts of alkyl phenolic resin, 2 parts of add-on type epoxy hardener, 4 parts of isocyanate curing agent,
5 parts of sheet nickel coated graphite powder, 6 parts of carbon black.
Preferably, preparation method includes the following steps：
A, it is added in agitator tank and stirs at low speed after mixing acrylic acid isooctyl polymer, butyl acrylate object, stirring speed
Rate is 100-300 revs/min, and time 8min-14min obtains mixture A；
B, the mixed solvent of toluene and ethyl acetate is added after mixing terpene resin, alkyl phenolic resin, it is high in agitator tank
Speed stirring, stirring rate are 900-1000 revs/min, and time 10min-22min obtains mixture B；
C, mixture B is added in mixture A, carbon black, sheet nickel coated graphite powder, mixing speed 600- is added while stirring
900 revs/min, time 10-15min obtains mixture C；
D, add-on type epoxy hardener and isocyanate curing agent are added in mixture C, is stirred after mixing, mixing speed
It is 300-600 revs/min, time 4min-8min obtains mixture D after standing 5min；
E, mixture D is filtered by 80 mesh filter screen to get conductive tape glue is arrived.
Compared with prior art, the beneficial effects of the invention are as follows：Preparation method of the present invention is simple, glue curing speed obtained
Degree is fast, is not easy to penetrate into the conductive fabric back side, is suitble to transfer coated, cut and with conductive fabric binding force it is good, conduct electricity very well, bonding is strong
Degree is high, not easily to fall off, improves the coating convenience and service performance of conductive fabric.Wherein, acrylic acid isooctyl is poly- in the present invention
Close object and butyl acrylate object mixing, be free to, effectively change glue glass transition temperature, pass through glue glass
The adjusting of glass temperature, to adapt to the requirement of Various Seasonal, different use environments to glue；The add-on type curable epoxide of addition and
Isocyanate curing agent, by the compounding of different proportion, agent can be improved the curing rate of glue, reduce curing time, make
Glue is not easy to penetrate into the back side of conductive fabric when obtaining transfer coated, improves the efficiency and yield of coating conductive fabric.In addition, this hair
The production method low manufacture cost of bright use, it can be ensured that each component material is sufficiently mixed, and further improves the performance of glue.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
The present invention provides the following technical solutions：A kind of conductive fabric glue, glue component include that acrylic acid is different in parts by weight
Pungent lipopolymer 20-40 parts, 30-60 parts of butyl acrylate object, 10-15 parts of terpene resin, 5-10 parts of alkyl phenolic resin,
1-3 parts of add-on type epoxy hardener, 2-5 parts of isocyanate curing agent, 4-6 parts of sheet nickel coated graphite powder, 6-8 parts of carbon black.
Embodiment one：It is suitble to spring and autumn
Glue component includes 25 parts of acrylic acid isooctyl polymer, 40 parts of butyl acrylate object, terpenes tree in parts by weight
12 parts of rouge, 6 parts of alkyl phenolic resin, 2 parts of add-on type epoxy hardener, 4 parts of isocyanate curing agent, sheet nickel coated graphite powder 5
Part, 6 parts of carbon black.
The preparation method of the present embodiment includes the following steps：
A, it is added in agitator tank and stirs at low speed after mixing acrylic acid isooctyl polymer, butyl acrylate object, stirring speed
Rate is 200 revs/min, and time 10min obtains mixture A；
B, the mixed solvent of toluene and ethyl acetate is added after mixing terpene resin, alkyl phenolic resin, it is high in agitator tank
Speed stirring, stirring rate are 900 revs/min, and time 15min obtains mixture B；
C, mixture B is added in mixture A, carbon black, sheet nickel coated graphite powder, mixing speed 800 is added while stirring
Rev/min, time 12min obtains mixture C；
D, add-on type epoxy hardener and isocyanate curing agent are added in mixture C, is stirred after mixing, mixing speed
It is 500 revs/min, time 6min, obtains mixture D after standing 5min；
E, mixture D is filtered by 80 mesh filter screen to get conductive tape glue is arrived.
Embodiment two：It is suitble to summer
Glue component includes 20 parts of acrylic acid isooctyl polymer, 40 parts of butyl acrylate object, terpenes tree in parts by weight
15 parts of rouge, 8 parts of alkyl phenolic resin, 3 parts of add-on type epoxy hardener, 4 parts of isocyanate curing agent, sheet nickel coated graphite powder 4
Part, 6 parts of carbon black.
The preparation method of the present embodiment includes the following steps：
A, it is added in agitator tank and stirs at low speed after mixing acrylic acid isooctyl polymer, butyl acrylate object, stirring speed
Rate is 150 revs/min, and time 12min obtains mixture A；
B, the mixed solvent of toluene and ethyl acetate is added after mixing terpene resin, alkyl phenolic resin, it is high in agitator tank
Speed stirring, stirring rate are 800 revs/min, and time 20min obtains mixture B；
C, mixture B is added in mixture A, carbon black, sheet nickel coated graphite powder, mixing speed 700 is added while stirring
Rev/min, time 15min obtains mixture C；
D, add-on type epoxy hardener and isocyanate curing agent are added in mixture C, is stirred after mixing, mixing speed
It is 400 revs/min, time 8min, obtains mixture D after standing 5min；
E, mixture D is filtered by 80 mesh filter screen to get conductive tape glue is arrived.
Embodiment three：It is suitble to winter
Glue component includes 33 parts of acrylic acid isooctyl polymer, 35 parts of butyl acrylate object, terpenes tree in parts by weight
10 parts of rouge, 6 parts of alkyl phenolic resin, 1 part of add-on type epoxy hardener, 2 parts of isocyanate curing agent, sheet nickel coated graphite powder 6
Part, 7 parts of carbon black.
The preparation method of the present embodiment includes the following steps：
A, it is added in agitator tank and stirs at low speed after mixing acrylic acid isooctyl polymer, butyl acrylate object, stirring speed
Rate is 250 revs/min, and time 14min obtains mixture A；
B, the mixed solvent of toluene and ethyl acetate is added after mixing terpene resin, alkyl phenolic resin, it is high in agitator tank
Speed stirring, stirring rate are 900 revs/min, and time 20min obtains mixture B；
C, mixture B is added in mixture A, carbon black, sheet nickel coated graphite powder, mixing speed 900 is added while stirring
Rev/min, time 15min obtains mixture C；
D, add-on type epoxy hardener and isocyanate curing agent are added in mixture C, is stirred after mixing, mixing speed
It is 600 revs/min, time 8min, obtains mixture D after standing 5min；
E, mixture D is filtered by 80 mesh filter screen to get conductive tape glue is arrived.
Experimental example：
It is tested for the property using glue made from various embodiments of the present invention, obtains data such as following table：
| Impedance（Ω） | Peeling force（Kg/25mm） | With conductive fabric binding force（kg/25mm） | Glue permeability（Whether face tissue can be sticked） | |
| Embodiment one | 0.012 | 1.35 | > 1.8 | It is no |
| Embodiment two | 0.009 | 1.25 | > 1.8 | It is no |
| Embodiment three | 0.015 | 1.45 | > 1.8 | It is no |
Preparation method of the present invention is simple, and glue curing speed obtained is fast, is not easy to penetrate into the conductive fabric back side, transfer is suitble to apply
Cloth, cut and with conductive fabric binding force it is good, conduct electricity very well, adhesive strength is high, and not easily to fall off, the coating for improving conductive fabric is convenient
Property and service performance.Wherein, the present invention in acrylic acid isooctyl polymer and butyl acrylate object mixing, can be free
, the effective glass transition temperature for changing glue, by the adjusting of glue glass transition temperature, to adapt to Various Seasonal, difference makes
Requirement with environment to glue；The add-on type curable epoxide and isocyanate curing agent of addition, by the compounding of different proportion, agent
The curing rate that can be improved glue, reduces curing time, so that glue is not easy to penetrate into the back of conductive fabric when transfer coated
Face improves the efficiency and yield of coating conductive fabric.In addition, the production method low manufacture cost that the present invention uses, it can be ensured that
Each component material is sufficiently mixed, and further improves the performance of glue.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (3)
1. a kind of conductive fabric glue, it is characterised in that：Glue component includes in parts by weight:Acrylic acid isooctyl polymer 20-
40 parts, 30-60 parts of butyl acrylate object, 10-15 parts of terpene resin, 5-10 parts of alkyl phenolic resin, add-on type epoxy it is solid
1-3 parts of agent, 2-5 parts of isocyanate curing agent, 4-6 parts of sheet nickel coated graphite powder, 6-8 parts of carbon black.
2. a kind of conductive fabric glue according to claim 1, it is characterised in that：The preferred composition proportion of glue component includes
25 parts of acrylic acid isooctyl polymer, 40 parts of butyl acrylate object, 12 parts of terpene resin, 6 parts of alkyl phenolic resin, addition
2 parts of type epoxy hardener, 4 parts of isocyanate curing agent, 5 parts of sheet nickel coated graphite powder, 6 parts of carbon black.
3. realizing a kind of preparation method of conductive fabric glue described in claim 1, it is characterised in that：Preparation method include with
Lower step：
A, it is added in agitator tank and stirs at low speed after mixing acrylic acid isooctyl polymer, butyl acrylate object, stirring speed
Rate is 100-300 revs/min, and time 8min-14min obtains mixture A；
B, the mixed solvent of toluene and ethyl acetate is added after mixing terpene resin, alkyl phenolic resin, it is high in agitator tank
Speed stirring, stirring rate are 900-1000 revs/min, and time 10min-22min obtains mixture B；
C, mixture B is added in mixture A, carbon black, sheet nickel coated graphite powder, mixing speed 600- is added while stirring
900 revs/min, time 10-15min obtains mixture C；
D, add-on type epoxy hardener and isocyanate curing agent are added in mixture C, is stirred after mixing, mixing speed
It is 300-600 revs/min, time 4min-8min obtains mixture D after standing 5min；
E, mixture D is filtered by 80 mesh filter screen to get conductive tape glue is arrived.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810415930.1A CN108913065A (en) | 2018-05-03 | 2018-05-03 | A kind of conductive fabric glue and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810415930.1A CN108913065A (en) | 2018-05-03 | 2018-05-03 | A kind of conductive fabric glue and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108913065A true CN108913065A (en) | 2018-11-30 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810415930.1A Pending CN108913065A (en) | 2018-05-03 | 2018-05-03 | A kind of conductive fabric glue and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110607144A (en) * | 2019-05-10 | 2019-12-24 | 南通康尔乐复合材料有限公司 | Conductive cloth glue for transfer coating and preparation method thereof |
| CN111253872A (en) * | 2020-03-21 | 2020-06-09 | 安徽富印新材料有限公司 | Electromagnetic shielding conductive adhesive tape |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090169852A1 (en) * | 2006-07-04 | 2009-07-02 | Jeongwan Choi | Conductive adhesive tape having different adhesion on both surfaces and method for manufacturing the same |
| CN101874089A (en) * | 2007-11-26 | 2010-10-27 | 3M创新有限公司 | Adhesive sheet and method for manufacturing same |
| CN107189721A (en) * | 2017-05-26 | 2017-09-22 | 江苏斯瑞达新材料科技有限公司 | A kind of conductive pressure sensitive glue composition and its application in production thickening bondline conductive tape |
-
2018
- 2018-05-03 CN CN201810415930.1A patent/CN108913065A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090169852A1 (en) * | 2006-07-04 | 2009-07-02 | Jeongwan Choi | Conductive adhesive tape having different adhesion on both surfaces and method for manufacturing the same |
| CN101874089A (en) * | 2007-11-26 | 2010-10-27 | 3M创新有限公司 | Adhesive sheet and method for manufacturing same |
| CN107189721A (en) * | 2017-05-26 | 2017-09-22 | 江苏斯瑞达新材料科技有限公司 | A kind of conductive pressure sensitive glue composition and its application in production thickening bondline conductive tape |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110607144A (en) * | 2019-05-10 | 2019-12-24 | 南通康尔乐复合材料有限公司 | Conductive cloth glue for transfer coating and preparation method thereof |
| CN111253872A (en) * | 2020-03-21 | 2020-06-09 | 安徽富印新材料有限公司 | Electromagnetic shielding conductive adhesive tape |
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Application publication date: 20181130 |